CN105532684A - Weed killer for tea garden - Google Patents

Weed killer for tea garden Download PDF

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Publication number
CN105532684A
CN105532684A CN201610021698.4A CN201610021698A CN105532684A CN 105532684 A CN105532684 A CN 105532684A CN 201610021698 A CN201610021698 A CN 201610021698A CN 105532684 A CN105532684 A CN 105532684A
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Prior art keywords
parts
weed killer
hydroxyl
killer herbicide
alpha
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王彩霞
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Yantai Is Along Grand Chemical Industry Science Co Ltd
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Yantai Is Along Grand Chemical Industry Science Co Ltd
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Priority to CN201610021698.4A priority Critical patent/CN105532684A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N45/00Biocides, pest repellants or attractants, or plant growth regulators, containing compounds having three or more carbocyclic rings condensed among themselves, at least one ring not being a six-membered ring
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/04Oxygen or sulfur attached to an aliphatic side-chain of a carbocyclic ring system
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02Amines; Quaternary ammonium compounds
    • A01N33/08Amines; Quaternary ammonium compounds containing oxygen or sulfur
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N35/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
    • A01N35/04Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing aldehyde or keto groups, or thio analogues thereof, directly attached to an aromatic ring system, e.g. acetophenone; Derivatives thereof, e.g. acetals
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/42Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing within the same carbon skeleton a carboxylic group or a thio analogue, or a derivative thereof, and a carbon atom having only two bonds to hetero atoms with at the most one bond to halogen, e.g. keto-carboxylic acids
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/44Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/24Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms
    • A01N43/26Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings
    • A01N43/28Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings with two hetero atoms in positions 1,3
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/501,3-Diazoles; Hydrogenated 1,3-diazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/10Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
    • A01N47/12Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, neither directly attached to a ring nor the nitrogen atom being a member of a heterocyclic ring

Abstract

The invention relates to pesticide, in particular to a weed killer for a tea garden. The weed killer is prepared from alpha-ketoglutaric acid, methoxyacetophenone, chloroacetaldehyde diethyl acetal, 4-aminobutyric acid, 3-methoxy-1,3,5(10)-trien-17-ketone and the like. The weed killer for the tea garden is environmentally friendly, does not damage the environment, and is high in weeding efficiency, complete in weeding varieties and low in cost, the preparation method is simple, more importantly, tea trees are not damaged, much labor force is saved for a fruit farmer, and the weed killer is suitable for being widely applied and popularized in the field of weed killers.

