CN105380844A - Neroli essential oil floral water and preparation method thereof - Google Patents
Neroli essential oil floral water and preparation method thereof Download PDFInfo
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- CN105380844A CN105380844A CN201510821317.6A CN201510821317A CN105380844A CN 105380844 A CN105380844 A CN 105380844A CN 201510821317 A CN201510821317 A CN 201510821317A CN 105380844 A CN105380844 A CN 105380844A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/02—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings containing insect repellants
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Abstract
The invention discloses neroli essential oil floral water and a preparation method thereof. The neroli essential oil floral water is prepared from the following components in percentage by weight: 1 to 5 percent of neroli essential oil, 0.3 to 2 percent of piperitol, 1 to 5 percent of blumea oil, 0.3 to 2 percent of eucalyptus oil, 0.3 to 2 percent of borneol, 0.3 to 2 percent of menthol, 1 to 10 percent of mother chrysanthemum extract, 1 to 10 percent of honeysuckle flowers extract, 1 to 10 percent of clove extract, 1 to 10 percent of lightyellow sophora root extract, 10 to 20 percent of ethyl alcohol and the balance of deionized water. The preparation method comprises the steps of preparation of the mother chrysanthemum extract, preparation of the honeysuckle extract, preparation of the clove extract, preparation of the lightyellow sophora root extract, preparation of an organic phase, preparation of a water phase and preparation of a finished product. The neroli essential oil floral water provided by the invention is pure in color, and gentle and pleasant in smell, has the function of mosquito repellent at the same time, and also has the excellent effect for treating insect bite dermatitis.
Description
Technical field
The present invention relates to a kind of floral water.
Background technology
Floral water is a kind of aqueous solution containing ethanol and essence, usually uses in summer, both can refreshment, also has certain repelling effect.Some now commercially available mosquito-repellent perfumes are mainly by adding anophelifuge, as dimethyl phthalate and diethyltoluamide reach the effect of anophelifuge, but these floral water easily cause the allergy of skin, for inapplicable skin sensitivity crowd.And the Herba Menthae cool smell of the floral water of current market is too dense, night, h.d. used such floral water can cause neural excitement to a certain degree unavoidably, unfavorable for falling asleep fast.
Summary of the invention
For above-mentioned technical problem, the invention provides a kind of orange blossom quintessence oil floral water and preparation method thereof and preparation method thereof.Orange blossom quintessence oil floral water of the present invention is made up of the component of following percentage by weight: orange blossom quintessence oil 1 ~ 5%, menthol 0.3 ~ 2%, Oleum Folium Artemisiae Argyi 1 ~ 5%, eucalyptus oil 0.3 ~ 2%, Borneolum Syntheticum 0.3 ~ 2%, Mentholum 0.3 ~ 2%, Flos Chrysanthemi Indici extract 1 ~ 10%, Flos Lonicerae extract 1 ~ 10%, Flos Caryophylli extract 1 ~ 10%, Radix Sophorae Flavescentis extract 1 ~ 10%, ethanol 10 ~ 20%, deionized water surplus.
Further, be made up of the component of following percentage by weight: orange blossom quintessence oil 2 ~ 4%, menthol 0.5 ~ 1%, Oleum Folium Artemisiae Argyi 2 ~ 4%, eucalyptus oil 0.5 ~ 1%, Borneolum Syntheticum 0.5 ~ 1%, Mentholum 0.5 ~ 1%, Flos Chrysanthemi Indici extract 3 ~ 7%, Flos Lonicerae extract 3 ~ 7%, Flos Caryophylli extract 3 ~ 7%, Radix Sophorae Flavescentis extract 3 ~ 7%, ethanol 12 ~ 18%, deionized water surplus.
Particularly, be made up of the component of following percentage by weight: orange blossom quintessence oil 3%, menthol 0.8%, Oleum Folium Artemisiae Argyi 3%, eucalyptus oil 0.8%, Borneolum Syntheticum 0.8%, Mentholum 0.8%, Flos Chrysanthemi Indici extract 5%, Flos Lonicerae extract 5%, Flos Caryophylli extract 5%, Radix Sophorae Flavescentis extract 5%, ethanol 16%, deionized water surplus.
