CN105418078A - Intelligent preparation method of special aid for novel special ceramic material - Google Patents
Intelligent preparation method of special aid for novel special ceramic material Download PDFInfo
- Publication number
- CN105418078A CN105418078A CN201510895074.0A CN201510895074A CN105418078A CN 105418078 A CN105418078 A CN 105418078A CN 201510895074 A CN201510895074 A CN 201510895074A CN 105418078 A CN105418078 A CN 105418078A
- Authority
- CN
- China
- Prior art keywords
- module
- executive signal
- digital signals
- signal
- receives
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- 229910010293 ceramic material Inorganic materials 0.000 title abstract 3
- 238000003756 stirring Methods 0.000 claims abstract description 49
- 239000000463 material Substances 0.000 claims abstract description 44
- 238000010438 heat treatment Methods 0.000 claims abstract description 34
- 239000007788 liquid Substances 0.000 claims abstract description 21
- 238000001035 drying Methods 0.000 claims abstract description 19
- 230000011664 signaling Effects 0.000 claims description 50
- 230000001960 triggered effect Effects 0.000 claims description 45
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 34
- 238000010298 pulverizing process Methods 0.000 claims description 34
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 32
- 238000007873 sieving Methods 0.000 claims description 26
- 239000000843 powder Substances 0.000 claims description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 21
- 229910052622 kaolinite Inorganic materials 0.000 claims description 21
- -1 polyoxyethylene Polymers 0.000 claims description 19
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 17
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 17
- 238000001914 filtration Methods 0.000 claims description 16
- 230000006698 induction Effects 0.000 claims description 16
- 239000008367 deionised water Substances 0.000 claims description 15
- 229910021641 deionized water Inorganic materials 0.000 claims description 15
- 239000003795 chemical substances by application Substances 0.000 claims description 13
- 239000002904 solvent Substances 0.000 claims description 13
- 239000012752 auxiliary agent Substances 0.000 claims description 12
- 239000004408 titanium dioxide Substances 0.000 claims description 10
- 239000001307 helium Substances 0.000 claims description 9
- 229910052734 helium Inorganic materials 0.000 claims description 9
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims description 9
- 238000001354 calcination Methods 0.000 claims description 8
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 7
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 7
- 229910052796 boron Inorganic materials 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- 239000000835 fiber Substances 0.000 claims description 7
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims description 5
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 5
- 238000002242 deionisation method Methods 0.000 claims description 3
- 230000007797 corrosion Effects 0.000 abstract description 6
- 238000005260 corrosion Methods 0.000 abstract description 6
- 238000000227 grinding Methods 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 14
- 239000010456 wollastonite Substances 0.000 description 10
- 229910052882 wollastonite Inorganic materials 0.000 description 10
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 8
- 239000000919 ceramic Substances 0.000 description 7
- 230000008569 process Effects 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 5
- 229910052582 BN Inorganic materials 0.000 description 5
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 5
- 239000004927 clay Substances 0.000 description 5
- 239000013078 crystal Substances 0.000 description 5
- 238000010304 firing Methods 0.000 description 5
- 238000005245 sintering Methods 0.000 description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- 229910052656 albite Inorganic materials 0.000 description 4
- 229910000480 nickel oxide Inorganic materials 0.000 description 4
- 229910052758 niobium Inorganic materials 0.000 description 4
- 239000010955 niobium Substances 0.000 description 4
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 4
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 239000011787 zinc oxide Substances 0.000 description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 239000012298 atmosphere Substances 0.000 description 3
- 238000000498 ball milling Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 239000000758 substrate Substances 0.000 description 3
- 229910052581 Si3N4 Inorganic materials 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 239000010433 feldspar Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000005543 nano-size silicon particle Substances 0.000 description 2
- 229910052573 porcelain Inorganic materials 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 229910002796 Si–Al Inorganic materials 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000012241 calcium silicate Nutrition 0.000 description 1
- 229910052918 calcium silicate Inorganic materials 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 229910052570 clay Inorganic materials 0.000 description 1
- 238000007596 consolidation process Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000005496 eutectics Effects 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229910052863 mullite Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 229910052903 pyrophyllite Inorganic materials 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 235000012222 talc Nutrition 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Abstract
The invention discloses an intelligent preparation method of a special aid for a novel special ceramic material. According to the intelligent preparation method, a sensing module senses the flowing of liquid and a material pressure T, and a PLC executes internal analytical calculation according to a sensing value and received digital signals and controls a grinding module, a conveying module, a timing module, a valve control module, a stirring module, a filtering-drying module and a heating module to execute related operations. According to the intelligent preparation method, the performance including good wear resistance, high rigidity and good tenacity, vibration resistance, heat resistance and corrosion resistance of the novel special ceramic material can be achieved; various parameters in a system can be accurately controlled, and the automation degree is high; furthermore, resources can be saved.
Description
Technical field
The present invention relates to control field, especially a kind of intelligent preparation method of special addition agent of new special stupalith.
Background technology
Current stupalith development rapidly, and is widely used in every field, as metallic substance, isolator, pipeline etc., but there is following problem in existing pottery: as fragility is too large, intensity is little, and temperature capacity is little etc., and working method cost is large, product benefit is low, and therefore need research wear resistance good, hardness is high, good toughness, vibration resistance, heat-resisting, the corrosion-resistant stupalith waiting excellent performance.
In the preparation process of stupalith, selecting of auxiliary agent is most important, directly affects the fragility of the stupalith of preparation, intensity and temperature capacity.
Summary of the invention
Goal of the invention of the present invention is: for above-mentioned Problems existing, a kind of intelligent preparation method of special addition agent of new special stupalith is provided, the stupalith wear resistance that can strengthen a kind of new special stupalith is good, hardness is high, good toughness, vibration resistance, heat-resisting, the performance such as corrosion-resistant, can parameters in accuracy-control system, and level of automation is high; Save resource.
