CN105696380A - Method capable of identifying pre-treatment uniformity of ink-jet printing textile - Google Patents

Method capable of identifying pre-treatment uniformity of ink-jet printing textile Download PDF

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Publication number
CN105696380A
CN105696380A CN201610161003.2A CN201610161003A CN105696380A CN 105696380 A CN105696380 A CN 105696380A CN 201610161003 A CN201610161003 A CN 201610161003A CN 105696380 A CN105696380 A CN 105696380A
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Prior art keywords
acid
ink
uniformity
pretreatment
fabric
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CN201610161003.2A
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CN105696380B (en
Inventor
房宽峻
高洪国
刘尊东
李付杰
侯长华
徐松林
郑建兵
徐承业
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SHANDONG HUANGHE DELTA INSTITUTE OF TEXTILE SCIENCE AND TECHNOLOGY Co Ltd
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SHANDONG HUANGHE DELTA INSTITUTE OF TEXTILE SCIENCE AND TECHNOLOGY Co Ltd
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Publication of CN105696380A publication Critical patent/CN105696380A/en
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Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/39General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using acid dyes
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • D06P1/48Derivatives of carbohydrates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642Compounds containing nitrogen
    • D06P1/649Compounds containing carbonamide, thiocarbonamide or guanyl groups
    • D06P1/6491(Thio)urea or (cyclic) derivatives
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673Inorganic compounds
    • D06P1/67391Salts or oxidising-compounds mixtures

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Coloring (AREA)
  • Ink Jet Recording Methods And Recording Media Thereof (AREA)

Abstract

The invention discloses a method capable of identifying the pre-treatment uniformity of an ink-jet printing textile and belongs to the technical field of ink-jet printing of textiles. The method comprises the following steps: preparing pre-treatment working liquid prepared from a marker, a thickening agent, urea, baking soda, soda ash, sodium sulfate, resist salt S and water; treating the textile with the pre-treatment working liquid, wherein the liquid carrying rate is 35 percent to 85 percent; drying to obtain a pre-treated textile; taking one part of the pre-treated textile and testing color difference deltaE of different points of the textile through a color tester; evaluating the pre-treatment uniformity through the color difference deltaE; if the color difference deltaE is smaller than or equal to 0.5, showing that the pre-treatment is uniform; otherwise, washing with water to fade the color, and pre-treating again. The method disclosed by the invention can be used for accurately and objectively reflecting the uniformity and stability of the pre-treatment of the ink-jet printing in time.

