CN105456078A - Cortex eucommiae exfoliating abrasive particles and preparation method and application thereof - Google Patents
Cortex eucommiae exfoliating abrasive particles and preparation method and application thereof Download PDFInfo
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- CN105456078A CN105456078A CN201510360913.9A CN201510360913A CN105456078A CN 105456078 A CN105456078 A CN 105456078A CN 201510360913 A CN201510360913 A CN 201510360913A CN 105456078 A CN105456078 A CN 105456078A
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- cortex eucommiae
- exfoliation
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Abstract
The invention provides preparation and application of cortex eucommiae exfoliating abrasive particles, and belongs to the technical field of daily-use chemical industry. The cortex eucommiae exfoliating abrasive particles are prepared through the steps of processing of cortex eucommiae bark, drying and smashing. The cortex eucommiae exfoliating abrasive particles are suitable for products such as different exfoliating abrasive sanitary bath foam, skin-care health-care creams and skin-care lotions. The particles are appropriate in hardness, contain active ingredients capable of sterilizing and resisting oxidation and are prepared into clean and skin-care products with other raw materials; the effects of whitening, moistening skin, keeping moisture, beautifying the skin, softening cutin, softening and tendering the skin and the like are achieved, the skin can be smooth and compact and can be rapidly moistened, melanin pigmentation is reduced, and self recovering of the skin is facilitated.
Description
Technical field
The invention belongs to daily-use chemical industry technical field, be specifically related to a kind of preparation method of Cortex Eucommiae exfoliation abrasive particle and the application on the products such as washing, skin protection, health thereof.
Background technology
Human body skin is under normal physiological status, and meeting sebum secreted, lubricates to keep skin.In order to protect skin health and good outward appearance, need the dirt often removed on skin, sebum, other secretions, dead corneocyte etc.On current cosmetics, clean bath shampoo market, arisen at the historic moment such as frosted de-cutin shower dew, frosted facial milk cleanser, the deep layer clean frosted such as scrubbing cream, frosted facial washing milk skin protection shower consumer goods.They are mainly by some fine granularity material massaging skin, remove impurity in old cutin on skin and pore, promote regenerative cell growth, to improve pachylosis, hydropenia, stiff phenomenon, and strengthen the absorption to follow-up skin care products.Abrasive particle can be divided into natural and synthesis abrasive particle, also can be divided into organic and inorganic abrasive particle, can also vary in size be divided into soft, medium, rigid abrasive particle with hardness or grain graininess.Wherein organically abrasive particle have natural as Semen Persicae shell, almond shell, corn cob, vegetable sponge granule etc., synthesis as polyethylene (PE), Polyethylene Glycol, PVC, polystyrene, urea resin particles etc.; Inorganic abrasive particle is as the Sal granule etc. of the soda of white carbon, kieselguhr, whiting, quartz sand, perlite particle, baking and baking.But synthetic high polymer class is as polyethylene (PE) abrasive particle, there is the defect being difficult to degrade, and some is with residual hazard, directly can threaten the natural environment that the mankind such as the health of human body self and marine organisms, water source and soil depend on for existence.Therefore, natural plant raw material becomes the raw material preparing exfoliation abrasive particle is problem anxious to be resolved now.
Summary of the invention
The object of the invention is, for described defect above, to provide a kind of Cortex Eucommiae exfoliation abrasive particle being raw material with Traditional Chinese medicine eucommia bark skin.
Another object of the present invention is to provide a kind of preparation method of Cortex Eucommiae exfoliation abrasive particle.
Another object of the present invention is to provide the application of one and Cortex Eucommiae exfoliation abrasive particle.
The object of the invention is to be achieved by the following technical programs.
A kind of Cortex Eucommiae exfoliation abrasive particle, is characterized in that, adopts following steps to make successively:
(1) processing of eucommia bark: choose and become tree in age (be good with smooth bark type) at trunk overhead 10 ~ more than 20cm position for more than 10 years, adopt part layer stripping or girding method to peel off bark; The bark peeled first pours boiling water on boiling hot, and then that the inner face of skin is relative in pairs, accumulation is set level; Surrounding Caulis et Folium Oryzae is wrapped, upper cover plank, and weighting material flattens through the vexed Hair Fixer heat of 6 one 7d, when bark inner face is in mulberry, brown, can takes out, dry; Removing rough bark (phellem layer), cleans, dries the strip being cut into wide 0.3 ~ 0.5cm;
(2) dry: the Cortex Eucommiae getting the strip of chopping, put in vacuum drying oven, at vacuum-0.03 ~-0.05MPa, at temperature 80 ~ 90 DEG C, be dried to moisture≤3%;
(3) pulverize: by the strip Cortex Eucommiae of drying with compound plastic moistureproof bag parcel, sealing, put refrigerator (
<-5 DEG C) freezing processing, then take out and pulverize rapidly, be sieved into 6 kinds of varigrained Cortex Eucommiae abrasive particles: below-20 ~+30(20 mesh sieve more than 30 mesh sieves, lower with) ,-30 ~+40 ,-40 ~+60 ,-60 ~+80 ,-80 ~+100 orders, namely damp-prrof packing obtains product.
