CN105373643B - A kind of leading edge simulation monitoring method that injection of polymer promotes - Google Patents

A kind of leading edge simulation monitoring method that injection of polymer promotes Download PDF

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CN105373643B
CN105373643B CN201510537423.1A CN201510537423A CN105373643B CN 105373643 B CN105373643 B CN 105373643B CN 201510537423 A CN201510537423 A CN 201510537423A CN 105373643 B CN105373643 B CN 105373643B
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polymer
concentration value
injection
value
sample point
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CN105373643A (en
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林杨
肖磊
张丽庆
郭艳
权国胜
王正欣
孔昭柯
刘艳华
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China Petroleum and Chemical Corp
Exploration and Development Research Institute of Sinopec Henan Oilfield Branch Co
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China Petroleum and Chemical Corp
Exploration and Development Research Institute of Sinopec Henan Oilfield Branch Co
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Abstract

The present invention relates to the leading edges that a kind of injection of polymer promotes to simulate monitoring method, belongs to oil recovering technical field.The present invention on experimental model sample point first by acquiring polymer solution concentration value;Then it is directed to the polymer concentration value that polymer solution concentration value on each sample point uses other positions of Kriging regression algorithm prediction model;The monitoring simulated to polymer advancing front is realized according to the polymer concentration value at predicted other positions of model.The present invention is in the way of mathematical geology, with Kriging regression method, according to the concentration value of several information samples inside and outside a region, a kind of estimation of linear unbias and mini-mum estimation variance is made to the region, to realize the monitoring simulated to whole region injection of polymer advancing front, and it can be adapted for the monitoring of cross-linked polymer advancing front simulation.

