CN105410897B - A kind of preparation method of mulberry leaf particle - Google Patents
A kind of preparation method of mulberry leaf particle Download PDFInfo
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- CN105410897B CN105410897B CN201510753220.6A CN201510753220A CN105410897B CN 105410897 B CN105410897 B CN 105410897B CN 201510753220 A CN201510753220 A CN 201510753220A CN 105410897 B CN105410897 B CN 105410897B
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- leaf
- extraction
- filtration
- bamboo
- added
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- 240000000249 Morus alba Species 0.000 title claims abstract description 72
- 235000008708 Morus alba Nutrition 0.000 title claims abstract description 72
- 239000002245 particle Substances 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 238000000605 extraction Methods 0.000 claims abstract description 109
- 238000010438 heat treatment Methods 0.000 claims abstract description 80
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 76
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 54
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 54
- 241001330002 Bambuseae Species 0.000 claims abstract description 54
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 54
- 239000011425 bamboo Substances 0.000 claims abstract description 54
- 238000001914 filtration Methods 0.000 claims abstract description 50
- 239000000284 extract Substances 0.000 claims abstract description 44
- 235000019441 ethanol Nutrition 0.000 claims abstract description 39
- 238000005119 centrifugation Methods 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 235000013305 food Nutrition 0.000 claims abstract description 14
- 239000000463 material Substances 0.000 claims abstract description 13
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 238000005469 granulation Methods 0.000 claims abstract description 5
- 230000003179 granulation Effects 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims abstract description 3
- 239000011347 resin Substances 0.000 claims description 18
- 229920005989 resin Polymers 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 4
- 239000006071 cream Substances 0.000 claims 1
- 238000002386 leaching Methods 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- 238000004064 recycling Methods 0.000 description 6
- 239000002893 slag Substances 0.000 description 6
- 235000001014 amino acid Nutrition 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 4
- 230000036541 health Effects 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 230000003712 anti-aging effect Effects 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- -1 Coumarins lactones Chemical class 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
- 240000003915 Lophatherum gracile Species 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 description 2
- 230000000975 bioactive effect Effects 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
- 230000008030 elimination Effects 0.000 description 2
- 238000003379 elimination reaction Methods 0.000 description 2
- XIRNKXNNONJFQO-UHFFFAOYSA-N ethyl hexadecanoate Chemical compound CCCCCCCCCCCCCCCC(=O)OCC XIRNKXNNONJFQO-UHFFFAOYSA-N 0.000 description 2
- LHGVFZTZFXWLCP-UHFFFAOYSA-N guaiacol Chemical compound COC1=CC=CC=C1O LHGVFZTZFXWLCP-UHFFFAOYSA-N 0.000 description 2
- IUJAMGNYPWYUPM-UHFFFAOYSA-N hentriacontane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCC IUJAMGNYPWYUPM-UHFFFAOYSA-N 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- KQNPFQTWMSNSAP-UHFFFAOYSA-N isobutyric acid Chemical compound CC(C)C(O)=O KQNPFQTWMSNSAP-UHFFFAOYSA-N 0.000 description 2
- FGKJLKRYENPLQH-UHFFFAOYSA-N isocaproic acid Chemical compound CC(C)CCC(O)=O FGKJLKRYENPLQH-UHFFFAOYSA-N 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- SCWKRWCUMCMVPW-UHFFFAOYSA-N phenyl n-methylcarbamate Chemical group CNC(=O)OC1=CC=CC=C1 SCWKRWCUMCMVPW-UHFFFAOYSA-N 0.000 description 2
- KZJWDPNRJALLNS-VJSFXXLFSA-N sitosterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CC[C@@H](CC)C(C)C)[C@@]1(C)CC2 KZJWDPNRJALLNS-VJSFXXLFSA-N 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 description 2
- XYHKNCXZYYTLRG-UHFFFAOYSA-N 1h-imidazole-2-carbaldehyde Chemical compound O=CC1=NC=CN1 XYHKNCXZYYTLRG-UHFFFAOYSA-N 0.000 description 1
- GOLORTLGFDVFDW-UHFFFAOYSA-N 3-(1h-benzimidazol-2-yl)-7-(diethylamino)chromen-2-one Chemical compound C1=CC=C2NC(C3=CC4=CC=C(C=C4OC3=O)N(CC)CC)=NC2=C1 GOLORTLGFDVFDW-UHFFFAOYSA-N 0.000 description 1