Description

A kind of tea place weed killer herbicide
Technical field
The present invention relates to a kind of agricultural chemicals, be specifically related to a kind of tea place weed killer herbicide.
Background technology
Tea tree, Theaceae, Camellia shrub or dungarunga, spray is without hair.Leaf keratin, Long Circle or ellipse.The leaf of tea tree can tea making, and seed can extract oil, and tea tree material is fine and closely woven, and its wood can be used for engraving.Distribution mainly concentrates between 16 degree, south latitude to north latitude 30 degree, and tea tree likes warm and moist weather, and during mean temperature of air more than 10 DEG C, bud starts to sprout, and growth optimum temperature is 20 ~ 25 DEG C; Annual precipitation will more than 1000 millimeters; The resistance to the moon of happiness light, is suitable for giving birth under diffused light; All one's life is divided into Seedling Stage, brephic, manhood and declining period.The age of tree can reach 100 or two hundred years, but economic age is generally 40 ~ 50 years.Southwestern China portion is the centre of origin of tea tree, has 60 countries to introduce a fine variety tea tree at present in the world.Also have arbor type tea tree in torrid areas up to 15-30 rice, base portion tree encloses more than 1.5 meters, and the age of tree can reach centuries to more than one thousand years.
Tealeaves is divided into six large kinds: green tea, black tea, black tea, Oolong tea, yellow tea, white tea.Often have tea useful physical and mental health, different tealeaves has different effects: green tea has the effects such as anti-ageing, reducing blood lipid, preventing arteriosclerosis, reduction angiocardiopathy; Black tea can help gastro-intestinal digestion, it is greasy to deoil, appetizing mouth, help to foster raw etc.; Black tea has lipopenicillinase, fat-reducing, softening effect such as human vas, angiocardiopathy preventing; Oolong tea has the effect such as skin makeup, opposing aging, weight reducing, anti-decayed tooth.
Tea tree is in planting process, and weeds are a great problems of puzzlement orchard worker.Weed in tea garden kind is many, and use weed killer herbicide to remove weeds thoroughly, efficiency is low, and cost is higher; Use and manually pull out, can not work the mischief to environment, but efficiency is too low.In order to meet the demand of large quantities of tea grower grower, be necessary to develop a kind of tea place weed killer herbicide.
Summary of the invention
The object of the invention is to solve removal weeds that above-mentioned prior art exists not thoroughly, efficiency is low, have the problems such as pollution to environment, provide a kind of and remove that weeds efficiency is high, environmental protection and tea place weed killer herbicide with low cost.
A kind of tea place weed killer herbicide, special character is to be prepared from by the raw material of following weight: alpha-KG 18-24 part, o-methoxyacetophenone 30-36 part, chloroacetal 27-31 part, 4-Aminobutanoicacid 41-45 part, 3-methoxyl group-1, 3, 5 (10)-female steroid triolefin-17-ketone 6-12 parts, 1-methylcyclopropanemethanol 13-19 part, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid 21-27 part, 1-(2-chloroethyl)-2-imidazolone 32-38 part, 1-amino-2-methyl propane-2-mercaptan 14-18 part.
Preferably, the tea place weed killer herbicide adopting the raw material of following weight to prepare has better herbicidal effect: alpha-KG 21 parts, o-methoxyacetophenone 30 parts, chloroacetal 31 parts, 4-Aminobutanoicacid 43 parts, 3-methoxyl group-1,3,5 (10)-female steroid triolefin-17-ketone 6 parts, 1-methylcyclopropanemethanol 19 parts, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid 24 parts, 1-(2-chloroethyl)-2-imidazolone 32 parts, 18 parts, 1-amino-2-methyl propane-2-mercaptan.
Further, in order to obtain herbicidal effect better tea place weed killer herbicide, described tea place weed killer herbicide also comprises the raw material of following weight: (2-carbamyl oxygen ethyl) trimethyl ammonium chloride 3-11 part, 4-Amino-3-phenylbutyric acid hydrochloride 48-56 part, 6-methyl-17 alpha-monohydric pregnant-4,6-diene-3,20-diketone acetate 34-40 part.
