CN105688437A - Crystallization kettle easy for material discharge - Google Patents
Crystallization kettle easy for material discharge Download PDFInfo
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- CN105688437A CN105688437A CN201410697955.7A CN201410697955A CN105688437A CN 105688437 A CN105688437 A CN 105688437A CN 201410697955 A CN201410697955 A CN 201410697955A CN 105688437 A CN105688437 A CN 105688437A
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- crystallization
- crystallization kettle
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Abstract
A crystallization kettle easy for material discharge includes a crystallization kettle body; the crystallization kettle body comprises a top cover, a bottom cover and a side wall forming into a cylindrical shape; the top cover and the top of the side wall are fixed; the bottom cover and the bottom of the side wall are fixed; the bottom cover is made of transparent glass; the bottom cover and the side wall are fixed by firing; and in reaction, the inside of the bottom cover is paved with a crystallization cloth. The crystallization kettle provided by the invention is convenient for crystallization reclaiming, so that the crystals are all on the crystallization cloth; and the crystallization cloth is taken out, and the crystals on the crystallization cloth are scraped, so as to collect more crystals, save labor and time of workers, and at the same time effectively improve the yield of the reaction.
Description
Technical field
The present invention relates to chemical field, be specifically related to a kind of crystallization kettle being prone to blowing。
Background technology
In chemical industry, the reactant of a lot of reactions is crystal habit, crystallization often precipitates out on the bottom of crystallization kettle, traditional has two kinds by the way that crystallization is taken out, a kind of is adopt to take out material machine the crystallization on bottom is extracted, another kind is that the crystallization on bottom is scraped down by the things such as the waddy of employing strip, but some crystalline solid is difficult to from scraped clean bottom or extracts a large amount of from reactor, and from discharging opening, crystalline solid is scraped, limitations is very big, both wasted time and energy, its productivity is not high yet, affect the normal operation of enterprise, substantially increase entreprise cost。
Therefore, the problems referred to above are the problems should paid attention to and solve in the design and use process of reactor。
Summary of the invention
For above-mentioned Problems existing, the present invention provides a kind of crystallization kettle being prone to blowing。
The technical solution of the present invention is: a kind of crystallization kettle being prone to blowing, including crystallization kettle body, described crystallization kettle body includes top cover, bottom and gusset, described gusset forms the top of cylindrical shape, described top cover and described gusset and fixes, and the bottom of described bottom and described gusset fixes, described bottom adopts clear glass to make, described bottom and described gusset are sintered to fix, and during reaction, are equipped with crystallization cloth inside described bottom。
Further improvement of the present invention is in that: the raw material making described bottom is safety glass。
Further improvement of the present invention is in that: offers the feed opening of big orifice on described bottom, and is fixed with bottom valve on described feed opening, described bottom valve is provided with thick type tremie pipe, and the pipe end of described tremie pipe is connected to takes out material machine。
Further improvement of the present invention is in that: be provided with the charging aperture for charging on described top cover。
A kind of crystallization kettle being prone to blowing of the present invention, it is necessary to the reaction of crystallization carries out in crystallization kettle body, and general crystallization can be tied on the bottom of crystallization kettle, if this crystallization is prone to draw out or extract out, only need to open bottom valve after the reaction, open and take out material machine, the crystalline solid on bottom is taken out material。Also bottom valve can be removed from feed opening, adopt the hard shape bar such as waddy to stretch into and the crystalline solid on bottom is scraped。But some crystalline solid is difficult to from scraped clean bottom, the present invention can adopt and be unloaded from feed opening by bottom valve, then crystallization cloth is laid on inside the bottom of crystallization kettle, the edge of crystallization cloth also can arrange clamp system, the fixture of the clamp system that the upper end of bottom also can supporting be arranged on fixing crystallization cloth, being fixed by crystallization cloth is laid on inside the bottom of crystallization kettle, just can make in crystallization kettle reacted crystallization on crystallization cloth, when taking crystallization, also only bottom valve need to be pulled down from feed opening, crystallization cloth be taken out and just may be used。
