CN105696091A - A flow controlled type reciprocating circling melt electrostatic spinning machine - Google Patents

A flow controlled type reciprocating circling melt electrostatic spinning machine Download PDF

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Publication number
CN105696091A
CN105696091A CN201511007205.3A CN201511007205A CN105696091A CN 105696091 A CN105696091 A CN 105696091A CN 201511007205 A CN201511007205 A CN 201511007205A CN 105696091 A CN105696091 A CN 105696091A
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CN
China
Prior art keywords
electrostatic spinning
guide rail
motor
controlled type
reciprocating
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Pending
Application number
CN201511007205.3A
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Chinese (zh)
Inventor
刘勇
张敬男
潘凯
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Beijing University of Chemical Technology
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Beijing University of Chemical Technology
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Application filed by Beijing University of Chemical Technology filed Critical Beijing University of Chemical Technology
Priority to CN201511007205.3A priority Critical patent/CN105696091A/en
Publication of CN105696091A publication Critical patent/CN105696091A/en
Pending legal-status Critical Current

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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/0007Electro-spinning
    • D01D5/0061Electro-spinning characterised by the electro-spinning apparatus
    • D01D5/0076Electro-spinning characterised by the electro-spinning apparatus characterised by the collecting device, e.g. drum, wheel, endless belt, plate or grid

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Textile Engineering (AREA)
  • Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)

Abstract

The invention provides a flow controlled type reciprocating circling melt electrostatic spinning machine and belongs to the field of electrostatic spinning and the mechanical field. The flow controlled type reciprocating circling melt electrostatic spinning machine comprises an electrostatic generator, a flow controlled type melt electrostatic spinning device and a reciprocating circling receiving device. The flow controlled type melt electrostatic spinning device mainly comprises a device pedestal, a material barrel, a plunger rod, a spinneret disc, a material barrel bottom plate, a heating element, a temperature sensor, a temperature control instrument, a guide rail frame, a propelling slider, a screw shaft, a guide rail, a coupler and a motor. The reciprocating circling receiving device mainly comprises a motor, a driving belt wheel, a driven belt wheel, a belt, a bearing, a hollow shaft, a reciprocating lever, a reciprocating rail, a collection board, a motor rack, a collection board support, a device rack, a height adjusting pillar, a guide rail frame, a propelling slider, a screw shaft, a guide rail, a coupler and a motor. The machine has the advantages that flow of melt electrostatic spinning is controllable, upward collection is realized and fiber films with uniform thickness can be prepared.