Description

A kind of method of recognizable ink-jet printed fabric pretreatment uniformity
Technical field
A kind of method that the present invention relates to recognizable ink-jet printed fabric pretreatment uniformity, belongs to textile inkjet printing field。
Background technology
In recent years, along with the increase of environmental protection pressure, labor cost, ink-jet printed because of significant advantages such as its environment-protection low-consumption, motility height, customized, the precision height rich colors of small lot personalization, obtain very fast growth。Reactive dye are ink-jet printed is one of the most frequently used ink-jet printed mode。Reactive dye and fiber need fixation in the basic conditions, and reactive dye facile hydrolysis in the basic conditions, and ink-jet decorating machine shower nozzle is more perishable in the basic conditions, therefore, can not add fixation alkaline agent in active dye ink-jet printing ink。Additionally, for ensureing reactive dye ink injection smoothness, generally control its viscosity in low viscosity scope, be about 8-20mPa s;Meanwhile, there is a large amount of gap between fabric fibre, between yarn, easily cause ink droplet imbibition, have a strong impact on ink-jet printed fineness and contour sharpness。
For the problems referred to above, the mode of pretreatment is generally adopted to be pre-applied on fabric by fixation alkaline agent, thickening agent, to provide reactive dye color fixing condition, the gap between fiberfill fibers, between yarn, and then reduce the imbibition degree of ink droplet, improve the fineness of pattern。
In ink-jet printed preprocessing process, it is possible to monitor uniformity and the stability of pretreatment accurately and in time, to improving, ink-jet printed end product quality is most important。At present, ink-jet printed end product can only be detected by the ink-jet printed enterprise of domestic major part, lacks accurately for preprocessing process control accuracy, in time, objectively monitors and measurement means。The stability of the indexs such as the color of uniform and stable and ink-jet printed finished product of ink-jet printed prefinished products, fastness has higher relatedness, ink-jet printed prefinished products uniformity is one of key factor affecting ink-jet printed finished product inherent quality stability, ink-jet printed prefinished products is uneven, the variation of ink-jet printed finished product color, pattern can be caused, affect the color of ink-jet printed finished product, fastness, change the style and features of ink-jet printed finished product。Therefore, in preprocessing process, setting up the Fast Evaluation that ink-jet printed prefinished products applies uniformity has very important meaning。
Through to existing achievement in research and literature retrieval, at present, both at home and abroad but without the research that ink-jet printed starching pretreatment fluid is applied uniformity characterizing method。
Summary of the invention
It is an object of the invention to for the problems referred to above, it is proposed that a kind of method of recognizable ink-jet printed fabric pretreatment uniformity, comprise the steps:
(1) preparation by 0.05 ~ 0.5% label, 2 ~ 5% thickening agent, 8 ~ 20% carbamide, 2 ~ 4% sodium bicarbonate, 0.5 ~ 1% soda, the pretreatment work liquid that forms of the Matrii Sulfas Exsiccatus of 1 ~ 3%, the reservehao S of 0.5 ~ 1.5% and water;
(2) fabric processes with described pretreatment work liquid, and liquid carrying rate is 35-85%, dries, obtains pretreating fabrics。
(3) uniformity of fabric pretreatment is judged by the uniformity of color on fabric after detecting pretreatment。
After pretreatment, on fabric, the uniformity of color is detected by colour photometer, test fabric difference aberration △ E, evaluates pretreatment pretreatment uniformity whereby, if aberration △ E≤0.5, then pretreatment is uniform, otherwise needs washing to take off, pretreatment again。
Described starching pretreatment fluid is made up of label, thickening agent, carbamide, sodium bicarbonate, soda, Matrii Sulfas Exsiccatus, reservehao S and water。Wherein label be with pretreated fabric preprocessing process, evaporate process, coloring matter that water-washing process does not react, label is after ink-jet printed fabric washing, can easily from fabric face eccysis, without the flower pattern of fabric and color are produced any impact, it is possible to accurately, in time, objectively respond the uniformity of ink-jet printed prefinished products。Described label is azogeramine, Xylene Red 3, Xylene Red 4, Xylene Red 5, Xylene Red 6, azogeramine 4, Xylene Red 37, Xylene Red 57, azogeramine 03, azogeramine 72, Acid Red 249, Xylene Red 301, Blue VRS, Acid Blue 7, acid blue 9, Blue VRS 1, acid blue 29, acid blue 41, ACID GREEN 25, acid black 20, acid black 23, acid black 26, acid orange 8, acid orange 50, acid orange 67, acid orange 127, the one of acid orange 156 or combination。Described thickening agent is sodium alginate, alginic acid ester, carboxymethyl cellulose, starch, modified starch, polyacrylate, polyacrylic acid, the one of polyacrylamide or combination。Thickening agent prevents dyestuff imbibition in spray printing post-drying and steaming procedure, keeps flower pattern and pattern contour definition。Carbamide increases the dissolubility of fabric face dyestuff。Sodium bicarbonate and soda provide reactive dye color fixing condition。Matrii Sulfas Exsiccatus promotes absorption and the fixation of reactive dye。Reservehao S prevents the destruction to reactive dye of the reducibility gas in steaming procedure。
Beneficial effects of the present invention
The present invention proposes a kind of method of recognizable ink-jet printed fabric pretreatment uniformity, it is possible to accurately, in time, objectively respond uniformity and the stability of ink-jet printed prefinished products。