The preparation method of orange blossom quintessence oil floral water of the present invention comprises the following steps:
(1). by described formula ratio, orange blossom quintessence oil, menthol, Oleum Folium Artemisiae Argyi, eucalyptus oil, Borneolum Syntheticum and Mentholum are dissolved in ethanol,
(2). by described formula ratio, dilute with deionized water after Flos Chrysanthemi Indici extract, Flos Lonicerae extract, Flos Caryophylli extract and Radix Sophorae Flavescentis extract are mixed;
(3). under stirring, the solution that step (1) is obtained is added in the obtained diluent of step (2), continue to be stirred to formation uniform solution, to obtain final product.
Particularly, the preparation method of described Flos Chrysanthemi Indici extract is as follows: shine dry grinding after being cleaned by Flos Chrysanthemi Indici; The volume fraction adding 5 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 30min; Volume fraction insoluble matter being added again 5 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 30min; Merge extractive liquid, to obtain final product.The wherein preferred 20kHz of supersonic frequency.
Particularly, the preparation method of described Flos Lonicerae extract is as follows: shine dry grinding after being cleaned by Flos Lonicerae; The volume fraction adding 5 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 30min; Volume fraction insoluble matter being added again 5 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 30min; Merge extractive liquid, to obtain final product.The wherein preferred 20kHz of supersonic frequency.
Particularly, the preparation method of described Flos Caryophylli extract is as follows: shine dry grinding after being cleaned by Flos Caryophylli; The volume fraction adding 3 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 40min; Volume fraction insoluble matter being added again 3 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 40min; Merge extractive liquid, to obtain final product.The wherein preferred 40kHz of supersonic frequency.
Particularly, the preparation method of described Radix Sophorae Flavescentis extract is as follows: shine dry grinding after being cleaned by Radix Sophorae Flavescentis; The volume fraction adding 3 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 40min; Volume fraction insoluble matter being added again 3 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 40min; Merge extractive liquid, to obtain final product.The wherein preferred 40kHz of supersonic frequency.
Radix Sophorae Flavescentis bitter in the mouth, cold in nature.GUIXIN, liver, stomach, large intestine, urinary bladder channel.There is heat clearing and damp drying, parasite killing, effect of diuresis.For hematodiarrhoea, have blood in stool, jaundice urine retention, leucorrhea with red and white discharge, swelling of the vulva pudendal pruritus, eczema, eczema, skin pruritus, scabies leprosy, external treatment trichomonal vaginitis.
Borneolum Syntheticum is the crisp crystallization of lamellar of water white transparency or white translucent; Gas delicate fragrance, acrid in the mouth, cool; GUIXIN, liver, lung meridian; Delicate fragrance a surname is loose, has refreshment of having one's ideas straightened out, and the loose poison of heat clearing away, effect of improving acuity of vision and removing nebula, cures mainly calentura unconsciousness due to high fever, apoplexy syncope due to accumulation of phlegm infantile convulsion, and heat-damp in summer hoodwinks key clearly, and sore throat is deaf, and aphtha tooth swells, carbuncle sore infantile malnutrition hemorrhoid, conjunctival congestion and swelling pain, pterygium.
Flos Caryophylli is warm in nature, acrid in the mouth, returns spleen, stomach, lung, kidney channel.Warming middle-JIAO to send down the adverse QI, reinforcing the kidney and supporting YANG, for Deficiency and coldness of spleen and stomach, singultus vomiting, lack of appetite and vomiting, trusted subordinate's cold type of pain.
Flos Lonicerae is cold in nature, sweet in the mouth, enters lung, the heart, stomach warp, has effect of heat-clearing and toxic substances removing, antiinflammatory, tonify deficiency treatment wind, has the effect of antipyretic and anti-inflammatory, resisting pathogenic microbes.
Flos Chrysanthemi Indici bitter in the mouth, pungent, cold nature, returns liver, heart channel.There is effect of heat-clearing and toxic substances removing, pathogenic fire purging suppressing the hyperactive liver, cure mainly furuncle carbuncle, conjunctival congestion and swelling pain, have a headache dizzy.
Oleum Folium Artemisiae Argyi principle active component is Pu Pin enol-4 and α-terpinenol, and can directly relax tracheal smooth muscle, and the tracheal smooth muscle spasm bring out antigen, acetylcholine and histamine and asthma all have protective effect.Also there is anti-allergic effects.
Eucalyptus oil is a kind of colourless to micro-yellow oily liquid, extracts, be also with Camphora abnormal smells from the patient somewhat, be with a little medicine gas, have certain bactericidal action in peculiar refrigerant spine Folium eucalypti globueli (Eucalyptus globulus Labill.) fragrance in Eucalyptus oil, cajuput oil, Oleum Camphora, Folium Lauri nobilis wet goods material.
