CN105498325A - Back-flush type filtering kettle for needle tar production - Google Patents

Back-flush type filtering kettle for needle tar production Download PDF

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Publication number
CN105498325A
CN105498325A CN201610017561.1A CN201610017561A CN105498325A CN 105498325 A CN105498325 A CN 105498325A CN 201610017561 A CN201610017561 A CN 201610017561A CN 105498325 A CN105498325 A CN 105498325A
Authority
CN
China
Prior art keywords
tar
kettle
needle
filter screen
still
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610017561.1A
Other languages
Chinese (zh)
Inventor
徐大鹏
冯英
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guang Xihong Reaches Bioenergy Science And Technology Ltd
Original Assignee
Guang Xihong Reaches Bioenergy Science And Technology Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guang Xihong Reaches Bioenergy Science And Technology Ltd filed Critical Guang Xihong Reaches Bioenergy Science And Technology Ltd
Priority to CN201610017561.1A priority Critical patent/CN105498325A/en
Publication of CN105498325A publication Critical patent/CN105498325A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/01Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/62Regenerating the filter material in the filter
    • B01D29/66Regenerating the filter material in the filter by flushing, e.g. counter-current air-bumps
    • B01D29/68Regenerating the filter material in the filter by flushing, e.g. counter-current air-bumps with backwash arms, shoes or nozzles
    • B01D29/688Regenerating the filter material in the filter by flushing, e.g. counter-current air-bumps with backwash arms, shoes or nozzles with backwash arms or shoes acting on the cake side
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/62Regenerating the filter material in the filter
    • B01D29/70Regenerating the filter material in the filter by forces created by movement of the filter element
    • B01D29/72Regenerating the filter material in the filter by forces created by movement of the filter element involving vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/76Handling the filter cake in the filter for purposes other than for regenerating
    • B01D29/86Retarding cake deposition on the filter during the filtration period, e.g. using stirrers
    • B01D29/865Retarding cake deposition on the filter during the filtration period, e.g. using stirrers by vibration of the liquid
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G31/00Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for
    • C10G31/09Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for by filtration
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10Feedstock materials
    • C10G2300/1037Hydrocarbon fractions

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Working-Up Tar And Pitch (AREA)

Abstract

The invention belongs to the field of needle tar deep processing and particularly relates to a back-flush type filtering kettle for needle tar production. A tar inlet (2) of the filtering kettle is formed in the top of a kettle body (1), a filter residue outlet (5) is formed in the middle of the kettle body (1), a needle tar outlet (11) is formed in the bottom of the kettle body (1), the tar inlet (2) of the filtering kettle extends into the kettle body (1) and is structured into a spray type tar distributor (4), a connection buckle A (7-1) and a connection buckle B (7-2) are arranged at the positions, in the middle, of the inner wall of the kettle body (1) and used for being connected with a flushing cover (6) which can be placed therein through the filter residue outlet (5), a filter screen (9) is arranged below the filter residue outlet (5) inside the kettle body (1), ultrasonic modules (8) are arranged above and below the filter screen (9), and a washing inlet A (10-1) and a washing inlet B (10-2) are formed in the two sides of the needle tar outlet (11). According to the back-flush type filtering kettle, petroleum resources are utilized sufficiently, the problem that the filter screen is difficult to maintain is solved, the service life of the filter screen is prolonged, and the excellent filtering effect is achieved.