- GWYFCOCPABKNJV-UHFFFAOYSA-M 3-Methylbutanoic acid Natural products CC(C)CC([O-])=O GWYFCOCPABKNJV-UHFFFAOYSA-M 0.000 description 1
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- 244000003416 Asparagus officinalis Species 0.000 description 1
- 235000005340 Asparagus officinalis Nutrition 0.000 description 1
- JMGZEFIQIZZSBH-UHFFFAOYSA-N Bioquercetin Natural products CC1OC(OCC(O)C2OC(OC3=C(Oc4cc(O)cc(O)c4C3=O)c5ccc(O)c(O)c5)C(O)C2O)C(O)C(O)C1O JMGZEFIQIZZSBH-UHFFFAOYSA-N 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- 239000005715 Fructose Substances 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 1
- OVSQVDMCBVZWGM-IDRAQACASA-N Hirsutrin Natural products O([C@H]1[C@H](O)[C@H](O)[C@H](O)[C@@H](CO)O1)C1=C(c2cc(O)c(O)cc2)Oc2c(c(O)cc(O)c2)C1=O OVSQVDMCBVZWGM-IDRAQACASA-N 0.000 description 1
- FVQOMEDMFUMIMO-UHFFFAOYSA-N Hyperosid Natural products OC1C(O)C(O)C(CO)OC1OC1C(=O)C2=C(O)C=C(O)C=C2OC1C1=CC=C(O)C(O)=C1 FVQOMEDMFUMIMO-UHFFFAOYSA-N 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- 240000002014 Phyllostachys nigra var. henonis Species 0.000 description 1
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 description 1
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 description 1
- 229930182558 Sterol Natural products 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 244000223014 Syzygium aromaticum Species 0.000 description 1
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 208000007536 Thrombosis Diseases 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 230000002929 anti-fatigue Effects 0.000 description 1
- 230000003579 anti-obesity Effects 0.000 description 1
- 230000001754 anti-pyretic effect Effects 0.000 description 1
- 230000000840 anti-viral effect Effects 0.000 description 1
- 239000000729 antidote Substances 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 239000002221 antipyretic Substances 0.000 description 1
- ZYGHJZDHTFUPRJ-UHFFFAOYSA-N benzo-alpha-pyrone Natural products C1=CC=C2OC(=O)C=CC2=C1 ZYGHJZDHTFUPRJ-UHFFFAOYSA-N 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- GWYFCOCPABKNJV-UHFFFAOYSA-N beta-methyl-butyric acid Natural products CC(C)CC(O)=O GWYFCOCPABKNJV-UHFFFAOYSA-N 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 235000015165 citric acid Nutrition 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 235000001671 coumarin Nutrition 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- IVTMALDHFAHOGL-UHFFFAOYSA-N eriodictyol 7-O-rutinoside Natural products OC1C(O)C(O)C(C)OC1OCC1C(O)C(O)C(O)C(OC=2C=C3C(C(C(O)=C(O3)C=3C=C(O)C(O)=CC=3)=O)=C(O)C=2)O1 IVTMALDHFAHOGL-UHFFFAOYSA-N 0.000 description 1
- 125000005909 ethyl alcohol group Chemical group 0.000 description 1
- 229940067592 ethyl palmitate Drugs 0.000 description 1
- 201000005577 familial hyperlipidemia Diseases 0.000 description 1
- 239000006025 fining agent Substances 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 235000011087 fumaric acid Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 235000013922 glutamic acid Nutrition 0.000 description 1
- 239000004220 glutamic acid Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000036449 good health Effects 0.000 description 1
- 235000011868 grain product Nutrition 0.000 description 1
- 229960001867 guaiacol Drugs 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- CDAISMWEOUEBRE-GPIVLXJGSA-N inositol Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@H](O)[C@@H]1O CDAISMWEOUEBRE-GPIVLXJGSA-N 0.000 description 1
- 229960000367 inositol Drugs 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- GXMWXESSGGEWEM-UHFFFAOYSA-N isoquercitrin Natural products OCC(O)C1OC(OC2C(Oc3cc(O)cc(O)c3C2=O)c4ccc(O)c(O)c4)C(O)C1O GXMWXESSGGEWEM-UHFFFAOYSA-N 0.000 description 1
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- MQYXUWHLBZFQQO-QGTGJCAVSA-N lupeol Chemical compound C1C[C@H](O)C(C)(C)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C)CC[C@@H](C(=C)C)[C@@H]5[C@H]4CC[C@@H]3[C@]21C MQYXUWHLBZFQQO-QGTGJCAVSA-N 0.000 description 1
- PKGKOZOYXQMJNG-UHFFFAOYSA-N lupeol Natural products CC(=C)C1CC2C(C)(CCC3C4(C)CCC5C(C)(C)C(O)CCC5(C)C4CCC23C)C1 PKGKOZOYXQMJNG-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- 208000015122 neurodegenerative disease Diseases 0.000 description 1
- 229940100688 oral solution Drugs 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
- 235000005875 quercetin Nutrition 0.000 description 1
- 229960001285 quercetin Drugs 0.000 description 1
- OVSQVDMCBVZWGM-QSOFNFLRSA-N quercetin 3-O-beta-D-glucopyranoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=C(C=2C=C(O)C(O)=CC=2)OC2=CC(O)=CC(O)=C2C1=O OVSQVDMCBVZWGM-QSOFNFLRSA-N 0.000 description 1
