CN105400345A - Computerized color mixing external wall flat-coating basic shallow-foundation paint and preparation method thereof - Google Patents
Computerized color mixing external wall flat-coating basic shallow-foundation paint and preparation method thereof Download PDFInfo
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- CN105400345A CN105400345A CN201510891527.2A CN201510891527A CN105400345A CN 105400345 A CN105400345 A CN 105400345A CN 201510891527 A CN201510891527 A CN 201510891527A CN 105400345 A CN105400345 A CN 105400345A
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Abstract
The invention relates to wall surface paint which is economical and capable of purifying odors and preventing mildew. The wall surface paint is prepared from water, cellulose, a pH conditioning agent, a dispersing agent, a wetting agent, a wetting antifreezing agent, an antifoaming agent, titanium dioxide, filler, emulsion, an opaque polymer, a film coalescing aid, an antibacterial preservative, a mildew-proof agent, a thickening agent and an organosilicon waterproofing agent. The wall surface paint has the advantages of being excellent in washing resistance, water resistance, alkali resistance and weather resistance. The compatibility and color contrast properties of the wall surface paint with color paste popular in the market are excellent, color mixing is accurate, and the repeatability is good; when construction is conducted, the wall surface paint is smooth and unhindered, the defoaming process is rapid, splatter resistance is excellent, and the fullness degree of a paint film is high. A preparation method of the wall surface paint is simple and rapid, the production process is easy to control, the manufacturing cost is low, the stability between different batches is good, the mixed color is accurate and reliable, and the storage stability is good. The paint film defects such as bubbling, disengagement, rain prints and bright specks do not occur on the paint film.
Description
Technical field
The present invention relates to architectural decoration water-borne coatings field, particularly the computer color-mixed exterior wall of one is flat is coated with basic shallow foundation paint and preparation method thereof.
Background technology
Along with aesthetic standards promote, human consumer also becomes more diverse to the requirement of building coating color and personalization, therefore traditional coating material production, artificial toning process cannot satisfy the demands of consumers.The introducing of modernization tinting system, factory only need produce three kinds of base paints (being respectively shallow foundation, middle base, dark base), dealer only needs basic mill base, just can recall thousands of kinds of colors rapidly, select with the personalization of satisfied different client and variation, thus improve the market competitiveness.
Current computer color-mixed base paint quality is on the market uneven, main deficiency has: one is, some computer color-mixed base paint does not distinguish inner-outer wall, does not generally have specific aim, namely carrys out appropriate design base paint according to the different performance demand of interior wall paint and exterior wall paint; Two are, the poor compatibility that on base paint and market, current color is starched, and color developing is bad, the phenomenon such as easily produce loose colour, grow dim; Three are, the not easily management and control of base paint production process, and the base paint difference that different batches is produced is comparatively large, cause the color that recalls not accurate enough; Four are, it is not good that the own performance (as abrasion resistance, water tolerance, alkali resistance, weathering resistance etc.) being coated with base paint equalled by exterior wall, can not meet the performance requriements of high-performance coatings with high weatherability.
Summary of the invention
The invention provides basic shallow foundation paint of the flat painting of a kind of computer color-mixed exterior wall and preparation method thereof, the abrasion resistance, water tolerance, alkali resistance, weathering resistance etc. of base paint prepared by the present invention are all very outstanding, and the consistency of starching with current color on market and color developing very excellent; This preparation method's simple and fast and production process is easy to management and control, low cost of manufacture and good stability between different batches, the color recalled accurately and reliably.
