CN105665104A - Superfine granule crushing device and crushing method - Google Patents

Superfine granule crushing device and crushing method Download PDF

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Publication number
CN105665104A
CN105665104A CN201610224484.7A CN201610224484A CN105665104A CN 105665104 A CN105665104 A CN 105665104A CN 201610224484 A CN201610224484 A CN 201610224484A CN 105665104 A CN105665104 A CN 105665104A
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China
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broken
pressure fluid
raw material
high pressure
ultra
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CN201610224484.7A
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CN105665104B (en
Inventor
邢东骏
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Chuzhou Jian Dun CNC Technology Co., Ltd.
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Suzhou Jinning Nano Technology Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C19/00Other disintegrating devices or methods
    • B02C19/06Jet mills

Abstract

The invention discloses a superfine granule crushing device and crushing method.The superfine granule crushing device comprises a crushing and mixing chamber provided with a high-pressure fluid input opening and a raw material input opening and a crushing nozzle.The superfine granule crushing method comprises the steps that a high-pressure fluid enters the crushing and mixing chamber through the high-pressure fluid input opening, and negative pressure is generated in the crushing and mixing chamber to enable raw materials to be sucked into the crushing and mixing chamber from the raw material input opening and mixed with the high-pressure fluid, so that the raw materials are sheared and crushed, first-time crushing is achieved, and first mixed materials containing the first-time crushing raw materials and the high-pressure fluid are formed; the first mixed materials are sprayed out through the crushing nozzle, a hole blasting effect is utilized for enabling the first-time crushing raw materials contained in the first mixed raw materials to be subjected to second-time crushing, and second mixed raw materials containing second-time crushing raw materials and the high-pressure fluid are formed.The superfine granule crushing device and crushing method can crush powered or granular or liquid raw materials to a micro or nano scale, the using performance of the materials is improved, and large-scale industrial production is achieved.

Description

A kind of ultra-fine grain shredder assembly and breaking method
Technical field
The present invention relates to a kind of ultra-fine grain shredder assembly, in particular to a kind of ultra-fine grain shredder assembly and utilize its breaking method that raw material carried out micron, nano level fragmentation, belong to disintegrating apparatus technical field.
Background technology
The preparation of nano material is the most important basic technology of nanotechnology research, what preparation nano material major part adopted at present is vapor phase process and liquid phase method, the feature such as these methods all exist complex process, it is meticulous to operate, cost is expensive or precursor power is difficult, a small amount of sample preparation in laboratory can only be realized, it is difficult to realize suitability for industrialized production.
Also have some preparation methods relating to nano level raw material at present, it is all first by object broken wall, or carries out high-temperature water by water, alcohol or carbonic acid gas equal solvent and boil, add tensio-active agent, and by methods such as stirring, ultrasonic activation, high pressure matter machine pulverizing, to obtain nano level raw material. But by these preparation method's equipment useds, mostly efficiency is low, and energy consumption is big, produces with maintenance cost all very high, and for realizing the scale operation of nano level raw material, existing installation is difficult to realize. Moreover, if the solvent added or tensio-active agent and raw material generation chemical reaction, also can produce derivative, the difficulty of nanometer shattering process can be improved further.
Thus, according to the shortcoming that existing nanometer of disintegrating apparatus exists, how to be improved further, it is to increase crushing efficiency, Simplified flowsheet method, become the research direction that current industry research staff is new.
Summary of the invention
The main purpose of the present invention is to provide a kind of ultra-fine grain shredder assembly and breaking method, to overcome deficiency of the prior art.
For realizing aforementioned invention object, the technical solution used in the present invention comprises:
Embodiments providing a kind of ultra-fine grain shredder assembly, it comprises:
Broken room, batch mixing chamber, there is high pressure fluid input aperture and feedstock input, high pressure fluid enters broken room, batch mixing chamber continuously through described high pressure fluid input aperture, and in the indoor generation negative pressure in broken batch mixing chamber, raw material is made to be inhaled into broken room, batch mixing chamber from feedstock input and mix with described high pressure fluid and by flow velocity difference shearing-crushing, formed and include the raw material of primary fragmentation and the first mixture of high pressure fluid;
Broken shower nozzle, for receiving the first mixture that described broken room, batch mixing chamber exports, and utilize hole explosion effect to make the raw material of the primary fragmentation contained by described first mixture by secondary breaking, thus formed and include the raw material of secondary breaking and the 2nd mixture of high pressure fluid.
