CN105685114A - Preparation method of novel smokeless mosquito-repellent incense - Google Patents
Preparation method of novel smokeless mosquito-repellent incense Download PDFInfo
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
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- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/20—Combustible or heat-generating compositions
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
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Abstract
The invention discloses a preparation method of novel smokeless mosquito-repellent incense, belonging to the technical field of preparation of the mosquito-repellent incense. The novel smokeless mosquito-repellent incense is prepared by the steps of preparing sludge carbon powder, preparing paste, molding the paste, drying the molded paste, spraying chemicals onto a dry mosquito-repellent incense blank, and the like. According to the preparation method, sludge carbon is taken as an incendiary agent, and an inorganic substance in the sludge carbon is taken as a flame retardant, so that not only is a new way provided for the resource utilization of the sludge carbon, but mass disafforestation caused by the mosquito-repellent incense industry is also avoided, and the preparation method of the novel smokeless mosquito-repellent incense is beneficial to environmental protection. The novel smokeless mosquito-repellent incense is non-toxic and harmless and can meet the requirement of environmental protection for the product; after the novel smokeless mosquito-repellent incense is burnt and absorbed by the human body, asthma, nerve poisoning and cancers are not caused; the novel smokeless mosquito-repellent incense has a smooth appearance, is free from fracture and mildew spots, and has the breaking-resistant strength of 425-456g and the ignition point time of 8.61-9.01h; in the burning process, smoke is not generated; the novel smokeless mosquito-repellent incense avoids a phenomenon of broken-end flameout when being burnt to an iron-tooth disk.
Description
Technical field
The invention belongs to mosquito incense preparing technical field, the preparation method being specifically related to a kind of Novel smokeless mosquito incense。
Background technology
Municipal sludge be sanitary sewage processing procedure in isolated solid matter。These solid matters be probably in sewage already, the suspended material that retains in various natural sedimentation ponds；It is likely in sewage disposal process to convert and is formed, in biological treatment and chemical treating process, original dissolved matter and colloidal substance the biological floe being transformed and suspended material。But in general, the mud of municipal sewage plant belongs to organic sludge, it is characterized in content of organics high (60%-80%), granule thin (0.02-0.2mm), the little (1.002-1.006g/cm of density3), become colloform texture, account for total 0.3%-0.5% processing the water yield。Moisture percentage in sewage sludge and content of organics are high, it is easy to rot smelly, it is possible to create serious secondary pollution。
Recent years, the Chinese government increased the dynamics of investment of sewage disposal, significant progress has been had in waste water control, investigated many sewage treatment techniques, new technique, and built up a lot of sewage treatment plant, improve the aggregate level of wastewater treatment in China, the treating capacity of municipal sewage increases year by year, by-product municipal sludge as municipal sewage treatment, annual production also sharply increases, how properly to dispose sewage plant sludge, and it can be used as a kind of new resource effectively to be utilized, it has also become environmental protection circle is deeply for the key subjects of concern。
One of approach that current recycling sludge utilizes is that mud is prepared Viability carbon, but due in sludge carbonization product inorganic matter more, sometimes account for more than 50%, adsorption capacity is little, and commercial value is little。Therefore, how mud carbonized product being carried out Deep utilization is an interesting and challenging problem。