A preparation method for Cortex Eucommiae exfoliation abrasive particle, is characterized in that, adopts following steps to make successively:
(1) processing of eucommia bark: choose and become tree in age (be good with smooth bark type) at trunk overhead 10 ~ more than 20cm position for more than 10 years, adopt part layer stripping or girding method to peel off bark; The bark peeled first pours boiling water on boiling hot, and then that the inner face of skin is relative in pairs, accumulation is set level; Surrounding Caulis et Folium Oryzae is wrapped, upper cover plank, and weighting material flattens through the vexed Hair Fixer heat of 6 one 7d, when bark inner face is in mulberry, brown, can takes out, dry; Removing rough bark (phellem layer), cleans, dries the strip being cut into wide 0.3 ~ 0.5cm;
(2) dry: the Cortex Eucommiae getting the strip of chopping, put in vacuum drying oven, at vacuum-0.03 ~-0.05MPa, at temperature 80 ~ 90 DEG C, be dried to moisture≤3%;
(3) pulverize: by the strip Cortex Eucommiae of drying with compound plastic moistureproof bag parcel, sealing, put refrigerator (
<-5 DEG C) freezing processing, then take out and pulverize rapidly, be sieved into 6 kinds of varigrained Cortex Eucommiae abrasive particles: below-20 ~+30(20 mesh sieve more than 30 mesh sieves, lower with) ,-30 ~+40 ,-40 ~+60 ,-60 ~+80 ,-80 ~+100 orders, namely damp-prrof packing obtains product.
Described Cortex Eucommiae exfoliation abrasive particle is applicable in the products such as different exfoliation frosted health bath lotion, stock skin health-care paste frost, facial treatment milk.
A preparation method for Cortex Eucommiae exfoliation exfoliating shower dew, adopts following steps to make successively:
(1) formula: Cortex Eucommiae exfoliation exfoliating shower dew is made up of the raw material of following masses part:
0.7 ~ 1.0 part, thickening agent card ripple 2020 (solid)
1% high yield value suspending agent activates aqueous solution 20.0 ~ 30.0 parts
Surfactant (comprise AES, K12,6501, APG, CAB-35) 19.0 ~ 23.0 parts
Wetting agent glycerol 3.0 ~ 1.0 parts
Cortex Eucommiae exfoliation abrasive particle (varigrained 1 or 2 kind) 2.0 ~ 5.0 parts
Chelating agen stabilizing agent EDTA0.5 ~ 1.5 part
PH adjusting agent boric acid 0.05 ~ 0.15 part
Antiseptic (comprising Sodium Methyl Hydroxybenzoate, isothiazolone) 0.1 ~ 0.3 part
Essence is appropriate
Deionized water surplus;
(2) formulation operations step:
A, get 1/3 water and add formula ratio thickening agent card ripple 2020, be heated to 60 DEG C, stir;
B, under strong stirring, high yield value suspending agent is added appropriate amount of deionized water mutually in hydration, prevent agglomerate; Then adding deionized water makes it be 1% concentration, activates 5 minutes with homogenizer at 7000 ~ 12000rpm homogenizing, obtains 1% high yield value suspending agent and activates aqueous solution;
C, get above-mentioned B and A gained solution and merge, and add balance deionized water, under agitation add formula ratio surfactant, wetting agent, Cortex Eucommiae exfoliation abrasive particle, EDTA, boric acid, antiseptic, essence successively, stir, deaeration, packs and get final product.
