CN105463888A - Dye formaldehyde-free fixing agent composition - Google Patents
Dye formaldehyde-free fixing agent composition Download PDFInfo
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- CN105463888A CN105463888A CN201510879898.9A CN201510879898A CN105463888A CN 105463888 A CN105463888 A CN 105463888A CN 201510879898 A CN201510879898 A CN 201510879898A CN 105463888 A CN105463888 A CN 105463888A
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Abstract
The invention discloses a dye formaldehyde-free fixing agent composition. The dye formaldehyde-free fixing agent composition comprises polyethyleneglycol 1000, N,N-dimethyl acetamide, DMPA (di-methylol-propionic acid), ethylenediamine, DETA (diethylenetriamine) and epoxy chloropropane. Ethylenediamine and DETA react at first, then the reactant reacts with epoxy chloropropane, and polyethyleneglycol 1000 and DMPA are used together, so that the dye formaldehyde-free fixing agent composition is provided to achieve the effect of improving the color fastness of dyed fabrics.
Description
Technical field
The present invention relates to dye fixing agent technical field, espespecially a kind of dyestuff aldehyde-free colour stabilizer composition.
Background technology
After fabric is dyed, although bright fabric can be dyed, but due on some dyestuff with water soluble group, make wet colour fastness poor, fugitive color and staining, make fabric stale, also can to other fabric staining, if by after washing, soap boiling, washing after textile dyeing, the COLOR FASTNESS of fabric still can not reach requirement, then need to use color-fixing agent process, improve the COLOR FASTNESS of DYED FABRICS.Traditional color-fixing agent contains carboxymethyl, can discharge free formaldehyde, and harmful when exceeding certain value, the effect of color-fixing agent makes dyestuff form water-fast dye salt, or makes dye molecule increase and be insoluble in water, so as to improving the fastness of dyestuff.
Summary of the invention
A kind of dyestuff aldehyde-free colour stabilizer of the present invention composition, it is characterized in that: the deficiency overcoming above-mentioned technology, ethylenediamine and diethylenetriamine is adopted to react, and further with epichlorohydrin reaction, be aided with the mode of cetomacrogol 1000 and dihydromethyl propionic acid, a kind of dyestuff aldehyde-free colour stabilizer composition is provided, realizes the object improving DYED FABRICS COLOR FASTNESS.
To achieve these goals, technical solution of the present invention is: a kind of dyestuff aldehyde-free colour stabilizer composition comprises cetomacrogol 1000, N, N-dimethylacetylamide, dihydromethyl propionic acid, ethylenediamine, diethylenetriamine, epoxychloropropane, each component and parts by mass thereof are:
Cetomacrogol 1000 10 ~ 15 parts
DMA 4 ~ 6 parts
Dihydromethyl propionic acid 5 ~ 7 parts
Ethylenediamine 3 ~ 5 parts
Diethylenetriamine 4 ~ 6 parts
Epoxychloropropane 4 ~ 7 parts
Distilled water 20 ~ 25 parts
Preparation method of the present invention is: by 4 ~ 6 parts of diethylenetriamines and 4 ~ 6 parts of N, N-dimethylacetylamide adds in the four-hole bottle that condenser, thermometer, agitator are housed, add after 3 ~ 5 parts of ethylenediamines at 100 DEG C of stirring reaction 1h, be warming up to 140 DEG C and drip 4 ~ 7 parts of epoxychloropropane, after reaction 1.5h, add 20 ~ 25 parts of distilled water and 5 ~ 7 parts of dihydromethyl propionic acids and 10 ~ 15 parts of cetomacrogol 1000s, obtain dyestuff aldehyde-free colour stabilizer composition.
Advantage and disadvantage of the present invention is: adopt ethylenediamine and diethylenetriamine to react, and further with epichlorohydrin reaction, be aided with the mode of cetomacrogol 1000 and dihydromethyl propionic acid, a kind of dyestuff aldehyde-free colour stabilizer composition is provided, reach the effect improving DYED FABRICS COLOR FASTNESS.
