CN105534801B - 一种含竹荪提取物的滋润唇膏及其制备方法 - Google Patents
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Abstract
本发明公开了一种含竹荪提取物的滋润唇膏及其制备方法,其所用原料按重量份计包括:竹荪提取物1~10份,油质成分80份,蜡质成分25~30份,羊毛脂5~8份,维生素E 1~2份。本发明采用不同极性的溶剂对竹荪所含不同营养成分进行提取,包括高浓度醇提、中浓度醇提和水提,再将所得竹荪提取物用于制备滋润唇膏,其制备方法简易,成本低,所得滋润唇膏保湿效果好,并具有消炎镇痛的功效,无副作用。
Description
技术领域
本发明属于日化用品技术领域,具体涉及一种具有消炎镇痛功效的含竹荪提取物的滋润唇膏及其制备方法。
背景技术
目前市面上大部分唇膏内所含的颜料、化学基质会吸收口唇黏膜细胞内的水分,使得口唇黏膜细胞发生脱水现象。而由于唇膏使用不当、外力刺激或是自身体质等原因引起的唇干、唇裂等唇部伤害越来越常见。这不仅仅影响容貌的美观,严重的还会对人的身心健康和生活质量造成影响。当前市售的唇膏主要功效为保湿和美容,具有消炎镇痛功效的极少。中国专利(CN 101156831A)公开了一种润唇膏,该产品采用植物蜡代替目前普遍使用的矿物蜡,并采用植物油脂代替目前普遍使用的矿物油脂和合成油脂,消除了矿物蜡、矿物油脂和合成油脂对唇部肌肤的刺激和毒性,避免了由石油提取物可能导致的人体皮肤湿疹样病变及由动物油脂可能导致的变态性接触性皮炎,但是这种润唇膏对已经发生炎症的唇部没有治疗作用。中国专利(CN 103027885A)公开了一种安全唇膏,该唇膏的成分安全无刺激,适于所有人使用,能有效滋润嘴唇,防止嘴唇干裂、起皮,但是这种润唇膏功效单一,不具备防晒、护色、预防唇炎、修复损伤等作用。
竹荪是“草八珍”之一,并有“天然食品防腐剂”之称。大量研究表明,竹荪提取液的抑菌效果非常显著,且其抗氧化、杀菌、消炎效果也十分显著。同时,竹荪有一定的吸水性和成膜性,即有很好的保湿作用,对人体的副作用小,适于所有人使用。本发明将竹荪菌托干品处理后,再经过三次提取得到的竹荪提取物用于唇膏的制备中,利用竹荪提取物的特性对唇部进行护理,使所得唇膏具有美容和医疗双重功效。
发明内容
本发明的目的在于提供一种具有消炎镇痛功效的含竹荪提取物的滋润唇膏及其制备方法,所得滋润唇膏对唇部有较好的护理作用。
为实现上述目的,本发明采用如下技术方案:
一种含竹荪提取物的滋润唇膏,所用原料按重量份计包括:竹荪提取物1~10份,油质成分80份,蜡质成分25~30份,羊毛脂5~8份,维生素E 1~2份;
所述油质成分为橄榄油、芦荟油、澳洲坚果油、乳木果油、杏仁油、小麦胚芽油、蓖麻油、葵花籽油、茶树油、花生油、大豆油、葡萄籽油中的任意一种或几种;
所述蜡质成分为巴西棕榈蜡、蓖麻蜡、蜂蜡、橄榄酯、霍霍巴脂、小烛树蜡、小花茉莉蜡中的任意一种或几种。
所述竹荪提取物的制备方法包括以下步骤:
1)将竹荪菌托干品经清洗除杂,30~50℃电热恒温鼓风干燥至恒重后粉碎,过80~100目筛,备用;
2)在步骤1)所得竹荪菌托粉中按料液比1:20~1:30加入质量浓度为80~95%的乙醇溶液,于70~90℃恒温回流提取3h后,过滤,滤液浓缩至膏状,然后真空冷冻干燥成粉状,密封置于4℃保存;