Detailed description of the invention
For further appreciating that the present invention, below in conjunction with embodiment, embodiment of the present invention is described, but it is to be understood that these describe to be intended merely to and further illustrate the features and advantages of the present invention, rather than limiting to the claimed invention。
The method of a kind of recognizable ink-jet printed fabric pretreatment uniformity provided by the invention particularly as follows:
First, preparation by 0.05 ~ 0.5% label, 2 ~ 5% thickening agent, 8 ~ 20% carbamide, 2 ~ 4% sodium bicarbonate, 0.5 ~ 1% soda, the pretreatment work liquid that forms of the Matrii Sulfas Exsiccatus of 1 ~ 3%, the reservehao S of 0.5 ~ 1.5% and water。Described label be with pretreated fabric preprocessing process, evaporate process, coloring matter that water-washing process does not react;
Described label is azogeramine, Xylene Red 3, Xylene Red 4, Xylene Red 5, Xylene Red 6, azogeramine 4, Xylene Red 37, Xylene Red 57, azogeramine 03, azogeramine 72, Acid Red 249, Xylene Red 301, Blue VRS, Acid Blue 7, acid blue 9, Blue VRS 1, acid blue 29, acid blue 41, ACID GREEN 25, acid black 20, acid black 23, acid black 26, acid orange 8, acid orange 50, acid orange 67, acid orange 127, the one of acid orange 156 or combination。
Described thickening agent is sodium alginate, alginic acid ester, carboxymethyl cellulose, starch, modified starch, polyacrylate, polyacrylic acid, the one of polyacrylamide or combination。
Then, fabric processes with described pretreatment work liquid, and liquid carrying rate is 35-85%, dries, obtains pretreating fabrics。
Finally, taking the pretreated fabric of part, by colour photometer, test fabric difference aberration △ E, evaluate pretreatment uniformity whereby, if aberration △ E≤0.5, then pretreatment is uniform, otherwise needs washing to take off, pretreatment again。
Embodiment 1
First, using with pretreated fabric preprocessing process, evaporate process, coloring matter Xylene Red 3 that water-washing process does not react is as label, the starching pretreatment fluid that preparation is made up of Xylene Red 30.5%, sodium alginate 4%, carbamide 10%, sodium bicarbonate 2%, soda 0.5%, Matrii Sulfas Exsiccatus 3%, reservehao S 1.5% and water 78.5%。
Then, fabric processes with described pretreatment work liquid on circular screen printer, and liquid carrying rate is 40%, dries, obtains pretreating fabrics。
Finally, take the pretreated pure cotton fabric of part, by Datacolor650 colour photometer, test fabric A, six difference aberration of B, C, D, E, F, evaluate pretreatment uniformity whereby。If aberration △ E≤0.5, then pretreatment is uniform, otherwise needs washing to take off, and again does pretreatment。
In the embodiment of the present invention 1, the color data of ink-jet printed pretreating fabrics adopts Datacolor650 colour photometer to test。Using Xylene Red 3 as the color data of the ink-jet printed pretreating fabrics of label in Table 1。
Being computed, the aberration △ E < 0.5 of six differences, the process uniformity of ink-jet printed pretreating fabrics is better, is suitable for reactive dye ink-jet printed。
Embodiment 2
First, using with pretreated fabric preprocessing process, evaporate process, coloring matter acid black 23 that water-washing process does not react is as label, the starching pretreatment fluid that preparation is made up of acid black 2 30.4%, carboxymethyl cellulose 3%, carbamide 15%, sodium bicarbonate 3%, soda 0.5%, Matrii Sulfas Exsiccatus 3%, reservehao S 1.5% and water 73.6%。
Then, fabric processes with described pretreatment work liquid on evenness calender machine, and liquid carrying rate is 70%, dries, obtains pretreating fabrics。
Finally, take the pretreated pure cotton fabric of part, by Datacolor650 colour photometer, test fabric A, six difference aberration of B, C, D, E, F, evaluate pretreatment uniformity whereby。If aberration △ E≤0.5, then pretreatment is uniform, otherwise needs washing to take off, and again does pretreatment。
In the embodiment of the present invention 2, the color data of ink-jet printed pretreating fabrics adopts Datacolor650 colour photometer to test。Using acid black 23 as the color data of the ink-jet printed pretreating fabrics of label in Table 2。
Being computed, the aberration △ E < 0.5 of six differences, the process uniformity of ink-jet printed pretreating fabrics is better, is suitable for reactive dye ink-jet printed。
Embodiment 3
First, using with pretreated fabric preprocessing process, evaporate process, coloring matter acid blue 41 that water-washing process does not react is as label, the starching pretreatment fluid that preparation is made up of acid blue 410.5%, sodium polyacrylate 2.5%, carbamide 12%, sodium bicarbonate 3.5%, soda 1%, Matrii Sulfas Exsiccatus 2%, reservehao S 1.5% and water 77%。
Then, fabric processes with described pretreatment work liquid on circular screen printer, and liquid carrying rate is 50%, dries, obtains pretreating fabrics。
Finally, take the pretreated pure cotton fabric of part, by Datacolor650 colour photometer, test fabric A, six difference aberration of B, C, D, E, F, evaluate pretreatment uniformity whereby。If aberration △ E≤0.5, then pretreatment is uniform, otherwise needs washing to take off, and again does pretreatment。
In the embodiment of the present invention 3, the color data of ink-jet printed pretreating fabrics adopts Datacolor650 colour photometer to test。Using acid blue 41 as the color data of the ink-jet printed pretreating fabrics of label in Table 3。
Being computed, the aberration △ E < 0.5 of six differences, the process uniformity of ink-jet printed pretreating fabrics is better, is suitable for reactive dye ink-jet printed。