Mosquito incense, from invention in 1880 existing more than 100 year so far, it is always up the essential product of family's mosquito killer, it is to be blended in by insecticidal active ingredient in the combustible material such as wood powder, then its smoulder in the regular hour is allowed, it is vaporized out by the active ingredient of parasite killing, after active ingredient such in certain space reaches finite concentration, just mosquito generation can be stimulated, drives, benumbs, knocks down and lethal effect。
Being now helical form with mosquito incense, therefore be referred to as coiled mosquito-repellent incense that total length 130cm generally can light 7-8h, after it, the temperature at 6-8mm place is at about 170 DEG C, is exactly in mosquito incense parasite killing and volatilization temperature needed for essence active ingredient。The basic processing technology of mosquito incense is the mixture such as incendiary agent, binding agent, fire retardant and dyestuff to be added water stir to make mosquito-repellent incense blank (i.e. dry body) then through kneading, crowded base, punch die, drying, then sprays insecticide on dry body surface and is just made for mosquito incense。The incendiary agent of mosquito incense dry body is mainly powdered carbon, fire retardant is clay etc., is mainly used in controlling burning velocity。
Existing mosquito incense binding agent mainly adopts composite adhesives such as carboxymethyl cellulose, polyacrylamide etc.。Adopting substantial amounts of composite adhesives in mosquito incense, bring substantial amounts of environmental protection and health problem, being absorbed by the body after the burning of these chemical substances to cause asthma, and neurotoxic, long-term suction even can cause cancer。Therefore, the mosquito incense binding agent how developing a kind of environmental protection becomes new research direction。
At present in the world, particularly in Asia, Africa, Latin America, the people exceeding world population more than 2/3 uses mosquito incense, and China produces in the world especially, uses, the big country of outlet mosquito incense, and annual production is more than 10,000,000,000 dishes。With single disc mosquito incense 15g, in mosquito incense, carbon content rate 70% calculates, then need consumption more than 1.05 × 10 every year5T powdered carbon, thus substantial amounts of number and bamboo will be cut down to meet requirement。
Summary of the invention
The preparation method that the present invention provides a kind of Novel smokeless mosquito incense, to solve according to a large amount of disafforestations existed in the composition of existing mosquito incense and preparation process, and adopt the binding agents such as a large amount of carboxymethyl cellulose, polyacrylamide, bring substantial amounts of environmental protection and health problem。The present invention utilizes mud carbon as incendiary agent, utilizes the inorganic matter in mud carbon as fire retardant, and the recycling not being only mud carbon provides a new approach, it also avoid a large amount of disafforestation of mosquito incense industry simultaneously, is conducive to environmental conservation；The Novel smokeless mosquito incense of the present invention is nontoxic, can meet the requirement to product of the environmental protection aspect, and being absorbed by the body after this Novel smokeless mosquito incense burning to cause asthma, neurotoxic, causes cancer；The Novel smokeless mosquito incense flat appearance of the present invention, without fracture, without mildew, fracture resistence force is strong, burning-point time foot, and combustion process is smokeless, crosses iron teeth dish not " broken end " flame-out。
For solving above technical problem, the present invention by the following technical solutions:
The preparation method of a kind of Novel smokeless mosquito incense, comprises the following steps:
S1: after mud is dried 20-23h at 106-110 DEG C; under the protection of nitrogen or carbon dioxide, it is warming up to 500-600 DEG C with the heating rate of 20-25 DEG C/min, carbonization 0.6-1h; cooled obtain mud carbon, by broken for described mud carbon dust cross 60-80 mesh sieve after prepare mud carbon dust；
