CN105687139A - Superfine maca powder and preparation method thereof - Google Patents
Superfine maca powder and preparation method thereof Download PDFInfo
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- CN105687139A CN105687139A CN201610134493.7A CN201610134493A CN105687139A CN 105687139 A CN105687139 A CN 105687139A CN 201610134493 A CN201610134493 A CN 201610134493A CN 105687139 A CN105687139 A CN 105687139A
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- meyenii walp
- lepidinm meyenii
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/31—Brassicaceae or Cruciferae (Mustard family), e.g. broccoli, cabbage or kohlrabi
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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Abstract
The invention discloses superfine maca powder and a preparation method thereof and belongs to the technical field of traditional Chinese medicines. The particle size of the superfine maca powder is small than or equal to 10 mu m. The preparation method of the superfine maca powder comprises steps as follows: fresh and high-quality maca is used as a raw material, cleansed, cut into maca slices, naturally aired and then subjected to coarse grinding and intermediate grinding; maca powder is subjected to low-temperature freeze-drying and the moisture content is controlled to be lower than or equal to 2%; the superfine maca powder is obtained through superfine grinding and total mixing. The superfine maca powder processed with the technology is uniform in particle and good in dispersity, maca active molecules with the healthcare effect are reserved during processing, and the bioavailability of the superfine maca powder is greatly higher than that of superfine maca powder on the market at present. The product can be applied to fields of foods, healthcare foods and the like.
Description
Technical field
The present invention relates to a kind of Lepidinm meyenii Walp micropowder and preparation method thereof, belong to Chinese medicine and food processing technology field。
Background technology
Lepidinm meyenii Walp, make again Maca (Maca, LepidiummeyemiiWalp), belong to Cruciferae (Cruciferae) separate row Vegetable spp likeness in form Radix Raphani tuber class is annual or 2 years raw herbaceous plant, originate in the mountain area, Andean, South America of height above sea level 3500～4500 meters in the middle part of Peru, locals is mainly used in as food, can use as conventional medicament, belong to pure natural labour and capital food。Early stage in 20th century, it is classified as rare plant in imminent danger in the world, until nineteen eighty-two, under the effort of the international organizations such as FAO (FAO (Food and Agriculture Organization of the United Nation)) and IPGRI (International Plant Genetic Resources Institute), Lepidinm meyenii Walp is worldwide widely popularized, and point out that Lepidinm meyenii Walp is a kind of nutrient safe food, it is possible to solve the health problem that multiple nutrients deficiency causes。Regulation according to " People's Republic of China's the law of food safety " and " new resource food management method " in 2011, approval pueraria root powder is as new resource food。Containing health-care effect active component such as macamide (macamides), Lepidinm meyenii Walp alkene (macaenes), glucosinolate, sterol, steroid in Lepidinm meyenii Walp, it it is a kind of natural food resource that full nutrition material can be provided to human body。Lepidinm meyenii Walp has resisting fatigue, defying age, endocrine regulation system, improves sexual function, improves fertility, improves effects such as sleeping, improve the quality of living。
Superfine powder be batch object particle space micron to nanometer between powder body material, micropowder is due to its fine size, and particle size distribution is little, uniform quality, thus it is big to have specific surface area, and biological activity is high。Chinese crude drug micropowder is to utilize superfine communication technique leading in the world that Chinese crude drug is implemented the pulvis that cell wall breaking processes。In Chinese crude drug, effective ingredient is stored in cell more, and superfine communication technique can break the cell wall in Chinese crude drug, makes intracellular effective ingredient fully discharge, thus improving the bioavailability of Chinese crude drug, is conducive to human body to the absorption of bioactive molecule and utilization。