Orange blossom quintessence oil extracts from bigarabe white petal, and main chemical compositions is australene, camphene, nopinene, α-terpinene, nerol, neryl acetate, farnesol, acid esters and indole.Having calming nerves effect, is the good prescription of Cure for insomnia, also can improve neuralgia, headache and dizzy.
Orange blossom quintessence oil floral water color of the present invention is pure and fresh, and abnormal smells from the patient is soft pleasant, can not produce stronger excitement, have function of driving mosquitoes simultaneously.Drive mosquito at one's side while user can be allowed to go to sleep peacefully as early as possible in hot summer away, finished product of the present invention adopts pure natural raw material to obtain, and safety non-toxic, has anophelifuge, antipruritic double effects, also has good effect to treatment insect dermatitis.
In order to understand better and implement, the following detailed description of the present invention.
Detailed description of the invention
preparation embodiment
The preparation method of orange blossom quintessence oil floral water of the present invention comprises the following steps:
(1) preparation of Flos Chrysanthemi Indici extract: shine dry grinding after being cleaned by Flos Chrysanthemi Indici; The volume fraction adding 5 times of weight is in the alcoholic solution of 50%, 20kHz supersound extraction 20 ~ 30min; Volume fraction insoluble matter being added again 5 times of weight is in the alcoholic solution of 50%, 20kHz supersound extraction 20 ~ 30min; Merge extractive liquid, to obtain final product.
(2) preparation of Flos Lonicerae extract: shine dry grinding after being cleaned by Flos Lonicerae; The volume fraction adding 5 times of weight is in the alcoholic solution of 50%, 20kHz supersound extraction 20 ~ 30min; Volume fraction insoluble matter being added again 5 times of weight is in the alcoholic solution of 50%, 20kHz supersound extraction 20 ~ 30min; Merge extractive liquid, to obtain final product.
(3) preparation of Flos Caryophylli extract: shine dry grinding after being cleaned by Flos Caryophylli; The volume fraction adding 3 times of weight is in the alcoholic solution of 50%, 40kHz supersound extraction 20 ~ 40min; Volume fraction insoluble matter being added again 3 times of weight is in the alcoholic solution of 50%, 40kHz supersound extraction 20 ~ 40min; Merge extractive liquid, to obtain final product.
(4) preparation of Radix Sophorae Flavescentis extract: shine dry grinding after being cleaned by Radix Sophorae Flavescentis; The volume fraction adding 3 times of weight is in the alcoholic solution of 50%, 40kHz supersound extraction 20 ~ 40min; Volume fraction insoluble matter being added again 3 times of weight is in the alcoholic solution of 50%, 40kHz supersound extraction 20 ~ 40min; Merge extractive liquid, to obtain final product.
(5). by table 1 formula ratio, orange blossom quintessence oil, menthol, Oleum Folium Artemisiae Argyi, eucalyptus oil, Borneolum Syntheticum and Mentholum are dissolved in ethanol,
(6). by table 1 formula ratio, dilute with deionized water after Flos Chrysanthemi Indici extract, Flos Lonicerae extract, Flos Caryophylli extract and Radix Sophorae Flavescentis extract that step (1) ~ (4) are obtained are mixed;
(7). under stirring, the solution that step (5) is obtained is added in the obtained diluent of step (6), continue to be stirred to formation uniform solution, to obtain final product.
The each component composition of < table 1, > by weight percentage
repelling effect embodiment
Reference literature method carries out testing (National Standard of the People's Republic of China, agriculture chemical registration is with hygienic insecticide indoor pharmacodynamic test and evaluate the 9th part repellant (GB/T13917.9-2009), 2009).
Attack is tested: growing × and wide × high for putting into 300 female mosquitos of Aedes albopictus of not sucking blood for 3-5 days after sprouting wings in the mosquito cage of 40cm × 30cm × 30cm.Tester's the back of the hand exposes 4cm × 4cm skin, and remainder tightly covers.Hands is goed deep in mosquito cage, stop 2min, close observation, find that mosquito stops falling, before its mouthpart will thrust skin, shake arm expelled, be designated as an examination worm and stop falling.Coming to stop the examination worm that falls, to be designated as attack more than the tester of 30 and examination worm qualified, and this person and this cage mosquito can carry out repellency test.
