CN105660888A - Camellia oil compound product and preparation method thereof - Google Patents

Camellia oil compound product and preparation method thereof Download PDF

Info

Publication number
CN105660888A
CN105660888A CN201610036389.4A CN201610036389A CN105660888A CN 105660888 A CN105660888 A CN 105660888A CN 201610036389 A CN201610036389 A CN 201610036389A CN 105660888 A CN105660888 A CN 105660888A
Authority
CN
China
Prior art keywords
camellia oil
royal jelly
honey
enzymolysis
parts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610036389.4A
Other languages
Chinese (zh)
Other versions
CN105660888B (en
Inventor
郭耀荣
郭震宇
林金科
黄建忠
吴松刚
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tian Sidun Bio Tech Ltd Fujian
Original Assignee
Tian Sidun Bio Tech Ltd Fujian
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tian Sidun Bio Tech Ltd Fujian filed Critical Tian Sidun Bio Tech Ltd Fujian
Priority to CN201610036389.4A priority Critical patent/CN105660888B/en
Publication of CN105660888A publication Critical patent/CN105660888A/en
Application granted granted Critical
Publication of CN105660888B publication Critical patent/CN105660888B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/007Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • A23D9/04Working-up

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Jellies, Jams, And Syrups (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)

Abstract

The invention discloses a camellia oil compound product and a preparation method thereof, comprising main materials according to parts by weight: 60-70 parts of camellia oil, 30-40 parts of royal honey, 250-300 parts of bee honey, 5-6 parts of vitamin C and 550-700 parts of purified water.The traditional natural materials are used in compatibility to prepare the product, and the product is free of toxic and side effects, is rich in nutrition and easy for human body to absorb and has good body regulatory function; by the use of enzymatic hydrolysis and low-temperature preparation process, the mutual dissolution of the camellia oil, royal honey and water is achieved, the method provides more and more sufficient nutrition and more convenience of eating than the traditional production method and is an efficient environment-friendly drink production technique.