Detailed description of the invention
Embodiment 1
A kind of dyestuff aldehyde-free colour stabilizer composition comprises cetomacrogol 1000, DMA, dihydromethyl propionic acid, ethylenediamine, diethylenetriamine, epoxychloropropane, and each component and parts by mass thereof are:
Cetomacrogol 1000 12 kilograms
DMA 5 kilograms
Dihydromethyl propionic acid 6 kilograms
Ethylenediamine 4 kilograms
Diethylenetriamine 5 kilograms
Epoxychloropropane 5.5 kilograms
Distilled water 22 kilograms
Its preparation method is: by 5 kilograms of diethylenetriamines and 5 kilograms of N, N-dimethylacetylamide adds in the four-hole bottle that condenser, thermometer, agitator are housed, add after 4 kilograms of ethylenediamines at 100 DEG C of stirring reaction 1h, be warming up to 140 DEG C and drip 5.5 kilograms of epoxychloropropane, after reaction 1.5h, add 22 kilograms of distilled water and 6 kilograms of dihydromethyl propionic acids and 12 kilograms of cetomacrogol 1000s, obtain dyestuff aldehyde-free colour stabilizer composition.
Embodiment 2
A kind of dyestuff aldehyde-free colour stabilizer composition comprises cetomacrogol 1000, DMA, dihydromethyl propionic acid, ethylenediamine, diethylenetriamine, epoxychloropropane, and each component and parts by mass thereof are:
Cetomacrogol 1000 10 kilograms
DMA 6 kilograms
Dihydromethyl propionic acid 5 kilograms
Ethylenediamine 5 kilograms
Diethylenetriamine 4 kilograms
Epoxychloropropane 7 kilograms
Distilled water 20 kilograms
Its preparation method is: by 4 kilograms of diethylenetriamines and 6 kilograms of N, N-dimethylacetylamide adds in the four-hole bottle that condenser, thermometer, agitator are housed, add after 5 kilograms of ethylenediamines at 100 DEG C of stirring reaction 1h, be warming up to 140 DEG C and drip 7 kilograms of epoxychloropropane, after reaction 1.5h, add 20 kilograms of distilled water and 5 kilograms of dihydromethyl propionic acids and 10 kilograms of cetomacrogol 1000s, obtain dyestuff aldehyde-free colour stabilizer composition.
Embodiment 3
A kind of dyestuff aldehyde-free colour stabilizer composition comprises cetomacrogol 1000, DMA, dihydromethyl propionic acid, ethylenediamine, diethylenetriamine, epoxychloropropane, and each component and parts by mass thereof are:
Cetomacrogol 1000 15 kilograms
DMA 4 kilograms
Dihydromethyl propionic acid 7 kilograms
Ethylenediamine 3 kilograms
Diethylenetriamine 6 kilograms
Epoxychloropropane 4 kilograms
Distilled water 25 kilograms
Its preparation method is: by 6 kilograms of diethylenetriamines and 4 kilograms of N, N-dimethylacetylamide adds in the four-hole bottle that condenser, thermometer, agitator are housed, add after 3 kilograms of ethylenediamines at 100 DEG C of stirring reaction 1h, be warming up to 140 DEG C and drip 4 kilograms of epoxychloropropane, after reaction 1.5h, add 25 kilograms of distilled water and 7 kilograms of dihydromethyl propionic acids and 15 kilograms of cetomacrogol 1000s, obtain dyestuff aldehyde-free colour stabilizer composition.
The above; embodiment is only be described the preferred embodiment of the present invention; not scope of the present invention is limited; under the prerequisite of spirit not departing from the technology of the present invention; the various distortion that this area engineers and technicians make technical scheme of the present invention and improvement, all should fall in protection domain that claims of the present invention determine.