As one of the preferred version of the present invention, described ultra-fine grain shredding unit also comprises: broken target, it is arranged on and the material outlet corresponding position of described broken shower nozzle, the 2nd mixture that described broken shower nozzle is exported directly clashes into described broken target, thus makes the raw material of the secondary breaking contained by described 2nd mixture by tertiary crushing.
Preferably, the raw material of described primary fragmentation or the raw material of secondary breaking have micron-level particle size or nano level particle diameter.
Preferred, the raw material of described secondary breaking or the raw material of tertiary crushing have micron-level particle size or nano level particle diameter.
Further, the pressure of described high pressure fluid is 350-400MPa, and described high pressure fluid is preferably water, it is also possible to be gas or oil, and is especially preferably water.
Described raw material can be powder shaped, particulate state, liquid state or other suitable form.
As another preferred version, described ultra-fine grain shredding unit also comprises: shredder assembly bucket, and for receiving the raw material of tertiary crushing, the top of described shredder assembly bucket and broken batch mixing chamber, bottom is provided with raw material delivery port.
Further, described broken room, batch mixing chamber is connected with device for supplying high-pressure fluid by high pressure fluid input aperture, and described high pressure fluid input aperture place is also provided with gland nut, is also provided with spiral shell cover core in described gland nut.
Further, described high pressure fluid input aperture is connected with a high pressure fluid nozzle, feedstock input is arranged at the side of broken room, batch mixing chamber, and the material conveying passage with broken indoor, batch mixing chamber is connected, material conveying passage is vertically arranged, and broken shower nozzle is arranged at the end of described material conveying passage.
Concrete, the arranged outside of described broken shower nozzle has shower nozzle set nut;
And/or it is provided with shower nozzle gripping sleeve between described broken shower nozzle and shower nozzle set nut.
Preferably, described broken target is arranged on broken target seat, the described broken U-shaped structure of target seat.
Preferably, described raw material delivery port is connected with vacuum concentrating apparatus.
The embodiment of the present invention additionally provides a kind of ultra-fine grain breaking method, mainly implements based on aforementioned ultra-fine grain shredder assembly, comprising:
High pressure fluid enters broken room, batch mixing chamber continuously by high pressure fluid input aperture, and in the indoor generation negative pressure in broken batch mixing chamber, make raw material from feedstock input be inhaled into broken batch mixing chamber indoor and mix with described high pressure fluid and by the poor shearing-crushing of flow velocity, produce first time broken, and formed and include the raw material of primary fragmentation and the first mixture of high pressure fluid;
First mixture is by broken shower nozzle ejection, and utilizes hole explosion effect to make the raw material of the primary fragmentation contained by described first mixture by secondary breaking, is thus formed and includes the raw material of secondary breaking and the 2nd mixture of high pressure fluid.
Preferably, described breaking method also comprises:
Described 2nd mixture directly impinges upon on described broken target, thus makes the raw material of the secondary breaking contained by described 2nd mixture by tertiary crushing, finally obtains the raw material of ultra-fine grain.
Further, normal pressure fluid enters device for supplying high-pressure fluid, by normal pressure pressurized with fluid to 350-400MPa, enters ultra-fine grain shredder assembly.
Compared with prior art, the advantage of the present invention comprises:
(1) the ultra-fine grain shredder assembly of the present invention, structure is simple, produce with maintenance cost low, crushing efficiency height, good stability, it is possible to fully broken raw material, the particularly raw material such as powder shaped, particulate state, liquid, make its internal particle size reach micro-/ nano rank, particularly Nano grade, thus greatly increase the use properties of material.
(2) the ultra-fine grain breaking method of the present invention, technological operation is simple, utilize high pressure fluid that raw material sucks broken room, batch mixing chamber, by regulating the pressure of high pressure fluid, broken number of times etc., can the degree of controlled fragmentation, it is achieved the abundant fragmentation of raw material, reaches micro-/ nano rank, particularly Nano grade, is easy to realize large-scale industrial production.