S2: take step S1 prepare mud carbon dust 140-160 part, anthracite 6-8 part, binding agent 24-30 part, mica powder 4-6 part, water 400-480 part, be 60-70 DEG C in temperature, rotating speed be under 200-300r/min stirring 1-2h, prepare pastel；
S3: be placed in model by the pastel that step S2 prepares, dry to water content≤10% after compacting, the demoulding at 45-55 DEG C, prepares mosquito incense dry body；
S4: mosquito incense liquid medicine be uniformly sprayed at the step S3 mosquito incense dry body surface prepared and dry water content≤7% at 30-35 DEG C, preparing Novel smokeless mosquito incense；
The preparation method of binding agent described in step S2, comprises the following steps:
S21: compound concentration is the potato starch pulp A of 22-25Be '；
S22: adding dimethyl adipate, dimethyl acetylamide in the potato starch pulp A of step S21 is stir cross-linked graft reaction 35-42min under 32-38 DEG C of condition in temperature, prepares slurry B；
S23: the slurry B of step S22 is delivered in drying machine and carries out pre-gelatinized and dry at temperature is 135-145 DEG C, prepare material C；
S24: after the material C of step S23 is pulverized, sieved, wind is delivered to separator and is collected, prepares binding agent。
Preferably, the concentration of dimethyl adipate described in step S22 is 1%-1.2%。
Preferably, described in step S22, the rotating speed of stirring is 100-120r/min。
Preferably, drying machine described in step S23 is cylindrical drier。
Preferably, water content≤6% of material C described in step S23。
Preferably, in step S24, material C crosses the sieve of 60-100 order after pulverizing。
Preferably, separator described in step S24 is whirlwind separator。
Preferably, mosquito incense liquid medicine described in step S4, in units of weight portion, including following raw material: d-allethrin 20-30 part, nemamort 10-20 part, Oleum menthae 2-4 part, Aesculus chinensis Bunge alcohol extract 1-3 part, Folium Artemisiae Argyi alcohol extract 1-3 part, leaf of tea tree alcohol extract 1-3 part。
The method have the advantages that
(1) present invention utilizes mud carbon as incendiary agent; utilize the inorganic matter in mud carbon as fire retardant; the recycling not being only mud carbon provides a new approach; improve the efficiency of sewage disposal; reduce the difficulty of sewage disposal; also avoid a large amount of disafforestation of mosquito incense industry, be conducive to environmental conservation；
(2) present invention adopts mica powder as adsorbent, and in minimizing preparation process, effective ingredient scatters and disappears, it is ensured that the product stability when storing；
(3) present invention adopts d-allethrin, nemamort, Aesculus chinensis Bunge alcohol extract, Folium Artemisiae Argyi alcohol extract, leaf of tea tree alcohol extract as mosquito incense liquid medicine, neither produces bad smell, can increase again the effect of killing mosquito during burning；
(4) increasing Oleum menthae in the Novel smokeless mosquito incense of the present invention, the gas delicate fragrance distributed is pleasant, is adapted at the places such as family, hotel, office and uses；
(5) the Novel smokeless mosquito incense of the present invention is nontoxic, can meet the requirement to product of the environmental protection aspect, and being absorbed by the body after this Novel smokeless mosquito incense burning to cause asthma, neurotoxic, causes cancer；
(6) present invention Novel smokeless mosquito incense flat appearance, without fracture, without mildew, fracture resistence force is strong, burning-point time foot, and combustion process is smokeless, crosses iron teeth dish not " broken end " flame-out。
Detailed description of the invention
For ease of being more fully understood that the present invention, being illustrated by following instance, these examples belong to protection scope of the present invention, but are not intended to protection scope of the present invention。
In an embodiment, the preparation method of Novel smokeless mosquito incense, comprise the following steps:
S1: after mud is dried 20-23h at 106-110 DEG C; under the protection of nitrogen or carbon dioxide, it is warming up to 500-600 DEG C with the heating rate of 20-25 DEG C/min, carbonization 0.6-1h; cooled obtain mud carbon, by broken for described mud carbon dust cross 60-80 mesh sieve after prepare mud carbon dust；