Description

A kind of Camellia oil compound product and its preparation method
Technical field
The invention belongs to Organic food beverage production technology field, it is specifically related to a kind of Camellia oil compound product and its preparation method.
Background technology
Camellia oil obtains from Theaceae (Camellia) oil tea (CamelliaoleiferaAbel) seeds, it is one of the most ancient woody edible vegetable oil of China, China is the country that plant of theaceae distribution is the widest in the world, it is tea oil production base maximum in the world, in addition only has the distribution of the state-owned minute quantity such as South East Asia, Japan. The place of production, center of oil tea is then distributed in Fujian of China, southwest and Hunan, south, Jiangxi, and its cultivation history has more than 2300, is the distinctive oil plant seeds of China, and China is the country of origin of oil tea. Tea oil tree grows in the Nan Ling moist climate region, subtropics not having to pollute, no pesticide grown, chemical fertilizer etc. in whole process of growth. Longitude and latitude and soil property benign climate nutritive ingredient height. Not containing harmful materials such as erucic acid, cholesterol, flavacin. Golden yellow color or pale yellow, quality is pure, clear, smell delicate fragrance, good taste. For Chinese Government advocates the woody edible vegetable oil of pure natural promoted, and the health care vegetable edible oil that international food and agricultural organization is first-elected. The nutrition of Disease Control and Prevention in China center and food safety the comparative study that Camellia oil and sweet oil carry out is shown, the composition of tea oil and sweet oil is despite similarity, but in fact the dietotherapy dual-use function of tea oil is better than sweet oil, also it is better than other any grease. Sweet oil reaches 75%-90% containing unsaturated fatty acids, and the unsaturated fatty acids in tea oil, then up to 85%-97%, is the hat of various edible oil. Containing the unexistent specific physiologically active substance tea-polyphenol of sweet oil and camellia glucoside in tea oil, can effectively improve cardiovascular and cerebrovascular diseases, reduce cholesterol and fasting plasma glucose, suppression triglyceride rising, anticancer is also had obvious effect. And Camellia oil contains squalene, and to regulating, function of human body has remarkable effect; The molecular structure of Camellia oil is also thinner than sweet oil, thus edible time do not worry side effect, have greasy.
Royal jelly (royaljelly) is the bee product that a class component is quite complicated, and it is along with the difference of bee species, age, season, pollen plant, and its chemical composition is also different.In general, its composition is: moisture content 64.5-69.5%, crude protein 11-14.5%, carbohydrate 13-15%, lipid 6.0%, mineral substance 0.4-2%, do not determine material 2.84-3.0%. The protein of royal jelly accounts for the 50% of royal jelly dry-matter, wherein has 2/3 for white protein, and 1/3 is sphaeroprotein, and the protein in royal jelly has more than 12 kinds. Amino acid accounts for the 1.8% of royal jelly dry weight, and 8 kinds of indispensable amino acids required in human body, have existence in royal jelly, and wherein proline content is the highest accounts for 63%, has found 20 seed amino acids at present in royal jelly. Royal jelly contains nucleic acid, wherein thymus nucleic acid (DNA) 201-223 microgram/gram aobvious heavy, Yeast Nucleic Acid 3.9-4.9 milligram/gram aobvious heavy. Royal jelly contains the carbohydrate of 20%-30% and more VITAMIN. Royal jelly contains the lipid acid of more than 26 kinds, and identified at present have 12 kinds, wherein in 10-HAD (10-HDA) content more than 1.4%, due in nature only in royal jelly containing this kind of material, so also it being referred to as Royaljelly acid. In addition also containing mineral substance, iron, copper, magnesium, zinc, potassium, sodium etc. Royal jelly is sticky thick soup compound, has the smell of a kind of typical phenol with acid, and taste is sour, puckery, slightly pungent, and aftertaste is slightly sweet. Royal jelly is in acid, and pH is 3.9-4.1, and acidity is between 32-54 milliliter 1NNaOH/100 gram, and it is insoluble to chloroform; Be partially soluble in water, all the other and water form suspension liquid; Alcohol is partly dissolved, partly precipitated.
Along with the development of food scientific technology, varieties of food items various drink in market is constantly weeded out the old and bring forth the new, all the natural fats and oils of Camellia oil there is a large amount of reports both at home and abroad, but Camellia oil is not developed fully as the natural matter of high-quality, for overcoming Camellia oil only as meals grease, utilization ratio is low had both wasted resource, did not give full play to again the deficiencies such as its nutritious healthy wide spectrum effect. Utilize the characteristic that enzyme has, select corresponding enzyme, carry out decomposing, its effective constituent being dissolved at Camellia oil and royal jelly, accelerate effective constituent release, Camellia oil, royal jelly and honey, aqueous phase are dissolved each other to be separated fused, and adopts low-temperature production process, keeps the stable of active substance composition, it is not destroyed, it is convenient to absorption of human body. Thus resource is fully utilized, it is to increase the utility value of raw material.
Summary of the invention