Description

The Tar production of back flush type needle-like is with filtering still
Technical field
The invention belongs to needle coke field of deep, be specifically related to a kind of back flush type needle-like Tar production and filter still.
Background technology
Needle coke is the fine quality greatly developed in carbon material, its outward appearance is silver gray, has the porosu solid of metallic luster, its structure has the texture that obviously flows, hole greatly and less and slightly ovalize, particle has larger length-width ratio, move towards just like the texture of threadiness or needle-like, that touches has lubrication sense, is the raw material producing the high-end carbon products such as ultra-high power graphite electrode, extraordinary carbon material, Carbon fiber and carbon fiber composites.According to the difference of raw materials for production, needle coke can be divided into oil system needle coke and coal-based needle coke two kinds.The output of current electric steel and refining furnace steel is in ascendant trend year by year, very considerable to the demand of high power and ultra high power graphite electrode, also more and more higher to the requirement of needle-shape coke raw material.
Needle coke process units comprises three unit: pretreatment of raw material, coking, calcining.Pretreatment of raw material is mainly removed coal tar, coal tar pitch or is returned the objectionable impurities such as the quinoline insolubles (QI) of joining in the raw materials such as pitch, and the method that pretreatment of raw material often adopts has: solvent treatment method, filtration method, centrifugal separation, hydrogenation method, upgrading method, solvent-hydrogenation method.Wherein filtration method gets quinoline insolubles by after coal tar or coal tar asphalt heating through filtering, and obtain product purification pitch, belong to simple physical method, its advantage is that technics comparing is simple, and technological parameter easily controls.Filter the material processing unit nucleus equipment of still as filtration method, direct motion and the long-term operation problem directly affecting material processing unit whether rational in infrastructure of its equipment.The structure also existing defects of current filtration still: single using filter screen as filter medium time, owing to limiting by considering netting index object, be difficult to the objectionable impurities such as quinoline insolubles in raw material to eliminate; During with filter screen and filter aid for filter medium, there is again the reduction of service life due to filtration material layer unbalance stress and affect the problem of purification of raw materials effect, and filter screen in use, due to the impact of granule foreign, easily cause filter net jam not smooth, filter efficiency is low, and filter screen is difficult to maintenance and the problem such as service life is short.
Summary of the invention
The present invention is directed to needle coke filter plant and be difficult to present situations such as being eliminated by the objectionable impurities such as quinoline insolubles in raw material, filter screen is difficult to maintenance, service life is short, there is provided a kind of back flush type needle-like Tar production to filter still, solve filter screen and be difficult to the problems such as maintenance, filter screen service life short, poor filtration effect.
The solution of the present invention is by realizing like this: still is filtered in a kind of back flush type needle-like Tar production, this filtration still comprises kettle 1, tar entrance 2, sludge outlet 5, needle coke oil export 11, tar entrance 2 is positioned at the top of kettle 1, sludge outlet 5 is positioned at the middle part of kettle 1, needle coke oil export 11 is positioned at the bottom of kettle 1, it is spray-type tar distributor 4 that the tar entrance 2 of this filtration still stretches into kettle 1 inner structure, inwall in the middle part of kettle 1 is provided with junction button A7-1 and junction button B7-2, junction button A7-1 and junction button B7-2 are for being connected the flushing cover 6 can inserted from sludge outlet 5, in kettle 1, the below of sludge outlet 5 is provided with filter screen 9, the upper-lower position of filter screen 9 is provided with ultrasonic module 8, washings import A10-1 and washings import B10-2 is provided with in needle coke oil export 11 both sides.
As further restriction of the present invention, the quantity of described ultrasonic module 8 is 1 ~ 4.The power bracket of ultrasonic module is 100 ~ 250Hz.
As further restriction of the present invention, described junction button A7-1 and junction button B7-2 is notch, inserts when rinsing cover 6 and firmly can block to pressing down, and when taking out flushing cover 6, left and right twisting can be deviate from.
As further restriction of the present invention, described tar entrance 2 is positioned at kettle 1 outside and is provided with tar inlet valve 3; Described washings import A10-1 and washings import B10-2 is provided with valve.
