CN105664828B - Chemical reaction kettle - Google Patents
Chemical reaction kettle Download PDFInfo
- Publication number
- CN105664828B CN105664828B CN201610206746.7A CN201610206746A CN105664828B CN 105664828 B CN105664828 B CN 105664828B CN 201610206746 A CN201610206746 A CN 201610206746A CN 105664828 B CN105664828 B CN 105664828B
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- CN
- China
- Prior art keywords
- flexible pipe
- reaction kettle
- stereoplasm tube
- distribution plate
- cone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
- B01J2204/005—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the outlet side being of particular interest
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The present invention relates to a kind of chemical reaction kettle, including autoclave body, feeding port and discharging nozzle, discharge duct opening's edge vertical direction arrangement are respectively set at the top and bottom of autoclave body, flexible pipe is that plastic film roll is formed around three layers, and the lower end of flexible pipe extends to the outside of stereoplasm tube lower end；Two trunnions are oppositely arranged on the outer tube wall of discharging nozzle, connector is that two iron wires are bent, and the hanging hole that the upper end of iron wire is bent to form is set on trunnion, the lower end of iron wire and stereoplasm tube Joint.It is used in above-mentioned technical proposal by the collocation of flexible pipe and stereoplasm tube, when reaction kettle blowing, stereoplasm tube is set in the outside of flexible pipe, feed liquid is reliably delivered in case bucket, after blowing, stereoplasm tube is unloaded, flexible pipe is rolled, convenient for the conveying of material on the downside of reaction kettle and walking about for personnel.
Description
The present invention be the applying date be on December 19th, 2014, application No. is: 2014107988708, entitled " chemical industry
The divisional application of the patent of invention of production reaction kettle ".
Technical field
The present invention relates to chemical production equipment fields, and in particular to a kind of chemical reaction kettle.
Background technique
Chemical industry workshop is mostly frame structure, and reaction kettle is fixed in the horizontal floor of frame, and autoclave body top is located at
Above floor, the lower part of autoclave body is located at below floor, and discharging nozzle is arranged in autoclave body bottom vertical, by vertical in discharging nozzle
Drain pipe is set, the feed liquid discharge splendid attire after reaction is used for other productions as raw material into case bucket.Since drain pipe is mostly
Rigid structure, can not deformation occurs, therefore, the setting of discharge duct can conveying to some materials, the generation of walking about of operator
Interference.
Summary of the invention
It is an object of the invention to provide a kind of chemical reaction kettles, can effectively solve the above problems, avoid discharge duct
It is arranged to the conveying of material, the generation interference of walking about of operator below reaction kettle.
To achieve the above object, the invention adopts the following technical scheme:
A kind of chemical reaction kettle, it is characterised in that: including autoclave body, feeding port is respectively set at the top and bottom of autoclave body and unloads
Expects pipe mouth, discharge duct opening's edge vertical direction arrangement are arranged discharge component at discharging nozzle, discharge component include by plastic film roll around
Flexible pipe, the upper end of flexible pipe fixed as one with discharging nozzle by rope, and the outer sheath of flexible pipe is equipped with stereoplasm tube, firmly
The upper end of matter pipe constitutes detachable connection cooperation by connector and discharging nozzle；Stereoplasm tube is pvc pipe；Flexible pipe is plastics
Film roll is formed around three layers, and the lower end of flexible pipe extends to the outside of stereoplasm tube lower end；It is oppositely arranged on the outer tube wall of discharging nozzle
Two trunnions, connector are that two iron wires are bent, and the hanging hole that the upper end of iron wire is bent to form is set on trunnion, the lower end of iron wire
With stereoplasm tube Joint.
It is used in above-mentioned technical proposal by the collocation of flexible pipe and stereoplasm tube, when reaction kettle blowing, stereoplasm tube is arranged
In the outside of flexible pipe, feed liquid is reliably delivered in case bucket, after blowing, stereoplasm tube is unloaded, flexible pipe
It rolls, convenient for the conveying of material on the downside of reaction kettle and walking about for personnel.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of reaction kettle discharge pit；
Fig. 2 is the structural schematic diagram of reaction kettle rabbling mechanism；
Fig. 3 is the structural schematic diagram of mounting plate；
Fig. 4 is the A-A cross-sectional view of Fig. 3；
Fig. 5 is the structural schematic diagram of annular rotating plate；
Fig. 6 is the structural schematic diagram at reactor feed；
Fig. 7 is the assembling schematic diagram of mounting plate and annular rotating plate.