- XXHSUYNZCSBPBG-GZIDCZEMSA-N quercetin 3-beta-gentiotrioside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)[C@H](OC[C@@H]2[C@H]([C@H](O)[C@@H](O)[C@H](OC=3C(C4=C(O)C=C(O)C=C4OC=3C=3C=C(O)C(O)=CC=3)=O)O2)O)O1 XXHSUYNZCSBPBG-GZIDCZEMSA-N 0.000 description 1
- FDRQPMVGJOQVTL-UHFFFAOYSA-N quercetin rutinoside Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC=2C(C3=C(O)C=C(O)C=C3OC=2C=2C=C(O)C(O)=CC=2)=O)O1 FDRQPMVGJOQVTL-UHFFFAOYSA-N 0.000 description 1
- XXHSUYNZCSBPBG-UHFFFAOYSA-N quercetin-3-gentotrioside Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OCC2C(C(O)C(O)C(OC=3C(C4=C(O)C=C(O)C=C4OC=3C=3C=C(O)C(O)=CC=3)=O)O2)O)O1 XXHSUYNZCSBPBG-UHFFFAOYSA-N 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 235000005493 rutin Nutrition 0.000 description 1
- ALABRVAAKCSLSC-UHFFFAOYSA-N rutin Natural products CC1OC(OCC2OC(O)C(O)C(O)C2O)C(O)C(O)C1OC3=C(Oc4cc(O)cc(O)c4C3=O)c5ccc(O)c(O)c5 ALABRVAAKCSLSC-UHFFFAOYSA-N 0.000 description 1
- IKGXIBQEEMLURG-BKUODXTLSA-N rutin Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@@H]1OC[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](OC=2C(C3=C(O)C=C(O)C=C3OC=2C=2C=C(O)C(O)=CC=2)=O)O1 IKGXIBQEEMLURG-BKUODXTLSA-N 0.000 description 1
- 229960004555 rutoside Drugs 0.000 description 1
- CDAISMWEOUEBRE-UHFFFAOYSA-N scyllo-inosotol Natural products OC1C(O)C(O)C(O)C(O)C1O CDAISMWEOUEBRE-UHFFFAOYSA-N 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 229940005605 valeric acid Drugs 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 150000008498 β-D-glucosides Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of preparation methods of mulberry leaf particle, including：The leaf of bamboo, which is added in ethyl alcohol, after crushing carries out primary heating extraction, and an extracting solution and a filter residue is obtained by filtration；Ethyl alcohol is added into a filter residue and carries out secondary temperature elevation extraction, secondary raffinate and secondary filter residue is obtained by filtration；Ethyl alcohol is added into secondary filter residue again and carries out heating extraction three times, extracting solution three times is obtained by filtration；By an extracting solution, secondary raffinate and extracting solution mixes three times, then purifies and separates after centrifugation are concentrated to give leaf of bamboo medicinal extract；After mulberry leaf and water mix after crushing, four heating extractions are carried out, No. four extracting solutions and four filter residues are obtained by filtration；Water is added into four filter residues and carries out five heating extractions, No. five extracting solutions are obtained by filtration；No. four extracting solutions and No. five extracting solutions are mixed, then purifies and separates after centrifugation are concentrated to give mulberry extract；Leaf of bamboo medicinal extract and mulberry extract are mixed, food auxiliary material is added and stirs evenly, granulation obtains mulberry leaf particle.
Description
Technical field
The present invention relates to health products processing technique field more particularly to a kind of preparation methods of mulberry leaf particle.
Background technology
Contain abundant rutin, Quercetin, Isoquercitrin, moracetin, cupreol, dish in mulberry leaf
Oily sterol, cupreol, β-D- glucosides, Lupeol, meso inositol etc..Contain acetic acid, propionic acid, fourth in volatile oil component
Acid, isobutyric acid, valeric acid, isovaleric acid, caproic acid, isocaproic acid, gaultherolin, guaiacol, adjacent phenyl methylcarbamate, phenyl methylcarbamate, cloves
Oily phenol etc., and containing oxalic acid, fumaric acid, tartaric acid, citric acid, succinic acid, palmitic acid, ethyl palmitate, hentriacontane, hydroxyl
The amino acid such as coumarin, sucrose, fructose, glucose, lucid asparagus amino acid and glutamic acid.Wherein 5 kinds of flavonoid active substance, micro
12 kinds of element, 5 kinds of amino acid.These bioactive ingredients have considerably more intense anti-aging, hypertension and hyperlipemia, reduce cholesterol,
Inhibit Fat Accumulation, inhibit thrombus life, antipyretic and antidote functions, free radical superfluous in organism can be removed well, prevent body
The effects that inner lipid peroxidating, improves the immunity of the human body, anti-aging.Mulberry leaf also have good beautifying skin and antiobesity action,
Especially the acne brown class of face is had a better effect.
In the leaf of bamboo containing 6 kinds of amino acid, flavones, phenolic compound, bioactive polysaccharide, Coumarins lactones, fragrance at
Point and various trace elements.The various trace elements that the leaf of bamboo contains have close relationship to the good health and a long life of human body.And the leaf of bamboo carries
Take liquid that there is antiactive oxygen free radical, anti-oxidant, anti-aging, antiviral and antifatigue, adjusting blood fat, the old degenerative disease of prevention
The biological effectiveness such as disease.
Invention content
In order to give full play to mulberry leaf, leaf of bamboo nutrition and health care of food function, mulberry leaf series of products are further developed and used, this
Invention provides a kind of preparation method of mulberry leaf particle.
A kind of preparation method of mulberry leaf particle proposed by the present invention, includes the following steps：
S1, in leaf of bamboo addition ethyl alcohol after crushing will once heat up and extract, an extracting solution is obtained by filtration and is filtered with primary
Slag；Ethyl alcohol is added into a filter residue and carries out secondary temperature elevation extraction, secondary raffinate and secondary filter residue is obtained by filtration；Again to secondary
Ethyl alcohol is added in filter residue and carries out heating extraction three times, extracting solution three times is obtained by filtration；By an extracting solution, secondary raffinate and three
Secondary extracting solution mixing, recycles ethyl alcohol, macroporous resin column purifies and separates is carried out after centrifugation, are then concentrated to give leaf of bamboo medicinal extract；
S2, after mixing mulberry leaf after crushing and water, four heatings is carried out and are extracted, No. four extracting solutions are obtained by filtration and four times are filtered
Slag；Water is added into four filter residues and carries out five heating extractions, No. five extracting solutions are obtained by filtration；No. four extracting solutions and five times are carried
It takes liquid to mix, macroporous resin column purifies and separates is carried out after centrifugation, are then concentrated to give mulberry extract；
S3, leaf of bamboo medicinal extract and mulberry extract are mixed, adds food auxiliary material and stirs evenly, granulation obtains mulberry leaf particle.
Wherein, the leaf of bamboo and mulberry leaf should first carry out cleaning impurity elimination, then crush, extraction.
The leaf of bamboo is the leaf of grass henon bamboo (bamboo), is authorized by state and the edible and medicinal natural plants of approval.
The leaf of bamboo includes two kinds of the fresh leaf of bamboo and lophatherum gracile, wherein the fresh leaf of bamboo is the fresh leaf of bamboo, lophatherum gracile is the leaf of bamboo after drying.
Preferably, in S1, the leaf of bamboo is added 115~125 parts a concentration of 30~55% after by weight crushing 28~32 parts
Ethyl alcohol in carry out primary heating extraction, an extracting solution and a filter residue is obtained by filtration；75~85 are added into a filter residue
The ethyl alcohol of part a concentration of 50~65% carries out secondary temperature elevation extraction, and secondary raffinate and secondary filter residue is obtained by filtration；Again to secondary
55~65 parts a concentration of 50~60% of ethyl alcohol is added in filter residue and carries out heating extraction three times, extracting solution three times is obtained by filtration；It will
Extracting solution, secondary raffinate and extracting solution mixing three times, recycling ethyl alcohol to relative density at 40 DEG C are 1.2~1.5, centrifugation
Macroporous resin column purifies and separates are carried out afterwards, are then concentrated to give leaf of bamboo medicinal extract.
Preferably, in S1, the temperature of primary heating extraction is 88~92 DEG C, time of primary heating extraction is 0.8~
1.2h。
Preferably, in S1, secondary temperature elevation extraction temperature be 83~87 DEG C, secondary temperature elevation extraction time be 0.8~
1.2h。
Preferably, in S1, the temperature of the extraction that heats up three times is 83~87 DEG C, time of the extraction that heats up three times is 35~
45min。
Preferably, in S2, four times heating extraction temperature be 88~92 DEG C, four times heating extraction times be 0.7~
1.3h。
Preferably, in S2, five times heating extraction temperature be 88~92 DEG C, five times heating extraction times be 0.8~
1.2h。
Preferably, in S2, after mulberry leaf and 75~85 parts of water mix after by weight crushing 18~23 parts, rise for four times
Temperature extraction, is obtained by filtration No. four extracting solutions and four filter residues；55~65 parts of water five heatings of progress are added into four filter residues to carry
It takes, No. five extracting solutions is obtained by filtration；No. four extracting solutions and No. five extracting solutions are mixed, macroporous resin column purifying point is carried out after centrifugation
From being then concentrated to give mulberry extract.
