CN105483896A - Production technology of carbon filament beating-up - Google Patents

Production technology of carbon filament beating-up Download PDF

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Publication number
CN105483896A
CN105483896A CN201510959623.6A CN201510959623A CN105483896A CN 105483896 A CN105483896 A CN 105483896A CN 201510959623 A CN201510959623 A CN 201510959623A CN 105483896 A CN105483896 A CN 105483896A
Authority
CN
China
Prior art keywords
pan
protofilaments
carbon fiber
beating
pan precursor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510959623.6A
Other languages
Chinese (zh)
Inventor
朱吉元
金力
傅建根
袁华中
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhejiang Jinggong Science and Technology Co Ltd
Original Assignee
Zhejiang Jinggong Science and Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhejiang Jinggong Science and Technology Co Ltd filed Critical Zhejiang Jinggong Science and Technology Co Ltd
Priority to CN201510959623.6A priority Critical patent/CN105483896A/en
Publication of CN105483896A publication Critical patent/CN105483896A/en
Pending legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D03WEAVING
    • D03CSHEDDING MECHANISMS; PATTERN CARDS OR CHAINS; PUNCHING OF CARDS; DESIGNING PATTERNS
    • D03C9/00Healds; Heald frames
    • D03C9/06Heald frames
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/20Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
    • D01F9/21Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D01F9/22Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/32Apparatus therefor
    • D01F9/328Apparatus therefor for manufacturing filaments from polyaddition, polycondensation, or polymerisation products
    • DTEXTILES; PAPER
    • D03WEAVING
    • D03CSHEDDING MECHANISMS; PATTERN CARDS OR CHAINS; PUNCHING OF CARDS; DESIGNING PATTERNS
    • D03C13/00Shedding mechanisms not otherwise provided for
    • DTEXTILES; PAPER
    • D03WEAVING
    • D03DWOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • DTEXTILES; PAPER
    • D03WEAVING
    • D03DWOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D49/00Details or constructional features not specially adapted for looms of a particular type

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Fibers (AREA)

Abstract

The invention relates to a production technology of carbon filament beating-up. The production technology comprises the following steps that 1, PAN protofilaments are divided into an upper layer and a lower layer, namely, the PAN protofilament layer containing singular numbers of the protofilaments and the PAN protofilament layer containing even numbers of the protofilaments according to the singular numbers and even numbers through a beating-up machine heald frame; 2, carbon fiber filaments or a weft storage mechanism with the carbon fiber filaments penetrates through openings of the upper layer and lower layer of the PAN protofilaments to make the carbon fiber filaments and the PAN protofilaments woven together; 3, the upper position and the lower position of the heald frame are exchanged, and then the positions of the upper layer PAN protofilaments and the lower layer PAN protofilaments are exchanged; 4, the carbon fiber filaments penetrate through the opening to be woven together with the PAN protofilaments. According to the production technology of carbon filament beating-up, the carbon fiber filaments and the PAN protofilaments are woven together, the problems that due to the fact that the property of the protofilaments is unstable and operation of equipment is unstable, when partial PAN protofilaments are broken, the PAN protofilaments are scattered in the equipment, or due to the fact that the manufacturing precision of the equipment is insufficient, the PAN protofilaments are overlapped, a fire or even an explosion is caused, and the carbon fiber filaments cannot operate normally are solved, the operability during filament breaking is improved, losses are reduced, and personnel safety is improved.

