CN105401414B - A kind of hard water resistance Real Silk Fabrics Degumming agent - Google Patents

A kind of hard water resistance Real Silk Fabrics Degumming agent Download PDF

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Publication number
CN105401414B
CN105401414B CN201510955844.6A CN201510955844A CN105401414B CN 105401414 B CN105401414 B CN 105401414B CN 201510955844 A CN201510955844 A CN 201510955844A CN 105401414 B CN105401414 B CN 105401414B
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water resistance
hard water
real silk
silk fabrics
agent
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CN105401414A (en
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潘世俊
胡小明
张立新
王祥荣
石继均
梅德祥
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JIANGSU XINYUAN SILK TECHNOLOGY Co.,Ltd.
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NAFUER GARMENT ORNAMENT CO LD NANTONG
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
    • D06M13/262—Sulfated compounds thiosulfates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
    • D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
    • D06M11/13—Ammonium halides or halides of elements of Groups 1 or 11 of the Periodic System
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/51—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
    • D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
    • D06M11/56—Sulfates or thiosulfates other than of elements of Groups 3 or 13 of the Periodic System
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/11—Compounds containing epoxy groups or precursors thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/165—Ethers
    • D06M13/17—Polyoxyalkyleneglycol ethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53—Polyethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/10—Animal fibres

Abstract

The invention discloses a kind of hard water resistance Real Silk Fabrics Degumming agent.Including following component and its parts by weight：Two sodium sulphate of alkyl：8‑25；Cardanol polyoxyethylene ether：5‑15；Maleic acrylic copolymer：2‑10；Fibroin protective agent：2‑10；Inorganic salts：2‑10；Sodium carbonate：2‑10；Water：50‑20.The present invention uses main ingredient of two sodium sulphate of alkyl as scouring agent, has the function of the metal ions such as excellent anticalcium, magnesium, improves scouring result.Cardanol polyoxyethylene ether is added, by synergistic effect, improves the scouring result of scouring agent, the quality of concise rear fabric can be improved.Auxiliary agent used is biodegradable compound, harmless, is conducive to the protection of environment.

Description

A kind of hard water resistance Real Silk Fabrics Degumming agent
Technical field
The present invention relates to TEXTILE CHEMICALSs, are related specifically to Real Silk Fabrics Degumming agent.
Background technology
Silk fabric dyeing and printing processing in, in order to embody the soft and smooth feel and fine quality of silk broadcloth, it is necessary to silk broadcloth into Concise processing of the row with degumming as the main purpose.Refinery practice further includes the dirts such as pigment, ash, oily wax on removal silk fiber Dirt improves the feel and capillary effect of silk.
General refinery practice carries out under weak basic condition, and silk gum acts through puffing, swelling, hydrolysis in alkalinity, finally Removing.Other than alkaline agent, also needs to that scouring agent is added in concise processing, to help smooth degumming, and ensure in degumming In journey by pH stable within the scope of certain, so that fibroin strength is injury-free, ensure that fabric has excellent handle, white The use value such as degree, capillary effect, strength.The addition of scouring agent will also improve the efficiency of degumming, shorten concise required time, save energy Source reduces production cost.
The method for refining of silk broadcloth is mainly by soap alkaline process, synthetic detergent method, biological enzyme etc., the type of silk scouring agent It is various, it is mostly the compound of one or more of surfactants and alkaline agent, chelating agent etc..Scouring of Silk adds man-hour requirement Using a large amount of water, the calcium and magnesium ion in water often forms insoluble compound deposition on the fabric, influences concise rear fabric Feel.Water consumption is big, to the more demanding of water quality, it is difficult to handle the calcium and magnesium ion in water, inevitable requirement scouring agent has anti- Hard water ability, to promote scouring result.
Invention content
The technical problem to be solved by the present invention is to overcome deficiencies in the prior art, provide hard water resistance Real Silk Fabrics Degumming Agent, the efficiency and silk of the raising concise processing of silk practice the quality of white silk fabric.
Including following component and its parts by weight：
Two sodium sulphate of alkyl：8-25；Cardanol polyoxyethylene ether：5-15；
Maleic acid-acrylic acid copolymer：2-10；Fibroin protective agent：2-10；
Inorganic salts：2-10；Sodium carbonate：2-10；
Water：50-20.
Further technical solution, two sodium sulphate of alkyl have following structure formula：
Wherein, n is the integer of 10-16.
The ethoxymer distribution (EO) of further technical solution, the cardanol polyoxyethylene ether is 8~16.
The molecular weight of further technical solution, the maleic acid-acrylic acid copolymer is 5000~20000.
Further technical solution, the fibroin protective agent are multicomponent alcoholics compound.
Further technical solution, the multicomponent alcoholics compound be glycerol-glucose, alkyl sucrose ester one kind or Their mixture.
Further technical solution, the inorganic salts are anhydrous sodium sulphate, salt or their mixture.
The cardanol polyoxyethylene ether is the polyoxyethylene addition product of natural cashew nut shell oil extract, the Malaysia Acid-acrylic copolymer is regular industrial product.
Two sodium sulphate of alkyl is hard water resistance surfactant, and pertinent literature is it has been reported that can pass through following reaction It is made：
The document is published in for Xiao Jinxin《Household chemicals science》Review paper " the ring of the 4th phase P6~P16 of volume 38 The surfactant economical and efficient synthetic method of border close friend ".
It is an advantage of the invention that：After the present invention uses abovementioned technology, using hard water resistance two sulphur of surfactant alkyl Main ingredient of the sour sodium as scouring agent, while surface-active is provided, the work(with metal ions such as excellent anticalcium, magnesium Can, improve scouring result.Addition is that cardanol polyoxyethylene ether prepared by raw material is answered with natural cashew nut shell oil extract Match, by synergistic effect, improve the scouring result of scouring agent, the quality of concise rear fabric can be improved.Auxiliary agent used is Environment-friendly type, biodegradable compound, it is harmless, be conducive to the protection of environment.
Specific implementation mode
With reference to embodiment, the invention will be further described：
Embodiment one：Hard water resistance Real Silk Fabrics Degumming agent 1 is formulated as follows：(based on important number)
Two sodium sulphate of dodecyl：16；Cardanol polyoxyethylene ether (EO=10)：8；
Maleic acid-acrylic acid copolymer (molecular weight=9000)：7；
Glycerol-glucose：5；
Anhydrous sodium sulphate：2；Sodium carbonate：5；
Water：57.
Embodiment two：Hard water resistance Real Silk Fabrics Degumming agent 2 is formulated as follows：(based on important number)
Two sodium sulphate of tetradecyl：12；Cardanol polyoxyethylene ether (EO=12)：12；
Maleic acid-acrylic acid copolymer (molecular weight=16000)：5；
Dodecyl sucrose ester：3；
Salt：3；Sodium carbonate：4；
Water：61.
Embodiment three：Hard water resistance Real Silk Fabrics Degumming agent 1 is formulated as follows：(based on important number)
Two sodium sulphate of palmityl：20；Cardanol polyoxyethylene ether (EO=10)：6；
Maleic acid-acrylic acid copolymer (molecular weight=12000)：6；
Glycerol-glucose：3；Dodecyl sucrose ester：2；
Anhydrous sodium sulphate：2；Sodium carbonate：5；
Water：56.
What has been described above is only a preferred embodiment of the present invention.It should be pointed out that for those of ordinary skill in the art For, without departing from the principle of the present invention, several variations and modifications can also be made, these also should be regarded as belonging to this hair Bright protection domain.

Claims (6)

1. a kind of hard water resistance Real Silk Fabrics Degumming agent, it is characterised in that：Including following component and its parts by weight：
Two sodium sulphate of alkyl：8-25；Cardanol polyoxyethylene ether：5-15；
Maleic acid-acrylic acid copolymer：2-10；Fibroin protective agent：2-10；
Anhydrous sodium sulphate, salt or their mixture：2-10；Sodium carbonate：2-10；Water：50-20.
2. a kind of hard water resistance Real Silk Fabrics Degumming agent according to claim 1, it is characterised in that：Two sulfuric acid of alkyl Sodium has following structure formula：
Wherein, n is the integer of 10-16.
3. a kind of hard water resistance Real Silk Fabrics Degumming agent according to claim 1, it is characterised in that：The anacardol polyoxy The ethoxymer distribution (EO) of vinethene is 8~16.
4. a kind of hard water resistance Real Silk Fabrics Degumming agent according to claim 1, it is characterised in that：The maleic acid-the third The molecular weight of olefin(e) acid copolymer is 5000~20000.
5. a kind of hard water resistance Real Silk Fabrics Degumming agent according to claim 1, it is characterised in that：The fibroin protective agent For multicomponent alcoholics compound.
6. a kind of hard water resistance Real Silk Fabrics Degumming agent according to claim 5, it is characterised in that：The polyalcohols It is glycerol-glucose, one kind of alkyl sucrose ester or their mixture to close object.
CN201510955844.6A 2015-12-18 2015-12-18 A kind of hard water resistance Real Silk Fabrics Degumming agent Active CN105401414B (en)

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106480726A (en) * 2016-10-14 2017-03-08 无锡市华诚印染剂厂 Silk fabric scouring agent
CN107177978A (en) * 2017-05-22 2017-09-19 如皋市下原科技创业服务有限公司 A kind of method for refining of real silk fabric
CN110835849B (en) * 2019-12-12 2022-03-11 太仓宝霓实业有限公司 High-performance environment-friendly scouring agent composition and preparation method thereof
CN111851069B (en) * 2020-07-18 2021-05-28 绍兴海成化工有限公司 All-in-one scouring agent and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101255655A (en) * 2008-04-02 2008-09-03 苏州大学 Silk broadcloth scouring agent
CN102220693A (en) * 2011-04-25 2011-10-19 苏州大学 Natural silk refining agent
CN105088792A (en) * 2015-08-26 2015-11-25 江苏恒源丝绸集团有限公司 Silk scouring agent

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101255655A (en) * 2008-04-02 2008-09-03 苏州大学 Silk broadcloth scouring agent
CN102220693A (en) * 2011-04-25 2011-10-19 苏州大学 Natural silk refining agent
CN105088792A (en) * 2015-08-26 2015-11-25 江苏恒源丝绸集团有限公司 Silk scouring agent

Non-Patent Citations (2)

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腰果酚聚氧乙烯醚的性能及其在洗衣液中的应用;朱会苏等;《日用化学品科学》;20130430;第36卷(第4期);第27-31页 *

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