Specific embodiment
In order to which objects and advantages of the present invention are more clearly understood, the present invention is carried out specifically with reference to embodiments
It is bright.It should be appreciated that following text is only used to describe one or more of specific embodiments of the invention, not to the present invention
The protection scope specifically requested carries out considered critical.
The present invention includes three inventive points: that is, the batch charging mechanism, shedding mechanism, rabbling mechanism of chemical reaction kettle are distinguished
The improvement of progress.
Technical solution that the present invention takes is as shown in Figure 1, a kind of chemical reaction kettle, including autoclave body, the top and bottom of autoclave body
Feeding port and discharging nozzle 71 is respectively set in portion, and discharging nozzle 71 is arranged along vertical direction, and discharging group is arranged at discharging nozzle 71
Part, discharge component include by plastic film roll around flexible pipe 72, the upper end of flexible pipe 72 and discharging nozzle 71 are consolidated by rope 74
It is connected in one (the upper end binding of flexible pipe 72 is set on the outer tube wall of discharging nozzle 71), the outer sheath of flexible pipe 72 is equipped with hard
The upper end of matter pipe 73, stereoplasm tube 73 constitutes detachable connection cooperation by connector 75 and discharging nozzle 71.Discharging nozzle 71
It is arranged in autoclave body bottom vertical, if the fixed stereoplasm tube 73 of setting carries out discharging directly at discharging nozzle 71, suspends shape in midair
The stereoplasm tube 73 of setting can convey the material below reaction kettle and the walking of operator impacts, and stereoplasm tube 73 also holds
It is easily hit curved or is fractureed.Therefore, in the present invention, by the combination of flexible pipe 72 and stereoplasm tube 73, the length of general flexible pipe 72
Just can have it is a bit of extend in hopper (feed liquid submergence flexible pipe 72 when avoiding bin full feed liquid), if being not provided with stereoplasm tube
73, when starting discharging, opening discharge valve feed liquid will be poured in flexible pipe 72, and the lower end of flexible pipe 72 will be swung from hopper
Mouth is detached from, so that feed liquid is splashed.Therefore, in the present invention, play the role of a fixed guide by being arranged stereoplasm tube 73, avoid
The generation of above situation guarantees the reliable blowing of reaction kettle.In reaction kettle blowing, stereoplasm tube 73 is set in the outer of flexible pipe 72
Side enables feed liquid to be reliably delivered in case bucket, after blowing, stereoplasm tube 73 is unloaded, flexible pipe 72 is rolled, and is convenient for
The conveying of material and walking about for personnel on the downside of reaction kettle.
Preferred scheme is that stereoplasm tube 73 is pvc pipe, and flexible pipe 72 is that plastic film roll is formed around three layers, flexible pipe 72
Lower end extends to the outside of 73 lower end of stereoplasm tube, and two trunnions are oppositely arranged on the outer tube wall of discharging nozzle 71, and connector 75 is two
Iron wire is bent, and the hanging hole that the upper end of iron wire is bent to form is set on trunnion, the lower end of iron wire and 73 Joint of stereoplasm tube.
The disassembly and installation operation of stereoplasm tube 73 in this way is the most convenient, while the long service life of stereoplasm tube 73 and flexible pipe 72.