S2: take step S1 prepare mud carbon dust 140-160 part, anthracite 6-8 part, binding agent 24-30 part, mica powder 4-6 part, water 400-480 part, be 60-70 DEG C in temperature, rotating speed be under 200-300r/min stirring 1-2h, prepare pastel；
S3: be placed in model by the pastel that step S2 prepares, dry to water content≤10% after compacting, the demoulding at 45-55 DEG C, prepares mosquito incense dry body；
S4: mosquito incense liquid medicine be uniformly sprayed at the step S3 mosquito incense dry body surface prepared and dry water content≤7% at 30-35 DEG C, preparing Novel smokeless mosquito incense。
Wherein, the preparation method of binding agent described in step S2, comprise the following steps:
S21: compound concentration is the potato starch pulp A of 22-25Be '；
S22: adding concentration to the potato starch pulp A in step S21 is 1%-1.2% dimethyl adipate, dimethyl acetylamide, is then 32-38 DEG C in temperature, speed of agitator is carry out cross-linked graft reaction 35-42min under 100-120r/min, prepares slurry B；
S23: the slurry B of step S22 is delivered in cylindrical drier and carries out pre-gelatinized and dry at temperature is 135-145 DEG C, prepare the material C of water content≤6%；
S24: the material C of step S23 is pulverized, crosses wind after 60-100 mesh sieve and deliver to whirlwind separator and be collected, prepare binding agent。
Wherein, mosquito incense liquid medicine described in step S4, in units of weight portion, including following raw material: d-allethrin 20-30 part, nemamort 10-20 part, Oleum menthae 2-4 part, Aesculus chinensis Bunge alcohol extract 1-3 part, Folium Artemisiae Argyi alcohol extract 1-3 part, leaf of tea tree alcohol extract 1-3 part。
Below by way of embodiment more specifically, the present invention will be described in detail。
Embodiment 1
The preparation method of a kind of Novel smokeless mosquito incense, comprises the following steps:
S1: after dry 23h, under the protection of nitrogen, with the heating rate of 20 DEG C/min, mud is warming up to 500 DEG C at 106 DEG C, carbonization 1h, cooled obtain mud carbon, will prepare mud carbon dust after described mud carbon dust broken mistake 60 mesh sieve；
S2: take step S1 prepare mud carbon dust 140 parts, 6 parts of anthracite, binding agent 24 parts, mica powder 4 parts, 400 parts of water, be 60 DEG C in temperature, rotating speed be under 200r/min stirring 2h, prepare pastel；
S3: be placed in model by the pastel that step S2 prepares, drying at 45 DEG C after compacting, the demoulding to water content is 10%, prepares mosquito incense dry body；
S4: mosquito incense liquid medicine is uniformly sprayed at step S3 prepare mosquito incense dry body surface and at 30 DEG C dry water content be 7%, prepare Novel smokeless mosquito incense。
Wherein, the preparation method of binding agent described in step S2, comprise the following steps:
S21: compound concentration is the potato starch pulp A of 22Be '；
S22: adding concentration to the potato starch pulp A in step S21 is 1% dimethyl adipate, dimethyl acetylamide, is then 32 DEG C in temperature, speed of agitator is carry out cross-linked graft reaction 42min under 100r/min, prepares slurry B；
S23: be delivered in cylindrical drier by the slurry B of step S22 to carry out pre-gelatinized and temperature be at 135 DEG C dry, prepared water content is the material C of 6%；
S24: the material C of step S23 is pulverized, crosses wind after 60 mesh sieves and deliver to whirlwind separator and be collected, prepare binding agent。
Wherein, mosquito incense liquid medicine described in step S4, in units of weight portion, including following raw material: d-allethrin 20 parts, nemamort 10 parts, Oleum menthae 2 parts, Aesculus chinensis Bunge alcohol extract 1 part, Folium Artemisiae Argyi alcohol extract 1 part, leaf of tea tree alcohol extract 1 part。
Embodiment 2
The preparation method of a kind of Novel smokeless mosquito incense, comprises the following steps:
S1: after dry 20h, under the protection of nitrogen or carbon dioxide, with the heating rate of 25 DEG C/min, mud is warming up to 600 DEG C at 110 DEG C, carbonization 0.6h, cooled obtain mud carbon, will prepare mud carbon dust after described mud carbon dust broken mistake 80 mesh sieve；