Preferably, in S3, the weight ratio of leaf of bamboo medicinal extract, mulberry extract and food auxiliary material is 0.8~1.1：0.9~1.2：
2.5~3.5.Wherein auxiliary material includes corrigent, fining agent, preservative etc., but oral solution auxiliary material with retain to greatest extent effectively at
It for the purpose of dividing and improving mouthfeel, therefore can be adjusted according to actual needs in process of production, without being defined.
Preferably, mulberry leaf plucking time is annual April to November, and leaf of bamboo plucking time is annual December to next year 3
Month.
The present invention obtains mulberry leaf particle using picking leaves, cleaning, impurity elimination, crushing, extraction, upper prop, concentration, mixing, granulation, most
The reservation of limits and the nutriment and active constituent extracted with mulberry leaf using the leaf of bamboo, have higher food nutrition and health care
Effect further develops and uses for the leaf of bamboo and mulberry leaf and provides new way, enriches the leaf of bamboo and mulberry leaf product line.
Particle is made by using mulberry extract and leaf of bamboo medicinal extract in the present invention, not only improves mulberry leaf and leaf of bamboo use value,
More rich mulberry leaf develop with leaf of bamboo series of products；The field of deep for having expanded mulberry leaf and the leaf of bamboo simultaneously, due to China's mulberry leaf
In the ascendant with leaf of bamboo exploitation, the present invention prepares auxotype particle using addition mulberry leaf with the leaf of bamboo, and that has widened product applies model
It encloses；The intension for also improving mulberry leaf grain products has played the development and utilization of the food, health product of integration of drinking and medicinal herbs, to day
Right plant exploitation has more far-reaching revolution meaning.
Specific implementation mode
In the following, technical scheme of the present invention is described in detail by specific embodiment.
Embodiment 1
A kind of preparation method of mulberry leaf particle proposed by the present invention, includes the following steps：
S1, by weight will 28 parts crush after the leaf of bamboo be added in 125 parts a concentration of 30% of ethyl alcohol and carry out primary heating and carry
It takes, the temperature of primary heating extraction is 92 DEG C, and the time of primary heating extraction is 0.8h, and an extracting solution and primary is obtained by filtration
Filter residue；85 parts a concentration of 50% of ethyl alcohol is added into a filter residue and carries out secondary temperature elevation extraction, the temperature of secondary temperature elevation extraction
It it is 87 DEG C, the time of secondary temperature elevation extraction is 0.8h, and secondary raffinate and secondary filter residue is obtained by filtration；Add again into secondary filter residue
Enter 65 parts a concentration of 50% of ethyl alcohol and carry out heating extraction three times, extracting solution three times is obtained by filtration, the temperature for the extraction that heats up three times
It it is 87 DEG C, the time for the extraction that heats up three times is 35min；By an extracting solution, secondary raffinate and extracting solution mixes three times, recycling
Ethyl alcohol to relative density at 40 DEG C is 1.5, and macroporous resin column purifies and separates are carried out after centrifugation, are then concentrated to give leaf of bamboo medicinal extract；
S2, after by weight mixing mulberry leaf after 18 parts of crushing and 85 parts of water, four heating extractions are carried out, four heatings carry
The temperature taken is 88 DEG C, and the time of four heating extractions is 1.3h, and No. four extracting solutions and four filter residues are obtained by filtration；Xiang Sici is filtered
55 parts of water are added in slag and carry out five heating extractions, the temperature of five heating extractions are 92 DEG C, and the times of five heating extractions are
No. five extracting solutions are obtained by filtration in 0.8h；No. four extracting solutions and No. five extracting solutions are mixed, macroporous resin column purifying is carried out after centrifugation
Separation, is then concentrated to give mulberry extract；
S3,1.1 parts of leaf of bamboo medicinal extract and 0.9 part of mulberry extract are mixed by weight, adds 3.5 parts of food auxiliary materials stirrings
Uniformly, it is granulated and obtains mulberry leaf particle.
Embodiment 2
A kind of preparation method of mulberry leaf particle proposed by the present invention, includes the following steps：
S1, by weight will 32 parts crush after the leaf of bamboo be added in 115 parts a concentration of 55% of ethyl alcohol and carry out primary heating and carry
It takes, the temperature of primary heating extraction is 88 DEG C, and the time of primary heating extraction is 1.2h, and an extracting solution and primary is obtained by filtration
Filter residue；75 parts a concentration of 65% of ethyl alcohol is added into a filter residue and carries out secondary temperature elevation extraction, the temperature of secondary temperature elevation extraction
It it is 83 DEG C, the time of secondary temperature elevation extraction is 1.2h, and secondary raffinate and secondary filter residue is obtained by filtration；Add again into secondary filter residue
Enter 55 parts a concentration of 60% of ethyl alcohol and carry out heating extraction three times, extracting solution three times is obtained by filtration, the temperature for the extraction that heats up three times
It it is 83 DEG C, the time for the extraction that heats up three times is 45min；By an extracting solution, secondary raffinate and extracting solution mixes three times, recycling
Ethyl alcohol to relative density at 40 DEG C is 1.2, and macroporous resin column purifies and separates are carried out after centrifugation, are then concentrated to give leaf of bamboo medicinal extract；
S2, after by weight mixing mulberry leaf after 23 parts of crushing and 75 parts of water, four heating extractions are carried out, four heatings carry
The temperature taken is 92 DEG C, and the time of four heating extractions is 0.7h, and No. four extracting solutions and four filter residues are obtained by filtration；Xiang Sici is filtered
65 parts of water are added in slag and carry out five heating extractions, the temperature of five heating extractions are 88 DEG C, and the times of five heating extractions are
No. five extracting solutions are obtained by filtration in 1.2h；No. four extracting solutions and No. five extracting solutions are mixed, macroporous resin column purifying is carried out after centrifugation
Separation, is then concentrated to give mulberry extract；
S3,0.8 part of leaf of bamboo medicinal extract and 1.2 parts of mulberry extracts mixed by weight, adds 2.5 parts of food auxiliary materials stirrings
Uniformly, it is granulated and obtains mulberry leaf particle.
Embodiment 3
A kind of preparation method of mulberry leaf particle proposed by the present invention, includes the following steps：
S1, by weight will 29 parts crush after the leaf of bamboo be added in 122 parts a concentration of 35% of ethyl alcohol and carry out primary heating and carry
It takes, the temperature of primary heating extraction is 91 DEG C, and the time of primary heating extraction is 0.9h, and an extracting solution and primary is obtained by filtration
Filter residue；82 parts a concentration of 55% of ethyl alcohol is added into a filter residue and carries out secondary temperature elevation extraction, the temperature of secondary temperature elevation extraction
It it is 86 DEG C, the time of secondary temperature elevation extraction is 0.9h, and secondary raffinate and secondary filter residue is obtained by filtration；Add again into secondary filter residue
Enter 63 parts a concentration of 52% of ethyl alcohol and carry out heating extraction three times, extracting solution three times is obtained by filtration, the temperature for the extraction that heats up three times
It it is 86 DEG C, the time for the extraction that heats up three times is 38min；By an extracting solution, secondary raffinate and extracting solution mixes three times, recycling
Ethyl alcohol to relative density at 40 DEG C is 1.4, and macroporous resin column purifies and separates are carried out after centrifugation, are then concentrated to give leaf of bamboo medicinal extract；
S2, after by weight mixing mulberry leaf after 19 parts of crushing and 82 parts of water, four heating extractions are carried out, four heatings carry
The temperature taken is 89 DEG C, and the time of four heating extractions is 1.2h, and No. four extracting solutions and four filter residues are obtained by filtration；Xiang Sici is filtered
63 parts of water are added in slag and carry out five heating extractions, the temperature of five heating extractions are 89 DEG C, and the times of five heating extractions are
No. five extracting solutions are obtained by filtration in 1.1h；No. four extracting solutions and No. five extracting solutions are mixed, macroporous resin column purifying is carried out after centrifugation
Separation, is then concentrated to give mulberry extract；
S3,0.9 part of leaf of bamboo medicinal extract and 1.1 parts of mulberry extracts mixed by weight, adds 2.8 parts of food auxiliary materials stirrings
Uniformly, it is granulated and obtains mulberry leaf particle.
Embodiment 4
A kind of preparation method of mulberry leaf particle proposed by the present invention, includes the following steps：
S1, by weight will 31 parts crush after the leaf of bamboo be added in 118 parts a concentration of 50% of ethyl alcohol and carry out primary heating and carry
It takes, the temperature of primary heating extraction is 89 DEG C, and the time of primary heating extraction is 1.1h, and an extracting solution and primary is obtained by filtration
Filter residue；78 parts a concentration of 60% of ethyl alcohol is added into a filter residue and carries out secondary temperature elevation extraction, the temperature of secondary temperature elevation extraction
It it is 84 DEG C, the time of secondary temperature elevation extraction is 1.1h, and secondary raffinate and secondary filter residue is obtained by filtration；Add again into secondary filter residue
Enter 57 parts a concentration of 58% of ethyl alcohol and carry out heating extraction three times, extracting solution three times is obtained by filtration, the temperature for the extraction that heats up three times
It it is 84 DEG C, the time for the extraction that heats up three times is 42min；By an extracting solution, secondary raffinate and extracting solution mixes three times, recycling
Ethyl alcohol to relative density at 40 DEG C is 1.3, and macroporous resin column purifies and separates are carried out after centrifugation, are then concentrated to give leaf of bamboo medicinal extract；
S2, after by weight mixing mulberry leaf after 22 parts of crushing and 78 parts of water, four heating extractions are carried out, four heatings carry
The temperature taken is 91 DEG C, and the time of four heating extractions is 0.8h, and No. four extracting solutions and four filter residues are obtained by filtration；Xiang Sici is filtered
57 parts of water are added in slag and carry out five heating extractions, the temperature of five heating extractions are 91 DEG C, and the times of five heating extractions are
No. five extracting solutions are obtained by filtration in 0.9h；No. four extracting solutions and No. five extracting solutions are mixed, macroporous resin column purifying is carried out after centrifugation
Separation, is then concentrated to give mulberry extract；
S3,1 part of leaf of bamboo medicinal extract and 1 part of mulberry extract mixed by weight, it is equal adds 3.3 parts of food auxiliary materials stirrings
Even, granulation obtains mulberry leaf particle.
Embodiment 5
A kind of preparation method of mulberry leaf particle proposed by the present invention, includes the following steps：
S1,300kg is crushed after the leaf of bamboo be added in the ethyl alcohol of 1200kg a concentration of 45% and carry out primary heating extraction, once
The temperature of heating extraction is 90 DEG C, and the time of primary heating extraction is 1h, and an extracting solution and a filter residue is obtained by filtration；Xiang Yi
In secondary filter residue be added 800kg a concentration of 58% ethyl alcohol carry out secondary temperature elevation extraction, secondary temperature elevation extraction temperature be 85 DEG C, two
The time of secondary heating extraction is 1h, and secondary raffinate and secondary filter residue is obtained by filtration；600kg concentration is added into secondary filter residue again
Heating extraction three times is carried out for 55% ethyl alcohol, extracting solution three times is obtained by filtration, the temperature for the extraction that heats up three times is 85 DEG C, three times
The time of heating extraction is 40min；By an extracting solution, secondary raffinate and extracting solution mixes three times, and recycling ethyl alcohol is to 40 DEG C
When relative density be 1.35, after centrifugation carry out macroporous resin column purifies and separates, be then concentrated to give leaf of bamboo medicinal extract；
S2,200kg is crushed after mulberry leaf and 800kg water mixing after, carry out four times heating extraction, four times heating extraction temperature
Degree is 90 DEG C, and the time of four heating extractions is 1h, and No. four extracting solutions and four filter residues are obtained by filtration；It is added into four filter residues
600kg water carries out five heating extractions, and the temperature of five heating extractions is 90 DEG C, and the time of five heating extractions is 1h, filtering
Obtain No. five extracting solutions；No. four extracting solutions and No. five extracting solutions are mixed, macroporous resin column purifies and separates are carried out after centrifugation, then
It is concentrated to give mulberry extract；
S3, leaf of bamboo medicinal extract and mulberry extract are mixed, adds food auxiliary material and stir evenly, wherein leaf of bamboo medicinal extract, mulberry leaf
The weight ratio of medicinal extract and food auxiliary material is 1:1:3, it is then granulated and obtains mulberry leaf particle.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (4)
1. a kind of preparation method of mulberry leaf particle, which is characterized in that include the following steps：
S1, the leaf of bamboo after crushing is added in a concentration of 30~55% ethyl alcohol once heat up and is extracted, primary extraction is obtained by filtration
Liquid and a filter residue；A concentration of 50~65% ethyl alcohol is added into a filter residue and carries out secondary temperature elevation extraction, is obtained by filtration secondary
Extracting solution and secondary filter residue；The ethyl alcohol for being added a concentration of 50~60% into secondary filter residue again carries out heating extraction three times, filtering
Obtain extracting solution three times；By an extracting solution, secondary raffinate and extracting solution mixes three times, recycles ethyl alcohol, is carried out after centrifugation big
Hole resin column purifies and separates, are then concentrated to give leaf of bamboo medicinal extract；
S2, after mixing mulberry leaf after crushing and water, four heatings is carried out and are extracted, No. four extracting solutions and four filter residues are obtained by filtration；
Water is added into four filter residues and carries out five heating extractions, No. five extracting solutions are obtained by filtration；No. four extracting solutions and five times are extracted
Liquid mixes, and macroporous resin column purifies and separates are carried out after centrifugation, are then concentrated to give mulberry extract；Four times the temperature extracted that heats up is
88~92 DEG C, the time of four heating extractions is 0.7~1.3h；The temperature of five heating extractions is 88~92 DEG C, five heatings
The time of extraction is 0.8~1.2h；
S3, leaf of bamboo medicinal extract and mulberry extract are mixed, adds food auxiliary material and stirs evenly, granulation obtains mulberry leaf particle；
In S1, the temperature of primary heating extraction is 88~92 DEG C, and the time of primary heating extraction is 0.8~1.2h, secondary temperature elevation
The temperature of extraction is 83~87 DEG C, and the time of secondary temperature elevation extraction is 0.8~1.2h, and the temperature for the extraction that heats up three times is 83~87
DEG C, the time for the extraction that heats up three times is 35~45min；
In S3, the weight ratio of leaf of bamboo medicinal extract, mulberry extract and food auxiliary material is 0.8~1.1：0.9~1.2：2.5~3.5.