Description

The production technology that a kind of carbon filament beats up
Technical field
The present invention relates to the production technology that a kind of relevant carbon fiber production process, particularly PAN precursor beat up in preoxidation process.
Background technology
Carbon fiber (CarbonFibre) is fibrous material with carbon element, and in chemical composition, carbon accounts for more than 90% of gross mass.Carbon fiber and composite thereof have high specific strength, and high ratio modulus is high temperature resistant, corrosion-resistant, endurance, creep resistant, conduction, heat transfer, with a series of excellent properties such as thermal coefficient of expansion is little, they both as structural material bearing load, can play a role as functional material again.Therefore, carbon fiber and composite development in recent years very rapid.
Through development for many years, only have viscose glue (cellulose) base fiber, pitch fibers and polyacrylonitrile (PAN) fiber three kinds of raw materials to prepare carbon fiber technique at present and achieve industrialization.
And the primary necessary requirement that high-quality PAN precursor in the technique of carbon fiber is manufacture high-performance carbon fibre prepared by PAN fiber, this is the summary of many years of experience.But current, in the preparation of PAN precursor, Large Copacity is polymerized, the key technologies such as quick spinning fall behind, and cause properties of product unstable, cause uncontrollable fracture of wire, this gives the homogeneous pre-oxidation of carbon fiber, Quick Oxidation carbonization and other processes causes various problem, particularly to the preoxidation process fracture of wire of key, can cause on fire, the even irremediable loss such as blast.
Summary of the invention
For the above-mentioned technical problem of prior art, the object of this invention is to provide a kind of production technology that can reduce fracture of wire impact, the carbon filament that fracture of wire process becomes simple is beaten up.
For achieving the above object, the present invention is achieved by the following technical solutions:
The production technology that carbon filament beats up, comprises the following steps:
(1) by the machine heald frame that beats up, PAN precursor is divided into by single even numbers two-layer up and down, is respectively individual layer PAN precursor and double-deck PAN precursor;
(2) pass individual layer PAN precursor and double-deck PAN precursor opening by carbon fiber wire or with the Chu Wei mechanism of carbon fiber wire, be woven together with PAN precursor;
(3) exchange heald frame upper-lower position, thus individual layer PAN precursor and double-deck PAN precursor upper-lower position are exchanged;
(4) carbon fiber wire is passed opening, be woven together with PAN precursor;
(5) after completing steps (4), keep at a certain distance away, continue to repeat above-mentioned step of beating up (1)-(4), reach object of beating up.
Beneficial effect of the present invention is as follows:
The production technology that carbon filament of the present invention beats up, carbon fiber wire and PAN precursor are woven together, solve because of reasons such as precursor unstable properties and equipment fluctuations of service, when causing part PAN precursor fracture of wire, PAN precursor is scattered in equipment or device fabrication precision causes PAN precursor overlapping not, causes on fire, even blast waits the problem that carbon fiber line can not normally run, improve operability during fracture of wire, reduce loss, improve personnel safety.
Accompanying drawing explanation
Fig. 1 is the schematic diagram of embodiment 1;
Fig. 2 is the schematic diagram of embodiment 2;
Wherein, 1 be single double-deck PAN precursor, 2 be carbon fiber wire, 3 be PAN precursor.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further illustrated, but protection scope of the present invention is not limited to this.
embodiment 1
As shown in Figure 1, the carbon fiber of the present embodiment 1 production technology of beating up comprises the following steps:
(1) by the machine heald frame that beats up (similar loom), PAN precursor 3 is divided into two-layer up and down by single even numbers;
(2) by carbon fiber wire 2, through two-layer PAN precursor opening, be woven together with PAN precursor;
(3) exchange heald frame upper-lower position, thus single double-deck PAN precursor 1 upper-lower position is exchanged;
(4) carbon fiber wire 3 is passed opening, be woven together with single double-deck PAN precursor 1;
(5) after completing steps (4), keep at a certain distance away, continue to repeat above-mentioned step of beating up (1)-(4), reach object of beating up.
embodiment 2
As shown in Figure 2, the carbon fiber of the present embodiment 2 production technology of beating up comprises the following steps:
(1) by the machine heald frame that beats up (similar loom), PAN precursor 1 is divided into two-layer up and down by single even numbers;
(2) by the Chu Wei mechanism with carbon fiber wire 2, through two-layer PAN precursor opening, be woven together with PAN precursor 1;
(3) exchange heald frame upper-lower position, thus single double-deck PAN precursor 1 upper-lower position is exchanged;
(4) carbon fiber wire 2 is continued across opening, be woven together (phantom line segments) with PAN precursor 1;
(5) after completing steps (4), keep at a certain distance away, continue to repeat above-mentioned step of beating up (1)-(4), reach object of beating up.
Above-described embodiment only illustrates inventive concept of the present invention for explaining, but not the restriction to rights protection of the present invention, all changes utilizing this design the present invention to be carried out to unsubstantiality, all should fall into protection scope of the present invention.