S2: take step S1 prepare mud carbon dust 160 parts, 8 parts of anthracite, binding agent 30 parts, mica powder 6 parts, 480 parts of water, be 70 DEG C in temperature, rotating speed be under 300r/min stirring 1h, prepare pastel；
S3: be placed in model by the pastel that step S2 prepares, drying at 55 DEG C after compacting, the demoulding to water content is 8%, prepares mosquito incense dry body；
S4: mosquito incense liquid medicine is uniformly sprayed at step S3 prepare mosquito incense dry body surface and at 35 DEG C dry water content be 5%, prepare Novel smokeless mosquito incense。
Wherein, the preparation method of binding agent described in step S2, comprise the following steps:
S21: compound concentration is the potato starch pulp A of 25Be '；
S22: adding concentration to the potato starch pulp A in step S21 is 1.2% dimethyl adipate, dimethyl acetylamide, is then 38 DEG C in temperature, speed of agitator is carry out cross-linked graft reaction 35min under 120r/min, prepares slurry B；
S23: be delivered in cylindrical drier by the slurry B of step S22 to carry out pre-gelatinized and temperature be at 145 DEG C dry, prepared water content is the material C of 5%；
S24: the material C of step S23 is pulverized, crosses wind after 100 mesh sieves and deliver to whirlwind separator and be collected, prepare binding agent。
Wherein, mosquito incense liquid medicine described in step S4, in units of weight portion, including following raw material: d-allethrin 30 parts, nemamort 20 parts, Oleum menthae 4 parts, Aesculus chinensis Bunge alcohol extract 3 parts, Folium Artemisiae Argyi alcohol extract 3 parts, leaf of tea tree alcohol extract 3 parts。
Embodiment 3
The preparation method of a kind of Novel smokeless mosquito incense, comprises the following steps:
S1: after dry 22h, under the protection of nitrogen or carbon dioxide, with the heating rate of 25 DEG C/min, mud is warming up to 550 DEG C at 108 DEG C, carbonization 0.8h, cooled obtain mud carbon, will prepare mud carbon dust after described mud carbon dust broken mistake 70 mesh sieve；
S2: take step S1 prepare mud carbon dust 150 parts, 7 parts of anthracite, binding agent 27 parts, mica powder 5 parts, 440 parts of water, be 65 DEG C in temperature, rotating speed be under 250r/min stirring 1.5h, prepare pastel；
S3: be placed in model by the pastel that step S2 prepares, drying at 50 DEG C after compacting, the demoulding to water content is 7%, prepares mosquito incense dry body；
S4: mosquito incense liquid medicine is uniformly sprayed at step S3 prepare mosquito incense dry body surface and at 32 DEG C dry water content be 4%, prepare Novel smokeless mosquito incense。
Wherein, the preparation method of binding agent described in step S2, comprise the following steps:
S21: compound concentration is the potato starch pulp A of 24Be '；
S22: adding concentration to the potato starch pulp A in step S21 is 1.1% dimethyl adipate, dimethyl acetylamide, is then 35 DEG C in temperature, speed of agitator is carry out cross-linked graft reaction 38min under 110r/min, prepares slurry B；
S23: be delivered in cylindrical drier by the slurry B of step S22 to carry out pre-gelatinized and temperature be at 140 DEG C dry, prepared water content is the material C of 4%；
S24: the material C of step S23 is pulverized, crosses wind after 80 mesh sieves and deliver to whirlwind separator and be collected, prepare binding agent。
Wherein, mosquito incense liquid medicine described in step S4, in units of weight portion, including following raw material: d-allethrin 250 parts, nemamort 15 parts, Oleum menthae 3 parts, Aesculus chinensis Bunge alcohol extract 2 parts, Folium Artemisiae Argyi alcohol extract 2 parts, leaf of tea tree alcohol extract 2 parts。
Embodiment 4
The preparation method of a kind of Novel smokeless mosquito incense, comprises the following steps:
S1: after dry 22h, under the protection of nitrogen or carbon dioxide, with the heating rate of 20 DEG C/min, mud is warming up to 600 DEG C at 107 DEG C, carbonization 0.6h, cooled obtain mud carbon, will prepare mud carbon dust after described mud carbon dust broken mistake 80 mesh sieve；