Description

A kind of flow rates controlled type back and forth circles round melt electrostatic spinning machine
Technical field
The present invention relates to a kind of flow rates controlled type back and forth to circle round melt electrostatic spinning machine, belong to electrostatic spinning field and mechanical field。
Background technology
Melt electrostatic spinning is the method utilizing electrostatic force that prepared by the drawing-off effect that molten polymer jet produces micro nanometer fiber。Solvent is not used, and the conduction needs of polymer is not high due to melt electrostatic spinning, so spinning cost and the pollution of environment is greatly reduced, and the type of polymer being applicable to melt electrostatic spinning is more。But, traditional melt electrostatic spinning, the fiber obtained is extremely difficult to nanoscale under the combined effect of gravity and electric field force。The collecting board upwards melt electrostatic spinning technology above spray webbing dish, electric field force and gravity is utilized can polymer jet to be stretched fully, thus obtaining the fiber of nanoscale。
In traditional electrostatic spinning technique, the position of collecting board is fixed often, is unfavorable for that fiber is evenly distributed on collecting board, and adopts the rotating collecting device moved back and forth, it is possible to overcome this defect。
Summary of the invention
The present invention proposes flow rates controlled type and back and forth circles round melt electrostatic spinning machine。Device is received including electrostatic generator, flow rates controlled type melt electrostatic spinning device and reciprocal convolution。Flow rates controlled type melt electrostatic spinning device mainly includes device pedestal, barrel, plunger rod, spray webbing dish, barrel chassis, heating element heater, temperature sensor, temperature controller, and guide rail bracket, propelling slide block, lead screw shaft, guide rail, shaft coupling and motor, wherein, barrel periphery is provided with heating element heater, temperature sensor is inserted the sidewall of barrel and is measured temperature, and by Temperature Feedback to temperature controller, the temperature controller feedback according to design temperature and temperature sensor, control heating element heater and barrel is heated;Spray webbing dish is arranged on barrel top by screw, the nozzle periphery of spray webbing dish is provided with a circle or a few circle pointed tooth groove, can effectively hinder the molten polymer flow overflowed by nozzle to heating element heater, and increase the quantity of taylor cone in electrostatic spinning, thus adding the yield of fiber;Barrel is vertically placed, it is fixed by bolts on device pedestal together with barrel chassis, device pedestal is made up of non-conductive, exotic material, plunger rod is arranged on barrel inner chamber through barrel chassis, can move up and down at vertical direction, the lower end of plunger rod and propelling shoe contact, slide block is advanced to be arranged in lead screw shaft and do the movement of vertical direction along guide rail, lead screw shaft and guide rails assembling are on guide rail bracket, guide rail bracket is fixed on the bottom of device pedestal, and the lower end of lead screw shaft is connected by shaft coupling with motor。
The present invention proposes a kind of flow rates controlled type and back and forth circles round melt electrostatic spinning machine。Wherein, reciprocal convolution reception device mainly includes motor, drive pulley, driven pulley, belt, bearing, hollow axle, reciprocating lever, reciprocating orbital, collecting board, motor rack, collecting board support, device frame, heighten post and guide rail bracket, advance slide block, lead screw shaft, guide rail, shaft coupling and motor, convolution receives device and is provided rotary power by motor by belt transmission or gear drive, the rotary speed receiving device is adjusted by the rotating speed of motor, driven pulley is connected with hollow axle and bearing, hollow axle adopts interference fit with bearing inner race, hollow axle lower end is fixed by bolts on collecting board support, bearing is arranged on reciprocating lever, reciprocating lever is cross section is rectangular stock, in the reciprocating orbital through hole on embedded device frame top, two ends, left and right, driven pulley is connected by belt with drive pulley, drive pulley is arranged on motor, motor is arranged on above reciprocating lever by motor rack by bolt, collecting board is fixed on collecting board support bottom, reciprocating lever is connected with advancing slide block, slide block is advanced to be arranged in lead screw shaft and do reciprocating translatory together with reciprocating lever along guide rail direction, speed is controlled by the motor on guide rail bracket, lead screw shaft and guide rails assembling are on guide rail bracket, guide rail bracket is fixed on the top of device frame, the right-hand member of lead screw shaft is connected by shaft coupling with motor, device frame is integrated with heightening post, heighten post and be placed in the preset hole of device pedestal, the distance between nozzle and collecting board can be adjusted by height adjustment knob。Driven pulley, hollow axle, reciprocating lever, device frame and collecting board support are made from a material that be electrically non-conductive。The positive high voltage end of electrostatic generator is connected to collecting board through described hollow axle, negativing ending grounding, region on the collecting board top corresponding with hollow axle bottom, cylindrical boss with groove is set, its role is to, closely collecting board is fixed on collecting board support bottom, and is easy to connect the positive high voltage end of electrostatic generator, reciprocal convolution receive device along hollow axle horizontally rotate time, do not affect the connection between positive high voltage end and the collecting board of electrostatic generator。The present invention is not when enabling described temperature controller, it is possible to carry out solution electrostatic spinning under room temperature state。