The technical basis that the present invention realizes and good result are: when filtration still is in filter process, filter screen be subject to granular substance blocking or colloid blocking more serious time, ultrasonic module 8 can be started, under the effect of ultrasonic vibration, slurry oil blocking on filter screen is eased, make filtration still improve the filter efficiency of needle coke, the filtration time of 1 ton of slurry oil, by 18 original ~ 22h, is reduced to 12 ~ 16h simultaneously, when filtering still and needing maintenance in the later stage, from the flushing cover 6 that sludge outlet 5 is inserted, close needle coke oil export 11, after forming hermetically-sealed construction, open washings import A10-1 and washings import B10-2 valve pours cleaning solution, start ultrasonic module to clean filter screen, clear complete after closedown washings import A10-1 and washings import B10-2 valve, waste liquid is exported suction filtration from flushing cover 6 go out, open washings import A10-1 again and washings import B10-2 valve gas injection makes filter screen rapid draing, backwash completes, take out and rinse cover 6, filter still to continue to come into operation.The service life that the present invention filters still filter screen can reach 9 ~ 12 months, and traditional filter screen service life is 3 ~ 6 months.The clearance of apparatus of the present invention quinoline insolubles (QI) reaches more than 98.5%.
figure of description
Fig. 1. the Tar production of back flush type needle-like is with filtering still.Identify in figure: 1: kettle, 2: tar entrance, 3: tar inlet valve, 4: spray-type tar distributor, 5: sludge outlet, 6: rinse cover, 7-1: junction button A, 7-2: junction button B, 8: ultrasonic module, 9: filter screen, 10-1: washings import A, 10-2: washings import B, 11: needle coke oil export.
Detailed description of the invention
Describe back flush type needle-like Tar production of the present invention below in conjunction with embodiment and accompanying drawing and filter still, these descriptions are not be further limited content of the present invention.
Embodiment 1
As shown in Figure 1, the Tar production of back flush type needle-like is with filtering still, this filtration still comprises kettle 1, tar entrance 2, sludge outlet 5, needle coke oil export 11, tar entrance 2 is positioned at the top of kettle 1, sludge outlet 5 is positioned at the middle part of kettle 1, needle coke oil export 11 is positioned at the bottom of kettle 1, it is spray-type tar distributor 4 that the tar entrance 2 of this filtration still stretches into kettle 1 inner structure, inwall in the middle part of kettle 1 is provided with junction button A7-1 and junction button B7-2, junction button A7-1 and junction button B7-2 are for being connected the flushing cover 6 can inserted from sludge outlet 5, in kettle 1, the below of sludge outlet 5 is provided with filter screen 9, the upper-lower position of filter screen 9 is provided with ultrasonic module 8, washings import A10-1 and washings import B10-2 is provided with in needle coke oil export 11 both sides.The quantity of described ultrasonic module 8 is 4.The power bracket of ultrasonic module is 100 ~ 250Hz.Described junction button A7-1 and junction button B7-2 is notch, inserts when rinsing cover 6 and firmly can block to pressing down, and when taking out flushing cover 6, left and right twisting can be deviate from.Described tar entrance 2 is positioned at kettle 1 outside and is provided with tar inlet valve 3; Described washings import A10-1 and washings import B10-2 is provided with valve.
Embodiment 2
The difference of the present embodiment and embodiment 1 is, the quantity of described ultrasonic module 8 is 2, and all the other structures are identical.
Embodiment 3
The difference of the present embodiment and embodiment 1 is, the quantity of described ultrasonic module 8 is 1, and all the other structures are identical.
Application Example 2
For the back flush type needle-like Tar production filtration still of embodiment 1 ~ 3, with the needle coke slurry oil residue produced after Guangxi factory of large-scale petroleum chemical oil refining refining product oil for raw material, in use procedure, open tar entrance 2, needle coke oil export 11, close sludge outlet 5, it is spray-type tar distributor 4 that tar stock enters kettle 1 inner structure from tar entrance 2, slurry oil dispersion is fallen into upper filter screen 9 by spray-type tar distributor 4, (when filter efficiency is low) now can start ultrasonic module 8 as required, and the power of ultrasonic module is between 200 ~ 250Hz.Needle coke after filtration is discharged from needle coke oil export 11.
When filtration still is in filter process, filter screen be subject to granular substance blocking or colloid blocking more serious time, can start ultrasonic module 8, the power of ultrasonic module is between 200 ~ 250Hz, and under the effect of ultrasonic vibration, the blocking of slurry oil on filter screen is eased, when filtering still and needing maintenance in the later stage, from the flushing cover 6 that sludge outlet 5 is inserted, close needle coke oil export 11, after forming hermetically-sealed construction, open washings import A10-1 and washings import B10-2 valve pours cleaning solution, start ultrasonic module to clean filter screen, the power of ultrasonic module is between 200 ~ 250Hz, clear complete after closedown washings import A10-1 and washings import B10-2 valve, waste liquid is exported suction filtration from flushing cover 6 go out, open washings import A10-1 again and washings import B10-2 valve gas injection makes filter screen rapid draing, backwash completes, take out and rinse cover 6, filter still to continue to come into operation.
The above embodiment of the present invention scheme is only can not limit the present invention to explanation of the present invention, indicate in claim that present device is formed and connected mode, and the scope of parameter of the present invention is not pointed out in above-mentioned explanation, therefore, any change in the implication suitable with claims of the present invention and scope, is all considered to be and is included in the scope of claims.