3)在步骤2)过滤后剩余的滤渣中按料液比1:15~1:25加入质量浓度为50~70%的乙醇溶液,于50~70℃、功率350W条件下超声波辅助提取0.5~1h,然后过滤,滤液浓缩至膏状,再真空冷冻干燥成粉状,密封置于4℃备用;
4)在步骤3)过滤后剩余的滤渣中按料液比1:20~1:40加入去离子水,于90~100℃恒温热水提取3h,然后抽滤,滤液浓缩后加入滤液体积3倍量、质量浓度为95%的乙醇溶液,醇沉过夜后离心,所得沉淀真空冷冻干燥成粉状,密封置于4℃备用;
5)将步骤2)、3)、4)所得粉状提取物混合,即为竹荪提取物。
所述含竹荪提取物的滋润唇膏的制备方法包括以下步骤:
1)将油质成分于80~90℃水浴加热3~5min,然后加入竹荪提取物,搅拌至混合液成稠状;
2)将蜡质成分于80~90℃水浴加热3~5min,趁热将其倒入步骤1)的稠状混合液中,搅拌5~10min至其完全融化,配成混合液;
3)将羊毛脂于80~90℃水浴加热3~10min,趁热与步骤2)所得混合液混合,搅拌混匀;
4)将步骤3)所得料液冷却至20~25℃后加入维生素E,并根据需要加入色素和香精,然后将混合料液置于真空干燥箱内,于60~70℃、200~220Pa条件下减压脱泡10~25min,再注入模具填充到包装材料中,0~4℃凝固1~2h后取出即得。
步骤4)中所述色素为日落黄、高粱红素中的任意一种或两种;所述香精为柠檬香精、草莓香精、薄荷香精中的任意一种或几种。
本发明的显著优点在于:本发明采用不同极性的溶剂对竹荪所含不同营养成分进行提取,包括高浓度醇提、中浓度醇提取和水提,并利用羊毛脂具有较好的乳化、润湿和渗透作用,各种蜡质为纯天然的滋润剂,制得一种具有消炎镇痛功效的含竹荪提取物的滋润唇膏。本发明制备方法简易,成本低,所得滋润唇膏保湿效果好,并具有消炎镇痛功效,且无副作用,适用于唇干、唇裂等唇部伤害的预防和护理。
具体实施方式
为了使本发明所述的内容更加便于理解,下面结合具体实施方式对本发明所述的技术方案做进一步的说明,但是本发明不仅限于此。
实施例一:一种草莓味含竹荪提取物的滋润唇膏
1. 竹荪提取物的制备方法:
1)将竹荪菌托干品经清洗除杂,30℃电热恒温鼓风干燥至恒重后粉碎,过80目筛,备用;
2)在步骤1)所得竹荪菌托粉中按料液比1:20加入质量浓度为95%的乙醇溶液,于70℃恒温回流提取3h后,过滤,滤液浓缩至膏状,然后真空冷冻干燥成粉状,密封置于4℃保存;
3)在步骤2)过滤后剩余的滤渣中按料液比1:15加入质量浓度为70%的乙醇溶液,于50℃、功率350W条件下超声波辅助提取1h,然后过滤,滤液浓缩至膏状,再真空冷冻干燥成粉状,密封置于4℃备用;
4)在步骤3)过滤后剩余的滤渣中按料液比1:20加入去离子水,于90℃恒温热水提取3h,然后抽滤,滤液浓缩后加入滤液体积3倍量、质量浓度为95%的乙醇溶液,醇沉过夜后离心,所得沉淀真空冷冻干燥成粉状,密封置于4℃备用;
5)将步骤2)、3)、4)所得粉状提取物混合,即为竹荪提取物。
2. 滋润唇膏的制备方法:
1)将橄榄油35重量份、芦荟油10重量份、蓖麻油10重量份、葵花籽油25重量份混合后,于80℃水浴加热5min,然后加入1重量份竹荪提取物,搅拌至混合液成稠状;
2)将巴西棕榈蜡5重量份、蓖麻蜡5重量份、橄榄酯20重量份混合后,于80℃水浴加热5min,趁热将其倒入步骤1)的稠状混合液中,搅拌5min至其完全融化,配成混合液;