Description

A kind of leading edge simulation monitoring method that injection of polymer promotes
Technical field
The present invention relates to the leading edges that a kind of injection of polymer promotes to simulate monitoring method, belongs to oil recovering technical field.
Background technology
Continental deposit oil reservoir by accumulating condition because influenced, and there is one for physical property distribution of the reservoir in interlayer and layer Determine the difference of degree.The oil reservoir of waterflooding extraction, in development late stage reservoir for a long time by the water eroding and flooding of outside fluid, degree of consolidation phase It migrates therewith to poor clay mineral and part skeleton particle and exacerbates the anisotropism of reservoir, in addition unfavorable grease stream Ratio is spent, causes injection liquid to advance by leaps and bounds along high permeability zone, macropore channelling, leads to the too early water logging of oil reservoir, remaining oil saturation is relatively High less permeable layer cannot be utilized reasonably, reduce water flooding effectiveness.Such as Henan Oil Field priority since " 95 " In Shuan He, Xia Ermen, ancient city etc., totally 16 series of strata have carried out polymer flooding and secondary poly- drive industrial applications, at present polymer flooding And one of the agent technology that crosslinked polymer flooding technology has become oil field development stable yields and delays production decline.But to polymer Or the numerical simulation study of crosslinked polymer flooding, it establishes on the basis of two-dimentional two-phase and D beam element mostly, function is simpler It is single, it is difficult to meet requirement of the Oil Field with the extensive fine reservoir polymer leading edge monitoring that block is entirety.
Invention content
The object of the present invention is to provide the leading edges that a kind of injection of polymer promotes to simulate monitoring method, to meet Oil Field With the requirement that block is whole extensive fine reservoir polymer leading edge monitoring.
The present invention provides a kind of leading edge simulation monitoring method that injection of polymer promotes to solve above-mentioned technical problem, should Monitoring method includes the following steps:
1) polymer solution concentration value is acquired on three dimensional physical cast experimental model sample point;
2) it is directed to polymer solution concentration value on each sample point and uses other positions of Kriging regression algorithm prediction model Polymer concentration value;
3) prison simulated to polymer advancing front is realized according to the polymer concentration value at predicted other positions of model It surveys.
The calculating process of Kriging method is as follows in the step 2):
A. using the polymer solution concentration value acquired on sample point as initial data, experiment half is solved in a single direction and is become Different function gamma*(h), by calculating γ*(h) value is mapped, and chooses theoretical model, is found out base station and is become journey;
B. the division that super block and time block are carried out according to the information state in region to be estimated, carries out returning block to Given information point;
C. centered on super block to be estimated, increase several super blocks to the periphery as a neighborhood, carry out sliding estimation;
D. according to parameter base station, become the model of journey and selection, golden equation in foundation gram;
E. it is that constraint is adjusted with unbiasedness and mini-mum estimation variance, golden equation, makes estimated value in solution gramMost preferably, it solves It is region to be estimated to obtain result
The semivariable function γ*(h) formula is:
Wherein Z (xi) it is xiThe observation at place, i.e., in sample point xiLocate the polymer solution concentration value of acquisition;N (h) is meter Calculate the number of numerical point, the i.e. number of sample point.
Equation employed in the step D is:
WhereinTo be estimated region true value ZVEstimated value;λiFor gram in golden weight coefficient;ZiFor in estimated value neighborhood Observation.
The step 1) is to simulate reservoir plane heterogeneity using plain heterogeneity rock core, in 1 mouthful of extraction well direction High infiltration strip is set, and injection of polymer (or cross-linked polymer) solution carries out the displacement of reservoir oil, dense in each sample point acquisition polymer along journey Angle value simultaneously monitors pressure.
The beneficial effects of the invention are as follows:The present invention on experimental model sample point first by acquiring polymer solution concentration Value;Then it is dense using the polymer at other positions of Kriging regression algorithm prediction model to be directed to polymer solution value on each sample point Angle value;The monitoring simulated to polymer advancing front is realized according to the polymer concentration value at predicted other positions of model.This Invention is in the way of mathematical geology, with Kriging regression method, according to the concentration of several information samples inside and outside a region Value, a kind of estimation of linear unbias and mini-mum estimation variance is made to the region, to realize to whole region injection of polymer The monitoring of (or cross-linked polymer) advancing front simulation.
Description of the drawings
Fig. 1 is the schematic diagram that selected three dimensional physical pours model in the embodiment of the present invention;
Fig. 2 is the note cross-linked polymer pressure-plotting at ten o'clock in the embodiment of the present invention;
Fig. 3 is the note cross-linked polymer pressure-plotting on ten fours in the embodiment of the present invention;
Fig. 4 is the note cross-linked polymer pressure-plotting of ten eights in the embodiment of the present invention;
Fig. 5 is the note cross-linked polymer pressure-plotting of two twelve-hours in the embodiment of the present invention;
Fig. 6 is the note cross-linked polymer pressure-plotting on two in the embodiment of the present invention;
Note cross-linked polymer concentration profile when Fig. 7 is the first sub-sampling in the embodiment of the present invention;
Note cross-linked polymer concentration profile when Fig. 8 is the second sub-sampling in the embodiment of the present invention;
Note cross-linked polymer concentration profile when Fig. 9 is third sub-sampling in the embodiment of the present invention.
Specific implementation mode
The specific implementation mode of the present invention is described further below in conjunction with the accompanying drawings.
The features such as it is high that the present invention be directed to oil field permeabilities, and anisotropism is strong, in order to understand fully in polymer flooding injection process Displacing fluid involves range problem, the leading edge simulation monitoring method that a kind of injection of polymer proposed promotes.This method is used Kriging regression method makes one kind according to certain characteristic data values of several information samples inside and outside a region to the region The estimation of linear unbias and mini-mum estimation variance, to realize the monitoring to whole region.