(3) the nano level raw material that preliminary treatment of the present invention obtains, adopts vacuum concentrating apparatus to concentrate further, and the medium obtained enters device for supplying high-pressure fluid again, can be recycled, and nontoxic pollution-free discharges.
(4) the whole technique of the present invention is physical action, does not produce chemical by-product, can be widely used in the technical fields such as pharmacy, chemical industry and biology.
Accompanying drawing explanation
Fig. 1 is the structural representation of ultra-fine grain shredder assembly in the preferred embodiment of the present invention;
Fig. 2 is the part structure for amplifying schematic diagram of Fig. 1;
Fig. 3 is the partial enlargement structural representation of broken shower nozzle in the preferred embodiment of the present invention.
Description of reference numerals: 1-shredder assembly bucket, 2-high pressure fluid transfer line, 20-high pressure fluid joint, 21-gland nut, 21a-spiral shell cover core, 3-raw material delivery port, 30-raw material out splice going splice, the broken room, batch mixing chamber of 4-, 40-material conveying passage, 5-high pressure fluid nozzle, 6-feedstock joint, the broken shower nozzle of 7-, 71-shower nozzle set nut, 72-shower nozzle gripping sleeve, the broken target of 8-, the broken target seat of 80-.
Embodiment
Providing a kind of ultra-fine grain shredder assembly among a typical embodiments of the present invention, it comprises:
Broken room, batch mixing chamber, there is high pressure fluid input aperture and feedstock input, high pressure fluid enters broken room, batch mixing chamber continuously through described high pressure fluid input aperture, and in the indoor generation negative pressure in broken batch mixing chamber, make raw material be inhaled into broken room, batch mixing chamber from feedstock input and mix with described high pressure fluid, owing to fluid flow velocity in pipeline is different, produce shear difference, and by flow velocity difference shearing-crushing, formed and include the raw material of primary fragmentation and the first mixture of high pressure fluid;
Broken shower nozzle, for receiving the first mixture that described broken room, batch mixing chamber exports, and utilize hole explosion effect to make the raw material of the primary fragmentation contained by described first mixture by secondary breaking, thus formed and include the raw material of secondary breaking and the 2nd mixture of high pressure fluid.
As one of the preferred version of the present invention, described ultra-fine grain shredding unit also comprises: broken target, it is arranged on and the material outlet corresponding position of described broken shower nozzle, the 2nd mixture that described broken shower nozzle is exported directly clashes into described broken target, thus makes the raw material of the secondary breaking contained by described 2nd mixture by tertiary crushing.
Preferably, the raw material of described primary fragmentation or the raw material of secondary breaking have micron-level particle size or nano level particle diameter.
Preferred, the raw material of described secondary breaking or the raw material of tertiary crushing have micron-level particle size or nano level particle diameter.
Further, the pressure of described high pressure fluid is 350-400MPa, and described high pressure fluid is preferably water, it is also possible to be gas or oil, and is especially preferably water.
Described raw material can be powder shaped, particulate state, liquid state or other suitable form.
As another preferred version, described ultra-fine grain shredding unit also comprises: shredder assembly bucket, and for receiving the raw material of tertiary crushing, the top of described shredder assembly bucket and broken batch mixing chamber, bottom is provided with raw material delivery port.
Further, described broken room, batch mixing chamber is connected with device for supplying high-pressure fluid by high pressure fluid input aperture, and described high pressure fluid input aperture place is also provided with gland nut, is also provided with spiral shell cover core in described gland nut.
Further, described high pressure fluid input aperture is connected with a high pressure fluid nozzle, feedstock input is arranged at the side of broken room, batch mixing chamber, and the material conveying passage with broken indoor, batch mixing chamber is connected, material conveying passage is vertically arranged, and broken shower nozzle is arranged at the end of described material conveying passage.
Concrete, the arranged outside of described broken shower nozzle has shower nozzle set nut;
And/or it is provided with shower nozzle gripping sleeve between described broken shower nozzle and shower nozzle set nut.
Preferably, described broken target is arranged on broken target seat, the described broken U-shaped structure of target seat.
Preferably, described raw material delivery port is connected with vacuum concentrating apparatus.