In order to improve human body to the absorption rate of effective active health care molecule in Lepidinm meyenii Walp, now how Lepidinm meyenii Walp is made powder shape。The method preparing Lepidinm meyenii Walp powder at present mainly includes following two:
The first: by physical method, either directly through mechanical means, Lepidinm meyenii Walp raw material being made powdery, the method is pure physical process, but has some microorganisms in the course of processing and pollute, and has certain risk to edible, need to process prevention and control。
The first: pass through chemical method, grinding and processing process needs add the chemical drugss such as ethanol, chemical processes can improve the stability of gained pueraria root powder, not oxidizable, but owing to adding the chemical drugss such as ethanol, Lepidinm meyenii Walp product can exist chemical residual unavoidably, pill taker is easily brought adverse effect。
The micropowder that is processed into Lepidinm meyenii Walp can improve dissolution rate and the dissolution rate of Lepidinm meyenii Walp health-care effect bioactive molecule。Improve the absorbance of Maca reactive molecule, improve bioavailability。Ultrafine powder particle diameter is little, and specific surface area increases, and becomes big with the contact area of gastrointestinal mucosa, and Adhesion enhancement makes Maca reactive molecule time of staying in digestive tract long, and Maca reactive molecule absorption is more abundant, thus improve the bioavailability of Maca reactive molecule。
Lepidinm meyenii Walp raw material is after micronizing, and granularity becomes more tiny, and effective ingredient is easier to dissolution, and Maca reactive molecule also strengthens accordingly, thus reducing Lepidinm meyenii Walp to make consumption, is greatly saved Lepidinm meyenii Walp raw material。
Only inquire Chinese invention patent " a kind of Lepidinm meyenii Walp super-micro wall-broken breaking method " (Chinese patent CN105326881A) report at present and adopt many starch-medium chain triglyceride mixed powder technology of preparing, this technology to add the chemical substances such as medium chain triglyceride, has the quality after affecting Lepidinm meyenii Walp processing。
Summary of the invention
Purpose: for solving the deficiencies in the prior art, the present invention provides a kind of Lepidinm meyenii Walp micropowder and preparation method thereof, and Lepidinm meyenii Walp micropowder mean diameter prepared by the method reaches ultra-fine powder particle diameter≤10 μm。
Technical scheme: for solving above-mentioned technical problem, the technical solution used in the present invention is:
The preparation method of a kind of Lepidinm meyenii Walp micropowder, comprises the following steps:
(1) adopting the fresh Lepidinm meyenii Walp provided through the planting base of organic Lepidinm meyenii Walp certification is raw material；
(2), after fresh Lepidinm meyenii Walp is cleaned and dried, it is cut into Lepidinm meyenii Walp thin slice；
(3) Lepidinm meyenii Walp thin slice is dried naturally to water content and drop to 8-12%；
(4) the Lepidinm meyenii Walp thin slice after drying is placed on 20B Universalpulverizer model pulverizer, is ground into coarse powder, then be crushed to the pueraria root powder within 80 orders in carrying out；
(5) at-20 DEG C to 0 DEG C, pueraria root powder being carried out lyophilization, water content drops within 2%；
(6) the ultra-fine mechanical crusher of pueraria root powder LHJ after lyophilization is carried out comminution by gas stream；
(7) pueraria root powder that comminution by gas stream is crossed is put into mixer carries out mixing 20-60 minute, obtain Lepidinm meyenii Walp micropowder。