Preferably, tea place weed killer herbicide, its parts by weight of raw materials proportioning is: (2-carbamyl oxygen ethyl) trimethyl ammonium chloride 7 parts, 4-Amino-3-phenylbutyric acid hydrochloride 48 parts, 6-methyl-17 alpha-monohydric pregnant-4,6-diene-3,20-diketone acetate 40 parts.
Preparation method of the present invention: add pure water, adds alpha-KG, o-methoxyacetophenone, chloroacetal while stirring, continues to be stirred to be uniformly dispersed, and is then heated to 60-80 DEG C; Slowly add 4-Aminobutanoicacid, 3-methoxyl group-1,3,5 (10)-female steroid triolefin-17-ketone, 1-methylcyclopropanemethanol, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid, stir and make it to dissolve; After add 1-(2-chloroethyl)-2-imidazolone, 1-amino-2-methyl propane-2-mercaptan successively, stir; Be cooled to 20-30 DEG C, stir and leave standstill 30-45 minute, namely obtain required tea place weed killer herbicide.
This tea place weed killer herbicide, environmental protection, is safe from harm to environment, removal weeds efficiency is high and removal kind is complete, and with low cost, preparation method is simple, the most important thing is not damage tea tree, for orchard worker economizes too much force, be adapted at wide popularization and application in weed killer herbicide field.
Embodiment
Below provide the specific embodiment of the present invention, be used for being further described the present invention.In the present invention, if no special instructions, each raw material all in working substance content for 100%.
In following examples, raw material introduction:
Alpha-KG, CAS accession number is: 328-50-7;
O-methoxyacetophenone, CAS accession number is: 579-74-8;
Chloroacetal, CAS accession number is: 621-62-5;
4-Aminobutanoicacid, CAS accession number is: 56-12-2;
3-methoxyl group-1,3,5 (10)-female steroid triolefin-17-ketone, CAS accession number is: 1624-62-0;
1-methylcyclopropanemethanol, CAS accession number is: 2746-14-7;
7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid, CAS accession number is: 363-24-6;
1-(2-chloroethyl)-2-imidazolone, CAS accession number is: 2387-20-4;
1-amino-2-methyl propane-2-mercaptan, CAS accession number is: 32047-53-3;
(2-carbamyl oxygen ethyl) trimethyl ammonium chloride, CAS accession number is: 51-83-2;
4-Amino-3-phenylbutyric acid hydrochloride, CAS accession number is: 1078-21-3;
6-methyl-17 alpha-monohydric pregnant-4,6-diene-3,20-diketone acetate, CAS accession number is: 595-33-5.
Embodiment 1
Weigh the raw material of following weight: alpha-KG 18g, o-methoxyacetophenone 36g, chloroacetal 29g, 4-Aminobutanoicacid 41g, 3-methoxyl group-1,3,5 (10)-female steroid triolefin-17-ketone 12g, 1-methylcyclopropanemethanol 16g, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid 21g, 1-(2-chloroethyl)-2-imidazolone 38g, 1-amino-2-methyl propane-2-mercaptan 16g.
The preparation method of the present embodiment tea place weed killer herbicide: add pure water, adds alpha-KG, o-methoxyacetophenone, chloroacetal while stirring, continues to be stirred to be uniformly dispersed, and is then heated to 60-80 DEG C; Slowly add 4-Aminobutanoicacid, 3-methoxyl group-1,3,5 (10)-female steroid triolefin-17-ketone, 1-methylcyclopropanemethanol, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid, stir and make it to dissolve; After add 1-(2-chloroethyl)-2-imidazolone, 1-amino-2-methyl propane-2-mercaptan successively, stir; Be cooled to 20-30 DEG C, stir and leave standstill 30-45 minute, namely obtain required tea place weed killer herbicide.
Embodiment 2
Weigh the raw material of following weight: alpha-KG 21g, o-methoxyacetophenone 30g, chloroacetal 31g, 4-Aminobutanoicacid 43g, 3-methoxyl group-1,3,5 (10)-female steroid triolefin-17-ketone 6g, 1-methylcyclopropanemethanol 19g, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid 24g, 1-(2-chloroethyl)-2-imidazolone 32g, 1-amino-2-methyl propane-2-mercaptan 18g.
The preparation method of the present embodiment tea place weed killer herbicide is with embodiment 1.
Embodiment 3
Weigh the raw material of following weight: alpha-KG 24g, o-methoxyacetophenone 33g, chloroacetal 27g, 4-Aminobutanoicacid 45g, 3-methoxyl group-1,3,5 (10)-female steroid triolefin-17-ketone 9g, 1-methylcyclopropanemethanol 13g, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid 27g, 1-(2-chloroethyl)-2-imidazolone 35g, 1-amino-2-methyl propane-2-mercaptan 14g.