The invention has the beneficial effects as follows: the crystallization kettle that the present invention is arranged is more convenient to crystallization feeding, both can conventionally still intercrystalline be extracted with taking out material machine, or stretch in the feed opening bottom crystallization kettle with the hard thing of strip crystallization is struck off, also new method can be adopted to be laid by crystallization cloth and to collect crystallization, make crystallization all on crystallization cloth, take out crystallization cloth the crystallization on crystallization cloth to be struck off outside still, the crystallization collected is more, therefore the productivity of reaction it is effectively increased, meanwhile, the cost of enterprise is saved。Crystalline solid on bottom is observed by the more convenient workman of bottom of transparence, also the laying of more convenient crystallization cloth, and safety glass is made so that bottom has better hardness。It is simple and convenient that the present invention collects crystallization, has extraordinary result of use。
Accompanying drawing explanation
Fig. 1 is the structural representation of a kind of crystallization kettle being prone to blowing of the present invention。
Wherein, 1-crystallization kettle body, 2-top cover, 3-bottom, 4-gusset, 5-crystallization cloth, 6-feed opening, 7-bottom valve, 8-tremie pipe, 9-takes out material machine, 10-charging aperture。
Detailed description of the invention
In order to deepen the understanding of the present invention, below in conjunction with drawings and Examples, the present invention being described in further detail, this embodiment is only used for explaining the present invention, protection scope of the present invention is not constituted and limits。
As shown in Figure 1, the present embodiment provides a kind of crystallization kettle being prone to blowing, a kind of crystallization kettle being prone to blowing, it is characterized in that: include crystallization kettle body 1, described crystallization kettle body 1 includes top cover 2, bottom 3 and gusset 4, described gusset 4 forms cylindrical shape, the top of described top cover 2 and described gusset 4 fixes, the bottom of described bottom 3 and described gusset 4 fixes, described bottom 3 adopts clear glass to make, described bottom 3 is sintered to fix with described gusset 4, during reaction, is equipped with crystallization cloth 5 inside described bottom 3。The raw material making described bottom 3 is safety glass。Offering the feed opening 6 of big orifice on described bottom 3, and be fixed with bottom valve 7 on described feed opening 6, described bottom valve 7 is provided with thick type tremie pipe 8, the pipe end of described tremie pipe 8 is connected to takes out material machine 9。Described top cover 2 is provided with the charging aperture 10 for charging。
A kind of crystallization kettle being prone to blowing of the present embodiment, it is necessary to the reaction of crystallization carries out in crystallization kettle body 1, general crystallization can be tied on the bottom 3 of crystallization kettle, if this crystallization is prone to draw out or extract out, only need to open bottom valve 7 after the reaction, open and take out material machine 9, the crystalline solid on bottom 3 is taken out material。Also bottom valve 7 can be removed from feed opening 6, adopt the hard shape bar such as waddy to stretch into and the crystalline solid on bottom 3 is scraped。But some crystalline solid is difficult to from scraped clean bottom 3, the present invention can adopt and be unloaded from feed opening 6 by bottom valve 7, then crystallization cloth 5 is laid on inside the bottom 3 of crystallization kettle, the edge of crystallization cloth 5 also can arrange clamp system, the fixture of the clamp system that the upper end of bottom 3 also can supporting be arranged on fixing crystallization cloth 5, it is laid on inside the bottom 3 of crystallization kettle by fixing for crystallization cloth 5, just can make in crystallization kettle reacted crystallization on crystallization cloth 5, when taking crystallization, also only bottom valve 7 need to be pulled down from feed opening 6, crystallization cloth 5 be taken out and just may be used。
