CN105603773A - 一种竹纤维面料染色剂 - Google Patents

一种竹纤维面料染色剂 Download PDF

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CN105603773A
CN105603773A CN201510974530.0A CN201510974530A CN105603773A CN 105603773 A CN105603773 A CN 105603773A CN 201510974530 A CN201510974530 A CN 201510974530A CN 105603773 A CN105603773 A CN 105603773A
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parts
powder
coloring agent
fiber fabric
leaf
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马晓飞
张连存
张丽
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ANHUI SANBAO COTTON KNITTING INVESTMENT Co Ltd
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ANHUI SANBAO COTTON KNITTING INVESTMENT Co Ltd
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Abstract

本发明公开了一种竹纤维面料染色剂，涉及染色剂技术领域，由如下重量份数的原料制成：天然染料100-110份、秸秆灰12-17份、棕榈蜡10-15份、葡萄糖苷10-15份、海泡石粉8-12份、十二烷基二甲基甜菜碱6-10份、二甲基二烯丙基氯化铵6-10份、纳米硅微粉5-8份、苏打粉4-6份、抗菌剂3-5份、异氰酸酯3-5份、稀土2-3份、亚麻籽油10-15份、乙二醇乙醚15-20份、水250-300份。本发明染色剂能有效提高染色牢度和上染率，减少染料的用量和印染废水的产生量，并且提高竹纤维面料的手感柔软度和外观质量；其中抗菌剂的加入能进一步大大提高竹纤维面料的抗菌抑菌能力，增强其使用效果。

Description

一种竹纤维面料染色剂
技术领域：
本发明涉及染色剂技术领域，具体涉及一种竹纤维面料染色剂。
背景技术：
竹纤维是从自然生长的竹子中提取的一种纤维素纤维，具有良好的透气性、瞬间吸水性、较强的耐磨性，同时又具有天然抗菌抑菌、除螨、防臭和抗紫外线功能。专家指出，竹纤维是一种真正意义上的天然环保型绿色纤维。竹纤维面料完全复制了竹纤维的固有特性，倍受消费者青睐，但目前竹纤维面料的染色大都采用化学染料，不仅增加了印染废水，而且对人体健康存在一定的威胁。
发明内容：
本发明所要解决的技术问题在于提供一种染色牢度、上染率高且安全环保的竹纤维面料染色剂。
本发明所要解决的技术问题采用以下的技术方案来实现：
一种竹纤维面料染色剂，由如下重量份数的原料制成：
天然染料100-110份、秸秆灰12-17份、棕榈蜡10-15份、葡萄糖苷10-15份、海泡石粉8-12份、十二烷基二甲基甜菜碱6-10份、二甲基二烯丙基氯化铵6-10份、纳米硅微粉5-8份、苏打粉4-6份、抗菌剂3-5份、异氰酸酯3-5份、稀土2-3份、亚麻籽油10-15份、乙二醇乙醚15-20份、水250-300份；
其制备方法如下：
(1)将天然染料、秸秆灰和纳米硅微粉加入水中，混合均匀后浸泡15min，然后于微波频率2450MHz、功率600W下微波处理10min，即得物料I；
(2)向海泡石粉中加入棕榈蜡和亚麻籽油，加热至80-90℃混合15min，待物料冷却至室温后再加入苏打粉和乙二醇乙醚，混合均匀即得物料II；
(3)向物料I中加入葡萄糖苷、十二烷基二甲基甜菜碱和二甲基二烯丙基氯化铵，混合物于超声频率40kHz、功率50W下超声处理30min，然后加入物料II、抗菌剂、异氰酸酯和稀土，充分混合均匀即可。
所述抗菌剂由如下重量份数的原料制成：银杏叶15份、樒树叶15份、臭椿叶12份、樟脑叶10份、花椒叶8份、松针茶6份、葡萄籽5份、雷公藤5份、桉叶油3份、沸石粉10份、羧甲基壳聚糖8份、纳米氧化铜2份、纳米二氧化钛2份，其制备方法为：(1)先将沸石粉和纳米氧化铜加入3倍重量乙醇中，先于超声频率40kHz、功率50W下超声处理20min，再于微波频率2450MHz、功率600W下微波处理10min，过滤，所得滤饼经真空干燥后粉碎成粉末，然后加入羧甲基壳聚糖和纳米二氧化钛，混合均匀即得粉料I；(2)将银杏叶、樟脑叶、松针茶、葡萄籽和雷公藤加入5倍重量水中，加热至沸腾状态保温1h，再将处理液与樒树叶、臭椿叶和花椒叶加入磨浆机中，经充分磨浆后过滤，滤液送入冷冻干燥机，所得固体经粉碎机制成粉末，即得粉料II；(3)将粉料I、粉料II和桉叶油充分混合均匀即可。
本发明的有益效果是：本发明以天然染料为主要原料，辅以纳米材料、稀土和多种功能助剂制得竹纤维面料染色剂，该染色剂能有效提高染色牢度和上染率，减少染料的用量和印染废水的产生量，并且提高竹纤维面料的手感柔软度和外观质量；其中抗菌剂的加入能进一步大大提高竹纤维面料的抗菌抑菌能力，增强其使用效果。
具体实施方式：
为了使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解，下面结合具体实施例，进一步阐述本发明。
实施例1
抗菌剂的制备：
(1)先将10份沸石粉和2份纳米氧化铜加入3倍重量乙醇中，先于超声频率40kHz、功率50W下超声处理20min，再于微波频率2450MHz、功率600W下微波处理10min，过滤，所得滤饼经真空干燥后粉碎成粉末，然后加入8份羧甲基壳聚糖和2份纳米二氧化钛，混合均匀即得粉料I；
(2)将15份银杏叶、10份樟脑叶、6份松针茶、5份葡萄籽和5份雷公藤加入5倍重量水中，加热至沸腾状态保温1h，再将处理液与15份樒树叶、12份臭椿叶和8份花椒叶加入磨浆机中，经充分磨浆后过滤，滤液送入冷冻干燥机，所得固体经粉碎机制成粉末，即得粉料II；
(3)将粉料I、粉料II和3份桉叶油充分混合均匀即可。
实施例2
(1)将100份天然染料、15份秸秆灰和5份纳米硅微粉加入250份水中，混合均匀后浸泡15min，然后于微波频率2450MHz、功率600W下微波处理10min，即得物料I；
(2)向8份海泡石粉中加入15份棕榈蜡和10份亚麻籽油，加热至80-90℃混合15min，待物料冷却至室温后再加入4份苏打粉和15份乙二醇乙醚，混合均匀即得物料II；
(3)向物料I中加入10份葡萄糖苷、8份十二烷基二甲基甜菜碱和6份二甲基二烯丙基氯化铵，混合物于超声频率40kHz、功率50W下超声处理30min，然后加入物料II、3份抗菌剂、5份异氰酸酯和2份稀土，充分混合均匀即可。
实施例3
(1)将110份天然染料、12份秸秆灰和7份纳米硅微粉加入300份水中，混合均匀后浸泡15min，然后于微波频率2450MHz、功率600W下微波处理10min，即得物料I；
(2)向10份海泡石粉中加入10份棕榈蜡和15份亚麻籽油，加热至80-90℃混合15min，待物料冷却至室温后再加入5份苏打粉和20份乙二醇乙醚，混合均匀即得物料II；
(3)向物料I中加入13份葡萄糖苷、6份十二烷基二甲基甜菜碱和8份二甲基二烯丙基氯化铵，混合物于超声频率40kHz、功率50W下超声处理30min，然后加入物料II、5份抗菌剂、3份异氰酸酯和3份稀土，充分混合均匀即可。
以上显示和描述了本发明的基本原理和主要特征和本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。

