CN105638850A - Freshness-retaining film for meat product and preparation method of freshness-retaining film - Google Patents

Freshness-retaining film for meat product and preparation method of freshness-retaining film Download PDF

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Publication number
CN105638850A
CN105638850A CN201610166911.0A CN201610166911A CN105638850A CN 105638850 A CN105638850 A CN 105638850A CN 201610166911 A CN201610166911 A CN 201610166911A CN 105638850 A CN105638850 A CN 105638850A
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CN
China
Prior art keywords
meat product
fresh
coating
freshness
keeping film
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Pending
Application number
CN201610166911.0A
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Chinese (zh)
Inventor
李景军
管骁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JIANGSU LONGLIFE GROUP CO Ltd
University of Shanghai for Science and Technology
Original Assignee
JIANGSU LONGLIFE GROUP CO Ltd
University of Shanghai for Science and Technology
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Publication date
Application filed by JIANGSU LONGLIFE GROUP CO Ltd, University of Shanghai for Science and Technology filed Critical JIANGSU LONGLIFE GROUP CO Ltd
Priority to CN201610166911.0A priority Critical patent/CN105638850A/en
Publication of CN105638850A publication Critical patent/CN105638850A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B4/00General methods for preserving meat, sausages, fish or fish products
    • A23B4/10Coating with a protective layer; Compositions or apparatus therefor

Abstract

The invention relates to a freshness-retaining film for a meat product and a preparation method of the freshness-retaining film. The freshness-retaining film is made by taking hordein and soybean polysaccharide with different ratios as main raw materials, and taking a plasticizer and a nano silicon dioxide particle filler for assisting. The preparation method comprises the following steps: a, dissolving the hordein in a 55% isopropyl alcohol solution of 80 DEG C, thus obtaining colloidal fluid A; b, adding the soybean polysaccharide, the plasticizer and the nano silicon dioxide into the colloidal fluid A in sequence, stirring for 15min by keeping the temperature of 80 DEG C, after dissolving uniformly, quickly cooling to 15 DEG C by water bath, and keeping for 1h, thus obtaining colloidal fluid B; c, directly immersing the meat product in the colloidal fluid B, and airing, thus obtaining the freshness-retaining film. The freshness-retaining film for the meat product and the preparation method have the advantages that the freshness-retaining film prepared by the method is high in food safety, and the mechanical property and barrier property of the freshness-retaining film are greatly improved.