The present embodiment provides the benefit that: the crystallization kettle that the present invention is arranged is more convenient to crystallization feeding, both can conventionally still intercrystalline be extracted with taking out material machine, or stretch in the feed opening bottom crystallization kettle with the hard thing of strip crystallization is struck off, also new method can be adopted to be laid by crystallization cloth and to collect crystallization, make crystallization all on crystallization cloth, take out crystallization cloth the crystallization on crystallization cloth to be struck off outside still, the crystallization collected is more, therefore the productivity of reaction it is effectively increased, meanwhile, the cost of enterprise is saved。Crystalline solid on bottom is observed by the more convenient workman of bottom of transparence, also the laying of more convenient crystallization cloth, and safety glass is made so that bottom has better hardness。It is simple and convenient that the present invention collects crystallization, has extraordinary result of use。
Claims (4)
1. the crystallization kettle being prone to blowing, it is characterized in that: include crystallization kettle body (1), described crystallization kettle body (1) includes top cover (2), bottom (3) and gusset (4), described gusset (4) forms cylindrical shape, the top of described top cover (2) and described gusset (4) fixes, the bottom of described bottom (3) and described gusset (4) fixes, described bottom (3) adopts clear glass to make, described bottom (3) and described gusset (4) are sintered to fix, during reaction, it is equipped with crystallization cloth (5) in described bottom (3) inner side。
2. a kind of crystallization kettle being prone to blowing according to claim 1, it is characterised in that: the raw material making described bottom (3) is safety glass。
3. a kind of crystallization kettle being prone to blowing according to claim 1, it is characterized in that: on described bottom (3), offer the feed opening (6) of big orifice, and on described feed opening (6), it is fixed with bottom valve (7), being provided with thick type tremie pipe (8) on described bottom valve (7), the pipe end of described tremie pipe (8) is connected to takes out material machine (9)。
4. a kind of crystallization kettle being prone to blowing according to claim 1, it is characterised in that: described top cover (2) is provided with the charging aperture (10) for charging。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201410697955.7A CN105688437A (en) | 2014-11-28 | 2014-11-28 | Crystallization kettle easy for material discharge |
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CN201410697955.7A CN105688437A (en) | 2014-11-28 | 2014-11-28 | Crystallization kettle easy for material discharge |
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CN105688437A true CN105688437A (en) | 2016-06-22 |
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CN201410697955.7A Pending CN105688437A (en) | 2014-11-28 | 2014-11-28 | Crystallization kettle easy for material discharge |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108031142A (en) * | 2017-12-13 | 2018-05-15 | 上海合全药物研发有限公司 | Simplified device and method for preparing large amount of micro-crystal seeds by wet grinding |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3900955A (en) * | 1973-10-15 | 1975-08-26 | Joseph C Peterson | Apparatus for recovering sulfuric acid and ferrous sulfate crystals from spent pickle solution |
CN201253500Y (en) * | 2008-08-28 | 2009-06-10 | 项文远 | Crystal separator |
CN202315390U (en) * | 2011-12-02 | 2012-07-11 | 成都雅途生物技术有限公司 | Crystallizer capable of filtering |
CN202844626U (en) * | 2012-08-14 | 2013-04-03 | 郴州金山冶金化工有限公司 | Cobalt sulfate crystal separating device |
CN203208718U (en) * | 2013-03-01 | 2013-09-25 | 浙江江北药业有限公司 | Semi-discharge device of crystallization kettle |
-
2014
- 2014-11-28 CN CN201410697955.7A patent/CN105688437A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3900955A (en) * | 1973-10-15 | 1975-08-26 | Joseph C Peterson | Apparatus for recovering sulfuric acid and ferrous sulfate crystals from spent pickle solution |
CN201253500Y (en) * | 2008-08-28 | 2009-06-10 | 项文远 | Crystal separator |
CN202315390U (en) * | 2011-12-02 | 2012-07-11 | 成都雅途生物技术有限公司 | Crystallizer capable of filtering |
CN202844626U (en) * | 2012-08-14 | 2013-04-03 | 郴州金山冶金化工有限公司 | Cobalt sulfate crystal separating device |
CN203208718U (en) * | 2013-03-01 | 2013-09-25 | 浙江江北药业有限公司 | Semi-discharge device of crystallization kettle |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108031142A (en) * | 2017-12-13 | 2018-05-15 | 上海合全药物研发有限公司 | Simplified device and method for preparing large amount of micro-crystal seeds by wet grinding |
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Application publication date: 20160622 |
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