In Chemical Manufacture, for the reliable progress for guaranteeing reaction, it is sometimes desirable to raw material is added dropwise in reaction solution dropwise, and
Carry out hybrid reaction is sufficiently stirred, such as produces the reaction kettle of microemulsion, needs oil phase substance being added dropwise to surfactant dropwise
Aqueous solution in reacted, and need to carry out during the reaction shear agitation be made microemulsion.Currently, not yet can be big
The reaction kettle of microemulsion is produced in batches, to find out its cause, being exactly to be difficult to solve the problems, such as that oil mutually feeds intake, therefore, the present invention is further
Scheme be that, as shown in Fig. 2, reaction kettle 30 includes the rabbling mechanism being arranged in autoclave body and autoclave body, rabbling mechanism includes vertical shape
The agitating shaft 31 of arrangement, first, second and third connecting rod 321,322,323 of the radial setting in the lower end of agitating shaft 31, first, second and third
The end of connecting rod 321,322,323 respectively stand shape be arranged the first, second and third stirring rod 331,332,333, first connecting rod 321,
Agitating paddle 341,342,343, agitating paddle is respectively set in the lower section of second stirring rod 332 and the upper section of third stirring rod 333
341, it 342,343 is constituted for a plate, the periphery of agitating shaft 31 is uniformly arranged the inlet tube 35 of three vertical shape arrangements, inlet tube
Three liquid distribution plate parts 36 are arranged at intervals on 35 pipe shaft, the middle part of each liquid distribution plate part 36 is offered to be led to for what agitating shaft 31 passed through
Hole, the inside of liquid distribution plate part 36 is arranged to cavity-like and the lower face of liquid distribution plate part 36 uniformly opens up liquid distributing hole, each inlet tube
Lumen is connected with the inner cavity of a liquid distribution plate part 36 respectively to be connect, the upper end of each inlet tube pass through after autoclave body with storage tank (oily phase
Storage tank) it is connected.The liquid distribution plate part 36 of stratiform arrangement, when oily phase is added dropwise, oil is mutually from each liquid distributing hole drop on liquid distribution plate part 36
Enter in the mixed liquor in reaction kettle, significantly improves production efficiency relative to traditional one after another drop of instillation.It is answered between each liquid distributing hole
Keep certain spacing.The rabbling mechanism of above structure can from different directions be stirred solution, improve the equal of mixing
Even property.Stirring rod and connecting rod be angle steel constitute, such intensity is big, convenient for agitating paddle 34 installation and rabbling mechanism it is steady
It is qualitative.
Preferred scheme is that liquid distribution plate part 36 is that the cone-shaped hood of an opening upwards is constituted, and opens up through-hole in the middle part of cone-shaped hood,
It is arranged to cavity-like inside the cover of cone-shaped hood, the syringe needle 361 for constituting liquid distributing hole is uniformly arranged in the outer cover of cone-shaped hood
(hollow), the length direction of syringe needle 361 and the perpendicular arrangement of the cover of cone-shaped hood, syringe needle are set on the cover of cone-shaped hood in round
It sets, and the length of syringe needle increases with the radius of cone-shaped hood and increased, it is best to instill the oily effect for mixing reaction in this way.
Since reaction kettle also needs to add solid material, such as surfactant, and while reacting, requires inside reaction kettle mostly
In air-tight state, therefore, more specifically scheme is the present invention, and as shown in FIG. 4,5,6, 7,60 top of autoclave body of reaction kettle is set
It is equipped with circular mounting plate 10, edge and the autoclave body 60 of mounting plate 10 fix as one, and the upper surface of mounting plate 10 offers ring
Shape slot 11 is equipped with annular rotating plate 20 in annular groove 11, and annular rotating plate 20 is by bearing assembly and mounting plate 10 along mounting plate 10
Core wire composition be rotatably assorted, on annular rotating plate 20 opposite two sides be respectively set constitute feeding port cast hopper 21, annular groove
Open up the scallop section 12 to lower recess on 11 slot bottom at opposite two positions respectively, the bottom surface of scallop section 12 opens up useful
In the material hole 13 of connection reaction kettle inner cavity, the projection of cast hopper 21, material hole 13 in same level is located on same circumference, ring
It is additionally provided with the first and second annular protrusion 16,15 for protruding from groove bottom on the slot bottom of shape slot 11, the first and second annular protrusion 16,