It is an object of the invention to provide a kind of Camellia oil compound product and its preparation method, select tradition crude substance to carry out compatibility, have no side effect, be rich in nutritive ingredient, be easy to absorption of human body, there is good adjustment body effect; Adopting enzymolysis, low-temperature growth technique, solve the mutually fused problem of Camellia oil, royal jelly and water, more traditional production method nutritive substance is higher more fully, edible more convenient, is the drink production technology of a kind of high-efficiency environment friendly.
For achieving the above object, the present invention adopts following technical scheme:
A kind of Camellia oil compound product, main raw material is counted by weight: Camellia oil 60-70 part, royal jelly 30-40 part, honey 250-300 part, vitamins C 5-6 part, purified water 550-700 part.
Preparation method comprises enzymolysis, filtration, preparation, filling, sterilization process, and wherein enzymolysis is for utilizing lipase and proteolytic enzyme to decompose Camellia oil and royal jelly respectively.
Concrete steps are as follows:
(1) qualified raw material is weighed: Camellia oil is the Camellia oil that squeezing tea seed obtains, and with fruital and fruity, oleic acid degree is lower than 1%;10-HAD >=the 1.4wt% of royal jelly; Honey meets GB/T18932.22 standard;
(2) enzymolysis, filtration: the Camellia oil lipase of its weight 1.0-2.0% is carried out enzymolysis, and the time is 2-3 hour, and temperature is 40-60 DEG C, filter, collect filtrate A; The royal jelly purified water of its weight 3-5 times and the proteolytic enzyme of 1.0-2.0% are carried out enzymolysis, and the time is 2-3 hour, and temperature is 40-60 DEG C, filters, and collects liquor B;
(3) prepare: by honey, vitamins C and the mixing of remaining purified water, add filtrate A and liquor B, stir evenly, be heated to 70-80 DEG C, decoct and boil 10-20 minute, then adopt 100-200 order membrane filtration;
(4) filling, sterilizing: by filling for step (3) gained feed liquid medicinal glass bottle, revolves lid sealing, sterilizing, temperature 105-110 DEG C, Operating Steam Pressure 0.20-0.25MPa, 5-10 minute time.
The enzyme activity of lipase is 100,000 U/g, and the enzyme activity of proteolytic enzyme is 200,000 U/g.
The remarkable advantage of the present invention is: selects tradition crude substance to carry out compatibility, has no side effect, be rich in nutritive ingredient, be easy to absorption of human body, have good adjustment body effect; Adopting enzymolysis, low-temperature growth technique, solve the mutually fused problem of Camellia oil, royal jelly and water, more traditional production method nutritive substance is higher more fully, edible more convenient, is the drink production technology of a kind of high-efficiency environment friendly.
Embodiment
Embodiment 1
Supplementary material: Camellia oil 6000g, royal jelly 3500g, honey 25000g, vitamins C 500g, purified water 65000g.
Preparation method:
1, raw material pre-treatment: qualified raw material is weighed by formula. Wherein Camellia oil is the Camellia oil oil 6000g that tea seed squeezing obtains, and with fruital and fruity, oleic acid degree is lower than 1%. Royal jelly 3500g, 10-hydroxyl-2 decylenic acid >=1.4%. Honey 25000g, answers GB/T18932.22 standard. Vitamins C 500g, purified water 65000g.
2, enzymolysis Camellia oil: by Camellia oil, carries out enzymolysis with the lipase 90g of the 1.5% of raw material total amount, and the time is 2-3 hour, and temperature is 40-60 DEG C, then filters, and collects filtrate A for subsequent use. Enzyme activity 100,000 U/g of lipase.
3, enzymolysis royal jelly: by royal jelly, with the purified water 14000g of the 4 of raw material total amount times, the proteolytic enzyme 52.5g of 1.5% carries out enzymolysis, and the time is 2-3 hour, and temperature is 40-60 DEG C, then filters, and collects liquor B for subsequent use. Enzyme activity 200,000 U/g of proteolytic enzyme.
4, honey 25000g, purified water 51000g, vitamins C 500g being pressed solid-liquid ratio configuration, merge Camellia oil filtrate A and royal jelly liquor B, stir evenly, be heated to 70-80 DEG C, decocting time 10-20 minute, then adopt membrane filtration, order number is 100-200 order.
5, by filling for step 4 gained feed liquid medicinal glass bottle, capacity 30ml, revolves lid sealing, then adopts autoclave sterilization pot. Temperature 105-110 DEG C, Operating Steam Pressure 0.20-0.25MPa, 5-10 minute time.
Embodiment 2
Supplementary material: Camellia oil 6500g, royal jelly 3500g, honey 30000g, vitamins C 500g, purified water 59500g. Preparation method is with embodiment 1.
Embodiment 3
Supplementary material: Camellia oil 7000g, royal jelly 4000g, honey 25000g, vitamins C 500g, purified water 63500g. Preparation method is with embodiment 1.
The main component (g/100g) of table 1 Camellia oil compound product
Content assaying method:
1, squalene content detection: the mensuration of squalene in gas chromatography determination DB31/T690-2013 vegetables oil.
2,10-HAD content detection: GB9697-2008 royal jelly standard test.
3, polyphenol content detection: GB/T8313-2008.
4, carbohydrate content measures: GB28050-2011.
5, total free aminoacids total amount: the mensuration of GB/T8314-2013 tea total free aminoacids total amount.
The foregoing is only the better embodiment of the present invention, all impartial changes done according to the present patent application patent scope, with modifying, all should belong to the covering scope of the present invention.