The Lepidinm meyenii Walp micropowder that the preparation method of above-mentioned Lepidinm meyenii Walp micropowder is made, grain diameter≤10 μm of 100%, mean diameter is 4.98 ± 0.32 μm, specific surface area is 2.91 ± 0.27 μm/g。
Beneficial effect: a kind of Lepidinm meyenii Walp micropowder provided by the invention and preparation method thereof, obtained Lepidinm meyenii Walp micropowder, grain diameter≤10 μm of 100%, mean diameter is 4.98 ± 0.32 μm, specific surface area is 2.91 ± 0.27 μm/g；Adopting the Lepidinm meyenii Walp micropowder granule that this processes becomes uniform, good dispersion, the course of processing remains Lepidinm meyenii Walp health-care effect bioactive molecule, and compared with Lepidinm meyenii Walp micropowder in the market, bioavailability is greatly improved。This product can be used for the fields such as Food and hygienical food。
Detailed description of the invention
Below in conjunction with embodiment, the present invention is illustrated:
The preparation method of Lepidinm meyenii Walp micropowder of the present invention, illustrates the present invention in conjunction with the embodiments:
1, adopting the fresh Lepidinm meyenii Walp provided through the planting base of organic Lepidinm meyenii Walp certification is raw material；
2, after clean for above-mentioned Lepidinm meyenii Walp drying, it is cut into Lepidinm meyenii Walp thin slice；
3, Lepidinm meyenii Walp thin slice is dried naturally to water content and drop to 8-12%；
4, the Lepidinm meyenii Walp thin slice after drying is placed on 20B Universalpulverizer model pulverizer, is ground into coarse powder, then within being crushed to 80 orders in carrying out；
5, above-mentioned pueraria root powder carries out low temperature (-20 DEG C to 0 DEG C) lyophilization, and water content drops within 2%；
6, the pueraria root powder after lyophilization is carried out comminution by gas stream with the ultra-fine mechanical crusher of LHJ again。
7, the pueraria root powder that comminution by gas stream is crossed is put into mixer carries out mixing 20-60 minute, obtain Lepidinm meyenii Walp micropowder。Detection mean diameter, powder delivery degree, and feature macamide dissolution rate more long-pending than table machine。
The Lepidinm meyenii Walp micropowder that the present invention is obtained, grain diameter≤10 μm of 100%, the Lepidinm meyenii Walp micropowder that mean diameter is 4.98 ± 0.32 μm, specific surface area is 2.91 ± 0.27 μm/g, this product can be used for the fields such as Food and hygienical food。
Below in conjunction with being embodied as being explained further the present invention, but the present invention is not done the restriction that task is formed by embodiment。
Embodiment 1
(1) taking the fresh Lepidinm meyenii Walp of 10KG is raw material, cleans up
(2) at room temperature naturally dry,
(3) fresh Lepidinm meyenii Walp is cut into Lepidinm meyenii Walp thin slice,
(4) naturally dry 32 days, drop to 10% to water content,
(5) coarse pulverization, is placed on above-mentioned Lepidinm meyenii Walp thin slice 20B Universalpulverizer model pulverizer, is ground into coarse powder, is broken into coarse powder, then within being crushed to 80 orders in carrying out。
(6) above-mentioned pueraria root powder being carried out frozen drying, water content drops within 2%。
(7) pueraria root powder after lyophilization is carried out comminution by gas stream with the ultra-fine mechanical crusher of LHJ again。
(8) pueraria root powder that comminution by gas stream is crossed is put into mixer carries out mixing 30 minutes, obtain Lepidinm meyenii Walp micropowder。Detection mean diameter, powder delivery degree, and feature macamide dissolution rate more long-pending than table machine。
Embodiment 2
(1) taking the fresh Lepidinm meyenii Walp of 10KG is raw material, cleans up
(2) at room temperature naturally dry,
(3) fresh Lepidinm meyenii Walp is cut into Lepidinm meyenii Walp thin slice,
(4) naturally dry 40 days, drop to 10% to water content,
(5) coarse pulverization, is placed on above-mentioned Lepidinm meyenii Walp thin slice 20B Universalpulverizer model pulverizer, is ground into coarse powder, is broken into coarse powder, then within being crushed to 80 orders in carrying out。
(6) above-mentioned pueraria root powder being carried out frozen drying, water content drops within 2%。
(7) pueraria root powder after lyophilization is carried out comminution by gas stream with the ultra-fine mechanical crusher of LHJ again。
(8) pueraria root powder that comminution by gas stream is crossed is put into mixer carries out mixing 60 minutes, obtain Lepidinm meyenii Walp micropowder。Detection mean diameter, powder delivery degree, and feature macamide dissolution rate more long-pending than table machine。
Lepidinm meyenii Walp micropowder prepared by the inventive method is adopted to have epigranular, good dispersion, it is possible to keeping Lepidinm meyenii Walp health-care effect bioactive molecule and Heat sensitive active molecule to greatest extent, be greatly improved Lepidinm meyenii Walp health-care effect bioactive molecule absorption rate。
Below disclosing the present invention with preferred embodiment, so it is not intended to limiting the invention, and all employings are equal to replacement or the technical scheme that obtains of equivalent transformation mode, all fall within protection scope of the present invention。
Claims (2)
1. a preparation method for Lepidinm meyenii Walp micropowder, comprises the following steps:
(1) adopting the fresh Lepidinm meyenii Walp provided through the planting base of organic Lepidinm meyenii Walp certification is raw material；
(2), after fresh Lepidinm meyenii Walp is cleaned and dried, it is cut into Lepidinm meyenii Walp thin slice；
(3) Lepidinm meyenii Walp thin slice is dried naturally to water content and drop to 8-12%；
(4) the Lepidinm meyenii Walp thin slice after drying is placed on 20B Universalpulverizer model pulverizer, is ground into coarse powder, then be crushed to the pueraria root powder within 80 orders in carrying out；
(5) at-20 DEG C to 0 DEG C, pueraria root powder being carried out lyophilization, water content drops within 2%；
(6) the ultra-fine mechanical crusher of pueraria root powder LHJ after lyophilization is carried out comminution by gas stream；
(7) pueraria root powder that comminution by gas stream is crossed is put into mixer carries out mixing 20-60 minute, obtain Lepidinm meyenii Walp micropowder。
2. a Lepidinm meyenii Walp micropowder, the preparation method of the Lepidinm meyenii Walp micropowder described in claim 1 is prepared from, it is characterized in that, grain diameter≤10 μm of described Lepidinm meyenii Walp micropowder 100%, mean diameter is 4.98 ± 0.32 μm, specific surface area is 2.91 ± 0.27 μm/g。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610134493.7A CN105687139A (en) | 2016-03-09 | 2016-03-09 | Superfine maca powder and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610134493.7A CN105687139A (en) | 2016-03-09 | 2016-03-09 | Superfine maca powder and preparation method thereof |
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| CN105687139A true CN105687139A (en) | 2016-06-22 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101416757A (en) * | 2008-12-08 | 2009-04-29 | 大连海晏堂生物有限公司 | Preparation method of beche-de-mer capsules |
| CN102716348A (en) * | 2012-07-04 | 2012-10-10 | 上海玉成干燥设备有限公司 | Method for preparing superfine rhizoma gastrodiae powder by vacuum freeze drying |
| CN103468511A (en) * | 2013-09-18 | 2013-12-25 | 无锡爱迪信光电科技有限公司 | Preparation method for maca daqu liquor |
| CN104323253A (en) * | 2014-11-06 | 2015-02-04 | 河北考力森生物科技有限公司 | Preparation method of ultra-fine maca powder |
-
2016
- 2016-03-09 CN CN201610134493.7A patent/CN105687139A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101416757A (en) * | 2008-12-08 | 2009-04-29 | 大连海晏堂生物有限公司 | Preparation method of beche-de-mer capsules |
| CN102716348A (en) * | 2012-07-04 | 2012-10-10 | 上海玉成干燥设备有限公司 | Method for preparing superfine rhizoma gastrodiae powder by vacuum freeze drying |
| CN103468511A (en) * | 2013-09-18 | 2013-12-25 | 无锡爱迪信光电科技有限公司 | Preparation method for maca daqu liquor |
| CN104323253A (en) * | 2014-11-06 | 2015-02-04 | 河北考力森生物科技有限公司 | Preparation method of ultra-fine maca powder |
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Application publication date: 20160622 |