15, the center of circle of scallop section 12 and annular groove 11 is respectively positioned on the core wire of mounting plate 10, and scallop section 12 is located at the first and second ring
Between shape protrusion 16,15, diameter of the diameter less than the second annular protrusion 15 of first annular protrusion 16, the opening of scallop section 12
Place is arranged the fan-shaped sealing ring 14 consistent with its, and the section of annular rotating plate 20 is to fall " convex " shape, the bottom surface of annular rotating plate 20 and
The slot bottom of annular groove 11 mutually reclines, the shoulder 22 of annular rotating plate 20 and the first and second annular protrusion 16,15 corresponding arrangements, bearing
Component includes the inside and outside bearing 19 at 20 inner and outer rings of annular rotating plate, 11 slot bottom of annular groove of first annular 16 inside of protrusion
And conduction hole 111 is opened up on 11 slot bottom of annular groove in 15 outside of the second annular protrusion respectively, the middle part of mounting plate 10, which is arranged, to be used
In the first and second mounting hole 17,18 of installation inlet tube 35 and shaft 36.In this way, can to throw by rotating annular rotating plate 20
Hopper 21 and the corresponding arrangement of feeding port, material is quickly added into reaction kettle, in addition, being fed intake by fan-shaped sealing structure
After autoclave body 60 is reliably sealed, guarantee subsequent reaction.Fan-shaped sealing ring and scallop section 12, so that sealing
Circle and the rotation direction of 20 bottom surface of annular rotating plate are perpendicular or consistent, prevent sealing ring from being pulled out by the rotation of annular rotating plate 20
It rises, causes poorly sealed.After setting bearing assembly, other external waste liquids and bearing oil are easy trickling to annular
The slot bottom of slot 11 impacts the sealing of fan-shaped sealing ring or causes reaction liquid from polluting into kettle is intracavitary, therefore passes through setting
First and second annular protrusion and conduction hole stop to these waste liquids and be discharged in time.It is provided by the invention above-mentioned to feed intake
Mechanism can individually be used for different chemical reaction kettles, guarantee the reliable progress of chemical reaction.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, in knowing the present invention after contents, without departing from the principle of the present invention, it can also be made several
Same transformation and substitution, these convert and substitute on an equal basis and also should be regarded as belonging to the scope of protection of the present invention.
Claims (1)
1. a kind of chemical reaction kettle, it is characterised in that: including autoclave body, feeding port and discharging is respectively set at the top and bottom of autoclave body
Nozzle, discharge duct opening's edge vertical direction arrangement are arranged discharge component at discharging nozzle, discharge component include by plastic film roll around
The upper end of flexible pipe, flexible pipe is fixed as one with discharging nozzle by rope, and the outer sheath of flexible pipe is equipped with stereoplasm tube, hard
The upper end of pipe constitutes detachable connection cooperation by connector and discharging nozzle；Stereoplasm tube is pvc pipe；Flexible pipe is plastic foil
Three layers of formation are wound, the lower end of flexible pipe extends to the outside of stereoplasm tube lower end；Two are oppositely arranged on the outer tube wall of discharging nozzle
Trunnion, connector be two iron wires bend, the hanging hole that the upper end of iron wire is bent to form is set on trunnion, the lower end of iron wire with
Stereoplasm tube Joint；
Rabbling mechanism is provided in autoclave body, rabbling mechanism includes the agitating shaft of vertical shape arrangement, the radial setting in the lower end of agitating shaft
First, second and third connecting rod, the end of the first, second and third connecting rod found shape respectively and the first, second and third stirring rod, the first connection are arranged
Agitating paddle is respectively set in the upper section of bar, the lower section of the second stirring rod and third stirring rod, and agitating paddle is that a plate is constituted, and stirs
The periphery for mixing axis is uniformly arranged the inlet tube of three vertical shape arrangements, is arranged at intervals with three liquid distribution plate parts on the pipe shaft of inlet tube,
The through-hole passed through for agitating shaft is offered in the middle part of each liquid distribution plate part, the inside of liquid distribution plate part is arranged to cavity-like and liquid distribution plate part