Claims (4)

1. a back flush type needle-like Tar production is with filtering still, this filtration still comprises kettle (1), tar entrance (2), sludge outlet (5), needle coke oil export (11), tar entrance (2) is positioned at the top of kettle (1), sludge outlet (5) is positioned at the middle part of kettle (1), needle coke oil export (11) is positioned at the bottom of kettle (1), it is characterized in that, it is spray-type tar distributor (4) that the tar entrance (2) of this filtration still stretches into kettle (1) inner structure, the inwall at kettle (1) middle part is provided with junction button A(7-1) and junction button B(7-2), junction button A(7-1) with junction button B(7-2) for being connected the flushing cover (6) can inserted from sludge outlet (5), the below of kettle (1) interior sludge outlet (5) is provided with filter screen (9), the upper-lower position of filter screen (9) is provided with ultrasonic module (8), washings import A(10-1 is provided with in needle coke oil export (11) both sides) and washings import B(10-2).
2. still is filtered in back flush type needle-like Tar production according to claim 1, and it is characterized in that, the quantity of described ultrasonic module (8) is 1 ~ 4.
3. still is filtered in back flush type needle-like Tar production according to claim 1, it is characterized in that, described junction button A(7-1) and junction button B(7-2) be notch, insert when rinsing cover (6) and firmly can block to pressing down, when taking out flushing cover (6), left and right twisting can be deviate from.
4. still is filtered in back flush type needle-like Tar production according to claim 1, and it is characterized in that, described tar entrance (2) is positioned at kettle (1) outside and is provided with tar inlet valve (3); Described washings import A(10-1) and washings import B(10-2) be provided with valve.
CN201610017561.1A 2016-01-12 2016-01-12 Back-flush type filtering kettle for needle tar production Pending CN105498325A (en)

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CN201610017561.1A CN105498325A (en) 2016-01-12 2016-01-12 Back-flush type filtering kettle for needle tar production

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Application Number Priority Date Filing Date Title
CN201610017561.1A CN105498325A (en) 2016-01-12 2016-01-12 Back-flush type filtering kettle for needle tar production

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Publication Number Publication Date
CN105498325A true CN105498325A (en) 2016-04-20

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111534325A (en) * 2020-05-11 2020-08-14 中国石油化工股份有限公司 Enhanced residual oil hydrogenation equipment, method and system
CN112044139A (en) * 2020-09-18 2020-12-08 安徽高博过滤科技有限公司 Filter for separating residual oil in cutting fluid and filtering method thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2328409Y (en) * 1998-03-04 1999-07-14 华南理工大学 Supersonic filter net cleaning device
CN101619233A (en) * 2009-07-28 2010-01-06 江汉大学 Method for filtering and removing catalyst powder in catalytic cracking oil slurry through ultrasonic irradiation
CN201551897U (en) * 2009-06-29 2010-08-18 湖南力合科技发展有限公司 Ultrasonic cleaning and filtering device
CN202778062U (en) * 2012-09-26 2013-03-13 河南龙宇煤化工有限公司 Box-type multilayer filter
CN203108297U (en) * 2013-03-15 2013-08-07 陕西煤业化工技术研究院有限责任公司 Filter kettle for needle coke production
CN204193624U (en) * 2014-09-09 2015-03-11 天津农禧源科技有限公司 Screening plant
CN204522502U (en) * 2015-01-23 2015-08-05 广西泓达生物能源科技有限公司 Cycle oil sizing device externally extracting oil filter plant

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2328409Y (en) * 1998-03-04 1999-07-14 华南理工大学 Supersonic filter net cleaning device
CN201551897U (en) * 2009-06-29 2010-08-18 湖南力合科技发展有限公司 Ultrasonic cleaning and filtering device
CN101619233A (en) * 2009-07-28 2010-01-06 江汉大学 Method for filtering and removing catalyst powder in catalytic cracking oil slurry through ultrasonic irradiation
CN202778062U (en) * 2012-09-26 2013-03-13 河南龙宇煤化工有限公司 Box-type multilayer filter
CN203108297U (en) * 2013-03-15 2013-08-07 陕西煤业化工技术研究院有限责任公司 Filter kettle for needle coke production
CN204193624U (en) * 2014-09-09 2015-03-11 天津农禧源科技有限公司 Screening plant
CN204522502U (en) * 2015-01-23 2015-08-05 广西泓达生物能源科技有限公司 Cycle oil sizing device externally extracting oil filter plant

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111534325A (en) * 2020-05-11 2020-08-14 中国石油化工股份有限公司 Enhanced residual oil hydrogenation equipment, method and system
CN112044139A (en) * 2020-09-18 2020-12-08 安徽高博过滤科技有限公司 Filter for separating residual oil in cutting fluid and filtering method thereof
CN112044139B (en) * 2020-09-18 2024-01-12 安徽高博过滤科技有限公司 Filter for separating residual oil in cutting fluid and filtering method thereof

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Application publication date: 20160420