S2: take step S1 prepare mud carbon dust 145 parts, 6 parts of anthracite, binding agent 26 parts, mica powder 5 parts, 420 parts of water, be 65 DEG C in temperature, rotating speed be under 250r/min stirring 1.5h, prepare pastel；
S3: be placed in model by the pastel that step S2 prepares, drying at 50 DEG C after compacting, the demoulding to water content is 9%, prepares mosquito incense dry body；
S4: mosquito incense liquid medicine is uniformly sprayed at step S3 prepare mosquito incense dry body surface and at 30 DEG C dry water content be 5%, prepare Novel smokeless mosquito incense。
Wherein, the preparation method of binding agent described in step S2, comprise the following steps:
S21: compound concentration is the potato starch pulp A of 23Be '；
S22: adding concentration to the potato starch pulp A in step S21 is 1% dimethyl adipate, dimethyl acetylamide, is then 33 DEG C in temperature, speed of agitator is carry out cross-linked graft reaction 41min under 100r/min, prepares slurry B；
S23: be delivered in cylindrical drier by the slurry B of step S22 to carry out pre-gelatinized and temperature be at 138 DEG C dry, prepared water content is the material C of 6%；
S24: the material C of step S23 is pulverized, crosses wind after 70 mesh sieves and deliver to whirlwind separator and be collected, prepare binding agent。
Wherein, mosquito incense liquid medicine described in step S4, in units of weight portion, including following raw material: d-allethrin 22 parts, nemamort 12 parts, Oleum menthae 2 parts, Aesculus chinensis Bunge alcohol extract 1 part, Folium Artemisiae Argyi alcohol extract 1 part, leaf of tea tree alcohol extract 1 part。
Embodiment 5
The preparation method of a kind of Novel smokeless mosquito incense, comprises the following steps:
S1: after dry 21h, under the protection of nitrogen or carbon dioxide, with the heating rate of 25 DEG C/min, mud is warming up to 600 DEG C at 109 DEG C, carbonization 0.6h, cooled obtain mud carbon, will prepare mud carbon dust after described mud carbon dust broken mistake 60 mesh sieve；
S2: take step S1 prepare mud carbon dust 155 parts, 8 parts of anthracite, binding agent 28 parts, mica powder 6 parts, 460 parts of water, be 70 DEG C in temperature, rotating speed be under 300r/min stirring 1h, prepare pastel；
S3: be placed in model by the pastel that step S2 prepares, drying at 55 DEG C after compacting, the demoulding to water content is 8%, prepares mosquito incense dry body；
S4: mosquito incense liquid medicine is uniformly sprayed at step S3 prepare mosquito incense dry body surface and at 35 DEG C dry water content be 6%, prepare Novel smokeless mosquito incense。
Wherein, the preparation method of binding agent described in step S2, comprise the following steps:
S21: compound concentration is the potato starch pulp A of 24Be '；
S22: adding concentration to the potato starch pulp A in step S21 is 1.2% dimethyl adipate, dimethyl acetylamide, is then 37 DEG C in temperature, speed of agitator is carry out cross-linked graft reaction 36min under 120r/min, prepares slurry B；
S23: be delivered in cylindrical drier by the slurry B of step S22 to carry out pre-gelatinized and temperature be at 142 DEG C dry, prepared water content is the material C of 3%；
S24: the material C of step S23 is pulverized, crosses wind after 90 mesh sieves and deliver to whirlwind separator and be collected, prepare binding agent。
Wherein, mosquito incense liquid medicine described in step S4, in units of weight portion, including following raw material: d-allethrin 28 parts, nemamort 18 parts, Oleum menthae 4 parts, Aesculus chinensis Bunge alcohol extract 3 parts, Folium Artemisiae Argyi alcohol extract 2 parts, leaf of tea tree alcohol extract 2 parts。
In embodiment 1-5 shown in the binder performance parameter list 1 of preparation。
Table 1 binder performance parameter
| Embodiment | Viscosity mPa.s | PH value | Moisture % | Outward appearance |
| 1 | 7787 | 6.3 | 5 | White powder |
| 2 | 8007 | 6.7 | 4 | White powder |
| 3 | 7876 | 6.4 | 3 | White powder |
| 4 | 7832 | 6.4 | 6 | White powder |
| 5 | 7918 | 6.5 | 3 | White powder |
In embodiment 1-5, the Novel smokeless mosquito incense performance parameter of preparation is as shown in table 2。
Table 2 mosquito incense performance parameter