The present invention proposes a kind of flow rates controlled type and back and forth circles round melt electrostatic spinning machine。Compared with melt electrostatic spinning, the present invention has two advantages: one, be capable of collecting board melt electrostatic spinning technology above spray webbing dish;Two, the equally distributed masking technique of fiber it is capable of。
Fig. 1 is that a kind of flow rates controlled type back and forth circles round the structural representation of melt electrostatic spinning machine
In figure: 101-electrostatic generator;102-positive high voltage end;201-driven pulley;202-belt;203-reciprocating lever;204-reciprocating orbital;205-bearing;206-bolt;207-hollow axle;208-cylindrical boss;209-collecting board support;210-collecting board;211-bolt;212-motor rack;213-motor;214-drive pulley;215-advances slide block;216-guide rail;217-lead screw shaft;218-shaft coupling;219-guide rail bracket;220-bolt;221-motor;301-temperature controller;302-temperature sensor;303-heating element heater;304-barrel;305-bolt;306-barrel chassis;307-plunger rod;308-advances slide block;309-shaft coupling;310-nozzle;311-pointed tooth groove;312-spray webbing dish;313-screw;314-guide rail;315-lead screw shaft;316-motor;317-guide rail bracket;318-bolt;319-device frame;320-heightens post;321-height adjustment knob;322-device pedestal;401-earth lead。
Detailed description of the invention
Hereinafter with reference to accompanying drawing, the present invention is further elaborated。It should be understood by those skilled in the art that, embodiment described here is merely illustrative, it is contemplated that the further feature being capable of phase same-action, the feature that accompanying drawing is drawn can zoom in or out as the case may be, additionally, the connected mode related in embodiment, the quantity of its connector and model can change as the case may be。
The present invention provides a kind of flow rates controlled type back and forth to circle round melt electrostatic spinning machine, as it is shown in figure 1, described flow rates controlled type back and forth circles round, melt electrostatic spinning machine includes electrostatic generator 101, flow rates controlled type melt electrostatic spinning device and reciprocal convolution and receives device。Flow rates controlled type melt electrostatic spinning device mainly includes device pedestal 322, barrel 304, plunger rod 307, spray webbing dish 312, barrel chassis 306, heating element heater 303, temperature sensor 302, temperature controller 301, and guide rail bracket 317, advance slide block 308, lead screw shaft 315, guide rail 317, shaft coupling 309 and motor 316, wherein, barrel 304 periphery is provided with heating element heater 303, temperature sensor 302 is inserted the sidewall of barrel 304 and is measured temperature, and by Temperature Feedback to temperature controller 301, the temperature controller 301 feedback according to design temperature and temperature sensor 302, control heating element heater 303 barrel 304 is heated;Spray webbing dish 312 is arranged on barrel 304 top by screw 313, nozzle 310 periphery of spray webbing dish 312 is provided with a circle or a few circle pointed tooth groove 311, can effectively hinder the molten polymer flow overflowed by nozzle 310 to heating element heater 303, and the quantity of taylor cone in electrostatic spinning process can be increased, thus add the yield of fiber;Barrel 304 is vertically placed, reinstate bolt 305 with barrel chassis 306 1 and be fixed on device pedestal 322, plunger rod 307 is arranged on barrel 304 inner chamber through barrel chassis 306, can move up and down at vertical direction, the lower end of plunger rod 307 contacts with advancing slide block 308, slide block 308 is advanced to be arranged in lead screw shaft 315 and do the movement of vertical direction along guide rail 314, lead screw shaft 315 and guide rail 314 are arranged on guide rail bracket 317, guide rail bracket 317 is fixed on the bottom of device pedestal 322 by bolt 318, and the lower end of lead screw shaft 315 is connected by shaft coupling 309 with motor 316。Reciprocal convolution receives device, and key component includes motor 213, drive pulley 214, driven pulley 201, belt 202, bearing 205, hollow axle 207, reciprocating lever 203, reciprocating orbital 204, collecting board 210, motor rack 212, collecting board support 209, device frame 319, heighten post 320 and guide rail bracket 219, advance slide block 215, lead screw shaft 217, guide rail 216, shaft coupling 218 and motor 221, driven pulley 201 is connected with hollow axle 207 and bearing 205, hollow axle 207 adopts interference fit with bearing 205 inner ring, hollow axle 207 lower end bolt 206 is fixed on collecting board support 209, bearing 205 is arranged on reciprocating lever 203, reciprocating lever 203 is rectangular stock for cross section, in reciprocating orbital 204 through hole on embedded device frame 319 top, two ends, left and right, driven pulley 201 is connected by belt 202 with drive pulley 214, drive pulley 214 is arranged on motor 213, motor 213 is arranged on above reciprocating lever 203 by motor rack 212 by bolt 211, collecting board 210 is fixed on collecting board support 209 bottom, reciprocating lever 203 is connected with advancing slide block 215, slide block 215 is advanced to be arranged in lead screw shaft 217 and do reciprocating translation together with reciprocating lever 203 along guide rail 216 direction, lead screw shaft 217 and guide rail 216 are arranged on guide rail bracket 219, guide rail bracket 219 is fixed on the top of device frame 319, the right-hand member of lead screw shaft 217 is connected by shaft coupling 218 with motor 221, device frame 319 is integrated with heightening post 320, heighten in the preset hole that post 320 is placed in device pedestal 322, the adjustment of spinning height is carried out by height adjustment knob 321。