Below with plain heterogeneity rock core (60*60*4.5cm) simulation reservoir plane heterogeneity (note four is adopted), this reality It is that the three dimensional physical that a note four is adopted pours model to apply the model chosen in example, and model is as shown in Figure 1, base station and change journey are ground Basic conception in matter statistics, base station refer to the particular value of experimental data, can voluntarily refer to according to the requirement of experiment of oneself The fixed numerical value (base station in the present embodiment refers to the concentration value that sampled point measures), it is other regions (in addition to sampled point) warp to become journey Cross the difference of centrifugal pump and base station value that Kriging method obtains.Permeability grade investigates 2,4 times two kinds, thereto 1 mouthful of extraction High infiltration strip is arranged in well direction, and model high infiltration strip and basic permeability choose 1200/600 × 10-3μm2, injection intensity meets It is required that cross-linked polymer carry out the displacement of reservoir oil, by along journey close sampling analyze and monitor pressure, determine that cross-linked polymer slug pushes away Into leading edge and its regularity of distribution.
1. the polymer solution concentration value (mg/l) acquired on experimental model sample point
(1) prepare rock core and installation equipment
1. with sand paper polishing rock core, ensure that core surface is smooth, cleans surface with alcohol, and dry rock core, measure rock core Size calculates apparent volume;
2. in core surface brush resinous coat, for preventing resin in casting process from largely penetrating into rock core;
3. in 5 mouthfuls of wells of upper surface drilling well of rock core, 8 pressure taps, as shown in Figure 1;
4. then rinsing rock core wellhole with clear water, and by rock core with hydrofluoric acid treatment pit shaft to prevent powder from blocking the borehole wall It is placed on drying in oven;
5. rock core well location is consolidated, rock core is put into clamper, thereto casting resin, is poured and covers clamper Model is pushed into baking oven, waits for hardening of resin by lid wherein 8 pressure taps connect sensor.
(2) initial oil, water saturation are established
1. vacuum pump is shifted to another a well, until all well locations by arbitrary a well to rock core vacuumizing to -0.1MPa It is evacuated to -0.1MPa;
2. hand pump is connected to injection well, other four mouthfuls of wells are closed, are saturated water flooding, presses and stops until pressure gauge rises After injecting a period of time, pressure does not decline, and stops injection, calculates the volume of injection water, i.e. rock pore volume;
3. being outlet water filling with constant flow pump by entrance and arbitrary a bite producing well of injection well, simultaneously closes off other three mouthfuls and adopt Oil well, the water filling into rock core record smooth pressure until pressure is steady, calculate rock core along this extraction well direction matrix permeability, separately Outer three mouthfuls of wells also repeat top-operation and measure permeability;
4. carrying out saturated oils operation, simulation oil is injected in injection well constant flow pump, waits for that arbitrary a bite extraction well is no longer discharged And it is constant it is fuel-displaced after close the well, until whole well locations saturation is fully completed, calculate saturation oil volume, and under the conditions of 81 DEG C Aging is more than 72 hours.
(3) experimental section
1. after abundant aging, a water drive is carried out with the flow of 1mL/min, each well connects Produced Liquid with test tube, and calculating contains Water rate changes, while all extraction well outlet ends are placed on same test tube every half an hour during water drive and measure rock core synthesis Moisture content, until composite water cut reaches 98%, one time water drive terminates;
2. injecting 0.1PV cross-linked polymer solutions with the flow of 0.5mL/min, solidifying, each well use in experimentation is fully waited Test tube connects Produced Liquid, calculates water-cut variation, while pressure point pressure change, and close sampling are respectively adopted in monitoring, is surveyed per half an hour Determine rock core composite water cut;
3. carrying out subsequent waterflooding with the flow of 1mL/min, monitored during water drive and respectively adopt pressure point pressure change, and intensive taken Sample, while comprehensive rock core composite water cut is measured every half an hour, until reaching 98%, experiment terminates;
4. measuring polymer concentration in each pressure tap and the sampling of each well, matched curve, as Figure 7-9, concentration value is really Surely be CdI_2-starch method measure sample point Produced Liquid polymer concentration value.
Respectively (10:00-10:15,14:00-14:15,18:00-18:15,22:00-22:15,2:00-2:15) it opens No. 1, No. 3, No. 5, No. 7 inner ring pressure taps, take liquid 15 minutes;(10:15-10:30,14:15-14:30,18:15-18:30,22: 15-22:30,2:15-2:30) No. 2, No. 4, No. 6,8 extra ring pressure taps are opened, take liquid 15 minutes;Summarize drafting injection pressure Distribution map, as shown in figures 2-6.
2. being finally inversed by the poly- of other positions of model using Kriging regression algorithm according to polymer solution value on each sample point Close object concentration value.
1) to obtain the polymer concentration value of each sample point as initial data, which is carried out at extra-high value Reason, checks whether Normal Distribution;
2) experiment with computing semivariable function, n direction;
Variation function is basic tool possessed by geostatistics, it both can be used for describing the space of regionalized variable Structure change, and its random variation can be described.Assuming that spatial point x only changes in one-dimensional x-axis, regionalized variable Z (x) The half of the difference of value at 2 points of x, x+h is defined as the semivariable functions of Z (x) in the direction of the x axis, i.e.,:
γ (x, h)=E (Z (x)-Z (x+h))/2
It is realistic on single direction to test semivariable function γ when meeting stationary hypothesis*(h) calculation formula is:
Z (x in formulai)—xiThe observation at place;
The number of N (h)-evaluation points
By calculating γ*(h) value is mapped, and chooses theoretical model (spherical, exponential model etc.), and find out base station, becomes journey.
3) division of super block and time block, and the just starting per places block and end are carried out according to the information state in region to be estimated Only number file is established, and to carrying out returning block to Given information point.
4) centered on super block to be estimated, increase several super blocks to the periphery as a neighborhood, be 8 in the present embodiment It is a, carry out sliding estimation;
5) according to parameter base station, become the model of journey and selection, seek γ (xi,xj) or r (xi, V), establish equation group.
Linear estimator is:
WhereinTo be estimated region true value ZVEstimated value;λiFor gram in golden weight coefficient;ZiFor in estimated value neighborhood Observation;Make estimated valueMost preferably, it is necessary to meet following two condition:
Unbiasedness
Estimate varianceIt is minimum
Pass through equation group:
It acquires:
Wherein λiFor gram in golden weight coefficient;γ(xi,xj) it is observation xiWith xjBetween semivariable function value;r(xi,V) For observation and the average variation function being estimated in area V between all the points;R (V, V) is to be estimated being averaged for all the points in area V Semivariable function;μ is Lagrangian constant.