Claims (2)

1.一种竹纤维面料染色剂，其特征在于，由如下重量份数的原料制成：
天然染料100-110份、秸秆灰12-17份、棕榈蜡10-15份、葡萄糖苷10-15份、海泡石粉8-12份、十二烷基二甲基甜菜碱6-10份、二甲基二烯丙基氯化铵6-10份、纳米硅微粉5-8份、苏打粉4-6份、抗菌剂3-5份、异氰酸酯3-5份、稀土2-3份、亚麻籽油10-15份、乙二醇乙醚15-20份、水250-300份；
其制备方法如下：
(1)将天然染料、秸秆灰和纳米硅微粉加入水中，混合均匀后浸泡15min，然后于微波频率2450MHz、功率600W下微波处理10min，即得物料I；
(2)向海泡石粉中加入棕榈蜡和亚麻籽油，加热至80-90℃混合15min，待物料冷却至室温后再加入苏打粉和乙二醇乙醚，混合均匀即得物料II；
(3)向物料I中加入葡萄糖苷、十二烷基二甲基甜菜碱和二甲基二烯丙基氯化铵，混合物于超声频率40kHz、功率50W下超声处理30min，然后加入物料II、抗菌剂、异氰酸酯和稀土，充分混合均匀即可。
2.根据权利要求1所述的竹纤维面料染色剂，其特征在于，所述抗菌剂由如下重量份数的原料制成：银杏叶15份、樒树叶15份、臭椿叶12份、樟脑叶10份、花椒叶8份、松针茶6份、葡萄籽5份、雷公藤5份、桉叶油3份、沸石粉10份、羧甲基壳聚糖8份、纳米氧化铜2份、纳米二氧化钛2份，其制备方法为：(1)先将沸石粉和纳米氧化铜加入3倍重量乙醇中，先于超声频率40kHz、功率50W下超声处理20min，再于微波频率2450MHz、功率600W下微波处理10min，过滤，所得滤饼经真空干燥后粉碎成粉末，然后加入羧甲基壳聚糖和纳米二氧化钛，混合均匀即得粉料I；(2)将银杏叶、樟脑叶、松针茶、葡萄籽和雷公藤加入5倍重量水中，加热至沸腾状态保温1h，再将处理液与樒树叶、臭椿叶和花椒叶加入磨浆机中，经充分磨浆后过滤，滤液送入冷冻干燥机，所得固体经粉碎机制成粉末，即得粉料II；(3)将粉料I、粉料II和桉叶油充分混合均匀即可。
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