Claims (4)

1. a Camellia oil compound product, it is characterised in that: main raw material is counted by weight: Camellia oil 60-70 part, royal jelly 30-40 part, honey 250-300 part, vitamins C 5-6 part, purified water 550-700 part.
2. prepare the method for Camellia oil compound product as claimed in claim 1 for one kind, it is characterised in that: comprising enzymolysis, filtration, preparation, filling, sterilization process, wherein enzymolysis is for utilizing lipase and proteolytic enzyme to decompose Camellia oil and royal jelly respectively.
3. method according to claim 2, it is characterised in that: concrete steps are as follows:
(1) qualified raw material is weighed: Camellia oil is the Camellia oil that squeezing tea seed obtains, and with fruital and fruity, oleic acid degree is lower than 1%; 10-HAD >=the 1.4wt% of royal jelly; Honey meets GB/T18932.22 standard;
(2) enzymolysis, filtration: the Camellia oil lipase of its weight 1.0-2.0% is carried out enzymolysis, and the time is 2-3 hour, and temperature is 40-60 DEG C, filter, collect filtrate A; The royal jelly purified water of its weight 3-5 times and the proteolytic enzyme of 1.0-2.0% are carried out enzymolysis, and the time is 2-3 hour, and temperature is 40-60 DEG C, filters, and collects liquor B;
(3) prepare: by honey, vitamins C and the mixing of remaining purified water, add filtrate A and liquor B, stir evenly, be heated to 70-80 DEG C, decoct and boil 10-20 minute, then adopt 100-200 order membrane filtration;
(4) filling, sterilizing: by filling for step (3) gained feed liquid medicinal glass bottle, revolves lid sealing, sterilizing, temperature 105-110 DEG C, Operating Steam Pressure 0.20-0.25MPa, 5-10 minute time.
4. method according to claim 3, it is characterised in that: the enzyme activity of lipase is 100,000 U/g, and the enzyme activity of proteolytic enzyme is 200,000 U/g.
CN201610036389.4A 2016-01-20 2016-01-20 A kind of camellia oil compound product and preparation method thereof Active CN105660888B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610036389.4A CN105660888B (en) 2016-01-20 2016-01-20 A kind of camellia oil compound product and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610036389.4A CN105660888B (en) 2016-01-20 2016-01-20 A kind of camellia oil compound product and preparation method thereof

Publications (2)

Publication Number Publication Date
CN105660888A true CN105660888A (en) 2016-06-15
CN105660888B CN105660888B (en) 2019-11-12

Family

ID=56301896

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610036389.4A Active CN105660888B (en) 2016-01-20 2016-01-20 A kind of camellia oil compound product and preparation method thereof

Country Status (1)

Country Link
CN (1) CN105660888B (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106172888A (en) * 2016-07-26 2016-12-07 宜春元博山茶油科技农业开发有限公司 It is suitable for child's Camellia oil and preparation method thereof
CN106172887A (en) * 2016-07-26 2016-12-07 宜春元博山茶油科技农业开发有限公司 Puerperal period Camellia oil and preparation method thereof
CN106262890A (en) * 2016-08-12 2017-01-04 贵州省玉屏县金心笛油脂开发有限公司 A kind of tea oil health-care product with hypolipemic function and preparation method thereof
CN111011793A (en) * 2019-12-16 2020-04-17 天津星宇航天生物科技有限公司 Preparation method of aerospace-grade royal jelly capable of rapidly recovering physical function