The embodiment of the present invention additionally provides a kind of ultra-fine grain breaking method, mainly implements based on aforementioned ultra-fine grain shredder assembly, comprising:
High pressure fluid enters broken room, batch mixing chamber continuously by high pressure fluid input aperture, and in the indoor generation negative pressure in broken batch mixing chamber, make raw material from feedstock input be inhaled into broken batch mixing chamber indoor and mix with described high pressure fluid and by the poor shearing-crushing of flow velocity, produce first time broken, and formed and include the raw material of primary fragmentation and the first mixture of high pressure fluid;
First mixture is by broken shower nozzle ejection, and utilizes hole explosion effect to make the raw material of the primary fragmentation contained by described first mixture by secondary breaking, is thus formed and includes the raw material of secondary breaking and the 2nd mixture of high pressure fluid.
Preferably, described breaking method also comprises:
Described 2nd mixture directly impinges upon on described broken target, thus makes the raw material of the secondary breaking contained by described 2nd mixture by tertiary crushing, finally obtains the raw material of ultra-fine grain.
Further, normal pressure fluid enters device for supplying high-pressure fluid, by normal pressure pressurized with fluid to 350-400MPa, enters ultra-fine grain shredder assembly.
The ultra-fine grain shredder assembly of the present invention, structure is simple, produce with maintenance cost low, crushing efficiency height, good stability, can fully broken raw material, the particularly raw material such as powder shaped, particulate state, liquid state, make its internal particle size reach micro-/ nano rank, particularly Nano grade, thus greatly increase the use properties of material; Processing method is simple to operate, utilizes high pressure fluid that raw material sucks broken room, batch mixing chamber, by regulating the pressure of high pressure fluid, broken number of times etc., it is possible to the degree of controlled fragmentation, it is achieved the abundant fragmentation of raw material, is easy to realize large-scale industrial production; And nontoxic pollution-free discharge, do not produce chemical by-product, the technical fields such as pharmacy, chemical industry and biology can be widely used in.
Below in conjunction with accompanying drawing and some typical case's case study on implementation, the technical scheme of the present invention is carried out clear, complete description.
Refer to shown in Fig. 1 to Fig. 2, for a kind of ultra-fine grain shredder assembly of the present embodiment, comprise shredder assembly bucket 1, the top of described shredder assembly bucket 1 is connected with high pressure fluid transfer line 2 by high pressure fluid joint 20, one end of described high pressure fluid transfer line 2 is connected with device for supplying high-pressure fluid, in order to produce high pressure fluid;The other end is connected with high pressure fluid joint 20 by a gland nut 21, is also provided with spiral shell cover core 21a in described gland nut 21.
Wherein, high pressure fluid is preferably water, in some cases, it is also possible to be gas or oil, and is especially preferably water.
The room, broken batch mixing chamber 4 of one sealing is set between described high pressure fluid joint 20 and the inside of shredder assembly bucket 1, there is high pressure fluid input aperture and feedstock input, described high pressure fluid transport pipe 2 is connected with high pressure fluid nozzle 5, high pressure fluid is through described high pressure fluid input aperture, high pressure fluid nozzle 5 enters broken room, batch mixing chamber continuously, and in the indoor generation negative pressure in broken batch mixing chamber, raw material is made to be inhaled into broken room, batch mixing chamber from the feedstock joint 6 of the feedstock input of the side of broken room, batch mixing chamber 4 and mix with described high pressure fluid, owing to fluid flow velocity in pipeline is different, produce shear difference, and by flow velocity difference shearing-crushing, formed and include the raw material of primary fragmentation and the first mixture of high pressure fluid.
Vertically being provided with material conveying passage 40 in described broken room, batch mixing chamber 4, the outlet of feedstock joint 6, high pressure fluid nozzle 5 is all connected with material conveying passage 40. Shown in Fig. 3, the end of described material conveying passage 40 is provided with broken shower nozzle 7, and wherein, the arranged outside of described broken shower nozzle has shower nozzle set nut 71, is provided with shower nozzle gripping sleeve 72 between described broken shower nozzle and shower nozzle set nut. Described broken shower nozzle 7 receives the first mixture that described broken room, batch mixing chamber exports, and utilize hole explosion effect to make the raw material of the primary fragmentation contained by described first mixture by secondary breaking, thus formed and include the raw material of secondary breaking and the 2nd mixture of high pressure fluid.