Description

A kind of fresh-keeping film-coating for meat product and its preparation method
Technical field
The invention belongs to meat preservation technical field, in particular to a kind of fresh-keeping film-coating for meat product, also relate to the preparation method of this fresh-keeping film-coating.
Background technology
The enhancing of the raising that meat product quality and preservation term are required by modern people and health of people consciousness, the edible freshness-keeping thin coat made with natural, safe material has become current research focus.
Edible film a kind of can eat and have the film of certain packaging protecting function, can be used as that barrier layer is entered by control water migration, oxygen, quality that the loss etc. of fats oxidn and volatile matter keeps processed food, extends shelf-lives. Edible packaging seen in daily life has a variety of, and each edible film has its weak point, such as the wafer in polyose film, though having edibility, but its intensity difference, meeting water and making moist cracky, and industrial scale is little, it is difficult to meet the demand of food product pack; The edibility casing that and for example the animal small intestine in protein film processes, although every performance is all better, but because of edibility is relatively low also cannot on a large scale for food product pack.
Therefore, research and develop a kind of edible safety fresh-keeping film-coating for meat product that is good and that can greatly improve mechanical property and barrier property to be necessary.
Summary of the invention
It is good and can greatly improve the fresh-keeping film-coating for meat product of mechanical property and barrier property that the technical problem to be solved in the present invention is to provide a kind of edible safety, also provides the preparation method of this fresh-keeping film-coating a kind of.
For solving the problems of the technologies described above, the technical scheme of the present invention is: a kind of fresh-keeping film-coating for meat product, and its innovative point is: the moiety of described fresh-keeping film-coating is by weight percentage:
Hordein 15%-20%;
Soybean polysaccharide 3%-5%;
Nano silicon 0.5%-1%;
Softening agent 3%-6%;
Surplus is mass concentration is the aqueous isopropanol of 55%.
Further, the particle diameter of described nano silicon is 50-100nm.
Further, described softening agent is a kind of in glycerine or polyoxyethylene glycol or both mixtures.
For the preparation of a method for the fresh-keeping film-coating of meat product, its innovative point is: described method comprises the steps:
(1) weigh: take the aqueous isopropanol that hordein, soybean polysaccharide, nano silicon, softening agent and mass concentration are 55% by weight percentage;
(2) glue liquid A is prepared: the mass concentration that hordein is dissolved in 80 DEG C is in the aqueous isopropanol of 55%, obtains glue liquid A;
(3) prepare glue liquid B: in glue liquid A, add soybean polysaccharide, softening agent and nano silicon successively, and when 80 DEG C insulated and stirred 15min, after being uniformly dissolved, and be rapidly cooled to 15 DEG C by water-bath and keep 1h to obtain glue liquid B;
(4) prepare fresh-keeping film-coating: with the glue liquid B submergence meat product 5��10s of preparation, then meat product is taken out and drain the fresh-keeping film-coating namely obtaining and being used for meat product.
It is an advantage of the current invention that:
(1) the present invention is used for the fresh-keeping film-coating of meat product, to derive from the hordein of natural plant raw material and soybean polysaccharide as main component, wherein, hordein belongs to the hydrophobic proteins in a class natural grain source, proline rich and L-glutamic acid, there is unique solvability, thermotolerance, film-forming properties, hydrophobicity, degradability and oxidation-resistance, thus it is applied to packaging material for food and compares environmental protection, and better than the fresh-keeping film-coating of animality source material on edible safety; In addition, the adding of nano silicon in fresh-keeping film-coating, improve the mechanical property of preservative film material, the tensile strength of preservative film increases, and when preservative film is shaping, pin-hole phenomena obviously reduces, it is to increase quality of forming film; Nano particle can significantly improve the barrier property of preservative film simultaneously, substantially improves the ability of fresh-keeping film-coating protection meat;
(2) the present invention is for the preparation of the method for the fresh-keeping film-coating of meat product, and this preparation method's technical process is simple, and the priority addition sequence of each component, ensure that the excellent properties of fresh-keeping film-coating; Meanwhile, in this preparation method, preparation condition is all easy to control and operation, and raw material sources are extensive, and then greatly reduces production cost.
Embodiment
The following examples can make professional and technical personnel more fully understand the present invention, but does not therefore limit the present invention among described scope of embodiments.
Embodiment 1
The present embodiment is used for the fresh-keeping film-coating of meat product, and the moiety of this fresh-keeping film-coating is by weight percentage: hordein 15%, soybean polysaccharide 3%, nano silicon 0.5%, glycerine 3%, and surplus is mass concentration is the aqueous isopropanol of 55%.
For the preparation of the method for the fresh-keeping film-coating of the present embodiment meat product, the method comprises the steps:
(1) weigh: take the aqueous isopropanol 78.5mL that hordein 15g, soybean polysaccharide 3g, nano silicon 0.5g, glycerine 3g and mass concentration are 55% by weight percentage;
(2) prepare glue liquid A: the hordein of 15g is dissolved in 80 DEG C, the mass concentration of 78.5mL be 55% aqueous isopropanol in, obtain glue liquid A;
(3) prepare glue liquid B: in glue liquid A, add 3g soybean polysaccharide, 3g glycerine and 0.5g nano silicon successively, and when 80 DEG C insulated and stirred 15min, after being uniformly dissolved, and be rapidly cooled to 15 DEG C by water-bath and keep 1h to obtain glue liquid B;
(4) prepare fresh-keeping film-coating: with the glue liquid B submergence meat jujube product 5s of preparation, then meat jujube product is taken out and drain the fresh-keeping film-coating namely obtaining and being used for meat product.
Embodiment 2
The present embodiment is used for the fresh-keeping film-coating of meat product, and the moiety of this fresh-keeping film-coating is by weight percentage: hordein 20%, soybean polysaccharide 5%, nano silicon 1%, glycerine 6%, and surplus is mass concentration is the aqueous isopropanol of 55%.
For the preparation of the method for the fresh-keeping film-coating of the present embodiment meat product, the method comprises the steps:
(1) weigh: take the aqueous isopropanol 68mL that hordein 20g, soybean polysaccharide 5g, nano silicon 1g, glycerine 6g and mass concentration are 55% by weight percentage;
(2) prepare glue liquid A: the hordein of 20g is dissolved in 80 DEG C, the mass concentration of 68mL be 55% aqueous isopropanol in, obtain glue liquid A;
(3) prepare glue liquid B: in glue liquid A, add 5g soybean polysaccharide, 6g glycerine and 1g nano silicon successively, and when 80 DEG C insulated and stirred 15min, after being uniformly dissolved, and be rapidly cooled to 15 DEG C by water-bath and keep 1h to obtain glue liquid B;
(4) prepare fresh-keeping film-coating: with the glue liquid B submergence sausage product 10s of preparation, then sausage product is taken out and drain the fresh-keeping film-coating namely obtaining and being used for meat product.
Embodiment 3
The present embodiment is used for the fresh-keeping film-coating of meat product, and the moiety of this fresh-keeping film-coating is by weight percentage: hordein 18%, soybean polysaccharide 4%, nano silicon 0.8%, polyoxyethylene glycol 5%, and surplus is mass concentration is the aqueous isopropanol of 55%.
For the preparation of the method for the fresh-keeping film-coating of the present embodiment meat product, the method comprises the steps:
(1) weigh: take the aqueous isopropanol 72mL that hordein 18g, soybean polysaccharide 4g, nano silicon 0.8g, polyoxyethylene glycol 5g and mass concentration are 55% by weight percentage;
(2) prepare glue liquid A: the hordein of 18g is dissolved in 80 DEG C, the mass concentration of 72mL be 55% aqueous isopropanol in, obtain glue liquid A;
(3) prepare glue liquid B: in glue liquid A, add 4g soybean polysaccharide, 5g polyoxyethylene glycol and 0.8g nano silicon successively, and when 80 DEG C insulated and stirred 15min, after being uniformly dissolved, and be rapidly cooled to 15 DEG C by water-bath and keep 1h to obtain glue liquid B;
(4) prepare fresh-keeping film-coating: with the glue liquid B submergence jerky product 6s of preparation, then jerky product is taken out and drain the fresh-keeping film-coating namely obtaining and being used for meat product.
Embodiment 4
The present embodiment is used for the fresh-keeping film-coating of meat product, and the moiety of this fresh-keeping film-coating is by weight percentage: hordein 16%, soybean polysaccharide 3.5%, nano silicon 0.6%, polyoxyethylene glycol 6%, and surplus is mass concentration is the aqueous isopropanol of 55%.
For the preparation of the method for the fresh-keeping film-coating of the present embodiment meat product, the method comprises the steps:
(1) weigh: take the aqueous isopropanol 74mL that hordein 16g, soybean polysaccharide 3.5g, nano silicon 0.6g, polyoxyethylene glycol 6g and mass concentration are 55% by weight percentage;
(2) prepare glue liquid A: the hordein of 16g is dissolved in 80 DEG C, the mass concentration of 74mL be 55% aqueous isopropanol in, obtain glue liquid A;
(3) glue liquid B is prepared: in glue liquid A, add 3.5g soybean polysaccharide, 6g polyoxyethylene glycol and 0.6g nano silicon successively, and when 80 DEG C insulated and stirred 15min, after being uniformly dissolved, and it is cooled to 15 DEG C by water-bath rapidly and keeps 1h to obtain glue liquid B;
(4) prepare fresh-keeping film-coating: with the glue liquid B submergence jerky product 6s of preparation, then jerky product is taken out and drain the fresh-keeping film-coating namely obtaining and being used for meat product.
Embodiment 5
The present embodiment is used for the fresh-keeping film-coating of meat product, and the moiety of this fresh-keeping film-coating is by weight percentage: hordein 17.5%, soybean polysaccharide 3.5%, nano silicon 0.75%, glycerine 2%, polyoxyethylene glycol 2.5%, surplus is mass concentration is the aqueous isopropanol of 55%.
For the preparation of the method for the fresh-keeping film-coating of the present embodiment meat product, the method comprises the steps:
(1) weigh: take the aqueous isopropanol 74mL that hordein 17.5g, soybean polysaccharide 3.5g, nano silicon 0.75g, glycerine 2g, polyoxyethylene glycol 2.5g and mass concentration are 55% by weight percentage;
(2) prepare glue liquid A: the hordein of 17.5g is dissolved in 80 DEG C, the mass concentration of 74mL be 55% aqueous isopropanol in, obtain glue liquid A;
(3) glue liquid B is prepared: in glue liquid A, add 3.5g soybean polysaccharide, 2g glycerine, 2.5g polyoxyethylene glycol and 0.75g nano silicon successively, and when 80 DEG C insulated and stirred 15min, after being uniformly dissolved, and it is cooled to 15 DEG C by water-bath rapidly and keeps 1h to obtain glue liquid B;
(4) prepare fresh-keeping film-coating: with the glue liquid B submergence sausage product 10s of preparation, then sausage product is taken out and drain the fresh-keeping film-coating namely obtaining and being used for meat product.
Following table is the performance table of embodiment 1��5 for the fresh-keeping film-coating of meat product.
Performance Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5
Tensile strength MPa 0.514 0.708 0.682 0.590 0.654
Pin-hole phenomena Nothing Nothing Nothing Nothing Nothing
Quality of forming film Better Good Good Good Good
Oxygen transmission coefficient (cm3.cm))/(cm2.s.Pa) 0.042 0.036 0.038 0.041 0.039
Water vapour transmission coefficient (g.mm)/(m2.d.kPa) 15.3 12.8 13.4 14.7 13.9
As can be seen from the above table, the fresh-keeping film-coating for meat product prepared in embodiment, all derive from hordein and the soybean polysaccharide of natural phant with main raw material of drawing materials, it is aided with softening agent and nanoparticulate fillers, and then substantially improve the edible safety of film material; The adding of nanometer silicon dioxide particle in preservative film, improving the mechanical property of preservative film material, the tensile strength of preservative film increases, and tensile strength can reach more than 0.5MPa; And preservative film shaping time pin-hole phenomena obviously reduce, embodiment equal free of pinholes phenomenon, it is to increase quality of forming film; Nano particle can significantly improve the barrier property of preservative film simultaneously, i.e. oxygen barrier and Steam by water bath gas performance; In addition, each embodiment is compared, and each performance perameter of embodiment 2 is all more excellent, and thus, embodiment 2 is most preferred embodiment.
More than show and describe the ultimate principle of the present invention and the advantage of main feature and the present invention. The technician of the industry should understand; the present invention is not restricted to the described embodiments; the principle that the present invention is just described described in above-described embodiment and specification sheets; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention. The claimed scope of the present invention is defined by appending claims and equivalent thereof.