Claims (1)

1. a carbon filament production technology of beating up, is characterized in that comprising the following steps:
(1) by the machine heald frame that beats up, being divided into two-layer up and down by PAN precursor by single even numbers, is single double-deck PAN precursor;
(2) pass single double-deck PAN precursor opening by carbon fiber wire or with the Chu Wei mechanism of carbon fiber wire, be woven together with PAN precursor;
(3) exchange heald frame upper-lower position, thus single double-deck PAN precursor upper-lower position is exchanged;
(4) carbon fiber wire is passed opening, be woven together with PAN precursor;
(5) after completing steps (4), keep at a certain distance away, continue to repeat above-mentioned step of beating up (1)-(4), reach object of beating up.
CN201510959623.6A 2015-12-21 2015-12-21 Production technology of carbon filament beating-up Pending CN105483896A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510959623.6A CN105483896A (en) 2015-12-21 2015-12-21 Production technology of carbon filament beating-up

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510959623.6A CN105483896A (en) 2015-12-21 2015-12-21 Production technology of carbon filament beating-up

Publications (1)

Publication Number Publication Date
CN105483896A true CN105483896A (en) 2016-04-13

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510959623.6A Pending CN105483896A (en) 2015-12-21 2015-12-21 Production technology of carbon filament beating-up

Country Status (1)

Country Link
CN (1) CN105483896A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106192080A (en) * 2016-07-22 2016-12-07 中国石油大学(北京) A kind of method improving carbon fiber yield rate
CN110128160A (en) * 2019-04-22 2019-08-16 湖南东映碳材料科技有限公司 A method of highly-conductive hot carbon carbon composite is prepared with the two-dimension netted object of pitch fibers precursor

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5175150A (en) * 1974-12-26 1976-06-29 Toray Industries Tansosenino renzokushijokaranaru senisokumatahaobijobutsu oyobi sonoseiho
US4173990A (en) * 1978-03-13 1979-11-13 Hitco Temporary fabric and method and apparatus for weaving same
US4497098A (en) * 1982-09-07 1985-02-05 Hitco Fill yarn removal apparatus
CN2057177U (en) * 1989-05-04 1990-05-16 中国科学院山西煤炭化学研究所 Device for producing pre-oxidation fibre
CN101161880A (en) * 2007-11-22 2008-04-16 吉林奇峰化纤股份有限公司 Method for preparing polyacrylonitrile-based carbon fiber precursor fiber
CN103562454A (en) * 2011-05-27 2014-02-05 三菱丽阳株式会社 Loom and weaving method using said loom

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5175150A (en) * 1974-12-26 1976-06-29 Toray Industries Tansosenino renzokushijokaranaru senisokumatahaobijobutsu oyobi sonoseiho
US4173990A (en) * 1978-03-13 1979-11-13 Hitco Temporary fabric and method and apparatus for weaving same
US4497098A (en) * 1982-09-07 1985-02-05 Hitco Fill yarn removal apparatus
CN2057177U (en) * 1989-05-04 1990-05-16 中国科学院山西煤炭化学研究所 Device for producing pre-oxidation fibre
CN101161880A (en) * 2007-11-22 2008-04-16 吉林奇峰化纤股份有限公司 Method for preparing polyacrylonitrile-based carbon fiber precursor fiber
CN103562454A (en) * 2011-05-27 2014-02-05 三菱丽阳株式会社 Loom and weaving method using said loom

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106192080A (en) * 2016-07-22 2016-12-07 中国石油大学(北京) A kind of method improving carbon fiber yield rate
CN110128160A (en) * 2019-04-22 2019-08-16 湖南东映碳材料科技有限公司 A method of highly-conductive hot carbon carbon composite is prepared with the two-dimension netted object of pitch fibers precursor
CN110128160B (en) * 2019-04-22 2021-05-11 湖南东映碳材料科技有限公司 Method for preparing high-thermal-conductivity carbon-carbon composite material from two-dimensional network of pitch fiber precursors

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Application publication date: 20160413