Being provided with broken target 8 below the material outlet corresponding position of described broken shower nozzle, described broken target 8 is arranged on broken target seat 80, the described broken U-shaped structure of target seat 80. Wherein, described broken target 8 is Wimet target, and the 2nd mixture that described broken shower nozzle exports directly impinges upon on described broken target, thus makes the raw material of the secondary breaking contained by described 2nd mixture by tertiary crushing.
The bottom of described shredder assembly bucket 1 is provided with raw material delivery port 3, and described raw material delivery port is connected with vacuum concentrating apparatus by raw material out splice going splice 30.
Breaking method and the principle of work of the present invention are specially:
First by device for supplying high-pressure fluid, common fluid is pressurized to 350-400MPa, high pressure fluid is successively through high pressure fluid transfer line 2, high pressure fluid nozzle 5 enters in broken room, batch mixing chamber 4, owing to the flow at high speed of high pressure fluid produces negative pressure in broken room, batch mixing chamber 4, raw material is made to be inhaled into indoor, broken batch mixing chamber from feedstock input and mix with described high pressure fluid, raw material flow at high speed after mixing, uneven due to flow velocity in pipeline, produce shear difference, raw material is produced first time shearing, produce first time broken, and formed and include the raw material of primary fragmentation and the first mixture of high pressure fluid.
First mixture flow to broken shower nozzle 7 by material conveying passage 40 and exports ejection, time pressure in an instant in outlet is down to suddenly zero from 350-400MPa, produce hole explosion, utilizing hole explosion effect to make the raw material of the primary fragmentation contained by described first mixture by secondary breaking, second time fragmentation is also the primary fragmentation of most critical. Thus formed and include the raw material of secondary breaking and the 2nd mixture of high pressure fluid.
Described 2nd mixture is along with swiftly flowing current, and third time directly impinges upon and raw material carries out on broken target 8 third time fragmentation, thus makes the raw material of the secondary breaking contained by described 2nd mixture by tertiary crushing, finally obtains the raw material of ultra-fine grain.
Wherein, the raw material in the present invention can be powder shaped, particulate state, liquid state or other suitable form. The raw material of the raw material of described primary fragmentation, the raw material of secondary breaking or tertiary crushing all at least has micron-level particle size or nano level particle diameter.
In the technological process of the present invention, general liquid starting material is provided by the producer having broken demand, the shredder assembly of the present invention can broken raw material, particularly powder shaped, particulate state, liquid raw material, its internal particle size is made to reach micro-/ nano rank, particularly Nano grade, thus greatly increase the use properties of material.
In an embodiment, raw material adopts white exterior coating, and material rate is: the water of 65%, the terra alba of 30%, 5% glue, material after treatment is thinner, and spraying postadhesion power is stronger, and luminance brightness is brighter.
The finished product micro/nano level material composition that the present invention obtains is identical with raw material, whole technological process is physical action, does not produce chemical by-product, and processing method is simple to operate, it is easy to realize large-scale industrial production, the technical fields such as pharmacy, chemical industry and biology can be widely used in.
Technology contents and the technology feature of the present invention have disclosed as above; but those of ordinary skill in the art still may do all replacement and the modification that do not deviate from spirit of the present invention based on the teaching of the present invention and announcement; therefore; protection domain of the present invention should be not limited to the content that embodiment discloses; and the various replacement and the modification that do not deviate from the present invention should be comprised, and contained by present patent application claim.

Claims (14)

1. a ultra-fine grain shredder assembly, it is characterised in that comprising:
Broken room, batch mixing chamber, there is high pressure fluid input aperture and feedstock input, high pressure fluid enters broken room, batch mixing chamber continuously through described high pressure fluid input aperture, and in the indoor generation negative pressure in broken batch mixing chamber, raw material is made to be inhaled into broken room, batch mixing chamber from feedstock input and mix with described high pressure fluid and by flow velocity difference shearing-crushing, formed and include the raw material of primary fragmentation and the first mixture of high pressure fluid;
Broken shower nozzle, for receiving the first mixture that described broken room, batch mixing chamber exports, and utilize hole explosion effect to make the raw material of the primary fragmentation contained by described first mixture by secondary breaking, thus formed and include the raw material of secondary breaking and the 2nd mixture of high pressure fluid.