Repellency test: be selected from the tester that 6 attacks are qualified, men and women half and half.Respectively draw the skin area of 5cm × 5cm at its both hands the back of the hand, wherein a hands presses 1.5mg/cm
2dose uniformity smear obtained anophelifuge gel, comparative example is by 1.5 μ l/cm
2dosage smear.By the 4cm × 4cm skin exposed wherein, remainder tightly covers, and another hands is blank.Smear repellent product 2h, hands is stretched into and is placed with 2min in the qualified mosquito cage of attack, observe and come to stop to fall to sucking blood with or without mosquito.Afterwards every 1h test once, as long as there is a mosquito to come to suck blood namely to sentence and make repellent product failure.The effective protecting time (h) of record repellent product.
Calculate: embodiment 1 ~ 5 and commercially available floral water are added the effective protecting time of this experiment 6 testers, take the mean as the effective protecting time of this product.The results are shown in Table 2:
< table 2 repelling effect result >
zest assessment embodiment
Reference literature method carries out testing (cosmetics health specification 2007 editions human skin patch).
Tested material: embodiment 1 ~ 5 gained sample that preparation embodiment is obtained.
Experimenter: totally 30 people, men and women half and half, 20 ~ 30 years old age, meets experimenter and volunteers inclusion criteria.
Test method: tested material is put into speckle examination device, consumption is 0.023g.Control wells is blank (declining any material).The non-stimulated tape sticker of speckle examination device being added with tested material is spread on back or the bent side of forearm of experimenter, gently press with palm and make it to stick equably on skin, continue 24h.30min after removal tested material speckle examination device, observes dermoreaction after impression disappears.If result is negative, after patch test, 24h and 48h observes once respectively again.Reaction result is recorded by table 3 (skin adverse reaction grade scale table).
< table 3 skin adverse reaction grade scale table >
Result of the test is in table 4:
< table 4 removes tested material later evaluation result >
The result that after patch test, 24h and 48h observes respectively is again with table 4.Above result display, mosquito-proof gel of the present invention is to the effect of human body skin nonirritant.
resultant effect embodiment
Utilize and feel that effect is moistened in the whitening of the orange blossom quintessence oil floral water come obtained by Evaluation operation example 1 ~ 5.Choose 50 ages the women of 20 ~ 50 years old as object on probation, stochastic averagina is divided into 5 groups, often organizes 10 people.With it the orange blossom quintessence oil floral water using embodiment 1 ~ 5 to obtain before sleeping every day is respectively sprayed on, use 1 month altogether.Then used orange blossom quintessence oil floral water is given a mark.Every result of use total score is 5 points: 5 be divided into best result, represents very well; 4 are divided into better; 3 are divided into and can accept; 2 be divided into bad; 1 is divided into and can not accepts.Be below every average, the results are shown in Table 5.Can draw, the resultant effect of trier to orange blossom quintessence oil floral water of the present invention has higher rating.
< table 5 effect expedition >
The present invention is not limited to above-mentioned embodiment, if do not depart from the spirit and scope of the present invention to various change of the present invention or distortion, if these are changed and distortion belongs within claim of the present invention and equivalent technologies scope, then the present invention is also intended to comprise these changes and distortion.
Claims (10)
1. an orange blossom quintessence oil floral water, is characterized in that being made up of the component of following percentage by weight: orange blossom quintessence oil 1 ~ 5%, menthol 0.3 ~ 2%, Oleum Folium Artemisiae Argyi 1 ~ 5%, eucalyptus oil 0.3 ~ 2%, Borneolum Syntheticum 0.3 ~ 2%, Mentholum 0.3 ~ 2%, Flos Chrysanthemi Indici extract 1 ~ 10%, Flos Lonicerae extract 1 ~ 10%, Flos Caryophylli extract 1 ~ 10%, Radix Sophorae Flavescentis extract 1 ~ 10%, ethanol 10 ~ 20%, deionized water surplus.
2. orange blossom quintessence oil floral water according to claim 1, is characterized in that being made up of the component of following percentage by weight: orange blossom quintessence oil 2 ~ 4%, menthol 0.5 ~ 1%, Oleum Folium Artemisiae Argyi 2 ~ 4%, eucalyptus oil 0.5 ~ 1%, Borneolum Syntheticum 0.5 ~ 1%, Mentholum 0.5 ~ 1%, Flos Chrysanthemi Indici extract 3 ~ 7%, Flos Lonicerae extract 3 ~ 7%, Flos Caryophylli extract 3 ~ 7%, Radix Sophorae Flavescentis extract 3 ~ 7%, ethanol 12 ~ 18%, deionized water surplus.