The present invention is achieved in that
Scheme (one):
A kind of computer color-mixed exterior wall is flat is coated with basic shallow foundation paint, and this paint is formulated according to following parts by weight proportioning by following component:
| Water | 9.77-25.2 part |
| Mierocrystalline cellulose | 0.2-0.6 part |
| PH adjusting agent | 0.05-0.25 part |
| Dispersion agent | 0.5-1 part |
| Wetting agent | 0.1-0.4 part |
| Frostproofer | 0.8-1.5 part |
| Wetting frostproofer | 0-0.4 part |
| Defoamer | 0.4-0.8 part |
| Titanium dioxide | 12-20 part |
| Filler | 22-35 part |
| Emulsion | 20-30 part |
| Opacifying polymers | 3-6 part |
| Film coalescence aid | 1-2 part |
| Fungicidal preservative | 0.1-0.3 part |
| Mould inhibitor | 0.2-0.4 part |
| Thickening material | 0.1-0.5 part |
| Waterproofing agent of organosilicon | 0.5-3 part |
Preferably, described pH adjusting agent is 2-amino-2-methyl-1-propanol, and described frostproofer is ethylene glycol or propylene glycol, and described Opacifying polymers is the microspheric aqueous emulsion polymer with core/shell structure of not film forming.
Preferably, described dispersion agent is a kind of in ammonium polyacrylate dipersant or polycarboxylate sodium's dispersion agent or their arbitrary combination.
Preferably, described wetting agent is poly-hydroxyalkyl ether nonionic wetting agent.
Preferably, described defoamer is a kind of in mineral oil defoaming agent or water-based organic silicon defoamer or their arbitrary combination.
Preferably, described filler is a kind of in water-ground limestone, calcined kaolin, barium sulfate, talcum powder and mica powder or their arbitrary combination.
Preferably, described waterproofing agent of organosilicon is the water-based emulsion of siloxane polymer.
Preferably, described film coalescence aid is a kind of in alcohol ester-12, dipropylene glycol methyl ether or dipropylene or their arbitrary combination.
Preferably, described thickening material is a kind of in alkali swelling type thickening material or polyurethanes thickening material or their arbitrary combination.
Scheme (two):
The method being coated with basic shallow foundation paint equalled by the one computer color-mixed exterior wall prepared described in scheme (), and the method comprises following step of sequentially carrying out:
1) under the rotating speed of 500-800 rev/min, add 9.77-25.2 part water and 0.2-0.6 part Mierocrystalline cellulose in a reservoir successively, keep this rotating speed to disperse 5-10 minute;
2) then improve rotating speed to 800-1200 rev/min, add 0.05-0.25 part pH adjusting agent, 0.5-1 part dispersion agent, 0.1-0.4 part wetting agent, 0.8-1.5 part frostproofer, 0-0.4 part soaks frostproofer, 0.2-0.4 part defoamer, 12-20 part titanium dioxide, 22-35 part filler;
Then improve rotating speed afterwards to 1500-1800 rev/min, under this rotating speed, be dispersed to fineness be greater than zero and be less than or equal to 60 microns;
3) last, reduce rotating speed to 600-800 rev/min, under this rotating speed, add 20-30 part emulsion, 3-6 part Opacifying polymers, 0.2-0.4 part defoamer, 1-2 part film coalescence aid, 0.1-0.3 part fungicidal preservative, 0.2-0.4 part mould inhibitor, 0.1-0.5 part thickening material and 0.5-3 part waterproofing agent of organosilicon successively, under this rotating speed, disperse 10-15 minute.
The present invention compared with prior art has the following advantages:
(1) property of the present invention is directed to is strong, and the performance requriements specially needed for exterior wall paint carries out formulating of recipe, and the properties (as abrasion resistance, water tolerance, alkali resistance, weathering resistance etc.) of prepared base paint is very excellent;
(2) by preferred thickened systems, wetting and dispersing system, antifoaming system etc., the consistency that the present invention not only starches with current color on market and color developing very excellent, toning is accurately and favorable reproducibility; And during construction smooth smooth and easy, froth breaking is exceedingly fast, anti-splashing is excellent, paint film fullness ratio is high.
(3) this preparation method's simple and fast and production process is easy to management and control, low cost of manufacture and good stability between different batches, the color recalled accurately and reliably.
(4) storage stability is good, and 50 DEG C of thermmal storages are after 60 days, and the viscosity B coefficent of base paint is no more than 5KU, and is not subject to the impact of thermmal storage with the properties such as consistency, color developing of mill base.
(5) add waterproofing agent of organosilicon, film of the present invention has outstanding water tolerance, initial stage water tolerance and initial stage resistance to rainprint, the paint marketing such as even if rain in 24h after construction, film of the present invention also there will not be bubbling, comes off, rainprint, speck.
Embodiment
Below in conjunction with specific embodiment, the present invention will be described in detail.
(1) embodiment is as follows:
Embodiment one:
A kind of computer color-mixed exterior wall is flat is coated with basic shallow foundation paint, and this paint is formulated according to following parts by weight proportioning by following component:
| Water | 9.77-25.2 part |
| Mierocrystalline cellulose | 0.2-0.6 part |
| PH adjusting agent | 0.05-0.25 part |
| Dispersion agent | 0.5-1 part |
| Wetting agent | 0.1-0.4 part |
| Frostproofer | 0.8-1.5 part |
| Wetting frostproofer | 0-0.4 part |
| Defoamer | 0.4-0.8 part |
| Titanium dioxide | 12-20 part |
| Filler | 22-35 part |
| Emulsion | 20-30 part |
| Opacifying polymers | 3-6 part |
| Film coalescence aid | 1-2 part |
| Fungicidal preservative | 0.1-0.3 part |
| Mould inhibitor | 0.2-0.4 part |
| Thickening material | 0.1-0.5 part |
| Waterproofing agent of organosilicon | 0.5-3 part |
Preferably, described pH adjusting agent is 2-amino-2-methyl-1-propanol, and described frostproofer is ethylene glycol or propylene glycol, and described Opacifying polymers is the Unihub E of Tao Shi.
Preferably, described dispersion agent is a kind of in ammonium polyacrylate dipersant or polycarboxylate sodium's dispersion agent or their arbitrary combination.
Preferably, described wetting agent is poly-hydroxyalkyl ether nonionic wetting agent.
Preferably, described defoamer is a kind of in mineral oil defoaming agent or water-based organic silicon defoamer or their arbitrary combination.
Preferably, described filler is a kind of in water-ground limestone, calcined kaolin, barium sulfate, talcum powder and mica powder or their arbitrary combination.
Preferably, described waterproofing agent of organosilicon is the water-based emulsion of siloxane polymer.
Preferably, described film coalescence aid is a kind of in alcohol ester-12, dipropylene glycol methyl ether or dipropylene or their arbitrary combination.
Preferably, described thickening material is a kind of in alkali swelling type thickening material or polyurethanes thickening material or their arbitrary combination.
Embodiment two:
The method being coated with basic shallow foundation paint equalled by the one computer color-mixed exterior wall prepared described in scheme (), and the method comprises following step of sequentially carrying out:
1) under the rotating speed of 500-800 rev/min, add 9.77-25.2 part water and 0.2-0.6 part Mierocrystalline cellulose in a reservoir successively, keep this rotating speed to disperse 5-10 minute;
2) then improve rotating speed to 800-1200 rev/min, add 0.05-0.25 part pH adjusting agent, 0.5-1 part dispersion agent, 0.1-0.4 part wetting agent, 0.8-1.5 part frostproofer, 0-0.4 part soaks frostproofer, 0.2-0.4 part defoamer, 12-20 part titanium dioxide, 22-35 part filler;
Then improve rotating speed afterwards to 1500-1800 rev/min, under this rotating speed, be dispersed to fineness be greater than zero and be less than or equal to 60 microns;
3) last, reduce rotating speed to 600-800 rev/min, under this rotating speed, add 20-30 part emulsion, 3-6 part Opacifying polymers, 0.2-0.4 part defoamer, 1-2 part film coalescence aid, 0.1-0.3 part fungicidal preservative, 0.2-0.4 part mould inhibitor, 0.1-0.5 part thickening material and 0.5-3 part waterproofing agent of organosilicon successively, under this rotating speed, disperse 10-15 minute.
(2) embodiment is as follows: further illustrate the present invention below by embodiment:
Embodiment 1
A kind of computer color-mixed exterior wall is flat is coated with basic shallow foundation paint, and it is prepared from according to following step of sequentially carrying out by the raw material of following weight proportioning:
1) under the rotating speed of 500 revs/min, add 22.4 parts of water and 0.2 part of Mierocrystalline cellulose successively, disperse 5 minutes under this rotating speed;
2) under the rotating speed of 800 revs/min, then add 0.25 part of pH adjusting agent, 0.5 part of dispersion agent, 0.1 part of wetting agent, 1.2 parts of frostproofers, 0.4 part of wetting frostproofer, 0.325 part of defoamer, 20 parts of titanium dioxides, 18 parts of water-ground limestones and 4 parts of mica powders, improve rotating speed to 1500 rev/min afterwards, under this rotating speed, be dispersed to fineness be less than or equal to 60 microns;
3) rotating speed to 600 rev/min is reduced, under this rotating speed, adding 25 parts of emulsions, 3 parts of Opacifying polymers, 0.325 part of defoamer, 1.5 parts of film coalescence aid, 0.1 part of fungicidal preservative, 0.2 part of mould inhibitor, 0.5 part of thickening material and 2 parts of waterproofing agent of organosilicon successively, under this rotating speed, disperseing 15 minutes to mixing.
Embodiment 2
A kind of computer color-mixed exterior wall is flat is coated with basic shallow foundation paint, and it is prepared from according to following step of sequentially carrying out by the raw material of following weight proportioning:
1) under the rotating speed of 800 revs/min, add 9.77 parts of water and 0.35 part of Mierocrystalline cellulose successively, disperse 10 minutes under this rotating speed;
2) under the rotating speed of 1200 revs/min, then add 0.15 part of pH adjusting agent, 1 part of dispersion agent, 0.4 part of wetting agent, 1.5 parts of frostproofers, 0 part of wetting frostproofer, 0.4 part of defoamer, 12 parts of titanium dioxides, 30 parts of water-ground limestones and 5 parts of calcined kaolins, improve rotating speed to 1800 rev/min afterwards, under this rotating speed, be dispersed to fineness be less than or equal to 60 microns;
3) rotating speed to 800 rev/min is reduced, under this rotating speed, adding 30 parts of emulsions, 6 parts of Opacifying polymers, 0.4 part of defoamer, 2 parts of film coalescence aid, 0.18 part of fungicidal preservative, 0.25 part of mould inhibitor, 0.1 part of thickening material and 0.5 part of waterproofing agent of organosilicon successively, under this rotating speed, disperseing 10 minutes to mixing.
Embodiment 3
A kind of computer color-mixed exterior wall is flat is coated with basic shallow foundation paint, and it is prepared from according to following step of sequentially carrying out by the raw material of following weight proportioning:
1) under the rotating speed of 650 revs/min, add 25.2 parts of water and 0.45 part of Mierocrystalline cellulose successively, disperse 7 minutes under this rotating speed;
2) under the rotating speed of 1000 revs/min, then add 0.1 part of pH adjusting agent, 0.7 part of dispersion agent, 0.2 part of wetting agent, 0.8 part of frostproofer, 0.25 part of wetting frostproofer, 0.2 part of defoamer, 17 parts of titanium dioxides, 23 parts of water-ground limestones and 3 parts of talcum powder, improve rotating speed to 1600 rev/min afterwards, under this rotating speed, be dispersed to fineness be less than or equal to 60 microns;
3) rotating speed to 700 rev/min is reduced, under this rotating speed, adding 20 parts of emulsions, 4 parts of Opacifying polymers, 0.2 part of defoamer, 1 part of film coalescence aid, 0.25 part of fungicidal preservative, 0.3 part of mould inhibitor, 0.35 part of thickening material and 3 parts of waterproofing agent of organosilicon successively, under this rotating speed, disperseing 12 minutes to mixing.
Embodiment 4
A kind of computer color-mixed exterior wall is flat is coated with basic shallow foundation paint, and it is prepared from according to following step of sequentially carrying out by the raw material of following weight proportioning:
1) under the rotating speed of 700 revs/min, add 18.2 parts of water and 0.6 part of Mierocrystalline cellulose successively, disperse 9 minutes under this rotating speed;
2) under the rotating speed of 1100 revs/min, then add 0.05 part of pH adjusting agent, 0.8 part of dispersion agent, 0.3 part of wetting agent, 1 part of frostproofer, 0.15 part of wetting frostproofer, the defoamer of 0.275 part, 15 parts of titanium dioxides, 25 parts of water-ground limestones and 5 parts of talcum powder, improve rotating speed to 1700 rev/min afterwards, under this rotating speed, be dispersed to fineness be less than or equal to 60 microns;
3) rotating speed to 750 rev/min is reduced, under this rotating speed, adding 25 parts of emulsions, 5 parts of Opacifying polymers, 0.275 part of defoamer, 1.5 parts of film coalescence aid, 0.3 part of fungicidal preservative, 0.4 part of mould inhibitor, 0.15 part of thickening material and 1 part of waterproofing agent of organosilicon successively, under this rotating speed, disperseing 13 minutes to mixing.
Above in each embodiment:
Mierocrystalline cellulose preferably adopts the sub-250HBR produced across dragon;
The AMP-95 that pH adjusting agent preferably adopts Tao Shi to produce;
The SN-5040 that dispersion agent preferably adopts Sheng Nuopuke to produce;
The SN-WET996 that wetting agent preferably adopts Sheng Nuopuke to produce;
The FT-68 that wetting frostproofer preferably adopts ashland to produce;
Frostproofer preferably adopts the propylene glycol of Depew Chemical Manufacture;
The NXZ that defoamer preferably adopts Hai Chuan to produce and the CF18404 that Blackburn is produced;
The 902+ that titanium dioxide preferably adopts Du Pont to produce;
Water-ground limestone preferably adopts the 800 order coarse whitings of agriculture-countryside-farmer;
Calcined kaolin preferably adopts the white calcined kaolin of ultra-fine height covering west and produce;
Mica powder preferably adopts the ultrafine mica powder of US business's chemistry;
The MS-1250 that talcum powder preferably adopts wide good fortune to produce;
6266 pure-acrylic emulsions that emulsion preferably adopts BASF to produce;
The Unihub E that Opacifying polymers preferably adopts Tao Shi to produce;
The texanol that film coalescence aid preferably adopts Yi Shiman to produce;
The HF that fungicidal preservative preferably adopts Sol to produce;
The EPW that mould inhibitor preferably adopts Sol to produce;
The RM-8W that TT935 and Tao Shi that thickening material preferably adopts ROHM AND HAAS to produce produces.
Waterproofing agent of organosilicon preferably adopts the WR1195 of sea profit chemical industry.
Test the basic shallow foundation paint of the flat painting of the computer color-mixed exterior wall obtained by each embodiment according to GB GB/T9755-2014, every technical feature data are as shown in the table:
Computer color-mixed exterior wall obtained by each embodiment put down the color developing that is coated with basic shallow foundation paint and reducing power data as shown in the table:
Shown by the practical application of the every experimental data in table and each embodiment, the technical requirements that the properties being coated with basic shallow foundation paint meets the premium grads of exterior wall paint in GB/T9755-2014 " the outer Wall coating of synthetic resin emulsion " put down by computer color-mixed exterior wall in the present invention prepared by each embodiment, and the consistency of to starch with current color on market and color developing very excellent, toning is accurately and favorable reproducibility; This preparation method's simple and fast and production process is easy to management and control, low cost of manufacture and good stability between different batches, the color recalled accurately and reliably.