2. ultra-fine grain shredder assembly according to claim 1, characterized by further comprising: broken target, it is arranged on and the material outlet corresponding position of described broken shower nozzle, the 2nd mixture that described broken shower nozzle is exported directly clashes into described broken target, thus makes the raw material of the secondary breaking contained by described 2nd mixture by tertiary crushing.
3. ultra-fine grain shredder assembly according to claim 1, it is characterised in that: the raw material of described primary fragmentation or the raw material of secondary breaking have micron-level particle size or nano level particle diameter.
4. ultra-fine grain shredder assembly according to claim 2, it is characterised in that: the raw material of described secondary breaking or the raw material of tertiary crushing have micron-level particle size or nano level particle diameter.
5. ultra-fine grain shredder assembly according to claim 1, it is characterised in that: the pressure of described high pressure fluid is 350-400MPa.
6. ultra-fine grain shredder assembly according to claim 2, it is characterised in that also comprise: shredder assembly bucket, for receiving the raw material of tertiary crushing, the top of described shredder assembly bucket and broken batch mixing chamber, bottom is provided with raw material delivery port.
7. ultra-fine grain shredder assembly according to claim 6, it is characterized in that: described broken room, batch mixing chamber is connected with device for supplying high-pressure fluid by high pressure fluid input aperture, described high pressure fluid input aperture place is also provided with gland nut, is also provided with spiral shell cover core in described gland nut.
8. ultra-fine grain shredder assembly according to claim 7, it is characterized in that: described high pressure fluid input aperture is connected with a high pressure fluid nozzle, feedstock input is arranged at the side of broken room, batch mixing chamber, and the material conveying passage with broken indoor, batch mixing chamber is connected, material conveying passage is vertically arranged, and broken shower nozzle is arranged at the end of described material conveying passage.
9. ultra-fine grain shredder assembly according to claim 1, it is characterised in that: the arranged outside of described broken shower nozzle has shower nozzle set nut;
And/or it is provided with shower nozzle gripping sleeve between described broken shower nozzle and shower nozzle set nut.
10. ultra-fine grain shredder assembly according to claim 2, it is characterised in that: described broken target is arranged on broken target seat, the described broken U-shaped structure of target seat.
11. ultra-fine grain shredder assemblys according to claim 6, it is characterised in that: described raw material delivery port is connected with vacuum concentrating apparatus.
12. 1 kinds of ultra-fine grain breaking methods, mainly implement based on ultra-fine grain shredder assembly according to any one of claim 1-11, it is characterised in that comprising:
High pressure fluid enters broken room, batch mixing chamber continuously by high pressure fluid input aperture, and in the indoor generation negative pressure in broken batch mixing chamber, make raw material from feedstock input be inhaled into broken batch mixing chamber indoor and mix with described high pressure fluid and by the poor shearing-crushing of flow velocity, produce first time broken, and formed and include the raw material of primary fragmentation and the first mixture of high pressure fluid;
First mixture is by broken shower nozzle ejection, and utilizes hole explosion effect to make the raw material of the primary fragmentation contained by described first mixture by secondary breaking, is thus formed and includes the raw material of secondary breaking and the 2nd mixture of high pressure fluid.
13. ultra-fine grain breaking methods according to claim 12, it is characterised in that also comprise:
Described 2nd mixture directly impinges upon on described broken target, thus makes the raw material of the secondary breaking contained by described 2nd mixture by tertiary crushing, finally obtains the raw material of ultra-fine grain.
14. ultra-fine grain breaking methods according to claim 12, it is characterised in that: normal pressure fluid enters device for supplying high-pressure fluid, by normal pressure pressurized with fluid to 350-400MPa, enters ultra-fine grain shredder assembly.
CN201610224484.7A 2016-04-12 2016-04-12 A kind of ultra-fine grain breaker and breaking method Active CN105665104B (en)

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US4619406A (en) * 1976-12-22 1986-10-28 Can-Am Engineering Corporation Hydraulic system and method of improving the working properties thereof
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CN110270426A (en) * 2019-06-26 2019-09-24 厦门一泰消防科技开发有限公司 Extinguishing chemical and preparation method thereof based on nanometer pulverization technology

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