The positive high voltage end 102 of electrostatic generator 101 is connected to collecting board 210 through described hollow axle 207, negativing ending grounding, region on collecting board 210 top corresponding with hollow axle 207 bottom, cylindrical boss 208 with groove is set, its role is to, closely collecting board 210 is fixed on collecting board support 209 bottom, and it is easy to connect the positive high voltage end 102 of electrostatic generator 101, reciprocal convolution receive device along hollow axle horizontally rotate time, do not affect the connection between the positive high voltage end 102 of electrostatic generator 101 and collecting board 210。
Concrete installation steps are, for flow rates controlled type melt electrostatic spinning device, heating element heater 303 is enclosed within barrel 304 periphery, and temperature sensor 302 inserts, through heating element heater 303, the tapping that barrel 304 sidewall is preset, and respectively heating element heater 303 and temperature sensor 302 is connected to temperature controller 301;Barrel 304 is vertically placed on the tapping that device pedestal 322 is preset, plunger rod 307 is pressed the direction shown in Fig. 1 and is inserted in barrel 304, installing barrel chassis 306, be fixed together with device pedestal 322 in barrel 304, barrel chassis 306 with bolt 305, spray webbing dish 312 is fixed after reinforced again;It is embedded on the guide rail 314 of guide rail bracket 317 by advancing slide block 308, lead screw shaft 315 is through advancing slide block 308 and being arranged on guide rail bracket 317, the lower end of lead screw shaft 315 is connected with motor 316 by shaft coupling 309, guide rail bracket 317 is fixed on the bottom of device pedestal 322 by bolt 318, and temperature controller 301, barrel chassis 306, guide rail bracket 317 are connected with earth lead 401。Reciprocal convolution receives device, collecting board 210 is fixed on the lower surface of collecting board support 209 by cylindrical boss 208, collecting board support 209 top and hollow axle 207 bottom are by bolt 206 compact siro spinning technology, hollow axle 207 is through bearing 205 endoporus being fixed on reciprocating lever 203, with driven pulley 201 by screw thread compact siro spinning technology;Motor rack 212 is arranged on reciprocating lever 203 by bolt 211, the motor 213 being provided with drive pulley 214 is fixed on motor rack 212, drive pulley 214 and driven pulley 201 is connected by belt 202, by in the reciprocating orbital 204 of the two ends embedded device frame 319 of reciprocating lever 203, and be connected with advancing slide block 215, and slide block 215 will be advanced to be embedded on the guide rail 216 of guide rail bracket 219, lead screw shaft 217 is through advancing slide block 215 and being arranged on guide rail bracket 219, the right-hand member of lead screw shaft 217 is connected with motor 221 by shaft coupling 218, by bolt 220, guide rail bracket 219 is fixed on the top of device frame 319, by in the preset hole heightening post 320 embedded device base 322 of device frame 319 bottom, tightened by height adjustment knob 321。Electrostatic generator 101, by the center of the positive high voltage end 102 of electrostatic generator 101 traverse hollow axle 207, is placed in the groove of cylindrical boss 208 on collecting board 210 top, and by negativing ending grounding。
The operating procedure specifically preparing nanofiber is: before preparation work starts, spinning distance is regulated by height adjustment knob 321, opening temp. control instrument 301 also sets spinning temperature, when barrel 304 temperature stabilization is when set temperature, polymer is added by the top of barrel 304, and cover spray webbing dish 312, be fixed on barrel 304 with screw 313。After polymer is fully melted, adjust reciprocal convolution and receive the distance between device and nozzle 310, open reciprocal convolution successively and receive the motor 213 of device, motor 221 and electrostatic generator 101, and adjusting required voltage, turn-on flow rate controls the motor 316 of device, makes the polymer melted flow out slowly under the effect of plunger rod 307, and form taylor cone, electric field force with under the synergy of contrary gravity, by the collecting board 210 of reciprocal circumnutation, prepare uniform nano fibrous membrane。
When fiber preparation work terminates, close the motor 316 of electrostatic generator 101, temperature controller 301, reciprocal the circle round motor 221 receiving device and motor 213 and volume control device successively, and fibrous membrane on collecting board 210 is collected。Use is complete every time all must dismantle the barrel 304 of flow rates controlled type melt electrostatic spinning device, spray webbing dish 312 and plunger rod 307 in time and clean out。