the invention has the beneficial effects as follows:above-mentioned Cortex Eucommiae exfoliation abrasive particle, with the Cortex Eucommiae of pure natural for raw material is made, Traditional Chinese medicine eucommia bark contains a large amount of chlorogenic acid, vanillic acid, caffeic acid and protocatechuic acid; The composition such as flavone (epicatechin and catechin), Polyphenols, aucubin and Geniposidic acid.Flavone, Polyphenols have good bacteriostatic activity and antioxidant activity, its lipid peroxidation suppression ratio higher than VC, DPPH free radical scavenging activity and VC and BHT close.The Geniposidic acid of the Cortex Eucommiae and aucubin have the activity promoting collage synthesis and epidermal cell proliferation.The effect that the monomeric compound such as chlorogenic acid, caffeic acid, epicatechol, catechol of the Cortex Eucommiae has AIDS virus resisting (HIV) to infect.The specific function composition energy slow releasing of Cortex Eucommiae abrasive particle parcel, reaches the effect of nursing and health care skin.In addition, the Cortex Eucommiae is still containing natural gutta-percha, and the characteristic of the trans-isoprene glue of this uniqueness gives Cortex Eucommiae material not only hard but also submissive material, particle soft or hard is suitable, and containing sterilization antioxidation isoreactivity composition, make clean, skin-protection product together with other raw materials, there is whitening and moistening skin, moisturizing skin care, the effects such as horny layer softening, soft skin skin care, can allow skin smooth compact, rapid Glycerin, desalination melanin pigmentation, impels skin self-regeneration.Its processing technique is easy, healthy and safe, is suitable for preparing skin care cosmetics application.The present invention has science, novelty, makes full use of China's natural resources of Chinese medicinal materials unique advantage, opens new way prepared by exfoliation abrasive particle.
Specific embodiment
Below the present invention is described further.
embodiment 1.
A kind of Cortex Eucommiae exfoliation abrasive particle, is characterized in that, adopts following steps to make successively:
(1) processing of eucommia bark: choose and become tree in age (be good with smooth bark type) at trunk overhead 10 ~ more than 20cm position for more than 10 years, adopt part layer stripping or girding method to peel off bark; The bark peeled first pours boiling water on boiling hot, and then that the inner face of skin is relative in pairs, accumulation is set level; Surrounding Caulis et Folium Oryzae is wrapped, upper cover plank, and weighting material flattens through the vexed Hair Fixer heat of 6 one 7d, when bark inner face is in mulberry, brown, can takes out, dry; Removing rough bark (phellem layer), cleans, dries the strip being cut into wide 0.3 ~ 0.5cm;
(2) dry: the Cortex Eucommiae getting the strip of chopping, put in vacuum drying oven, at vacuum-0.03 ~-0.05MPa, at temperature 80 ~ 90 DEG C, be dried to moisture≤3%;
(3) pulverize: by the strip Cortex Eucommiae of drying with compound plastic moistureproof bag parcel, sealing, put refrigerator (
<-5 DEG C) freezing processing, then take out and pulverize rapidly, be sieved into 6 kinds of varigrained Cortex Eucommiae abrasive particles :-20 ~+30 ,-40 ~+60 order particles are for subsequent use.
A preparation method for Cortex Eucommiae exfoliation exfoliating shower dew, adopts following steps to make successively:
(1) formula composition: preparation 1000g.
Card ripple 2020 (solid) 8.0g, AXCELCG-PX height yield value suspending agent 1% aqueous solution 250.0g, Dodecyl Polyoxyethylene Ether sodium sulfate 67.0g, sodium lauryl sulphate 20.0g, Cortex cocois radicis oleoyl diethanolamine 60.0g, Plantacare APG 1200G 25.0g, glycerol 60.0g, Cortex Eucommiae exfoliation abrasive particle (-20 ~+30) 15g, Cortex Eucommiae exfoliation abrasive particle (-40 ~+60) 15g, EDTA1.0g, boric acid 0.1g, Sodium Methyl Hydroxybenzoate 1.0g, isothiazolone 1.0g, essence 6.0g, deionized water surplus.
(2) preparation manipulation step.
Get 100ml deionized water, under strong stirring, AXCELCG-PX height yield value suspending agent 4.0g is added hydration in aqueous phase, prevents agglomerate.Then add 296ml deionized water, activate 5min with homogenizer at 7000 ~ 10000rpm, obtain 1%AXCELCG-PX height yield value suspending agent and activate aqueous solution, for subsequent use.