Above-mentioned embodiment is just explained in detail technical scheme of the present invention, and the present invention has more than and is only confined to above-described embodiment, and every any improvement according to the principle of the invention or replacement, all should within protection scope of the present invention.
Claims (10)
1. computer color-mixed exterior wall is flat is coated with a basic shallow foundation paint, it is characterized in that: this paint is formulated according to following parts by weight proportioning by following component:
2. computer color-mixed exterior wall according to claim 1 is flat is coated with basic shallow foundation paint, it is characterized in that: described pH adjusting agent is 2-amino-2-methyl-1-propanol; Described frostproofer is ethylene glycol or propylene glycol; Described Opacifying polymers is the microspheric aqueous emulsion polymer with core/shell structure of not film forming.
3. computer color-mixed exterior wall according to claim 1 is flat is coated with basic shallow foundation paint, it is characterized in that: described dispersion agent is a kind of in ammonium polyacrylate dipersant or polycarboxylate sodium's dispersion agent or their arbitrary combination.
4. computer color-mixed exterior wall according to claim 1 is flat is coated with basic shallow foundation paint, it is characterized in that: described wetting agent is poly-hydroxyalkyl ether nonionic wetting agent.
5. computer color-mixed exterior wall according to claim 1 is flat is coated with basic shallow foundation paint, it is characterized in that: described defoamer is a kind of in mineral oil defoaming agent or water-based organic silicon defoamer or their arbitrary combination.
6. computer color-mixed exterior wall according to claim 1 is flat is coated with basic shallow foundation paint, it is characterized in that: described filler is a kind of in water-ground limestone, calcined kaolin, barium sulfate, talcum powder or mica powder or their arbitrary combination.
7. computer color-mixed exterior wall according to claim 1 is flat is coated with basic shallow foundation paint, it is characterized in that: described waterproofing agent of organosilicon is the water-based emulsion of siloxane polymer.
8. computer color-mixed exterior wall according to claim 1 is flat is coated with basic shallow foundation paint, it is characterized in that: described film coalescence aid is a kind of in alcohol ester-12, dipropylene glycol methyl ether or dipropylene or their arbitrary combination.
9. computer color-mixed exterior wall according to claim 1 is flat is coated with basic shallow foundation paint, it is characterized in that: described thickening material is a kind of in alkali swelling type thickening material or polyurethanes thickening material or their arbitrary combination.
10. the preparation method being coated with basic shallow foundation paint equalled by the computer color-mixed exterior wall prepared according to any one of claim 1-9, it is characterized in that: the preparation method of this paint comprises following step of sequentially carrying out:
1) under the rotating speed of 500-800 rev/min, add 9.77-25.2 part water and 0.2-0.6 part Mierocrystalline cellulose in a reservoir successively, keep this rotating speed to disperse 5-10 minute;
2) then improve rotating speed to 800-1200 rev/min, add 0.05-0.25 part pH adjusting agent, 0.5-1 part dispersion agent, 0.1-0.4 part wetting agent, 0.8-1.5 part frostproofer, 0-0.4 part soaks frostproofer, 0.2-0.4 part defoamer, 12-20 part titanium dioxide and 22-35 part filler;
Then improve rotating speed to 1500-1800 rev/min, under this rotating speed, be dispersed to fineness be greater than zero and be less than or equal to 60 microns;
3) last, reduce rotating speed to 600-800 rev/min, add 20-30 part emulsion, 3-6 part Opacifying polymers, 0.2-0.4 part defoamer, 1-2 part film coalescence aid, 0.1-0.3 part fungicidal preservative, 0.2-0.4 part mould inhibitor, 0.1-0.5 part thickening material and 0.5-3 part waterproofing agent of organosilicon successively, keep 600-800 rev/min to disperse 10-15 minute.
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| Publication number | Publication date |
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| CN105400345B (en) | 2017-08-25 |
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