2. according to the preparation method of mulberry leaf particle described in right 1, which is characterized in that in S1, by weight crush 28~32 parts
The leaf of bamboo, which is added in 115~125 parts a concentration of 30~55% of ethyl alcohol, afterwards carries out primary heating extraction, and an extracting solution is obtained by filtration
With a filter residue；75~85 parts a concentration of 50~65% of ethyl alcohol is added into a filter residue and carries out secondary temperature elevation extraction, filtering
Obtain secondary raffinate and secondary filter residue；55~65 parts a concentration of 50~60% of ethyl alcohol is added into secondary filter residue again and carries out three
Secondary heating extraction, is obtained by filtration extracting solution three times；By an extracting solution, secondary raffinate and extracting solution mixes three times, recycles second
Alcohol to relative density at 40 DEG C is 1.2~1.5, and macroporous resin column purifies and separates are carried out after centrifugation, is then concentrated to give leaf of bamboo leaching
Cream.
3. according to the preparation method of the mulberry leaf particle of right 1 or 2, which is characterized in that in S2, by weight by 18~23 parts of powder
After mulberry leaf and 75~85 parts of water mix after broken, four heating extractions are carried out, No. four extracting solutions and four filter residues are obtained by filtration；Xiang Si
55~65 parts of water are added in secondary filter residue and carry out five heating extractions, No. five extracting solutions are obtained by filtration；By No. four extracting solutions and five times
Extracting solution mixes, and macroporous resin column purifies and separates are carried out after centrifugation, are then concentrated to give mulberry extract.
4. according to the preparation method of the mulberry leaf particle of right 1 or 2, which is characterized in that mulberry leaf plucking time be annual April extremely
November, leaf of bamboo plucking time are March annual December to next year.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1066055C (en) * | 1998-03-17 | 2001-05-23 | 浙江农业大学 | Production method for extracting flavonoid compound extract or powder from bamboo leaf |
| CN102742903A (en) * | 2012-07-05 | 2012-10-24 | 徐州林泉绿色食品饮料厂 | Mulberry leaf health care beverage and preparation method thereof |
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| CN101036698B (en) * | 2007-04-17 | 2010-05-19 | 广东中烟工业有限责任公司 | Mulberry leaf extract and its preparing process and application |
| CN102429146A (en) * | 2011-10-21 | 2012-05-02 | 陕西科技大学 | Method for producing mulberry leaf oral liquid |
| CN103860921A (en) * | 2012-12-11 | 2014-06-18 | 镇江市丹徒区南山溪园茶叶专业合作社 | Extraction method of bamboo leaf flavone |
| CN104274534A (en) * | 2013-07-03 | 2015-01-14 | 周伯扬 | Preparation technology of total-component mulberry leaf extract |
| KR20150048296A (en) * | 2013-10-25 | 2015-05-07 | 산청기능성콩 영농조합법인 | Simplicity food with unpolished rice as the principal material |
| CN104547045B (en) * | 2014-12-25 | 2017-07-04 | 福州嘉佑化学科技有限公司 | A kind of leaf of Moringa compound granules and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1066055C (en) * | 1998-03-17 | 2001-05-23 | 浙江农业大学 | Production method for extracting flavonoid compound extract or powder from bamboo leaf |
| CN102742903A (en) * | 2012-07-05 | 2012-10-24 | 徐州林泉绿色食品饮料厂 | Mulberry leaf health care beverage and preparation method thereof |
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