Get 157.0ml deionized water, be heated to 60 DEG C, under stirring, slowly add 8.0g card ripple 2020 powder, continue to stir, make it be homogeneous transparent liquid, then the AXCELCG-PX height yield value suspending agent 1% aqueous solution 250.0g getting above-mentioned activation merges.313.9ml deionized water is added to above-mentioned amalgamation liquid, under agitation add formula ratio Dodecyl Polyoxyethylene Ether sodium sulfate, sodium lauryl sulphate, Cortex cocois radicis oleoyl diethanolamine, Plantacare APG 1200G, glycerol, Cortex Eucommiae exfoliation abrasive particle, EDTA, boric acid, Sodium Methyl Hydroxybenzoate, isothiazolone successively, stopping is heated, be down to after room temperature until temperature, add recipe quantity essence, stir, deaeration, packs and get final product.
The explanation of above-mentioned specific embodiment is not limitation of the present invention.The art person skilled, in essential scope of the present invention, the change made, change, interpolation or replacement, all should belong to protection scope of the present invention.
Claims (9)
1. a Cortex Eucommiae exfoliation abrasive particle, is characterized in that, adopts following steps to make successively:
(1) processing of eucommia bark: choose and become set at trunk overhead 10 ~ 20cm more than position age for more than 10 years, adopts part layer stripping or girding method to peel off bark; The bark peeled first pours boiling water on boiling hot, and then that the inner face of skin is relative in pairs, accumulation is set level; Surrounding Caulis et Folium Oryzae is wrapped, upper cover plank, and weighting material flattens through the vexed Hair Fixer heat of 6 one 7d, when bark inner face is in mulberry, brown, can takes out, dry; Removing rough bark, cleans, dries the strip being cut into wide 0.3 ~ 0.5cm;
(2) dry: the Cortex Eucommiae getting the strip of chopping, put in vacuum drying oven and dry;
(3) pulverize: by the strip Cortex Eucommiae of drying compound plastic moistureproof bag parcel, sealing, put refrigerator freezing process, refrigerator temperature
<-5 DEG C, then take out and pulverize rapidly, be sieved into 6 kinds of varigrained Cortex Eucommiae abrasive particles :-20 ~+30 ,-30 ~+40 ,-40 ~+60 ,-60 ~+80 ,-80 ~+100 orders, namely damp-prrof packing obtains product.
2. a kind of Cortex Eucommiae exfoliation abrasive particle according to claim 1, is characterized in that: the drying baker drying condition in described step (2) is at vacuum-0.03 ~-0.05MPa, at temperature 80 ~ 90 DEG C, is dried to moisture≤3%.
3. a preparation method for Cortex Eucommiae exfoliation abrasive particle, is characterized in that, adopts following steps to make successively:
(1) processing of eucommia bark: choose and become set at trunk overhead 10 ~ 20cm more than position age for more than 10 years, adopts part layer stripping or girding method to peel off bark; The bark peeled first pours boiling water on boiling hot, and then that the inner face of skin is relative in pairs, accumulation is set level; Surrounding Caulis et Folium Oryzae is wrapped, upper cover plank, and weighting material flattens through the vexed Hair Fixer heat of 6 one 7d, when bark inner face is in mulberry, brown, can takes out, dry; Removing rough bark, cleans, dries the strip being cut into wide 0.3 ~ 0.5cm;
(2) dry: the Cortex Eucommiae getting the strip of chopping, put in vacuum drying oven and dry;
(3) pulverize: by the strip Cortex Eucommiae of drying compound plastic moistureproof bag parcel, sealing, put refrigerator freezing process, refrigerator temperature
<-5 DEG C, then take out and pulverize rapidly, be sieved into 6 kinds of varigrained Cortex Eucommiae abrasive particles :-20 ~+30 ,-30 ~+40 ,-40 ~+60 ,-60 ~+80 ,-80 ~+100 orders, namely damp-prrof packing obtains product.
4. the preparation method of a kind of Cortex Eucommiae exfoliation abrasive particle according to claim 3, is characterized in that: the drying baker drying condition in described step (2) is at vacuum-0.03 ~-0.05MPa, at temperature 80 ~ 90 DEG C, is dried to moisture≤3%.
5. an application for Cortex Eucommiae exfoliation abrasive particle, is characterized in that: be applicable in exfoliation frosted health bath lotion, stock skin health-care paste frost, facial treatment milk product.