The preparation method of the present embodiment tea place weed killer herbicide is with embodiment 1.
Embodiment 4
Weigh the raw material of following weight: alpha-KG 21g, o-methoxyacetophenone 30g, chloroacetal 31g, 4-Aminobutanoicacid 43g, 3-methoxyl group-1, 3, 5 (10)-female steroid triolefin-17-ketone 6g, 1-methylcyclopropanemethanol 19g, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid 24g, 1-(2-chloroethyl)-2-imidazolone 32g, 1-amino-2-methyl propane-2-mercaptan 18g, (2-carbamyl oxygen ethyl) trimethyl ammonium chloride 3g, 4-Amino-3-phenylbutyric acid hydrochloride 56g, 6-methyl-17 alpha-monohydric pregnant-4, 6-diene-3, 20-diketone acetate 37g.
The preparation method of the present embodiment tea place weed killer herbicide: add pure water, adds alpha-KG, o-methoxyacetophenone, chloroacetal while stirring, continues to be stirred to be uniformly dispersed, and is then heated to 60-80 DEG C; Slowly add 4-Aminobutanoicacid, 3-methoxyl group-1,3,5 (10)-female steroid triolefin-17-ketone, 1-methylcyclopropanemethanol, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid, stir and make it to dissolve; After add 1-(2-chloroethyl)-2-imidazolone, 1-amino-2-methyl propane-2-mercaptan, (2-carbamyl oxygen ethyl) trimethyl ammonium chloride, 4-Amino-3-phenylbutyric acid hydrochloride, 6-methyl-17 alpha-monohydric pregnant-4 successively, 6-diene-3,20-diketone acetate, stirs; Be cooled to 20-30 DEG C, stir and leave standstill 30-45 minute, namely obtain required tea place weed killer herbicide.
Embodiment 5
Weigh the raw material of following weight: alpha-KG 21g, o-methoxyacetophenone 30g, chloroacetal 31g, 4-Aminobutanoicacid 43g, 3-methoxyl group-1, 3, 5 (10)-female steroid triolefin-17-ketone 6g, 1-methylcyclopropanemethanol 19g, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid 24g, 1-(2-chloroethyl)-2-imidazolone 32g, 1-amino-2-methyl propane-2-mercaptan 18g, (2-carbamyl oxygen ethyl) trimethyl ammonium chloride 7g, 4-Amino-3-phenylbutyric acid hydrochloride 48g, 6-methyl-17 alpha-monohydric pregnant-4, 6-diene-3, 20-diketone acetate 40g.
The preparation method of the present embodiment tea place weed killer herbicide is with embodiment 4.
Embodiment 6
Weigh the raw material of following weight: alpha-KG 21g, o-methoxyacetophenone 30g, chloroacetal 31g, 4-Aminobutanoicacid 43g, 3-methoxyl group-1, 3, 5 (10)-female steroid triolefin-17-ketone 6g, 1-methylcyclopropanemethanol 19g, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid 24g, 1-(2-chloroethyl)-2-imidazolone 32g, 1-amino-2-methyl propane-2-mercaptan 18g, (2-carbamyl oxygen ethyl) trimethyl ammonium chloride 11g, 4-Amino-3-phenylbutyric acid hydrochloride 52g, 6-methyl-17 alpha-monohydric pregnant-4, 6-diene-3, 20-diketone acetate 34g.
The preparation method of the present embodiment tea place weed killer herbicide is with embodiment 4.
Test case
Drug effect situation below with regard to weed killer herbicide does following test, and details is in table 1.Illustrate: use weed killer herbicide 60 days " Invest, Then Investigate "s, drug effect is with 0-100 classification, and 100 expressions are prevented and kill off or death completely, and 0 represents not damage; Blank example is not for use weed killer herbicide.
Table 1: the drug effect situation of tea place weed killer herbicide
Can find out from upper table, weed killer herbicide is used to significantly improve the efficiency removing weeds, and this weed killer herbicide does not injure tea tree, wherein the removal efficiency of embodiment 5 is the highest, reaches 98.2 to the clearance of lady's-grass, 96.6 are reached to the clearance of knotweed, 98.8 are reached to the clearance of lamb's-quarters, 98.9 are reached to the clearance of cogongrass, 99.7 are reached to the clearance of Bermuda grass, 98.8 are reached to the clearance of ditch millet, 99.5 are reached to the clearance of the rhizome of nutgrass flatsedge.This tea place weed killer herbicide, the efficiency removing weeds is high, is suitable for wide popularization and application in weed killer herbicide field.