3. orange blossom quintessence oil floral water according to claim 2, is characterized in that being made up of the component of following percentage by weight: orange blossom quintessence oil 3%, menthol 0.8%, Oleum Folium Artemisiae Argyi 3%, eucalyptus oil 0.8%, Borneolum Syntheticum 0.8%, Mentholum 0.8%, Flos Chrysanthemi Indici extract 5%, Flos Lonicerae extract 5%, Flos Caryophylli extract 5%, Radix Sophorae Flavescentis extract 5%, ethanol 16%, deionized water surplus.
4. prepare a method for the orange blossom quintessence oil floral water described in claims 1 to 3 any one, it is characterized in that comprising the following steps:
(1). by described formula ratio, orange blossom quintessence oil, menthol, Oleum Folium Artemisiae Argyi, eucalyptus oil, Borneolum Syntheticum and Mentholum are dissolved in ethanol,
(2). by described formula ratio, dilute with deionized water after Flos Chrysanthemi Indici extract, Flos Lonicerae extract, Flos Caryophylli extract and Radix Sophorae Flavescentis extract are mixed;
(3). under stirring, the solution that step (1) is obtained is added in the obtained diluent of step (2), continue to be stirred to formation uniform solution, to obtain final product.
5. the preparation method of orange blossom quintessence oil floral water according to claim 4, is characterized in that: the preparation method of described Flos Chrysanthemi Indici extract is as follows: shine dry grinding after being cleaned by Flos Chrysanthemi Indici; The volume fraction adding 5 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 30min; Volume fraction insoluble matter being added again 5 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 30min; Merge extractive liquid, to obtain final product.
6. the preparation method of orange blossom quintessence oil floral water according to claim 4, is characterized in that: the preparation method of described Flos Lonicerae extract is as follows: shine dry grinding after being cleaned by Flos Lonicerae; The volume fraction adding 5 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 30min; Volume fraction insoluble matter being added again 5 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 30min; Merge extractive liquid, to obtain final product.
7. the preparation method of the orange blossom quintessence oil floral water according to claim 5 or 6, is characterized in that: described ultrasonic frequency is 40kHz.
8. the preparation method of orange blossom quintessence oil floral water according to claim 4, is characterized in that: the preparation method of described Flos Caryophylli extract is as follows: shine dry grinding after being cleaned by Flos Caryophylli; The volume fraction adding 3 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 40min; Volume fraction insoluble matter being added again 3 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 40min; Merge extractive liquid, to obtain final product.
9. the preparation method of orange blossom quintessence oil floral water according to claim 4, is characterized in that: the preparation method of described Radix Sophorae Flavescentis extract is as follows: shine dry grinding after being cleaned by Radix Sophorae Flavescentis; The volume fraction adding 3 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 40min; Volume fraction insoluble matter being added again 3 times of weight is in the alcoholic solution of 50%, supersound extraction 20 ~ 40min; Merge extractive liquid, to obtain final product.
10. the preparation method of orange blossom quintessence oil floral water according to claim 8 or claim 9, is characterized in that: described ultrasonic frequency is 40kHz.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106148012A (en) * | 2016-08-25 | 2016-11-23 | 安徽瑞璞牡丹科技有限公司 | A kind of extracting method of mild orange blossom quintessence oil |
| CN111481455A (en) * | 2020-04-02 | 2020-08-04 | 广州市逸轩精细化工有限公司 | Floral water and preparation method thereof |
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| CN103655718A (en) * | 2012-08-30 | 2014-03-26 | 北京妙心堂医药科技有限公司 | Traditional Chinese medicine composition, preparation, and floral water and application method thereof |
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| CN103655718A (en) * | 2012-08-30 | 2014-03-26 | 北京妙心堂医药科技有限公司 | Traditional Chinese medicine composition, preparation, and floral water and application method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106148012A (en) * | 2016-08-25 | 2016-11-23 | 安徽瑞璞牡丹科技有限公司 | A kind of extracting method of mild orange blossom quintessence oil |
| CN111481455A (en) * | 2020-04-02 | 2020-08-04 | 广州市逸轩精细化工有限公司 | Floral water and preparation method thereof |
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