Claims (3)

1. the method for a recognizable ink-jet printed fabric pretreatment uniformity, it is characterised in that the method comprises the steps:
(1) preparation by 0.05 ~ 0.5% label, 2 ~ 5% thickening agent, 8 ~ 20% carbamide, 2 ~ 4% sodium bicarbonate, 0.5 ~ 1% soda, the pretreatment work liquid that forms of the Matrii Sulfas Exsiccatus of 1 ~ 3%, the reservehao S of 0.5 ~ 1.5% and water;
(2) fabric processes with described pretreatment work liquid, and liquid carrying rate is 35-85%, dries;
(3) uniformity of fabric pretreatment is judged by the uniformity of color on fabric after detecting pretreatment。
2. the method for a kind of recognizable ink-jet printed fabric pretreatment uniformity according to claim 1, it is characterized in that, described label is azogeramine, Xylene Red 3, Xylene Red 4, Xylene Red 5, Xylene Red 6, azogeramine 4, Xylene Red 37, Xylene Red 57, azogeramine 03, azogeramine 72, Acid Red 249, Xylene Red 301, Blue VRS, Acid Blue 7, acid blue 9, Blue VRS 1, acid blue 29, acid blue 41, ACID GREEN 25, acid black 20, acid black 23, acid black 26, acid orange 8, acid orange 50, acid orange 67, acid orange 127, one or more of acid orange 156。
3. the method for a kind of recognizable ink-jet printed fabric pretreatment uniformity according to claim 1, it is characterized in that, described thickening agent is sodium alginate, alginic acid ester, carboxymethyl cellulose, starch, modified starch, polyacrylate, polyacrylic acid, the one of polyacrylamide or combination。
CN201610161003.2A 2016-03-21 2016-03-21 A kind of method of recognizable ink-jet printed fabric pretreatment uniformity Active CN105696380B (en)

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Cited By (7)

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Publication number Priority date Publication date Assignee Title
CN107090724A (en) * 2017-05-18 2017-08-25 杭州科迈数码纺织技术有限公司 A kind of digit printing technique of polyester-cotton fabric
CN110029511A (en) * 2019-04-19 2019-07-19 天津工业大学 A kind of process for surface preparation of ink-jet printed pretreating agent and silk fabric
CN110616576A (en) * 2019-09-26 2019-12-27 珠海佳印数码科技有限公司 Digital printing white ink treatment fluid and preparation method thereof
CN111395020A (en) * 2020-05-15 2020-07-10 愉悦家纺有限公司 Method for repairing color of cellulose fiber textile
CN111607989A (en) * 2020-05-27 2020-09-01 山东黄河三角洲纺织科技研究院有限公司 Digital printing method for textile in wet state
CN112080952A (en) * 2020-09-14 2020-12-15 山东黄河三角洲纺织科技研究院有限公司 Method for improving ink-jet printing permeation effect of cellulose fiber fabric
CN113834786A (en) * 2021-08-09 2021-12-24 鲁丰织染有限公司 Rapid detection method for color difference quality of cloth under pretreatment

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107090724A (en) * 2017-05-18 2017-08-25 杭州科迈数码纺织技术有限公司 A kind of digit printing technique of polyester-cotton fabric
CN110029511A (en) * 2019-04-19 2019-07-19 天津工业大学 A kind of process for surface preparation of ink-jet printed pretreating agent and silk fabric
CN110029511B (en) * 2019-04-19 2021-09-24 天津工业大学 Ink-jet printing pretreating agent and surface pretreatment method of silk fabric
CN110616576A (en) * 2019-09-26 2019-12-27 珠海佳印数码科技有限公司 Digital printing white ink treatment fluid and preparation method thereof
CN111395020A (en) * 2020-05-15 2020-07-10 愉悦家纺有限公司 Method for repairing color of cellulose fiber textile
CN111395020B (en) * 2020-05-15 2022-08-26 愉悦家纺有限公司 Method for repairing color of cellulose fiber textile
CN111607989A (en) * 2020-05-27 2020-09-01 山东黄河三角洲纺织科技研究院有限公司 Digital printing method for textile in wet state
CN112080952A (en) * 2020-09-14 2020-12-15 山东黄河三角洲纺织科技研究院有限公司 Method for improving ink-jet printing permeation effect of cellulose fiber fabric
CN113834786A (en) * 2021-08-09 2021-12-24 鲁丰织染有限公司 Rapid detection method for color difference quality of cloth under pretreatment
CN113834786B (en) * 2021-08-09 2024-04-12 鲁丰织染有限公司 Rapid detection method for cloth color difference quality under pretreatment

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