The technical solution used in the present invention is as follows:
The intelligent preparation method of the intelligent preparation system of the special addition agent of new special stupalith, it comprises the following steps:
Step 1: by place for each device, opens a kind of intelligent preparation system power supply of special addition agent of new special stupalith;
Step 2: dropped into by the kaolinite of predetermined dose 01 in shredding unit, trigger the trigger button one pulverized in module, after trigger button one first time is triggered, starts shredding unit, and to time block transmitting digital signals 001; Time block receives digital signaling zero 01, to PLC transmitting digital signals 101 after startup timing register one, 15min, and stops timing; PLC receives numerary signal 101, transmits executive signal 201 to valve control module, transmits executive signal 301 to delivery module simultaneously, transmits executive signal 501 to pulverizing module;
Step 3: pulverize module and receive executive signal 501, close shredding unit; Valve control module receives executive signal 201, opens magnetic valve one, closes after the scheduled time 01; Kaolinite after then pulverizing enters transport unit by magnetic valve one; Delivery module receives executive signal 301, starts transport unit, material is delivered to sieving equipment, crosses 40 mesh sieves; Obtain kaolinite powder;
Step 4: the trigger button triggering solvent modules, after described trigger button is triggered, open the magnetic valve of polyoxyethylene glycol case and deionization water tank, after the deionized water of the polyoxyethylene glycol of predetermined dose 01 and predetermined dose 02 is discarded to whipping appts, shut electromagnetic valve;
Step 5: trigger the trigger button two on whipping appts, after described trigger button two first time is triggered, starts whipping appts, and to time block transmitting digital signals 002; Time block receives digital signaling zero 02, to PLC transmitting digital signals 102 after startup timing register two, 15min, and stops timing; PLC receives numerary signal 102, transmits executive signal 401 to stirring module; Stir module and receive executive signal 401, close whipping appts;
Step 6: be added in whipping appts by kaolinite powder, triggers the trigger button two on whipping appts, after described trigger button two first time is triggered, starts whipping appts, and to time block transmitting digital signals 003; Time block receives digital signaling zero 03, to PLC transmitting digital signals 103 after startup timing register three, 20min, and stops timing; PLC receives numerary signal 103, transmits executive signal 402 to stirring module; Stir module and receive executive signal 402, close whipping appts;
Step 7: be added in whipping appts by the silane coupling agent kh-550 of predetermined dose 02, triggers the trigger button two on whipping appts, after described trigger button two third time is triggered, starts whipping appts, and to time block transmitting digital signals 004; Time block receives digital signaling zero 04, to PLC transmitting digital signals 104 after startup timing register four, 20min, and stops timing; PLC receives numerary signal 104, transmits executive signal 403 to stirring module; Stir module and receive executive signal 403, close whipping appts; Obtain liquid A;
Step 8: dropped into by the titanium dioxide of predetermined dose 03 in shredding unit, trigger the trigger button one pulverized in module, after trigger button one second time is triggered, starts shredding unit, and to time block transmitting digital signals 005; Time block receives digital signaling zero 05, to PLC transmitting digital signals 105 after startup timing register five, 15min; Receive numerary signal 105, transmit executive signal 202 to valve control module, transmit executive signal 302 to delivery module simultaneously, transmit executive signal 502 to pulverizing module;
Step 9: pulverize module and receive executive signal 502, close shredding unit; Valve control module receives executive signal 202, opens magnetic valve one, closes after the scheduled time 02; Titanium dioxide after then pulverizing enters transport unit by magnetic valve one; Delivery module receives executive signal 302, starts transport unit, material is delivered to sieving equipment and cross 40 mesh sieves; Obtain titania powder;
Step 10: titania powder, the nanometer silicon carbide of predetermined dose 04 and the nanometer boron fibre of predetermined dose 05 after sieving are added in whipping appts; Trigger the trigger button two on whipping appts, after described trigger button 2 is triggered for the 4th time, start whipping appts, and to time block transmitting digital signals 006; Time block receives digital signaling zero 06, to PLC transmitting digital signals 106 after startup timing register six, 20min; PLC receives numerary signal 106, transmits executive signal 404, and transmit executive signal 203 to valve control module to stirring module; Stir module and receive executive signal 404, close whipping appts; Valve control module receives executive signal 203, opens magnetic valve two; Then material enters in dry filtrating equipment;
Step 11: the liquid inductor block induced liquid in induction module flows through, and to PLC transmitting digital signals 010; PLC receives digital signaling zero 10, transmits executive signal 601 to filtration drying module; Filtration drying module receives executive signal 601, starts dry filtrating equipment;
Step 12: dropped into by the material after dry filter in shredding unit, trigger the trigger button one pulverized in module, after trigger button one third time is triggered, starts shredding unit, and to time block transmitting digital signals 007; Time block receives digital signaling zero 07, after starting timing register seven, 15min, to PLC transmitting digital signals 107; Receive numerary signal 107, transmit executive signal 204 to valve control module, transmit executive signal 303 to delivery module simultaneously, transmit executive signal 503 to pulverizing module;
Step 13: pulverize module and receive executive signal 503, close shredding unit; Valve control module receives executive signal 204, opens magnetic valve one, closes after the scheduled time 03; Material after then pulverizing enters transport unit by magnetic valve one; Delivery module receives executive signal 303, starts transport unit, material is delivered to sieving equipment and cross 120 mesh sieves;
Step 14: the material after sieving is placed in heating unit, the pressure transmitter induction material pressure T in induction module, as T>100N, to PLC transmitting digital signals 011; PLC receives digital signaling zero 11, transmits executive signal 701 to heating module, and transmits executive signal 205 to valve control module; Heating module receives executive signal 701, starts heating unit, and is heated to 823 DEG C; Valve control module receives executive signal 205, opens magnetic valve three, in heating unit, passes into helium, closes after the scheduled time 04; After the material calcining 3h after heating, air cooling is to room temperature;
Step 15: material step 14 obtained drops in shredding unit, triggers the trigger button one pulverized in module, after trigger button 1 is triggered for the 4th time, starts shredding unit, and to time block transmitting digital signals 008; Time block receives digital signaling zero 08, after starting timing register eight, 15min, to PLC transmitting digital signals 108; PLC receives numerary signal 108, transmits executive signal 206 to valve control module, transmits executive signal 304 to delivery module simultaneously, transmits executive signal 504 to pulverizing module;
Step 16: pulverize module executive signal 504, closes shredding unit; Valve control module receives executive signal 206, opens magnetic valve one, closes after the scheduled time 05; Delivery module executive signal 304, start transport unit, material is delivered to sieving equipment 50 mesh sieves, obtain auxiliary agent.
The intelligent preparation system of the special addition agent of new special stupalith, it comprises: PLC, induction module, pulverizing module, delivery module, time block, valve control module, stirring module, filtration drying module and heating module;
Induction module comprises the liquid inductor block being located at dry filtrating equipment entrance and the pressure transmitter being located at heating unit; Liquid inductor block is used for induced liquid and flows through, and to PLC transmitting digital signals 010; Described pressure transmitter for responding to material pressure T, as T>100N, to PLC transmitting digital signals 011;
Pulverize module and comprise shredding unit, described shredding unit is provided with trigger button one, after described trigger button one first time is triggered, starts shredding unit, and to time block transmitting digital signals 001; After trigger button one second time is triggered, start shredding unit, and to time block transmitting digital signals 005; After trigger button one third time is triggered, start shredding unit, and to time block transmitting digital signals 007; After trigger button 1 is triggered for the 4th time, start shredding unit, and to time block transmitting digital signals 008; Receive executive signal 501, executive signal 502, executive signal 503 or executive signal 504, close shredding unit;
Time block comprises timing register one, timing register two, timing register three, timing register four, timing register five, timing register six, timing register seven and timing register eight; For receiving digital signaling zero 01, after starting timing register one, 15min, (described 15min is what set in advance) is to PLC transmitting digital signals 101, and stops timing; Receive digital signaling zero 02, to PLC transmitting digital signals 102 after startup timing register two, 15min, and stop timing; Receive digital signaling zero 03, to PLC transmitting digital signals 103 after startup timing register three, 20min, and stop timing; Receive digital signaling zero 04, to PLC transmitting digital signals 104 after startup timing register four, 20min, and stop timing; Receive digital signaling zero 05, to PLC transmitting digital signals 105 after startup timing register five, 15min, receive digital signaling zero 06, to PLC transmitting digital signals 106 after startup timing register six, 20min; Receive digital signaling zero 07, after starting timing register seven, 15min, to PLC transmitting digital signals 107; Receive digital signaling zero 08, after starting timing register eight, 15min, to PLC transmitting digital signals 108;
PLC respectively with induction module, pulverize module, delivery module, time block, valve control module, stirring module, filtration drying module be connected with heating module; For receiving numerary signal 101, transmitting executive signal 201 to valve control module, transmitting executive signal 301 to delivery module simultaneously, transmit executive signal 501 to pulverizing module; Receive numerary signal 102, transmit executive signal 401 to stirring module; Receive numerary signal 103, transmit executive signal 402 to stirring module; Receive numerary signal 104, transmit executive signal 403 to stirring module; Receive numerary signal 105, transmit executive signal 202 to valve control module, transmit executive signal 302 to delivery module simultaneously, transmit executive signal 502 to pulverizing module; Receive numerary signal 106, transmit executive signal 404 to stirring module, and transmit executive signal 203 to valve control module; Receive digital signaling zero 10, transmit executive signal 601 to filtration drying module; Receive numerary signal 107, transmit executive signal 204 to valve control module, transmit executive signal 303 to delivery module simultaneously, transmit executive signal 503 to pulverizing module; Receive digital signaling zero 11, transmit executive signal 701 to heating module, and transmit executive signal 205 to valve control module; Receive numerary signal 108, transmit executive signal 206 to valve control module, transmit executive signal 304 to delivery module simultaneously, transmit executive signal 504 to pulverizing module;
Valve control module comprise be located at shredding unit lower end magnetic valve one, be located at the magnetic valve two of whipping appts and be located at the magnetic valve three of helium storing unit; Receive executive signal 201, open magnetic valve one, close after the scheduled time 01; Receive executive signal 202, open magnetic valve one, close after the scheduled time 02; Receive executive signal 203, open magnetic valve two; Receive executive signal 204, open magnetic valve one, close after the scheduled time 03; Receive executive signal 205, open magnetic valve three, close after the scheduled time 04; Receive executive signal 206, open magnetic valve one, close after the scheduled time 05;
Delivery module comprises is located at the transport unit of shredding unit to sieving equipment, for receiving executive signal 301, executive signal 302, executive signal 303 or executive signal 304, starting transport unit, material is delivered to sieving equipment;
Stir module and comprise whipping appts, described whipping appts is provided with trigger button two, after described trigger button two first time is triggered, starts whipping appts, and to time block transmitting digital signals 002; Receive executive signal 401, close whipping appts; After described trigger button two first time is triggered, start whipping appts, and to time block transmitting digital signals 003; Receive executive signal 402, close whipping appts; After described trigger button two third time is triggered, start whipping appts, and to time block transmitting digital signals 004; Receive executive signal 403, close whipping appts; After described trigger button 2 is triggered for the 4th time, start whipping appts, and to time block transmitting digital signals 006; Receive executive signal 404, close whipping appts;
Filtration drying module comprises dry filtrating equipment, for receiving executive signal 601, starts dry filtrating equipment;
Heating module comprises heating unit, for receiving executive signal 701, starting heating unit, and being heated to 823 DEG C.
Owing to adopting such scheme, described induction module accurately the flowing through and material pressure value of induced liquid, avoids manual triggers, increases level of automation;
Shredding unit by crushing material extremely pre-sizing, makes whole process with one-level raw material as raw material, can decrease expense with certain speed; Facilitate the operation of whole process; Set grinding time or churning time in advance according to the degree of grinding of material or stirring extent, decrease the manually operated trouble of staff, increase level of automation; The setting of valve control module, total startup controlling each magnetic valve and closedown, setting up of transport unit, avoids the trouble that staff moves material;
Further, also comprise solvent modules and comprise solvent device, described solvent device is provided with trigger button, described solvent device is provided with polyoxyethylene glycol bin and deionized water bin, described polyoxyethylene glycol bin and deionized water bin are connected to conduit, the described conduit the other end stretches in whipping appts, described conduit is provided with magnetic valve, described magnetic valve is provided with flow measurement instrument, after described trigger button is triggered, opens solenoid valve, after the deionized water of the polyoxyethylene glycol of predetermined dose 01 and predetermined dose 02 is released, shut electromagnetic valve.
Owing to adopting such scheme, the deionized water of the polyoxyethylene glycol of predetermined dose 01 and predetermined dose 02 is put into whipping appts and is fully mixed by solvent modules.
Further, described sieving equipment is provided with 40 mesh sieves of horizontal, 120 mesh sieves and 50 mesh sieves.
Owing to adopting such scheme, different material is placed in required sieve, avoids the trouble of frequently changing sieve, increase level of automation;
Further, described timing register stops timing, auto zero; Be provided with linking conduit between described whipping appts and dry filtrating equipment, described conduit is provided with magnetic valve two.
In sum, owing to have employed technique scheme, the invention has the beneficial effects as follows:
The stupalith wear resistance that 1, can strengthen a kind of new special stupalith is good, the performances such as hardness is high, good toughness, and vibration resistance is heat-resisting, corrosion-resistant;
2, the parameters in energy accuracy-control system, level of automation is high; Save resource.
Accompanying drawing explanation
Examples of the present invention will be described by way of reference to the accompanying drawings, wherein:
Fig. 1 is a kind of System Control Figure of intelligent preparation system of special addition agent of new special stupalith.
Embodiment
All features disclosed in this specification sheets, or the step in disclosed all methods or process, except mutually exclusive feature and/or step, all can combine by any way.
Arbitrary feature disclosed in this specification sheets (comprising any accessory claim, summary), unless specifically stated otherwise, all can be replaced by other equivalences or the alternative features with similar object.That is, unless specifically stated otherwise, each feature is an example in a series of equivalence or similar characteristics.
As shown in Figure 1, a kind of intelligent preparation system of special addition agent of new special stupalith, it comprises: PLC, induction module, pulverizing module, delivery module, time block, valve control module, stirring module, filtration drying module and heating module;
Induction module comprises the liquid inductor block being located at dry filtrating equipment entrance and the pressure transmitter being located at heating unit; Liquid inductor block is used for induced liquid and flows through, and to PLC transmitting digital signals 010; Described pressure transmitter for responding to material pressure T, as T>100N, to PLC transmitting digital signals 011;
Pulverize module and comprise shredding unit, described shredding unit is provided with trigger button one, after described trigger button one first time is triggered, starts shredding unit, and to time block transmitting digital signals 001; After trigger button one second time is triggered, start shredding unit, and to time block transmitting digital signals 005; After trigger button one third time is triggered, start shredding unit, and to time block transmitting digital signals 007; After trigger button 1 is triggered for the 4th time, start shredding unit, and to time block transmitting digital signals 008; Receive executive signal 501, executive signal 502, executive signal 503 or executive signal 504, close shredding unit;
Time block comprises timing register one, timing register two, timing register three, timing register four, timing register five, timing register six, timing register seven and timing register eight; For receiving digital signaling zero 01, after starting timing register one, 15min, (described 15min is what set in advance) is to PLC transmitting digital signals 101, and stops timing; Receive digital signaling zero 02, to PLC transmitting digital signals 102 after startup timing register two, 15min, and stop timing; Receive digital signaling zero 03, to PLC transmitting digital signals 103 after startup timing register three, 20min, and stop timing; Receive digital signaling zero 04, to PLC transmitting digital signals 104 after startup timing register four, 20min, and stop timing; Receive digital signaling zero 05, to PLC transmitting digital signals 105 after startup timing register five, 15min, receive digital signaling zero 06, to PLC transmitting digital signals 106 after startup timing register six, 20min; Receive digital signaling zero 07, after starting timing register seven, 15min, to PLC transmitting digital signals 107; Receive digital signaling zero 08, after starting timing register eight, 15min, to PLC transmitting digital signals 108;
PLC respectively with induction module, pulverize module, delivery module, time block, valve control module, stirring module, filtration drying module be connected with heating module; For receiving numerary signal 101, transmitting executive signal 201 to valve control module, transmitting executive signal 301 to delivery module simultaneously, transmit executive signal 501 to pulverizing module; Receive numerary signal 102, transmit executive signal 401 to stirring module; Receive numerary signal 103, transmit executive signal 402 to stirring module; Receive numerary signal 104, transmit executive signal 403 to stirring module; Receive numerary signal 105, transmit executive signal 202 to valve control module, transmit executive signal 302 to delivery module simultaneously, transmit executive signal 502 to pulverizing module; Receive numerary signal 106, transmit executive signal 404 to stirring module, and transmit executive signal 203 to valve control module; Receive digital signaling zero 10, transmit executive signal 601 to filtration drying module; Receive numerary signal 107, transmit executive signal 204 to valve control module, transmit executive signal 303 to delivery module simultaneously, transmit executive signal 503 to pulverizing module; Receive digital signaling zero 11, transmit executive signal 701 to heating module, and transmit executive signal 205 to valve control module; Receive numerary signal 108, transmit executive signal 206 to valve control module, transmit executive signal 304 to delivery module simultaneously, transmit executive signal 504 to pulverizing module;
Valve control module comprise be located at shredding unit lower end magnetic valve one, be located at the magnetic valve two of whipping appts and be located at the magnetic valve three of helium storing unit; Receive executive signal 201, open magnetic valve one, close after the scheduled time 01; Receive executive signal 202, open magnetic valve one, close after the scheduled time 02; Receive executive signal 203, open magnetic valve two; Receive executive signal 204, open magnetic valve one, close after the scheduled time 03; Receive executive signal 205, open magnetic valve three, close after the scheduled time 04; Receive executive signal 206, open magnetic valve one, close after the scheduled time 05;
Delivery module comprises is located at the transport unit of shredding unit to sieving equipment, for receiving executive signal 301, executive signal 302, executive signal 303 or executive signal 304, starting transport unit, material is delivered to sieving equipment;
Stir module and comprise whipping appts, described whipping appts is provided with trigger button two, after described trigger button two first time is triggered, starts whipping appts, and to time block transmitting digital signals 002; Receive executive signal 401, close whipping appts; After described trigger button two first time is triggered, start whipping appts, and to time block transmitting digital signals 003; Receive executive signal 402, close whipping appts; After described trigger button two third time is triggered, start whipping appts, and to time block transmitting digital signals 004; Receive executive signal 403, close whipping appts; After described trigger button 2 is triggered for the 4th time, start whipping appts, and to time block transmitting digital signals 006; Receive executive signal 404, close whipping appts;
Filtration drying module comprises dry filtrating equipment, for receiving executive signal 601, starts dry filtrating equipment;
Heating module comprises heating unit, for receiving executive signal 701, starting heating unit, and being heated to 823 DEG C.
Also comprise solvent modules and comprise solvent device, described solvent device is provided with trigger button, described solvent device is provided with polyoxyethylene glycol bin and deionized water bin, described polyoxyethylene glycol bin and deionized water bin are connected to conduit, the described conduit the other end stretches in whipping appts, described conduit is provided with magnetic valve, described magnetic valve is provided with flow measurement instrument, after described trigger button is triggered, opens solenoid valve, after the deionized water of the polyoxyethylene glycol of predetermined dose 01 and predetermined dose 02 is released, shut electromagnetic valve.
Described sieving equipment is provided with 40 mesh sieves of horizontal, 120 mesh sieves and 50 mesh sieves.
Described timing register stops timing, auto zero; Be provided with linking conduit between described whipping appts and dry filtrating equipment, described conduit is provided with magnetic valve two.
The intelligent preparation method of the intelligent preparation system of the intelligent preparation system of the special addition agent of new special stupalith, it comprises the following steps:
Step 1: by place for each device, opens a kind of intelligent preparation system power supply of special addition agent of new special stupalith;
Step 2: dropped into by the kaolinite of predetermined dose 01 in shredding unit, trigger the trigger button one pulverized in module, after trigger button one first time is triggered, starts shredding unit, and to time block transmitting digital signals 001; Time block receives digital signaling zero 01, to PLC transmitting digital signals 101 after startup timing register one, 15min, and stops timing; PLC receives numerary signal 101, transmits executive signal 201 to valve control module, transmits executive signal 301 to delivery module simultaneously, transmits executive signal 501 to pulverizing module;
Step 3: pulverize module and receive executive signal 501, close shredding unit; Valve control module receives executive signal 201, opens magnetic valve one, closes after the scheduled time 01; Kaolinite after then pulverizing enters transport unit by magnetic valve one; Delivery module receives executive signal 301, starts transport unit, material is delivered to sieving equipment, crosses 40 mesh sieves; Obtain kaolinite powder;
Step 4: the trigger button triggering solvent modules, after described trigger button is triggered, open the magnetic valve of polyoxyethylene glycol case and deionization water tank, after the deionized water of the polyoxyethylene glycol of predetermined dose 01 and predetermined dose 02 is discarded to whipping appts, shut electromagnetic valve;
Step 5: trigger the trigger button two on whipping appts, after described trigger button two first time is triggered, starts whipping appts, and to time block transmitting digital signals 002; Time block receives digital signaling zero 02, to PLC transmitting digital signals 102 after startup timing register two, 15min, and stops timing; PLC receives numerary signal 102, transmits executive signal 401 to stirring module; Stir module and receive executive signal 401, close whipping appts;
Step 6: be added in whipping appts by kaolinite powder, triggers the trigger button two on whipping appts, after described trigger button two first time is triggered, starts whipping appts, and to time block transmitting digital signals 003; Time block receives digital signaling zero 03, to PLC transmitting digital signals 103 after startup timing register three, 20min, and stops timing; PLC receives numerary signal 103, transmits executive signal 402 to stirring module; Stir module and receive executive signal 402, close whipping appts;
Step 7: be added in whipping appts by the silane coupling agent kh-550 of predetermined dose 02, triggers the trigger button two on whipping appts, after described trigger button two third time is triggered, starts whipping appts, and to time block transmitting digital signals 004; Time block receives digital signaling zero 04, to PLC transmitting digital signals 104 after startup timing register four, 20min, and stops timing; PLC receives numerary signal 104, transmits executive signal 403 to stirring module; Stir module and receive executive signal 403, close whipping appts; Obtain liquid A;
Step 8: dropped into by the titanium dioxide of predetermined dose 03 in shredding unit, trigger the trigger button one pulverized in module, after trigger button one second time is triggered, starts shredding unit, and to time block transmitting digital signals 005; Time block receives digital signaling zero 05, to PLC transmitting digital signals 105 after startup timing register five, 15min; Receive numerary signal 105, transmit executive signal 202 to valve control module, transmit executive signal 302 to delivery module simultaneously, transmit executive signal 502 to pulverizing module;
Step 9: pulverize module and receive executive signal 502, close shredding unit; Valve control module receives executive signal 202, opens magnetic valve one, closes after the scheduled time 02; Titanium dioxide after then pulverizing enters transport unit by magnetic valve one; Delivery module receives executive signal 302, starts transport unit, material is delivered to sieving equipment and cross 40 mesh sieves; Obtain titania powder;
Step 10: titania powder, the nanometer silicon carbide of predetermined dose 04 and the nanometer boron fibre of predetermined dose 05 after sieving are added in whipping appts; Trigger the trigger button two on whipping appts, after described trigger button 2 is triggered for the 4th time, start whipping appts, and to time block transmitting digital signals 006; Time block receives digital signaling zero 06, to PLC transmitting digital signals 106 after startup timing register six, 20min; PLC receives numerary signal 106, transmits executive signal 404, and transmit executive signal 203 to valve control module to stirring module; Stir module and receive executive signal 404, close whipping appts; Valve control module receives executive signal 203, opens magnetic valve two; Then material enters in dry filtrating equipment;
Step 11: the liquid inductor block induced liquid in induction module flows through, and to PLC transmitting digital signals 010; PLC receives digital signaling zero 10, transmits executive signal 601 to filtration drying module; Filtration drying module receives executive signal 601, starts dry filtrating equipment;
Step 12: dropped into by the material after dry filter in shredding unit, trigger the trigger button one pulverized in module, after trigger button one third time is triggered, starts shredding unit, and to time block transmitting digital signals 007; Time block receives digital signaling zero 07, after starting timing register seven, 15min, to PLC transmitting digital signals 107; Receive numerary signal 107, transmit executive signal 204 to valve control module, transmit executive signal 303 to delivery module simultaneously, transmit executive signal 503 to pulverizing module;
Step 13: pulverize module and receive executive signal 503, close shredding unit; Valve control module receives executive signal 204, opens magnetic valve one, closes after the scheduled time 03; Material after then pulverizing enters transport unit by magnetic valve one; Delivery module receives executive signal 303, starts transport unit, material is delivered to sieving equipment and cross 120 mesh sieves;
Step 14: the material after sieving is placed in heating unit, the pressure transmitter induction material pressure T in induction module, as T>100N, to PLC transmitting digital signals 011; PLC receives digital signaling zero 11, transmits executive signal 701 to heating module, and transmits executive signal 205 to valve control module; Heating module receives executive signal 701, starts heating unit, and is heated to 823 DEG C; Valve control module receives executive signal 205, opens magnetic valve three, in heating unit, passes into helium, closes after the scheduled time 04; After the material calcining 3h after heating, air cooling is to room temperature;
Step 15: material step 14 obtained drops in shredding unit, triggers the trigger button one pulverized in module, after trigger button 1 is triggered for the 4th time, starts shredding unit, and to time block transmitting digital signals 008; Time block receives digital signaling zero 08, after starting timing register eight, 15min, to PLC transmitting digital signals 108; PLC receives numerary signal 108, transmits executive signal 206 to valve control module, transmits executive signal 304 to delivery module simultaneously, transmits executive signal 504 to pulverizing module;
Step 16: pulverize module executive signal 504, closes shredding unit; Valve control module receives executive signal 206, opens magnetic valve one, closes after the scheduled time 05; Delivery module executive signal 304, start transport unit, material is delivered to sieving equipment 50 mesh sieves, obtain auxiliary agent.
A kind of new special stupalith in the present invention is:
A kind of new special stupalith, described new special stupalith is made up of the raw material of following weight part: red clay 40-50 part, albite 1-3 part, nano level aluminium sesquioxide 5-7 part, nickel oxide 1-3 part, zinc oxide 1-3 part, Niobium Pentxoxide 5-7 part, boron nitride 5-7 part, wollastonite 5-7 part, sodium zirconate 3-4 part, auxiliary agent 5-7 part.
Described special addition agent is made up of the raw material of following weight part: nano-silicon nitride 0.8-1.2 part, nanometer boron fibre 0.6-0.9 part, silane coupling agent kh-5500.6-0.8 part, polyoxyethylene glycol 0.3-0.4, deionized water 20-25 part, kaolinite 12-17 part, titanium dioxide 5-7 part.
The preparation method of described auxiliary agent is: pulverized by kaolinite, cross 40 mesh sieves, obtain kaolinite powder, polyoxyethylene glycol is added in deionized water, stir, kaolinite powder after sieving is added wherein, stir 20min, add silane coupling agent kh-550, stir 20min, obtain liquid A, titanium dioxide is pulverized, cross 40 mesh sieves, and nanometer silicon carbide then, nanometer boron fibre joins in liquid A together, stir 20min, filtration drying, 120 mesh sieves are crossed after pulverizing, under helium atmosphere, after calcining 3h at being heated to 820-830 DEG C, air cooling is to room temperature, then pulverize, cross 50 mesh sieves, obtain auxiliary agent.
Described new special stupalith is made up of the raw material of following weight part: red clay 45 parts, albite 2 parts, nano level aluminium sesquioxide 6 parts, nickel oxide 2 parts, 2 parts, zinc oxide, Niobium Pentxoxide 6 parts, boron nitride 6 parts, wollastonite 6 parts, sodium zirconate 3.2 parts, auxiliary agent 6.5 parts;
The component of described auxiliary agent is counted by weight: nano-silicon nitride 0.9 part, nanometer boron fibre 0.7 part, silane coupling agent kh-5500.65 part, polyoxyethylene glycol 0.36 part, deionized water 23 parts, 14 parts, kaolinite, titanium dioxide 6 parts;
The preparation method of described auxiliary agent is: pulverized by kaolinite, cross 40 mesh sieves, obtain kaolinite powder, polyoxyethylene glycol is added in deionized water, stir, kaolinite powder after sieving is added wherein, stir 20min, add silane coupling agent kh-550, stir 20min, obtain liquid A, titanium dioxide is pulverized, cross 40 mesh sieves, and nanometer silicon carbide then, nanometer boron fibre joins in liquid A together, stir 20min, filtration drying, 120 mesh sieves are crossed after pulverizing, under helium atmosphere, after calcining 3h at being heated to 823 DEG C, air cooling is to room temperature, then pulverize, cross 50 mesh sieves, obtain auxiliary agent.
Prepare a method for above-mentioned new special stupalith, comprise the following steps:
Step 1, red clay, albite, wollastonite, nano level aluminium sesquioxide and Niobium Pentxoxide to be mixed, then ball mill abrasive dust is put into, cross 230 mesh sieves, again auxiliary agent and boron nitride are sent into ball milling 18-20h in ball mill, add potassium hydroxide again, continue ball milling 2-3h, being washed to pH value is 7-8, filters and obtains powder;
Step 2, will filter the powder that obtains using helium as shielding gas, at 880-900 DEG C, calcine 4-6h, then air cooling is to room temperature, sends into ball mill abrasive dust, crosses 120 mesh sieves, obtains powder particle A;
Step 3, sodium zirconate, nickel oxide, zinc oxide and powder particle A mixed and stir, being heated to 980-990 DEG C, and calcining 1-3h, ball mill pulverizing, crossing 80 mesh sieves, obtain powder particle B;
Step 4, powder particle B to be mixed with the ratio of deionized water in 4:3, then put into ball mill ball milling 16-18h, then moulding, in the atmosphere of helium, 800-900 DEG C of temperature lower calcination 2h, then temperature is increased to 1200-1350 DEG C, calcining 4-5h, insulation 1-2h, last air cooling is to room temperature.
To the formation of its component and Action Specification as follows: red clay has good toughness, it is plastic that normal temperature meets water, micro-ly dry can to carve, half-driedly to press, absolutely dryly to grind, red clay burns to 900 DEG C and pottery can be become to fill water, burn to 1230 DEG C of then porcelain, can not absorb water completely and corrosion-and high-temp-resistant, join in pottery, the intensity of pottery can also be increased, improve the performance of rub resistance, and increase its work-ing life; Albite is as a kind of solvent materials in pottery, and the main porcelain that rises turns use into, and namely utilize the high temperature fusibility of sodium, reduce blank firing temperature, ex-colleague plays the effect of stable blank; Nano-aluminium oxide can improve the properties of pottery, the crystal grain of pottery, crystal boundary and the combination between them can be made all to be in nanometer level, the refinement number of grain boundaries of pottery is increased considerably, make the intensity of pottery, toughness and superplasticity greatly improve further, can ceramic sintering temperature be reduced; Zinc oxide, as a kind of important ceramic chemical industry flux raw material, has stronger fluxing action, can reduce the coefficient of expansion of pottery, improve its thermostability, and the machinery of pottery and electrical property can be made to improve; Niobium Pentxoxide in pottery as a kind of property-modifying additive; Boron nitride can improve the resistance to sudden heating of pottery, in rapid heat cycle situation, reduce the possibility of ceramic fracture, improve the thermostability of pottery, because boron nitride has the layered crystal structure being similar to graphite, also be just provided with physical and chemical performance like graphite-phase, make pottery electrical isolation, thermal expansivity and and most metals not infiltrate etc. in possess good performance; Nickel oxide can improve the corrosion resistance nature of pottery.
The effect of wollastonite is mainly reflected in the following aspects: one is reduce firing temperature, shorten firing period, traditional silicate ceramics mainly uses the Si-Al system raw materials such as quartz, feldspar, kaolinite, talcum, pyrophyllite, high temperature burns till the crystallisate phase mainly mullite of generation, add wollastonite, then can form Si-Al-Ca eutectic system, resultant phase mainly lime feldspar, just can realize sintering at a lower temperature, this wherein, wollastonite mainly plays the effect fluxing and reduce firing temperature.Meanwhile, because crystal form of grammite is pin column, the quick loss of moisture that can be in base substrate provides passage, thus accelerates drying rate, shortens drying cycle, enhances productivity; Two is reduce to burn till contraction and product defect, due to any fugitive constituents such as itself the not moisture and carbonates of wollastonite, does not produce gas in sintering process, greatly reduces the possibility that ceramic firing body produces gas hole defect, can significantly improve the quality of pottery; Three is reduce the thermal expansion in the wet swelling of base substrate and sintering process, and wollastonite itself does not absorb water, and can avoid the wet swelling of ceramic body, simultaneously, the thermal expansivity of wollastonite is little and linearly expand, and can reduce the thermal expansion of base substrate in sintering process, avoids producing expansion crack; Four is the physical strengths that can improve goods, and the rambling arrangement of wollastonite needle-like crystal forms pilotaxitic texture, by the melt institute consolidation that partial melting produces, can strengthen structural stability and the physical strength of sintered compact.
In sum, owing to have employed technique scheme, the invention has the beneficial effects as follows: not only intensity is high for new special stupalith of the present invention, resistance to corrosion and resistance of oxidation extremely strong, good toughness, high temperature resistant, and the rub resistance ability on its surface improves greatly, and surface is less scaling, simultaneously, by optimizing existing ceramic preparation technique, selecting suitable processing parameter, making the properties of new special stupalith more stable.
The present invention is not limited to aforesaid embodiment.The present invention expands to any new feature of disclosing in this manual or any combination newly, and the step of the arbitrary new method disclosed or process or any combination newly.
Claims (1)
1. an intelligent preparation method for the special addition agent of new special stupalith, it is characterized in that, it comprises the following steps:
Step 1: by place for each device, opens a kind of intelligent preparation system power supply of special addition agent of new special stupalith;
Step 2: dropped into by the kaolinite of predetermined dose 01 in shredding unit, trigger the trigger button one pulverized in module, after trigger button one first time is triggered, starts shredding unit, and to time block transmitting digital signals 001; Time block receives digital signaling zero 01, to PLC transmitting digital signals 101 after startup timing register one, 15min, and stops timing; PLC receives numerary signal 101, transmits executive signal 201 to valve control module, transmits executive signal 301 to delivery module simultaneously, transmits executive signal 501 to pulverizing module;
Step 3: pulverize module and receive executive signal 501, close shredding unit; Valve control module receives executive signal 201, opens magnetic valve one, closes after the scheduled time 01; Kaolinite after then pulverizing enters transport unit by magnetic valve one; Delivery module receives executive signal 301, starts transport unit, material is delivered to sieving equipment, crosses 40 mesh sieves; Obtain kaolinite powder;
Step 4: the trigger button triggering solvent modules, after described trigger button is triggered, open the magnetic valve of polyoxyethylene glycol case and deionization water tank, after the deionized water of the polyoxyethylene glycol of predetermined dose 01 and predetermined dose 02 is discarded to whipping appts, shut electromagnetic valve;
Step 5: trigger the trigger button two on whipping appts, after described trigger button two first time is triggered, starts whipping appts, and to time block transmitting digital signals 002; Time block receives digital signaling zero 02, to PLC transmitting digital signals 102 after startup timing register two, 15min, and stops timing; PLC receives numerary signal 102, transmits executive signal 401 to stirring module; Stir module and receive executive signal 401, close whipping appts;
Step 6: be added in whipping appts by kaolinite powder, triggers the trigger button two on whipping appts, after described trigger button two first time is triggered, starts whipping appts, and to time block transmitting digital signals 003; Time block receives digital signaling zero 03, to PLC transmitting digital signals 103 after startup timing register three, 20min, and stops timing; PLC receives numerary signal 103, transmits executive signal 402 to stirring module; Stir module and receive executive signal 402, close whipping appts;
Step 7: be added in whipping appts by the silane coupling agent kh-550 of predetermined dose 02, triggers the trigger button two on whipping appts, after described trigger button two third time is triggered, starts whipping appts, and to time block transmitting digital signals 004; Time block receives digital signaling zero 04, to PLC transmitting digital signals 104 after startup timing register four, 20min, and stops timing; PLC receives numerary signal 104, transmits executive signal 403 to stirring module; Stir module and receive executive signal 403, close whipping appts; Obtain liquid A;
Step 8: dropped into by the titanium dioxide of predetermined dose 03 in shredding unit, trigger the trigger button one pulverized in module, after trigger button one second time is triggered, starts shredding unit, and to time block transmitting digital signals 005; Time block receives digital signaling zero 05, to PLC transmitting digital signals 105 after startup timing register five, 15min; Receive numerary signal 105, transmit executive signal 202 to valve control module, transmit executive signal 302 to delivery module simultaneously, transmit executive signal 502 to pulverizing module;
Step 9: pulverize module and receive executive signal 502, close shredding unit; Valve control module receives executive signal 202, opens magnetic valve one, closes after the scheduled time 02; Titanium dioxide after then pulverizing enters transport unit by magnetic valve one; Delivery module receives executive signal 302, starts transport unit, material is delivered to sieving equipment and cross 40 mesh sieves; Obtain titania powder;
Step 10: titania powder, the nanometer silicon carbide of predetermined dose 04 and the nanometer boron fibre of predetermined dose 05 after sieving are added in whipping appts; Trigger the trigger button two on whipping appts, after described trigger button 2 is triggered for the 4th time, start whipping appts, and to time block transmitting digital signals 006; Time block receives digital signaling zero 06, to PLC transmitting digital signals 106 after startup timing register six, 20min; PLC receives numerary signal 106, transmits executive signal 404, and transmit executive signal 203 to valve control module to stirring module; Stir module and receive executive signal 404, close whipping appts; Valve control module receives executive signal 203, opens magnetic valve two; Then material enters in dry filtrating equipment;
Step 11: the liquid inductor block induced liquid in induction module flows through, and to PLC transmitting digital signals 010; PLC receives digital signaling zero 10, transmits executive signal 601 to filtration drying module; Filtration drying module receives executive signal 601, starts dry filtrating equipment;
Step 12: dropped into by the material after dry filter in shredding unit, trigger the trigger button one pulverized in module, after trigger button one third time is triggered, starts shredding unit, and to time block transmitting digital signals 007; Time block receives digital signaling zero 07, after starting timing register seven, 15min, to PLC transmitting digital signals 107; Receive numerary signal 107, transmit executive signal 204 to valve control module, transmit executive signal 303 to delivery module simultaneously, transmit executive signal 503 to pulverizing module;
Step 13: pulverize module and receive executive signal 503, close shredding unit; Valve control module receives executive signal 204, opens magnetic valve one, closes after the scheduled time 03; Material after then pulverizing enters transport unit by magnetic valve one; Delivery module receives executive signal 303, starts transport unit, material is delivered to sieving equipment and cross 120 mesh sieves;