Claims (7)

1. a flow rates controlled type back and forth circles round melt electrostatic spinning machine, it is characterized in that, including electrostatic generator, flow rates controlled type melt electrostatic spinning device and reciprocal convolution receive device, described flow rates controlled type melt electrostatic spinning device mainly includes device pedestal, barrel, plunger rod, spray webbing dish, barrel chassis, heating element heater, temperature sensor, temperature controller, and guide rail bracket, advance slide block, lead screw shaft, guide rail, shaft coupling and motor, wherein, described barrel periphery is provided with heating element heater, described temperature sensor is inserted the sidewall of barrel and is measured temperature, and by Temperature Feedback to temperature controller, the described temperature controller feedback according to design temperature and temperature sensor, control heating element heater barrel is heated, described spray webbing dish is arranged on barrel top, described barrel is vertically fixed on device pedestal, and fixed by barrel chassis, described plunger rod is arranged on barrel inner chamber, can move up and down at vertical direction, the lower end of plunger rod and described propelling shoe contact, described propelling slide block is arranged in described lead screw shaft and does the movement of vertical direction along described guide rail, described lead screw shaft and described guide rails assembling are on described guide rail bracket, described guide rail bracket is fixed on the bottom of device pedestal, the lower end of described lead screw shaft is connected by described shaft coupling with described motor。
2. flow rates controlled type according to claim 1 back and forth circles round melt electrostatic spinning machine, and the described flow rates controlled type melt electrostatic spinning machine that back and forth circles round farther includes: reciprocal convolution receives device, mainly includes motor, drive pulley, driven pulley, belt, bearing, hollow axle, reciprocating lever, reciprocating orbital, collecting board, motor rack, collecting board support, device frame, heighten post and guide rail bracket, advance slide block, lead screw shaft, guide rail, shaft coupling and motor, described driven pulley is connected with described hollow axle and described bearing, hollow axle lower end is fixed on described collecting board support, bearing is arranged on described reciprocating lever, reciprocating lever is cross section is rectangular stock, two ends, left and right are inserted in the through hole of the reciprocating orbital on described device frame top, driven pulley is connected by belt with drive pulley, drive pulley is arranged on described motor, described motor is arranged on above reciprocating lever by described motor rack, collecting board is fixed on collecting board support bottom, reciprocating lever is connected with described propelling slide block, described propelling slide block is arranged in described lead screw shaft and does reciprocating translatory together with reciprocating lever along described guide rail direction, described lead screw shaft and described guide rails assembling are on described guide rail bracket, described guide rail bracket is fixed on the top of device frame, the right-hand member of described lead screw shaft is connected by described shaft coupling with described motor, described device frame and described post of heightening are integrated, heighten in the preset hole that post is placed in described device pedestal;Electrostatic generator, the positive high voltage end of described electrostatic generator is connected to collecting board, negativing ending grounding through described hollow axle。
3. flow rates controlled type according to claim 1 back and forth circles round melt electrostatic spinning machine, and wherein, the nozzle periphery of described spray webbing dish is provided with pointed tooth groove, and quantity is a circle or a few circle。
4. flow rates controlled type according to claim 1 back and forth circles round melt electrostatic spinning machine, wherein, described device pedestal is made up of non-conductive, exotic material, and described driven pulley, described hollow axle, described reciprocating lever, described device frame and described collecting board support are made from a material that be electrically non-conductive。
5. flow rates controlled type according to claim 2 back and forth circles round melt electrostatic spinning machine, wherein, it is possible to realize the device that described collecting board support planar rotates, is belt transmission or gear drive。
6. flow rates controlled type according to claim 2 back and forth circles round melt electrostatic spinning machine, wherein, when not enabling described temperature controller, it is possible to carry out solution electrostatic spinning under room temperature state。
7. flow rates controlled type according to claim 2 back and forth circles round melt electrostatic spinning machine, wherein, distance between described collecting board and described nozzle is adjusted by described height adjustment knob, the reciprocal gait of march of described reciprocating lever is adjusted by the motor on described guide rail bracket, and the rotary speed of described reception device is adjusted by the motor on described motor rack。
CN201511007205.3A 2015-12-30 2015-12-30 A flow controlled type reciprocating circling melt electrostatic spinning machine Pending CN105696091A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109930210A (en) * 2019-04-02 2019-06-25 闽江学院 A kind of electrostatic spinning micro nanometer fiber collection apparatus for placing
CN110331450A (en) * 2019-06-14 2019-10-15 中鸿纳米纤维技术丹阳有限公司 A kind of nanofiber assembly type injection equipment