| Detection project | Standard-required | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Weight (g) | ≥ 40 | 40.65 | 40.93 | 40.81 | 40.72 | 40.86 |
| Thickness (mm) | ≥ 19 | 19.31 | 19.88 | 19.59 | 19.43 | 19.78 |
| Fracture resistence force (g) | ≥ 250 | 425 | 456 | 441 | 433 | 448 |
| Water content (%) | ≤ 7 | 7 | 5 | 4 | 5 | 6 |
| Burning-point time (h) | ≥ 8 | 8.61 | 9.01 | 8.79 | 8.69 | 8.9 |
Above content is it cannot be assumed that the present invention is embodied as being confined to these explanations; for general technical staff of the technical field of the invention; without departing under present inventive concept premise; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by submitted claims。
Claims (1)
1. the preparation method of a Novel smokeless mosquito incense, it is characterised in that comprise the following steps:
S1: after mud is dried 20-23h at 106-110 DEG C; under the protection of nitrogen or carbon dioxide, it is warming up to 500-600 DEG C with the heating rate of 20-25 DEG C/min, carbonization 0.6-1h; cooled obtain mud carbon, by broken for described mud carbon dust cross 60-80 mesh sieve after prepare mud carbon dust；
S2: take step S1 prepare mud carbon dust 140-160 part, anthracite 6-8 part, binding agent 24-30 part, mica powder 4-6 part, water 400-480 part, be 60-70 DEG C in temperature, rotating speed be under 200-300r/min stirring 1-2h, prepare pastel；
S3: be placed in model by the pastel that step S2 prepares, dry to water content≤10% after compacting, the demoulding at 45-55 DEG C, prepares mosquito incense dry body；
S4: mosquito incense liquid medicine be uniformly sprayed at the step S3 mosquito incense dry body surface prepared and dry water content≤7% at 30-35 DEG C, preparing Novel smokeless mosquito incense；
Wherein, the preparation method of binding agent described in step S2, comprise the following steps:
S21: compound concentration is the potato starch pulp A of 22-25Be '；
S22: adding concentration to the potato starch pulp A in step S21 is 1%-1.2% dimethyl adipate, dimethyl acetylamide, is then 32-38 DEG C in temperature, speed of agitator is carry out cross-linked graft reaction 35-42min under 100-120r/min, prepares slurry B；
S23: the slurry B of step S22 is delivered in cylindrical drier and carries out pre-gelatinized and dry at temperature is 135-145 DEG C, prepare the material C of water content≤6%；
S24: the material C of step S23 is pulverized, crosses wind after 60-100 mesh sieve and deliver to whirlwind separator and be collected, prepare binding agent；
Mosquito incense liquid medicine described in step S4, in units of weight portion, including following raw material: d-allethrin 20-30 part, nemamort 10-20 part, Oleum menthae 2-4 part, Aesculus chinensis Bunge alcohol extract 1-3 part, Folium Artemisiae Argyi alcohol extract 1-3 part, leaf of tea tree alcohol extract 1-3 part。
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101810165A (en) * | 2010-03-19 | 2010-08-25 | 中山大学 | Smokeless mosquito incense blank and preparation method thereof |
| CN102754658A (en) * | 2012-06-25 | 2012-10-31 | 安徽立康杀虫制品有限公司 | Smokeless mosquito coil and preparation method thereof |
| CN104041486A (en) * | 2014-06-13 | 2014-09-17 | 华侨大学 | Mosquito-repellent incense prepared from sewage sludge |
| CN105248458A (en) * | 2015-11-16 | 2016-01-20 | 梁俊 | Powdered valerian mosquito-repellent incense and preparation method thereof |
-
2016
- 2016-03-25 CN CN201610175416.6A patent/CN105685114A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101810165A (en) * | 2010-03-19 | 2010-08-25 | 中山大学 | Smokeless mosquito incense blank and preparation method thereof |
| CN102754658A (en) * | 2012-06-25 | 2012-10-31 | 安徽立康杀虫制品有限公司 | Smokeless mosquito coil and preparation method thereof |
| CN104041486A (en) * | 2014-06-13 | 2014-09-17 | 华侨大学 | Mosquito-repellent incense prepared from sewage sludge |
| CN105248458A (en) * | 2015-11-16 | 2016-01-20 | 梁俊 | Powdered valerian mosquito-repellent incense and preparation method thereof |
Non-Patent Citations (4)
| Title |
|---|
| "《中华传统文化知识一本通》" * |
| 张玉龙等: "《淀粉胶黏剂》", 31 January 2008, 化学工业出版社 * |
| 朱成璞: "《卫生杀虫药械应用指南》", 31 March 1989, 上海交通大学出版社 * |
| 李东光: "《150种卫生消杀灭产品配方与制作》", 30 September 2011, 化学工业出版社 * |
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