Claims (4)

1. the fresh-keeping film-coating for meat product, it is characterised in that: the moiety of described fresh-keeping film-coating is by weight percentage:
Hordein 15%-20%;
Soybean polysaccharide 3%-5%;
Nano silicon 0.5%-1%;
Softening agent 3%-6%;
Surplus is mass concentration is the aqueous isopropanol of 55%.
2. the fresh-keeping film-coating for meat product according to claim 1, it is characterised in that: the particle diameter of described nano silicon is 50-100nm.
3. the fresh-keeping film-coating for meat product according to claim 1, it is characterised in that: described softening agent is a kind of in glycerine or polyoxyethylene glycol or both mixtures.
4. prepare described in claim 1 method of the fresh-keeping film-coating for meat product for one kind, it is characterised in that: described method comprises the steps:
(1) weigh: take the aqueous isopropanol that hordein, soybean polysaccharide, nano silicon, softening agent and mass concentration are 55% by weight percentage;
(2) glue liquid A is prepared: the mass concentration that hordein is dissolved in 80 DEG C is in the aqueous isopropanol of 55%, obtains glue liquid A;
(3) prepare glue liquid B: in glue liquid A, add soybean polysaccharide, softening agent and nano silicon successively, and when 80 DEG C insulated and stirred 15min, after being uniformly dissolved, and be rapidly cooled to 15 DEG C by water-bath and keep 1h to obtain glue liquid B;
(4) prepare fresh-keeping film-coating: with the glue liquid B submergence meat product 5��10s of preparation, then meat product is taken out and drain the fresh-keeping film-coating namely obtaining and being used for meat product.
CN201610166911.0A 2016-03-23 2016-03-23 Freshness-retaining film for meat product and preparation method of freshness-retaining film Pending CN105638850A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106261548A (en) * 2016-08-17 2017-01-04 安徽省怀远县金淮河食品有限公司 Edible membrane material prepared by a kind of wheat bran
CN106306430A (en) * 2016-08-20 2017-01-11 蚌埠市天网渔需用品有限公司 Preparation method of granular bait film-coating material
CN111393693A (en) * 2020-03-31 2020-07-10 海南健康管理职业技术学院 Preparation method of nano silicon dioxide/polyvinyl alcohol/carapace liquefied product preservative film material

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CN103666254A (en) * 2013-12-10 2014-03-26 上海理工大学 Film-forming solution, and preparation method and application thereof
CN104705387A (en) * 2014-08-16 2015-06-17 高邮市红太阳食品有限公司 Special film preservative for cooked salted duck egg and film coating process

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1177911A (en) * 1995-01-20 1998-04-01 火星有限公司 Edible products having inorganic coatings
CN102660179A (en) * 2012-03-20 2012-09-12 常熟市屹浩食品包装材料有限公司 Fresh-keeping packaging material with composite coating of PVA-liquid paraffin and with combined modification of nanosized TiO2-SiO2 and preparation method thereof
CN103666254A (en) * 2013-12-10 2014-03-26 上海理工大学 Film-forming solution, and preparation method and application thereof
CN104705387A (en) * 2014-08-16 2015-06-17 高邮市红太阳食品有限公司 Special film preservative for cooked salted duck egg and film coating process

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Title
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106261548A (en) * 2016-08-17 2017-01-04 安徽省怀远县金淮河食品有限公司 Edible membrane material prepared by a kind of wheat bran
CN106306430A (en) * 2016-08-20 2017-01-11 蚌埠市天网渔需用品有限公司 Preparation method of granular bait film-coating material
CN111393693A (en) * 2020-03-31 2020-07-10 海南健康管理职业技术学院 Preparation method of nano silicon dioxide/polyvinyl alcohol/carapace liquefied product preservative film material
CN111393693B (en) * 2020-03-31 2022-08-26 海南健康管理职业技术学院 Preparation method of nano silicon dioxide/polyvinyl alcohol/carapace liquefied product preservative film material

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Application publication date: 20160608