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1899093A (en) * 2006-07-18 2007-01-24 杭州保灵有限公司 Method for preparing water soluble royal jelly
CN1904011A (en) * 2006-07-31 2007-01-31 上海应用技术学院 Preparation method of fish flavour essence
CN102771863A (en) * 2012-07-23 2012-11-14 重庆市畜牧科学院 Beverage with royal jelly flavor
CN104839720A (en) * 2015-05-31 2015-08-19 安庆市孝柱食品科技有限公司 Tea oil oral liquid

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1899093A (en) * 2006-07-18 2007-01-24 杭州保灵有限公司 Method for preparing water soluble royal jelly
CN1904011A (en) * 2006-07-31 2007-01-31 上海应用技术学院 Preparation method of fish flavour essence
CN102771863A (en) * 2012-07-23 2012-11-14 重庆市畜牧科学院 Beverage with royal jelly flavor
CN104839720A (en) * 2015-05-31 2015-08-19 安庆市孝柱食品科技有限公司 Tea oil oral liquid

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
黄甫等: "脂肪酶催化米糠油水解反应的研究", 《北京化工大学学报》 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106172888A (en) * 2016-07-26 2016-12-07 宜春元博山茶油科技农业开发有限公司 It is suitable for child's Camellia oil and preparation method thereof
CN106172887A (en) * 2016-07-26 2016-12-07 宜春元博山茶油科技农业开发有限公司 Puerperal period Camellia oil and preparation method thereof
CN106262890A (en) * 2016-08-12 2017-01-04 贵州省玉屏县金心笛油脂开发有限公司 A kind of tea oil health-care product with hypolipemic function and preparation method thereof
CN111011793A (en) * 2019-12-16 2020-04-17 天津星宇航天生物科技有限公司 Preparation method of aerospace-grade royal jelly capable of rapidly recovering physical function

Also Published As

Publication number Publication date
CN105660888B (en) 2019-11-12

Similar Documents

Publication Publication Date Title
CN102604796B (en) Preparation method of fermentation type plant flower rice wine
CN101343603B (en) Rose liquor wine and preparation thereof
CN103289871B (en) Pawpaw distilled liquor and preparation method thereof
CN109439477A (en) A kind of numb beer of fire and preparation method thereof
CN105941700A (en) Hippophae rhamnoide-Fu tea and preparation technology thereof
CN104673589A (en) Formula and preparation method for moringa health wine
CN105660888A (en) Camellia oil compound product and preparation method thereof
CN102224960B (en) Cyperus esculentus beverage and preparation method thereof
CN105995341A (en) Preparation method of selenium-rich blueberry vinegar drink
CN102618413B (en) Production method of traditional Chinese medicine alcoholic drink
CN103211029B (en) Matcha powder soybean milk and preparation method thereof
CN103194352B (en) Rose sweet white wine beverage and preparation method thereof
CN110343589A (en) A kind of glutinous rice health preserving wine and its brewage process adding traditional Chinese medicine ingredients
CN105533068B (en) A kind of processing method of Moringa solid fermentation tea
CN112680312B (en) Fermented olive fruit vinegar and production method thereof
CN105505668A (en) Castanea mollissima fruit wine preparation method
CN105942100A (en) Mulberry health-care compound beverage
CN107535934A (en) A kind of Blueberry frozen and preparation method thereof
CN105273919B (en) A kind of preparation method of bamboo wine
CN105349339A (en) Eyesight improving oil camellia wine and preparing method thereof
CN105613844A (en) Tea tree product and preparation method thereof
CN106857901B (en) Tea blending method and compound tea
KR101755118B1 (en) Manufacture of extract solution and capsules of ginseng-allium hookeri compound fermentation using microorganism
CN105861251A (en) Blueberry healthcare baijiu product
CN105524783A (en) Brewing method of Japanese Peristrophe Herb health red koji wine

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant