CN105352785B - Catch up with sour device and control method - Google Patents

Catch up with sour device and control method Download PDF

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Publication number
CN105352785B
CN105352785B CN201510706090.0A CN201510706090A CN105352785B CN 105352785 B CN105352785 B CN 105352785B CN 201510706090 A CN201510706090 A CN 201510706090A CN 105352785 B CN105352785 B CN 105352785B
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electromagnet
sample cup
liquid
casing
controller
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CN105352785A (en
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顾捷
刘琴
李铁军
钟志
王范盛
祝银
尤炬炬
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Zhejiang Marine Fisheries Research Institute
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Zhejiang Marine Fisheries Research Institute
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44Sample treatment involving radiation, e.g. heat

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
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  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Devices For Use In Laboratory Experiments (AREA)
  • Automatic Analysis And Handling Materials Therefor (AREA)

Abstract

The invention discloses one kind to catch up with sour device and control method, including controller, display, memory, for accommodating the casing of steam, air inlet pipe, escape pipe on casing, the support for supporting m sample cup for liquid and the first motor for driving support to rotate, m >=6;Casing is provided with heat-conducting plate, and heat-conducting plate is provided with the m grooves for being used to place sample cup for liquid.The present invention has the characteristics of security is good, catches up with sour precision height, catches up with sour quality conformance good.

Description

Catch up with sour device and control method
Technical field
The present invention relates to technical field of experiment equipment, more particularly, to a kind of security it is good, catch up with that sour precision is high, catches up with sour quality Uniformity it is good catch up with sour device and control method.
Background technology
Acid experiment is caught up with to usually require to rush to the acid solution in sample cup for liquid into the 10% of remaining former volume from original volume To 20%, experiment is needed to spend longer time, if during acid is caught up with, staff is busy to be left, in sample cup for liquid Acid solution is easy to be evaporated or steamed Jiao.Staff usually requires to operate multiple experiments simultaneously, it is impossible to look at one always Individual experiment, there is a possibility that the failure of an experiment, add experimental cost, and potential safety hazard be present.
Chinese patent mandate publication number:204085998U, publication date on January 7th, 2015 is authorized, it is auxiliary to disclose a kind of gas Acceleration is helped to catch up with sour device, including blowing needle, feeder, pressure gauge and flow-limiting valve, wherein, blowing needle is located at the examination for catching up with sour device Above pipe, blowing needle is connected by pipeline with feeder, and pressure is provided between connection blowing needle and the pipeline of feeder Power table and flow-limiting valve, feeder are air compressor, are provided with the inner tube of blowing needle for preventing acid from entering inside it One-way membrane.Weak point existing for the invention is that the acid solution of multiple sample cup for liquid can not be carried out catching up with acid.
The content of the invention
The goal of the invention of the present invention be in order to overcome it is of the prior art catch up with sour device to need artificial monitoring, it is hidden to there is safety The deficiency of trouble, there is provided a kind of security is good, catch up with sour precision is high, catch up with sour quality conformance it is good catch up with sour device and control method.
To achieve these goals, the present invention uses following technical scheme:
One kind catches up with sour device, including controller, display, memory, for accommodating the casing of steam, on casing Air inlet pipe, escape pipe, the support for supporting m sample cup for liquid and the first motor for driving support to rotate, m >=6;On casing Provided with heat-conducting plate, heat-conducting plate is provided with the m grooves for being used to place sample cup for liquid;
Temperature sensor is provided with casing, magnetic valve is equipped with air inlet pipe and escape pipe, each groove circumferentially arrange by shape Row;The support includes pillar, the horizontal strut that the m bars located at pillar upper end are radially distributed, located at each horizontal strut On annulus;Each sample cup for liquid is located in each annulus respectively;The casing at the center of circle position of each groove is provided with vertical slot, and first Motor is located in vertical slot, and the lifting structure for being used for driving the lifting of the first motor, the rotating shaft of the first motor and pillar are provided with vertical slot Lower end connects;Controller is electric with display, memory, the first motor, 2 magnetic valves, temperature sensor and lifting structure respectively Connection.
Air inlet pipe and escape pipe are used to vapor is inputted and exported into casing, and casing is used to preserve vapor, heat-conducting plate For by the heat derives in casing, each groove to be used to heat to each sample cup for liquid respectively, and elevating mechanism and the first motor are used In driving support lifting and rotation, heated so as to move on to each sample cup for liquid successively in different grooves, eliminate different grooves The influence caused by acid is caught up with of the temperature difference at place, because each sample cup for liquid heats by each groove successively, each sample cup for liquid Acid can be caught up with identical progress, eliminate the otherness for catching up with acid.The temperature that temperature sensor is used in detection case body, controller are used Analysis judgement is carried out in the data to detection, and sends control instruction.
When reach it is predetermined controller controls support to rise by elevating mechanism when catching up with the sour time, each sample cup for liquid from Recessing, so as to terminate to catch up with acid automatically, it effectively prevent the generation that the acid solution in sample cup for liquid was evaporated or steamed the problem of burnt. Conventional efficient is effectively increased, improves and catches up with sour precision, reduce experimental cost, eliminate potential safety hazard.
Therefore, the present invention is with security is good, catch up with sour precision height, catches up with sour quality conformance good;Improve and catch up with sour precision, drop The characteristics of low experimental cost.
Preferably, the lifting structure includes first located at the permanent magnet of the first motor lower portion and located at vertical slot bottom Electromagnet, the second electromagnet and the 3rd electromagnet, for the first electromagnet in cylinder, the second electromagnet and the 3rd electromagnet are in cylinder Shape, the first electromagnet are located inside the second electromagnet, and the 3rd electromagnet is located at outside the second electromagnet, and vertical slot madial wall is provided with The rib extended to inner side, permanent magnet lower surface are provided with cushion pad, and the first electromagnet, the second electromagnet and the 3rd electromagnet are equal It is electrically connected with the controller.
Preferably, the support is provided with vibrator, vibrator is electrically connected with the controller.
Preferably, the second motor is provided with the bottom half, the rotating shaft of the second motor and the montant stretched into casing Connection, montant are provided with least three helical blades.
Montant and each helical blade form agitator, and the second motor can drive agitator to disturb vapor, so that The steam temperature of each groove is identical.
Preferably, the madial wall of vertical slot is provided with least 2 guide grooves, the first motor is provided with and every guide groove phase The sliding block of cooperation, each bar guide groove upper end are equipped with baffle plate;Each sample cup for liquid is cylindrical, and each sample cup for liquid includes being located at Extension edge on top edge, each sample cup for liquid are made by tetrafluoroethene material.
A kind of control method for catching up with sour device, comprises the following steps:
(6-1) casing heats
It is provided with memory and catches up with sour duration T, the normal temperature section of casing is [A1, A2];
The magnetic valve of controller control air inlet pipe is opened, the closed electromagnetic valve of escape pipe, and air inlet pipe is passed through water to casing and steamed Vapour, the temperature in temperature sensor detection case body, as temperature >=A of casing2, the magnetic valve opening of controller control escape pipe, Deflated to casing;
As temperature≤A of casing1, the magnetic valve opening of controller control air inlet pipe, casing air inlet is given, so that casing Temperature stabilization is in [A1, A2] interval range in;
(6-2) places sample cup for liquid
The sample cup for liquid of m anti-acid corrosions is taken, the acid solution that capacity is P is added in each sample cup for liquid, by m sample Cup is placed individually on each annulus, runing rest, each sample cup for liquid is contacted with corresponding bottom portion of groove and side wall, groove Heated to sample cup for liquid;After heating L1 minutes, step (6-3) is transferred to;
(6-3) sample cup for liquid change place heats
(6-3-1) controller controls support to rise by lifting structure, the rotation of the first motor driven support;
(6-3-2) then, controller controls support to land by lifting structure, makes before each sample cup for liquid respectively enters it In the adjacent grooves of the groove at place, and sample cup for liquid is set to be contacted with corresponding bottom portion of groove and side wall;
After L1 minutes, when heating time duration < T, return to step (6-3-1);
When heating time duration >=T, controller controls support to rise by lifting structure, and each sample cup for liquid is away from recessed Groove, the information that controller control display shows current time and catches up with acid to terminate.
Preferably, lifting structure includes the permanent magnet located at the first motor lower portion and the first electromagnetism located at vertical slot bottom Iron, the second electromagnet and the 3rd electromagnet, the first electromagnet are cylindrical in shape in cylinder, the second electromagnet and the 3rd electromagnet, First electromagnet is located inside the second electromagnet, and the 3rd electromagnet is located at outside the second electromagnet, vertical slot madial wall be provided with to The rib of inner side extension, permanent magnet lower surface are provided with cushion pad, the first electromagnet, the second electromagnet and the 3rd electromagnet with Controller electrically connects;The step controller controls support to rise by lifting structure, is replaced by following step:
Controller is powered successively to the first electromagnet, the second electromagnet and the 3rd electromagnet, makes the first electromagnet, the second electricity The phase near-end polarity all same of magnet and the 3rd electromagnetism and permanent magnet, support are gradually increasing;
The step controller controls support to land by lifting structure, is replaced by following step:
Controller is powered successively to the first electromagnet, the second electromagnet and the 3rd electromagnet, makes the first electromagnet, the second electricity The phase near-end polarity of magnet and the 3rd electromagnetism and permanent magnet is contrary, and support is gradually reduced.
Preferably, support is provided with vibrator, vibrator is electrically connected with the controller;It is characterized in that
In to sample cup for liquid heating process, controller control vibrator vibrations, and step (6-3-2) is replaced by following steps Change:
Then, controller controls support to land by lifting structure, each sample cup for liquid is respectively enterd its place previous In the adjacent grooves of groove, and sample cup for liquid is set to be contacted with corresponding bottom portion of groove and side wall;
After L1 minutes, when heating time duration < 80%T, return to step (6-3-1);
When heating time duration >=80%T, controller by lifting structure control support rise, each sample cup for liquid from Recessing, the information that controller control display shows current time and catches up with acid to terminate.
The setting of vibrator, the evaporation rate of acid can be accelerated, improve conventional efficient.
Preferably, also comprise the following steps:
When heating time duration reaches after T/2, in each sample cup for liquid heating process, controller passes through elevating mechanism It is 2 millimeters to 4 millimeters to make spacing of each sample cup for liquid between corresponding bottom portion of groove, makes recess sidewall and corresponding sample Cup contact.
Preferably, being provided with the second motor in bottom half, the rotating shaft of the second motor is connected with the montant stretched into casing, Montant is provided with least three helical blades;It is characterized in that
Also comprise the following steps between step (6-1) and step (6-2):
Controller controls each helical blade rotation of the second motor driven, and the water vapour in casing is stirred.
Therefore, the present invention has the advantages that:Security is good, catches up with sour precision height, catches up with sour quality conformance good;Improve Catch up with sour precision, reduce experimental cost.
Brief description of the drawings
Fig. 1 is a kind of structural representation of the present invention;
Fig. 2 is a kind of structural representation of the support of the present invention;
Fig. 3 is a kind of structural representation of the elevating mechanism of the present invention;
Fig. 4 is a kind of structural representation of each electromagnet of the present invention;
Fig. 5 is a kind of theory diagram of the present invention;
Fig. 6 is a kind of flow chart of embodiments of the invention 1.
In figure:Controller 1, display 2, memory 3, casing 4, air inlet pipe 5, escape pipe 6, support 7, the first motor 8, lead Hot plate 9, groove 10, temperature sensor 11, magnetic valve 12, vertical slot 13, lifting structure 14, vibrator 15, the second motor 16, level Pole 71, annulus 72, permanent magnet 120, the first electromagnet 121, the second electromagnet 122, the 3rd electromagnet 123.
Embodiment
The present invention will be further described with reference to the accompanying drawings and detailed description.
Embodiment 1
Embodiment as shown in Figure 1, shown in Figure 5 is that one kind catches up with sour device, including controller 1, display 2, memory 3, is used for Accommodate the casing 4 of steam, air inlet pipe 5, escape pipe 6 on casing, the support 7 for supporting 8 sample cup for liquid and for band First motor 8 of dynamic support rotation;Casing is provided with heat-conducting plate 9, and heat-conducting plate is provided with 8 grooves for being used to place sample cup for liquid 10;Temperature sensor 11 is provided with casing, magnetic valve 12 is equipped with air inlet pipe and escape pipe, each groove circumferentially arrange by shape Row;
As shown in Fig. 2 support includes pillar, 8 horizontal struts 71 being radially distributed located at pillar upper end, is located at Annulus 72 on each horizontal strut;Each sample cup for liquid is located in each annulus respectively;As shown in Figure 1, Figure 3, each groove The casing at center of circle position is provided with vertical slot 13, and the first motor is located in vertical slot, is provided with vertical slot and is used to drive the lifting of the first motor Lifting structure 14, the rotating shaft of the first motor is connected with lower rod end;As shown in figure 5, controller respectively with display, storage Device, the first motor, 2 magnetic valves, temperature sensor and lifting structure electrical connection.
The madial wall of vertical slot is provided with 3 guide grooves, and the first motor is provided with the sliding block being engaged with every guide groove, respectively Bar guide groove upper end is equipped with baffle plate;Each sample cup for liquid is cylindrical, and each sample cup for liquid includes prolonging on top edge Side is stretched, each sample cup for liquid is made by tetrafluoroethene material.
As shown in fig. 6, a kind of control method for catching up with sour device, comprises the following steps:
Step 100, casing heats
It is provided with memory and catches up with sour duration T, the normal temperature section of casing is [A1, A2];
The magnetic valve of controller control air inlet pipe is opened, the closed electromagnetic valve of escape pipe, and air inlet pipe is passed through water to casing and steamed Vapour, the temperature in temperature sensor detection case body, as temperature >=A of casing2, the magnetic valve opening of controller control escape pipe, Deflated to casing;
As temperature≤A of casing1, the magnetic valve opening of controller control air inlet pipe, casing air inlet is given, so that casing Temperature stabilization is in [A1, A2] interval range in;
Step 200, sample cup for liquid is placed
The sample cup for liquid of 8 anti-acid corrosions is taken, the acid solution that capacity is P is added in each sample cup for liquid, by 8 samples Cup is placed individually on each annulus, runing rest, each sample cup for liquid is contacted with corresponding bottom portion of groove and side wall, groove Heated to sample cup for liquid;After heating L1 minutes, step 300 is transferred to;
Step 300, sample cup for liquid change place heats
Step 310, controller controls support to rise by lifting structure, the rotation of the first motor driven support;
Step 320, then, controller controls support to land by lifting structure, each sample cup for liquid is respectively enterd its it In the adjacent grooves of the groove at preceding place, and sample cup for liquid is set to be contacted with corresponding bottom portion of groove and side wall;
After L1 minutes, when heating time duration < T, return to step 310;
When heating time duration >=T, controller controls support to rise by lifting structure, and each sample cup for liquid is away from recessed Groove, the information that controller control display shows current time and catches up with acid to terminate.
T is 2 hours in the present embodiment;A1For 195 DEG C, A2For 205 DEG C;The vapor that air inlet pipe is input to casing is pressure 1170kpa, the vapor that 210 degrees Celsius of temperature;L1 is 3 minutes.
Embodiment 2
Embodiment 2 includes all structure and step parts in embodiment 1, as shown in Figure 3, Figure 4, the lifting of embodiment 2 Structure includes the permanent magnet 120 located at the first motor lower portion and the first electromagnet 121, the second electromagnet located at vertical slot bottom 122 and the 3rd electromagnet 123, the first electromagnet be cylindrical in shape in cylinder, the second electromagnet and the 3rd electromagnet, the first electromagnetism Iron is located inside the second electromagnet, and the 3rd electromagnet is located at outside the second electromagnet, and vertical slot madial wall, which is provided with to inner side, to be extended Rib, permanent magnet lower surface is provided with cushion pad, the first electromagnet, the second electromagnet and the 3rd electromagnet with controller electricity Connection.
Control support to rise by lifting structure the step controller of embodiment 1 in embodiment 2, replace with:
Controller is powered successively to the first electromagnet, the second electromagnet and the 3rd electromagnet, makes the first electromagnet, the second electricity The phase near-end polarity all same of magnet and the 3rd electromagnetism and permanent magnet, support are gradually increasing;
Control support to land by lifting structure the step controller of embodiment 1, replace with:
Controller is powered successively to the first electromagnet, the second electromagnet and the 3rd electromagnet, makes the first electromagnet, the second electricity The phase near-end polarity of magnet and the 3rd electromagnetism and permanent magnet is contrary, and support is gradually reduced.
Also include in embodiment 2, as shown in figure 5, support is provided with vibrator 15, vibrator is electrically connected with the controller;
In to sample cup for liquid heating process, controller control vibrator vibrations, embodiment 2 replaces the step 320 of embodiment 1 It is changed to:
Then, controller controls support to land by lifting structure, each sample cup for liquid is respectively enterd its place previous In the adjacent grooves of groove, and sample cup for liquid is set to be contacted with corresponding bottom portion of groove and side wall;
After L1 minutes, when heating time duration < 80%T, return to step 310;
When heating time duration >=80%T, controller by lifting structure control support rise, each sample cup for liquid from Recessing, the information that controller control display shows current time and catches up with acid to terminate.
Embodiment 3
Embodiment 3 includes all structure and step parts of embodiment 1, also comprises the following steps:
When heating time duration reaches after T/2, in each sample cup for liquid heating process, controller passes through elevating mechanism It is 2 millimeters to make spacing of each sample cup for liquid between corresponding bottom portion of groove, recess sidewall is contacted with corresponding sample cup for liquid.
Embodiment 3 also includes following structure:As shown in figure 5, being provided with the second motor 16 in bottom half, the second motor turns Axle is connected with the montant stretched into casing, and montant is provided with least three helical blades;
Embodiment 3 increases following steps between the step 100 and step 200 of embodiment 1:
Controller controls each helical blade rotation of the second motor driven, and the water vapour in casing is stirred.
It should be understood that the present embodiment is only illustrative of the invention and is not intended to limit the scope of the invention.In addition, it is to be understood that After having read the content of the invention lectured, those skilled in the art can make various changes or modifications to the present invention, these etc. Valency form equally falls within the application appended claims limited range.

Claims (10)

1. one kind catches up with sour device, it is characterized in that, including controller (1), display (2), memory (3), for accommodating steam Casing (4), air inlet pipe (5), escape pipe (6) on casing, the support (7) for supporting m sample cup for liquid and for driving The first motor (8) of support rotation, m >=6;Casing is provided with heat-conducting plate (9), and heat-conducting plate is provided with m and is used to place sample cup for liquid Groove (10);
Temperature sensor (11) is provided with casing, is equipped with magnetic valve (12) in air inlet pipe and escape pipe, each groove is circumferentially Shape arranges;The support includes pillar, the horizontal strut (71) that the m bars located at pillar upper end are radially distributed, located at each Annulus (72) on horizontal strut;Each sample cup for liquid is located in each annulus respectively;On the casing at the center of circle position of each groove Provided with vertical slot (13), the first motor is located in vertical slot, and the lifting structure (14) for being used for driving the lifting of the first motor is provided with vertical slot, The rotating shaft of first motor is connected with lower rod end;Controller respectively with display, memory, the first motor, 2 magnetic valves, temperature Spend sensor and lifting structure electrical connection.
2. according to claim 1 catch up with sour device, it is characterized in that, the lifting structure is included located at the first motor lower portion Permanent magnet (120) and the first electromagnet (121), the second electromagnet (122) and the 3rd electromagnet (123) located at vertical slot bottom, First electromagnet is cylindrical in shape in cylinder, the second electromagnet and the 3rd electromagnet, and the first electromagnet is located in the second electromagnet Portion, the 3rd electromagnet are located at outside the second electromagnet, and vertical slot madial wall is provided with the rib extended to inner side, permanent magnet lower surface Cushion pad is provided with, the first electromagnet, the second electromagnet and the 3rd electromagnet are electrically connected with the controller.
3. according to claim 1 catch up with sour device, it is characterized in that, the support is provided with vibrator, vibrator (15) with Controller electrically connects.
4. according to claim 1 catch up with sour device, it is characterized in that, the second motor (16) is provided with the bottom half, the The rotating shaft of two motors is connected with the montant stretched into casing, and montant is provided with least three helical blades.
5. sour device is caught up with according to claim 1 or 2 or 3 or 4, it is characterized in that, the madial wall of vertical slot is provided with least 2 Guide groove, the first motor are provided with the sliding block being engaged with every guide groove, and each bar guide groove upper end is equipped with baffle plate;Each examination Sample cup is cylindrical, and each sample cup for liquid includes the extension edge on top edge, and each sample cup for liquid is by tetrafluoroethene material Material is made.
6. a kind of control method for catching up with sour device suitable for described in claim 1, it is characterized in that, comprise the following steps:
(6-1) casing heats
It is provided with memory and catches up with sour duration T, the normal temperature section of casing is [A1, A2];
The magnetic valve of controller control air inlet pipe is opened, and the closed electromagnetic valve of escape pipe, air inlet pipe is passed through water vapour to casing, temperature The temperature spent in sensor detection box body, as temperature >=A of casing2, the magnetic valve of controller control escape pipe is opened, to casing Deflate;
As temperature≤A of casing1, the magnetic valve opening of controller control air inlet pipe, casing air inlet is given, so that the temperature of casing Stabilization is in [A1, A2] interval range in;
(6-2) places sample cup for liquid
The sample cup for liquid of m anti-acid corrosions is taken, the acid solution that capacity is P is added in each sample cup for liquid, by m sample cup for liquid point It is not placed on each annulus, runing rest, each sample cup for liquid is contacted with corresponding bottom portion of groove and side wall, groove is to examination Sample cup heats;After heating L1 minutes, step (6-3) is transferred to;
(6-3) sample cup for liquid change place heats
(6-3-1) controller controls support to rise by lifting structure, the rotation of the first motor driven support;
(6-3-2) then, controller controls support to land by lifting structure, each sample cup for liquid is respectively enterd its place previous Groove adjacent grooves in, and sample cup for liquid is contacted with corresponding bottom portion of groove and side wall;
After L1 minutes, when heating time duration < T, return to step (6-3-1);
When heating time duration >=T, controller controls support to rise by lifting structure, and each sample cup for liquid is away from groove, The information that controller control display shows current time and catches up with acid to terminate.
7. the control method according to claim 6 for catching up with sour device, lifting structure is included located at the first motor lower portion forever Magnet and the first electromagnet, the second electromagnet and the 3rd electromagnet located at vertical slot bottom, the first electromagnet in cylinder, second Electromagnet and the 3rd electromagnet are cylindrical in shape, and the first electromagnet is located inside the second electromagnet, and the 3rd electromagnet is positioned at the second electricity Outside magnet, vertical slot madial wall is provided with the rib extended to inner side, and permanent magnet lower surface is provided with cushion pad, the first electromagnetism Iron, the second electromagnet and the 3rd electromagnet are electrically connected with the controller;It is characterized in that
The step controller controls support to rise by lifting structure, is replaced by following step:
Controller is powered successively to the first electromagnet, the second electromagnet and the 3rd electromagnet, makes the first electromagnet, the second electromagnet With the phase near-end polarity all same of the 3rd electromagnetism and permanent magnet, support is gradually increasing;
The step controller controls support to land by lifting structure, is replaced by following step:
Controller is powered successively to the first electromagnet, the second electromagnet and the 3rd electromagnet, makes the first electromagnet, the second electromagnet It is contrary with the phase near-end polarity of the 3rd electromagnetism and permanent magnet, support is gradually reduced.
8. the control method according to claim 6 for catching up with sour device, support is provided with vibrator, vibrator and controller electricity Connection;It is characterized in that
In to sample cup for liquid heating process, controller control vibrator vibrations, and step (6-3-2) is replaced by following steps:
Then, controller controls support to land by lifting structure, each sample cup for liquid is respectively enterd the groove at its place previous Adjacent grooves in, and sample cup for liquid is contacted with corresponding bottom portion of groove and side wall;
After L1 minutes, when heating time duration < 80%T, return to step (6-3-1);
When heating time duration >=80%T, controller controls support to rise by lifting structure, and each sample cup for liquid is away from recessed Groove, the information that controller control display shows current time and catches up with acid to terminate.
9. the control method according to claim 6 for catching up with sour device, it is characterized in that, also comprise the following steps:
When heating time duration reaches after T/2, in each sample cup for liquid heating process, controller is made often by elevating mechanism Spacing of the individual sample cup for liquid between corresponding bottom portion of groove is 2 millimeters to 4 millimeters, recess sidewall is connect with corresponding sample cup for liquid Touch.
10. according to the control method for catching up with sour device described in claim 6 or 7 or 8 or 9, the second motor is provided with bottom half, The rotating shaft of second motor is connected with the montant stretched into casing, and montant is provided with least three helical blades;It is characterized in that
Also comprise the following steps between step (6-1) and step (6-2):
Controller controls each helical blade rotation of the second motor driven, and the water vapour in casing is stirred.
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