3)将羊毛脂5重量份于80℃水浴加热10min,趁热与步骤2)所得混合液混合,搅拌混匀;
4)将步骤3)所得料液冷却至20℃后加入维生素E 1重量份,并加入高粱红素1重量份、草莓香精1重量份,然后将混合料液置于真空干燥箱内,于60℃、200Pa条件下减压脱泡25min,再注入模具填充到包装材料中,0℃凝固1h后取出即得。
实施例二:一种柠檬味含竹荪提取物的滋润唇膏
1. 竹荪提取物的制备方法:
1)将竹荪菌托干品经清洗除杂,40℃电热恒温鼓风干燥至恒重后粉碎,过80目筛,备用;
2)在步骤1)所得竹荪菌托粉中按料液比1:25加入质量浓度为90%的乙醇溶液,于80℃恒温回流提取3h后,过滤,滤液浓缩至膏状,然后真空冷冻干燥成粉状,密封置于4℃保存;
3)在步骤2)过滤后剩余的滤渣中按料液比1:20加入质量浓度为60%的乙醇溶液,于60℃、功率350W条件下超声波辅助提取0.5h,然后过滤,滤液浓缩至膏状,再真空冷冻干燥成粉状,密封置于4℃备用;
4)在步骤3)过滤后剩余的滤渣中按料液比1:30加入去离子水,于95℃恒温热水提取3h,然后抽滤,滤液浓缩后加入滤液体积3倍量、质量浓度为95%的乙醇溶液,醇沉过夜后离心,所得沉淀真空冷冻干燥成粉状,密封置于4℃备用;
5)将步骤2)、3)、4)所得粉状提取物混合,即为竹荪提取物。
2. 滋润唇膏的制备方法:
1)将澳洲坚果油40重量份、乳木果油25重量份、茶树油10重量份、花生油5重量份混合后,于85℃水浴加热4min,然后加入1~10重量份竹荪提取物,搅拌至混合液成稠状;
2)将蜂蜡10重量份、霍霍巴脂10重量份、小花茉莉蜡5重量份混合后,于85℃水浴加热4min,趁热将其倒入步骤1)的稠状混合液中,搅拌8min至其完全融化,配成混合液;
3)将羊毛脂6重量份于85℃水浴加热5min,趁热与步骤2)所得混合液混合,搅拌混匀;
4)将步骤3)所得料液冷却至22℃后加入维生素E 2重量份,并加入日落黄2重量份、柠檬香精1重量份,然后将混合料液置于真空干燥箱内,于65℃、210Pa条件下减压脱泡20min,再注入模具填充到包装材料中,2℃凝固1.5h后取出即得。
实施例三:一种薄荷味含竹荪提取物的滋润唇膏
1. 竹荪提取物的制备方法:
1)将竹荪菌托干品经清洗除杂,50℃电热恒温鼓风干燥至恒重后粉碎,过100目筛,备用;
2)在步骤1)所得竹荪菌托粉中按料液比1:30加入质量浓度为80%的乙醇溶液,于90℃恒温回流提取3h后,过滤,滤液浓缩至膏状,然后真空冷冻干燥成粉状,密封置于4℃保存;
3)在步骤2)过滤后剩余的滤渣中按料液比1:25加入质量浓度为50%的乙醇溶液,70℃、功率350W条件下超声波辅助提取0.5h,然后过滤,滤液浓缩至膏状,再真空冷冻干燥成粉状,密封置于4℃备用;
4)在步骤3)过滤后剩余的滤渣中按料液比1:40加入去离子水,于100℃恒温热水提取3h,然后抽滤,滤液浓缩后加入滤液体积3倍量、质量浓度为95%的乙醇溶液,醇沉过夜后离心,所得沉淀真空冷冻干燥成粉状,密封置于4℃备用;
5)将步骤2)、3)、4)所得粉状提取物混合,即为竹荪提取物。
2. 滋润唇膏的制备方法:
1)将乳木果油25重量份、杏仁油35重量份、小麦胚芽油5重量份、大豆油15重量份混合后,于90℃水浴加热3min,然后加入1~10重量份竹荪提取物,搅拌至混合液成稠状;
2)将蜂蜡10重量份、小烛树蜡5重量份、小花茉莉蜡10重量份混合后,于90℃水浴加热3min,趁热将其倒入步骤1)的稠状混合液中,搅拌10min至其完全融化,配成混合液;