Claims (4)

1. the leading edge that a kind of injection of polymer promotes simulates monitoring method, which is characterized in that the monitoring method includes the following steps:
1) polymer solution concentration value is acquired on three dimensional physical cast experimental model sample point;
2) it is directed to the polymerization that polymer solution concentration value on each sample point uses other positions of Kriging regression algorithm prediction model Object concentration value;
3) monitoring simulated to polymer advancing front is realized according to the polymer concentration value at predicted other positions of model;
The calculating process of Kriging method is as follows in the step 2):
A. using the polymer solution concentration value acquired on sample point as initial data, experiment semivariation letter is solved in a single direction Number γ*(h), by calculating γ*(h) value is mapped, and chooses theoretical model, is found out base station and is become journey;
B. the division that super block and time block are carried out according to the information state in region to be estimated, carries out returning block to Given information point;
C. centered on super block to be estimated, increase several super blocks to the periphery as a neighborhood, carry out sliding estimation;
D. according to parameter base station, become the model of journey and selection, golden equation in foundation gram;
E. it is that constraint is adjusted with unbiasedness and mini-mum estimation variance, golden equation, makes estimated value in solution gramMost preferably, solution obtains As a result it is region to be estimated.
2. the leading edge that injection of polymer according to claim 1 promotes simulates monitoring method, which is characterized in that described half becomes Different function gamma*(h) formula is:
Wherein Z (xi) it is xiThe observation at place, i.e., in sample point xiLocate the polymer solution concentration value of acquisition;N (h) is to calculate number It is worth the number of point, the i.e. number of sample point.
3. the leading edge that injection of polymer according to claim 2 promotes simulates monitoring method, which is characterized in that the step Equation employed in D is:
WhereinTo be estimated region true value ZVEstimated value;λiFor gram in golden weight coefficient;ZiFor the observation in estimated value neighborhood Value.
4. the leading edge that injection of polymer according to claim 1 promotes simulates monitoring method, which is characterized in that the step 1) it is that reservoir plane heterogeneity is simulated using plain heterogeneity rock core, high infiltration strip is set in extraction well direction, injection is strong It spends satisfactory transfer drive polymerization-filling object and carries out the displacement of reservoir oil, polymer concentration value is acquired in each sample point along journey and monitor pressure.
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