Step 14: the material after sieving is placed in heating unit, the pressure transmitter induction material pressure T in induction module, as T>100N, to PLC transmitting digital signals 011; PLC receives digital signaling zero 11, transmits executive signal 701 to heating module, and transmits executive signal 205 to valve control module; Heating module receives executive signal 701, starts heating unit, and is heated to 823 DEG C; Valve control module receives executive signal 205, opens magnetic valve three, in heating unit, passes into helium, closes after the scheduled time 04; After the material calcining 3h after heating, air cooling is to room temperature;
Step 15: material step 14 obtained drops in shredding unit, triggers the trigger button one pulverized in module, after trigger button 1 is triggered for the 4th time, starts shredding unit, and to time block transmitting digital signals 008; Time block receives digital signaling zero 08, after starting timing register eight, 15min, to PLC transmitting digital signals 108; PLC receives numerary signal 108, transmits executive signal 206 to valve control module, transmits executive signal 304 to delivery module simultaneously, transmits executive signal 504 to pulverizing module;
Step 16: pulverize module executive signal 504, closes shredding unit; Valve control module receives executive signal 206, opens magnetic valve one, closes after the scheduled time 05; Delivery module executive signal 304, start transport unit, material is delivered to sieving equipment 50 mesh sieves, obtain auxiliary agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510895074.0A CN105418078B (en) | 2015-12-08 | 2015-12-08 | The intelligent preparation method of the special addition agent of special ceramic material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510895074.0A CN105418078B (en) | 2015-12-08 | 2015-12-08 | The intelligent preparation method of the special addition agent of special ceramic material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105418078A true CN105418078A (en) | 2016-03-23 |
| CN105418078B CN105418078B (en) | 2018-06-01 |
Family
ID=55496697
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510895074.0A Active CN105418078B (en) | 2015-12-08 | 2015-12-08 | The intelligent preparation method of the special addition agent of special ceramic material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105418078B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2786112Y (en) * | 2004-11-30 | 2006-06-07 | 张尚杰 | Full-automatic high-pressured grout forming production line |
| CN104355602A (en) * | 2014-10-29 | 2015-02-18 | 安徽省皖捷液压科技有限公司 | Special ceramic and preparation method thereof |
| CN204569745U (en) * | 2015-04-07 | 2015-08-19 | 内蒙古科技大学 | A kind of foamed ceramics production line |
-
2015
- 2015-12-08 CN CN201510895074.0A patent/CN105418078B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2786112Y (en) * | 2004-11-30 | 2006-06-07 | 张尚杰 | Full-automatic high-pressured grout forming production line |
| CN104355602A (en) * | 2014-10-29 | 2015-02-18 | 安徽省皖捷液压科技有限公司 | Special ceramic and preparation method thereof |
| CN204569745U (en) * | 2015-04-07 | 2015-08-19 | 内蒙古科技大学 | A kind of foamed ceramics production line |
Non-Patent Citations (1)
| Title |
|---|
| 江伴东 等: "PLC可编程控制器在日用陶瓷生产线上应用", 《中国陶瓷》 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105418078B (en) | 2018-06-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107399988B (en) | Method for preparing alumina-silicon carbide composite porous ceramic by using aluminum-silicon industrial waste residues | |
| CN112125651B (en) | Preparation method of compact calcium hexaluminate-corundum complex phase ceramic | |
| CN105418054B (en) | A kind of preparation method of special ceramic material | |
| CN101734910B (en) | Method for preparing porous alumina ceramic core | |
| CN105130410B (en) | A kind of preparation method of Fast back-projection algorithm CBN grinding tool vitrified bonds | |
| CN105503160B (en) | A kind of alumina ceramic chip of new-energy automobile quaternary system 95 and its processing method | |
| CN103351165A (en) | Porous ceramic prepared by adopting different inorganic binders and preparation method thereof | |
| CN103013442A (en) | Alpha-alumina-based abrasive and preparation method thereof | |
| CN104371703B (en) | A kind of method that petroleum fracturing propping agent is prepared by raw material of aluminous fly-ash | |
| CN105481347A (en) | Novel special ceramic material and preparation method thereof | |
| CN101423412B (en) | Method for preparing high performance silicon oxide combining silicon carbide refractory by low-temperature sintering | |
| CN205223027U (en) | Novel intelligent preparation system of special auxiliary agent of special ceramics material | |
| CN109399941A (en) | A method of micro-crystalline ceramic is prepared using flyash and waste slag | |
| CN105439620A (en) | Method for preparing porous silicon nitride by spark plasma sintering | |
| CN104446459B (en) | Preparation method for the Bubble zirconia insulating product of tungsten sintering intermediate frequency furnace | |
| CN104556879A (en) | Method for preparing square brick | |
| CN103755265B (en) | Preparation method of high-strength square brick | |
| CN104496432A (en) | Preparation method of modified sintered corundum | |
| CN105418078A (en) | Intelligent preparation method of special aid for novel special ceramic material | |
| CN105399402A (en) | System and method for intelligent preparation of novel special ceramic material | |
| CN205205029U (en) | Novel intelligent preparation system of special ceramics material | |
| CN105404233A (en) | Intelligent preparation system and intelligent preparation method of special assistant of novel special ceramic material | |
| CN102701612A (en) | Manufacturing method of composite phosphorus slag powder | |
| CN102731129B (en) | Method for preparing composite fracturing propping agent by using gold tailings and forsterite fibers | |
| CN105108665A (en) | Ceramic bond abrasive disc and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information |
Inventor after: Cui Changrui Inventor after: Zhao Dezhi Inventor before: Zeng Li |
|
| CB03 | Change of inventor or designer information | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20180502 Address after: 221200 Suining airport in Xuzhou County, Jiangsu province. Applicant after: JIANGSU ZHONGCHENG COMPOSITE MATERIAL CO., LTD. Address before: 610000 No. 1, 5, No. 31, 1 south two section, Wuhou District first ring road, Chengdu, Sichuan. Applicant before: CHENGDU DESHANNENG TECHNOLOGY CO., LTD. |
|
| TA01 | Transfer of patent application right | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20190429 Address after: 050000 No. 42 Qianjin Street, Beipucheng Village, Zhangjiazhuang Town, Gaocheng District, Shijiazhuang City, Hebei Province Patentee after: Pei Huiyong Address before: 221200 Suining airport in Xuzhou County, Jiangsu province. Patentee before: JIANGSU ZHONGCHENG COMPOSITE MATERIAL CO., LTD. |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20190513 Address after: 221200 Suining airport in Xuzhou County, Jiangsu province. Patentee after: JIANGSU ZHONGCHENG COMPOSITE MATERIAL CO., LTD. Address before: 050000 No. 42 Qianjin Street, Beipucheng Village, Zhangjiazhuang Town, Gaocheng District, Shijiazhuang City, Hebei Province Patentee before: Pei Huiyong |
|
| TR01 | Transfer of patent right |