3)将羊毛脂8重量份于90℃水浴加热3min,趁热与步骤2)所得混合液混合,搅拌混匀;
4)将步骤3)所得料液冷却至25℃后加入维生素E 2重量份,并加入薄荷香精1重量份,然后将混合料液置于真空干燥箱内,于70℃、220Pa条件下减压脱泡10min,再注入模具填充到包装材料中,4℃凝固2h后取出即得。
本发明制备方法简易,成本低,所得滋润唇膏保湿效果好,并具有消炎镇痛功效,且无副作用,适用于唇干、唇裂等唇部伤害的预防和护理。
以上所述仅为本发明的较佳实施例,凡依本发明申请专利范围所做的均等变化与修饰,皆应属本发明的涵盖范围。
Claims (3)
1. 一种含竹荪提取物的滋润唇膏,其特征在于:所用原料按重量份计包括:竹荪提取物1~10份,油质成分80份,蜡质成分25~30份,羊毛脂5~8份,维生素E 1~2份;
所述油质成分为橄榄油、芦荟油、澳洲坚果油、乳木果油、杏仁油、小麦胚芽油、蓖麻油、葵花籽油、茶树油、花生油、大豆油、葡萄籽油中的任意一种或几种;
所述蜡质成分为巴西棕榈蜡、蓖麻蜡、蜂蜡、橄榄酯、霍霍巴脂、小烛树蜡、小花茉莉蜡中的任意一种或几种;
所述竹荪提取物的制备方法包括以下步骤:
1)将竹荪菌托干品经清洗除杂,30~50℃干燥至恒重后粉碎,过80~100目筛,备用;
2)将步骤1)所得竹荪菌托粉经乙醇回流提取后过滤,滤液浓缩至膏状,然后真空冷冻干燥成粉状;
3)将步骤2)过滤后剩余的滤渣采用超声波辅助提取,然后过滤,滤液浓缩至膏状,再真空冷冻干燥成粉状;
4)将步骤3)过滤后剩余的滤渣用热水提取,然后抽滤,滤液浓缩后加入滤液体积3倍量、质量浓度为95%的乙醇溶液,醇沉过夜后离心,所得沉淀真空冷冻干燥成粉状;
5)将步骤2)、3)、4)所得粉状提取物混合,即为竹荪提取物;
其中,步骤2)所述乙醇回流提取是按料液比1:20~1:30在竹荪菌托粉中加入质量浓度为80~95%的乙醇溶液,于70~90℃恒温回流提取3h;
步骤3)所述超声波辅助提取是按料液比1:15~1:25在滤渣中加入质量浓度为50~70%的乙醇溶液,于50~70℃、超声功率350W条件下提取0.5~1h;
步骤4)所述热水提取是按料液比1:20~1:40在滤渣中加入去离子水,于90~100℃恒温提取3h。
2.根据权利要求1所述的含竹荪提取物的滋润唇膏,其特征在于:其制备方法包括以下步骤:
1)将油质成分于80~90℃水浴加热3~5min,然后加入竹荪提取物,搅拌至混合液成稠状;
2)将蜡质成分于80~90℃水浴加热3~5min,趁热将其倒入步骤1)的稠状混合液中,搅拌5~10min至其完全融化,配成混合液;
3)将羊毛脂于80~90℃水浴加热3~10min,趁热与步骤2)所得混合液混合,搅拌混匀;
4)将步骤3)所得料液冷却至20~25℃后加入维生素E,并根据需要加入色素和香精,然后将混合料液置于真空干燥箱内,于60~70℃、200~220Pa条件下减压脱泡10~25min,再注入模具填充到包装材料中,0~4℃凝固1~2h后取出即得。
3.根据权利要求2所述的含竹荪提取物的滋润唇膏,其特征在于:步骤4)中所述色素为日落黄、高粱红素中的任意一种或两种;
所述香精为柠檬香精、草莓香精、薄荷香精中的任意一种或几种。
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