Lower face uniformly open up liquid distributing hole, the lumen of each inlet tube is connected with the inner cavity of a liquid distribution plate part respectively to be connect, each feed liquor
The upper end of pipe is connected after passing through autoclave body with storage tank；
Reaction kettle is the reaction kettle for producing microemulsion, and the liquid distribution plate part of stratiform arrangement, when oily phase is added dropwise, oil is mutually from liquid distribution plate part
On each liquid distributing hole instill reaction kettle in mixed liquor in, liquid distribution plate part be an opening upwards cone-shaped hood constitute, cone-shaped hood
Middle part opens up through-hole, is arranged to cavity-like inside the cover of cone-shaped hood, is uniformly arranged in the outer cover of cone-shaped hood for constituting cloth
The syringe needle of fluid apertures, the length direction of syringe needle and the perpendicular arrangement of the cover of cone-shaped hood, syringe needle are in round on the cover of cone-shaped hood
Setting, and the length of syringe needle increases with the radius of cone-shaped hood and is increased.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610206746.7A CN105664828B (en) | 2014-12-19 | 2014-12-19 | Chemical reaction kettle |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610206746.7A CN105664828B (en) | 2014-12-19 | 2014-12-19 | Chemical reaction kettle |
| CN201410798870.8A CN104587900B (en) | 2014-12-19 | 2014-12-19 | Chemical Manufacture reactor |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410798870.8A Division CN104587900B (en) | 2014-12-19 | 2014-12-19 | Chemical Manufacture reactor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105664828A CN105664828A (en) | 2016-06-15 |
| CN105664828B true CN105664828B (en) | 2019-01-11 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610206746.7A Expired - Fee Related CN105664828B (en) | 2014-12-19 | 2014-12-19 | Chemical reaction kettle |
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| Country | Link |
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| CN (1) | CN105664828B (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003305358A (en) * | 2002-04-12 | 2003-10-28 | Is:Kk | Method for melting filter cake and device therefor |
| CN2915869Y (en) * | 2006-06-19 | 2007-06-27 | 闫亚萍 | Folding type soft body methane pool |
| CN102251947A (en) * | 2010-05-17 | 2011-11-23 | 吴树木 | Small-sized pedal-type inflator with extension pipe group |
| CN202808790U (en) * | 2012-09-26 | 2013-03-20 | 德阳嘉龙机械制造有限公司 | Marsh gas generating device |
| CN203090901U (en) * | 2013-02-18 | 2013-07-31 | 蚌埠市新瑞有机硅有限公司 | Reaction kettle |
| CN203400696U (en) * | 2013-08-13 | 2014-01-22 | 海宁胜晖化学工业有限公司 | Discharging device of antifoaming agent reaction kettle |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN203170328U (en) * | 2013-05-03 | 2013-09-04 | 潍坊兴信技术服务有限公司 | Reaction kettle |
-
2014
- 2014-12-19 CN CN201610206746.7A patent/CN105664828B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003305358A (en) * | 2002-04-12 | 2003-10-28 | Is:Kk | Method for melting filter cake and device therefor |
| CN2915869Y (en) * | 2006-06-19 | 2007-06-27 | 闫亚萍 | Folding type soft body methane pool |
| CN102251947A (en) * | 2010-05-17 | 2011-11-23 | 吴树木 | Small-sized pedal-type inflator with extension pipe group |
| CN202808790U (en) * | 2012-09-26 | 2013-03-20 | 德阳嘉龙机械制造有限公司 | Marsh gas generating device |
| CN203090901U (en) * | 2013-02-18 | 2013-07-31 | 蚌埠市新瑞有机硅有限公司 | Reaction kettle |
| CN203400696U (en) * | 2013-08-13 | 2014-01-22 | 海宁胜晖化学工业有限公司 | Discharging device of antifoaming agent reaction kettle |
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| Publication number | Publication date |
|---|---|
| CN105664828A (en) | 2016-06-15 |
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| TA01 | Transfer of patent application right |
Effective date of registration: 20181121 Address after: 317101 Taizhou City, Zhejiang Province, three county Zhuhai Ao town Lingkou Applicant after: Three Men Huamai chemical products Co. Ltds Address before: 246002 No. 1318 Jixian North Road, Yixiu District, Anqing City, Anhui Province Applicant before: Cheng Yehong |
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| TR01 | Transfer of patent right |
Effective date of registration: 20201012 Address after: 314599 block A-03, phase II Industrial Zone, Tongxiang Economic Development Zone, Jiaxing City, Zhejiang Province Patentee after: Jintong chemical (Tongxiang) Co.,Ltd. Address before: 317101, Zhejiang Province, Taizhou County, three counties, Ao Ao Town, Ling Kou Patentee before: Three Men Huamai chemical products Co. Ltds |
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Granted publication date: 20190111 Termination date: 20211219 |
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| CF01 | Termination of patent right due to non-payment of annual fee |