Claims (4)

1. a tea place weed killer herbicide, it is characterized in that being prepared from by the raw material of following weight: alpha-KG 18-24 part, o-methoxyacetophenone 30-36 part, chloroacetal 27-31 part, 4-Aminobutanoicacid 41-45 part, 3-methoxyl group-1, 3, 5 (10)-female steroid triolefin-17-ketone 6-12 parts, 1-methylcyclopropanemethanol 13-19 part, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid 21-27 part, 1-(2-chloroethyl)-2-imidazolone 32-38 part, 1-amino-2-methyl propane-2-mercaptan 14-18 part.
2. tea place weed killer herbicide as claimed in claim 1, it is characterized in that parts by weight of raw materials proportioning is: alpha-KG 21 parts, o-methoxyacetophenone 30 parts, chloroacetal 31 parts, 4-Aminobutanoicacid 43 parts, 3-methoxyl group-1,3,5 (10)-female steroid triolefin-17-ketone 6 parts, 1-methylcyclopropanemethanol 19 parts, 7-[3-hydroxyl-2-(3-hydroxyl-1-octenyl)-5-oxocyclopentyl]-5-heptenoic acid 24 parts, 1-(2-chloroethyl)-2-imidazolone 32 parts, 18 parts, 1-amino-2-methyl propane-2-mercaptan.
3. tea place weed killer herbicide as claimed in claim 1 or 2, characterized by further comprising the raw material of following weight: (2-carbamyl oxygen ethyl) trimethyl ammonium chloride 3-11 part, 4-Amino-3-phenylbutyric acid hydrochloride 48-56 part, 6-methyl-17 alpha-monohydric pregnant-4,6-diene-3,20-diketone acetate 34-40 part.
4. tea place weed killer herbicide as claimed in claim 3, it is characterized in that parts by weight of raw materials proportioning is: (2-carbamyl oxygen ethyl) trimethyl ammonium chloride 7 parts, 4-Amino-3-phenylbutyric acid hydrochloride 48 parts, 6-methyl-17 alpha-monohydric pregnant-4,6-diene-3,20-diketone acetate 40 parts.
CN201610021698.4A 2016-01-14 2016-01-14 Weed killer for tea garden Pending CN105532684A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105424857A (en) * 2015-12-01 2016-03-23 浙江汇能生物股份有限公司 High performance liquid chromatography analysis method for dimethyl cysteamine hydrochloride
CN107568252A (en) * 2017-10-11 2018-01-12 三江县稻香山茶油生态发展有限公司 A kind of herbicide in tea oil tree seedling seedbed and preparation method thereof
WO2019061508A1 (en) * 2017-09-30 2019-04-04 张旭东 Spring tea herbicide and preparation method therefor

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003094618A1 (en) * 2002-05-13 2003-11-20 Ceres Environmental Solution Industry Incorporated Urea based natural herbicide compositions
WO2005087691A1 (en) * 2004-03-04 2005-09-22 Yamashita Thomas T Methods for treating a plant exposed to a phytotoxicant
US20070249699A1 (en) * 2003-01-09 2007-10-25 Coleman Robert D Pesticide compositions and methods for their use
WO2010022251A2 (en) * 2008-08-22 2010-02-25 Plant Health Care, Inc. Gaba/pesticidal combinations

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003094618A1 (en) * 2002-05-13 2003-11-20 Ceres Environmental Solution Industry Incorporated Urea based natural herbicide compositions
US20070249699A1 (en) * 2003-01-09 2007-10-25 Coleman Robert D Pesticide compositions and methods for their use
WO2005087691A1 (en) * 2004-03-04 2005-09-22 Yamashita Thomas T Methods for treating a plant exposed to a phytotoxicant
WO2010022251A2 (en) * 2008-08-22 2010-02-25 Plant Health Care, Inc. Gaba/pesticidal combinations

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
刘长令: "咪唑啉酮类除草剂的创制经纬", 《农药》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105424857A (en) * 2015-12-01 2016-03-23 浙江汇能生物股份有限公司 High performance liquid chromatography analysis method for dimethyl cysteamine hydrochloride
WO2019061508A1 (en) * 2017-09-30 2019-04-04 张旭东 Spring tea herbicide and preparation method therefor
CN107568252A (en) * 2017-10-11 2018-01-12 三江县稻香山茶油生态发展有限公司 A kind of herbicide in tea oil tree seedling seedbed and preparation method thereof

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