6. the application of a kind of Cortex Eucommiae exfoliation abrasive particle according to right 5, is characterized in that: prepare a kind of Cortex Eucommiae exfoliation exfoliating shower dew, adopts following steps to make successively:
(1) formula: Cortex Eucommiae exfoliation exfoliating shower dew is made up of the raw material of following masses part:
20200.7 ~ 1.0 parts, thickening agent card ripple
1% high yield value suspending agent activates aqueous solution 20.0 ~ 30.0 parts
19.0 ~ 23.0 parts, surfactant
Wetting agent glycerol 3.0 ~ 1.0 parts
Cortex Eucommiae exfoliation abrasive particle 2.0 ~ 5.0 parts
Chelating agen stabilizing agent EDTA0.5 ~ 1.5 part
PH adjusting agent boric acid 0.05 ~ 0.15 part
Antiseptic 0.1 ~ 0.3 part
Essence is appropriate
Deionized water surplus;
Formulation operations step:
A, get 1/3 water and add formula ratio thickening agent card ripple 2020, be heated to 60 DEG C, stir;
B, under strong stirring, high yield value suspending agent is added appropriate amount of deionized water mutually in hydration, prevent agglomerate; Then adding deionized water makes it be 1% concentration, activates 5 minutes with homogenizer at 7000 ~ 12000rpm homogenizing, obtains 1% high yield value suspending agent and activates aqueous solution;
C, get above-mentioned B and A gained solution and merge, and add balance deionized water, under agitation add formula ratio surfactant, wetting agent, Cortex Eucommiae exfoliation abrasive particle, EDTA, boric acid, antiseptic, essence successively, stir, deaeration, packs and get final product.
7. the application of a kind of Cortex Eucommiae exfoliation abrasive particle according to right 6, is characterized in that: described thickening agent card ripple 2020 is solid.
8. the application of a kind of Cortex Eucommiae exfoliation abrasive particle according to right 6, is characterized in that: described surfactant comprise AES, K12,6501, APG, CAB-35.
9. the application of a kind of Cortex Eucommiae exfoliation abrasive particle according to right 6, is characterized in that: described antiseptic comprises Sodium Methyl Hydroxybenzoate, isothiazolone.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510360913.9A CN105456078B (en) | 2015-06-26 | 2015-06-26 | A kind of bark of eucommia exfoliating abrasive particle and preparation method and application |
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| CN201510360913.9A CN105456078B (en) | 2015-06-26 | 2015-06-26 | A kind of bark of eucommia exfoliating abrasive particle and preparation method and application |
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| CN105456078A true CN105456078A (en) | 2016-04-06 |
| CN105456078B CN105456078B (en) | 2018-01-23 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106420473A (en) * | 2016-10-24 | 2017-02-22 | 澳宝化妆品（惠州）有限公司 | Preparation method of passion fruit seed shells and shower gel containing passion fruit seed shells |
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| CN102885726A (en) * | 2011-07-19 | 2013-01-23 | 上海家化联合股份有限公司 | Eucommia extract product, its preparation method and application thereof |
| KR20130026029A (en) * | 2011-09-05 | 2013-03-13 | 주식회사 제닉 | Cosmetic composition for scrubbing |
| CN103784339A (en) * | 2014-01-27 | 2014-05-14 | 钟春燕 | Abrasive skin cleaning product free of emulsifier |
| CN104490984A (en) * | 2014-12-25 | 2015-04-08 | 井冈山大学 | Preparation method of eucommia bark superfine powder |
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2015
- 2015-06-26 CN CN201510360913.9A patent/CN105456078B/en active Active
Patent Citations (5)
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| CN102885726A (en) * | 2011-07-19 | 2013-01-23 | 上海家化联合股份有限公司 | Eucommia extract product, its preparation method and application thereof |
| KR20130026029A (en) * | 2011-09-05 | 2013-03-13 | 주식회사 제닉 | Cosmetic composition for scrubbing |
| CN102716175A (en) * | 2012-07-04 | 2012-10-10 | 上海玉成干燥设备有限公司 | Superfine eucommia ulmoides powder and preparation method thereof |
| CN103784339A (en) * | 2014-01-27 | 2014-05-14 | 钟春燕 | Abrasive skin cleaning product free of emulsifier |
| CN104490984A (en) * | 2014-12-25 | 2015-04-08 | 井冈山大学 | Preparation method of eucommia bark superfine powder |
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Cited By (1)
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| CN106420473A (en) * | 2016-10-24 | 2017-02-22 | 澳宝化妆品（惠州）有限公司 | Preparation method of passion fruit seed shells and shower gel containing passion fruit seed shells |
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Address after: 343100 No. 5 Ji'an Avenue, Jinggangshan Economic and Technological Development Zone, Ji'an City, Jiangxi Province Patentee after: Puzheng Pharmaceutical Group Co., Ltd. Address before: 343000 Jinggangshan economic and Technological Development Zone, Ji'an, Jiangxi Patentee before: Puzheng Pharmaceutical Co.,Ltd. |