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KR20110078016A (en) * 2009-12-30 2011-07-07 주식회사 효성 Drum type spinning block and electrospinning device with the same
CN205329217U (en) * 2015-12-30 2016-06-22 北京化工大学 Spin formula fuse -element electrospinning machines in controlled type of flow

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Publication number Priority date Publication date Assignee Title
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KR20110078016A (en) * 2009-12-30 2011-07-07 주식회사 효성 Drum type spinning block and electrospinning device with the same
CN101871130A (en) * 2010-07-06 2010-10-27 北京化工大学 Novel straight-strut electrostatic spinning spray nozzle
CN205329217U (en) * 2015-12-30 2016-06-22 北京化工大学 Spin formula fuse -element electrospinning machines in controlled type of flow

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109930210A (en) * 2019-04-02 2019-06-25 闽江学院 A kind of electrostatic spinning micro nanometer fiber collection apparatus for placing
CN109930210B (en) * 2019-04-02 2020-06-05 闽江学院 Electrostatic spinning micro-nano fiber collecting and placing device
CN110331450A (en) * 2019-06-14 2019-10-15 中鸿纳米纤维技术丹阳有限公司 A kind of nanofiber assembly type injection equipment
CN110331450B (en) * 2019-06-14 2021-06-18 中鸿纳米纤维技术丹阳有限公司 Assembled injection mechanism of nanofiber

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