Claims (1)
1. a dyestuff aldehyde-free colour stabilizer composition, it is characterized in that: described dyestuff aldehyde-free colour stabilizer composition comprises cetomacrogol 1000, N, N-dimethylacetylamide, dihydromethyl propionic acid, ethylenediamine, diethylenetriamine, epoxychloropropane, each component and parts by mass thereof are:
Cetomacrogol 1000 10 ~ 15 parts
DMA 4 ~ 6 parts
Dihydromethyl propionic acid 5 ~ 7 parts
Ethylenediamine 3 ~ 5 parts
Diethylenetriamine 4 ~ 6 parts
Epoxychloropropane 4 ~ 7 parts
Distilled water 20 ~ 25 parts;
Its preparation method is: by 4 ~ 6 parts of diethylenetriamines and 4 ~ 6 parts of N, N-dimethylacetylamide adds in the four-hole bottle that condenser, thermometer, agitator are housed, add after 3 ~ 5 parts of ethylenediamines at 100 DEG C of stirring reaction 1h, be warming up to 140 DEG C and drip 4 ~ 7 parts of epoxychloropropane, after reaction 1.5h, add 20 ~ 25 parts of distilled water and 5 ~ 7 parts of dihydromethyl propionic acids and 10 ~ 15 parts of cetomacrogol 1000s, obtain dyestuff aldehyde-free colour stabilizer composition.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510879898.9A CN105463888A (en) | 2015-12-06 | 2015-12-06 | Dye formaldehyde-free fixing agent composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510879898.9A CN105463888A (en) | 2015-12-06 | 2015-12-06 | Dye formaldehyde-free fixing agent composition |
Publications (1)
| Publication Number | Publication Date |
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| CN105463888A true CN105463888A (en) | 2016-04-06 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510879898.9A Pending CN105463888A (en) | 2015-12-06 | 2015-12-06 | Dye formaldehyde-free fixing agent composition |
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| CN (1) | CN105463888A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106541724A (en) * | 2016-12-12 | 2017-03-29 | 郑州艾莫弗信息技术有限公司 | A kind of ink-jet paper color fixing agent and preparation method thereof |
| CN106702790A (en) * | 2016-12-12 | 2017-05-24 | 刘海平 | Preparation method of novel fluorescent acidic color fixing agent and prepared color fixing agent |
| CN107524005A (en) * | 2017-07-26 | 2017-12-29 | 江苏新瑞贝科技股份有限公司 | A kind of antistatic textile auxiliary and its preparation technology |
| CN107523995A (en) * | 2017-07-26 | 2017-12-29 | 江苏新瑞贝科技股份有限公司 | A kind of textile auxiliary that graphene is applied in finishing process |
| CN108118557A (en) * | 2016-12-12 | 2018-06-05 | 郑州艾莫弗信息技术有限公司 | A kind of paper surface color fixing agent and preparation method thereof |
| CN110655825A (en) * | 2019-09-29 | 2020-01-07 | 安徽虹源医药包装有限公司 | Glazing ink and glazing process thereof |
| CN112281480A (en) * | 2020-10-30 | 2021-01-29 | 周银川 | Preparation process of textile auxiliary |
| CN116905255A (en) * | 2023-05-04 | 2023-10-20 | 江西德盛精细化学品有限公司 | Color fixing agent for fabric and preparation method thereof |
-
2015
- 2015-12-06 CN CN201510879898.9A patent/CN105463888A/en active Pending
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106541724A (en) * | 2016-12-12 | 2017-03-29 | 郑州艾莫弗信息技术有限公司 | A kind of ink-jet paper color fixing agent and preparation method thereof |
| CN106702790A (en) * | 2016-12-12 | 2017-05-24 | 刘海平 | Preparation method of novel fluorescent acidic color fixing agent and prepared color fixing agent |
| CN108118557A (en) * | 2016-12-12 | 2018-06-05 | 郑州艾莫弗信息技术有限公司 | A kind of paper surface color fixing agent and preparation method thereof |
| CN106702790B (en) * | 2016-12-12 | 2019-01-01 | 江西德盛精细化学品有限公司 | A kind of preparation method of fluorescence acidic color fixing agent and color fixing agent obtained |
| CN107524005A (en) * | 2017-07-26 | 2017-12-29 | 江苏新瑞贝科技股份有限公司 | A kind of antistatic textile auxiliary and its preparation technology |
| CN107523995A (en) * | 2017-07-26 | 2017-12-29 | 江苏新瑞贝科技股份有限公司 | A kind of textile auxiliary that graphene is applied in finishing process |
| CN110655825A (en) * | 2019-09-29 | 2020-01-07 | 安徽虹源医药包装有限公司 | Glazing ink and glazing process thereof |
| CN112281480A (en) * | 2020-10-30 | 2021-01-29 | 周银川 | Preparation process of textile auxiliary |
| CN116905255A (en) * | 2023-05-04 | 2023-10-20 | 江西德盛精细化学品有限公司 | Color fixing agent for fabric and preparation method thereof |
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Application publication date: 20160406 |
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| WD01 | Invention patent application deemed withdrawn after publication |