CN105344786A - Forming method for artificial aging-state aluminum alloy sheet - Google Patents

Forming method for artificial aging-state aluminum alloy sheet Download PDF

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Publication number
CN105344786A
CN105344786A CN201510660966.2A CN201510660966A CN105344786A CN 105344786 A CN105344786 A CN 105344786A CN 201510660966 A CN201510660966 A CN 201510660966A CN 105344786 A CN105344786 A CN 105344786A
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China
Prior art keywords
artificial aging
aluminum alloy
alloy sheet
manufacturing process
aluminium alloy
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CN201510660966.2A
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Chinese (zh)
Inventor
陈军洲
李惠曲
何维维
刘铭
伊琳娜
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BEIJING INSTITUTE OF AERONAUTICAL MATERIALS CHINA AVIATION INDUSTRY GROUP Corp
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BEIJING INSTITUTE OF AERONAUTICAL MATERIALS CHINA AVIATION INDUSTRY GROUP Corp
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Priority to CN201510660966.2A priority Critical patent/CN105344786A/en
Publication of CN105344786A publication Critical patent/CN105344786A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21DWORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21D22/00Shaping without cutting, by stamping, spinning, or deep-drawing
    • B21D22/02Stamping using rigid devices or tools
    • B21D22/06Stamping using rigid devices or tools having relatively-movable die parts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21DWORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21D37/00Tools as parts of machines covered by this subclass
    • B21D37/16Heating or cooling

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)

Abstract

The invention provides a forming method for an artificial aging-state aluminum alloy sheet. A mold is cleaned through detergent and mold cleaning glue, the roughness of the surface of the mold is improved, and scratches to the surface of a part in the forming process are reduced. A board is preheated through a rapid induction heating method, and the forming performance of materials is effectively improved. In addition, due to the fact that the heating time is short, re-dissolution of precipitated phase and recrystallization of the materials are avoided, and accordingly the performance of the materials is not changed in the heating process. Cooling treatment is conducted on the mold, heat of the part can be taken away rapidly in the forming process, and accordingly the performance of the materials is not changed in the forming process. The artificial aging-state aluminum alloy sheet is formed through the forming method, the process is simple, the cost is low, and large-scale industrial production can be achieved easily.

Description

A kind of manufacturing process of artificial aging state aluminium alloy sheet
Technical field
The present invention relates to a kind of manufacturing process of golden thin plate, specifically relate to a kind of manufacturing process of artificial aging state aluminium alloy sheet.
Background technology
Aluminium alloy, with combination properties such as its higher fracture toughness, good anti-fatigue performance and good corrosion resistances, is widely used as the agent structure of metal plate parts and aircraft.Because 7475-T761-T761 aluminium alloy sheet is through artificial aging, room temperature forming property is 1/3rd of annealed state sheet material, percentage elongation also only has about 10%, be significantly less than the percentage elongation of 20% of annealing sheet material, therefore resilience is serious after causing part forming, part manufacture process produces cracking, so, at present the annealed sheet that adopts is shaped more, carry out after shaping quenching, school shape, artificial aging.Although also can realize the manufacture of part through such PROCESS FOR TREATMENT, there is grain coarsening, intensity decline, skid wire, the surface tear such as repeating heat treatment and cause, the drawback such as energy consumption is high, production efficiency is low.Therefore, need to seek a kind of cheap for manufacturing cost, machinability better and can keep the manufacturing process of material property.
Disclosing one in CN103695817 can the synchronous quenching formed technique of heat-treatable aluminum alloy, quench comprising with aqueous medium, but need again to quench and subsequent artefacts's timeliness makes material arrive using state, this forming efficiency is lower, energy consumption is larger, and it has certain limitation, below 1.0mm sheet material is not suitable for the material of repetition heat treatment number of times.
CN102974675A discloses thermo shaping method after a kind of aluminum alloy sheet metal component solid solution shrend, this method needs mold heated, then by heat transfer, Part temperature is improved, forming property is improved, but the material processed in the prior art is at 150 DEG C ~ 400 DEG C temperature range stay longer, and the time is uncertain, this means to produce considerable influence to material property.Disclosed in prior art, (" ML377 aluminum alloy heat stability study ") shows, aluminium alloy stops more than 200 DEG C, and material property will decline to a great extent, and it is comparatively large to mold heated energy consumption, and efficiency is lower.
Summary of the invention
The object of the present invention is to provide a kind of manufacturing process of artificial aging state aluminium alloy sheet, the deficiency such as overcome that efficiency in existing preparation process of aluminium alloy is lower, energy consumption is comparatively large and material property is low, this technique have cheap for manufacturing cost, machinability better and can keep the advantages such as material property.
For achieving the above object, the present invention is by the following technical solutions:
A manufacturing process for artificial aging state aluminium alloy sheet, described method comprises following processing step:
(1) cleaning solution is prepared;
(2) cleaning die is to Ra0.6 ~ 0.8 surface roughness;
(3) clean 7475-T761 aluminum alloy slab;
(4) bed die placed successively flexible heat insulating mattress and aluminum alloy slab and be fixed;
(5) by Dry ice cleaning mold extremely-20 DEG C ~-10 DEG C surface temperatures;
(6) with eddy-current heating, with 100 DEG C/s ~ 200 DEG C/s programming rate, aluminum alloy slab is heated to 500 DEG C ~ 520 DEG C, insulation 2-3min, removes described heat insulating mattress, stamping and pressurize;
(7) part of trimming correction step (6) obtains final part shape.
First preferred version of described a kind of artificial aging state aluminium alloy sheet manufacturing process, in described step (1), by mass, described cleaning solution comprises: hydrochloric acid 40-50g, EDTA0.2-0.3 gram, corrosion inhibiter 65-70g, water 1000-1100 gram.
Second preferred version of described a kind of artificial aging state aluminium alloy sheet manufacturing process, in described step (3), described the clean of aluminum alloy slab surface is comprised: with the clean cotton wiping aluminum alloy slab surface being moistened with ethanol or acetone, to wiping cotton without after greasy dirt, the manual polishing aluminum alloy slab surface of emergy that deionized water and granularity are 20 μm is dipped in fine sand felt, at least clean 5min by deionized water again, with without oily anhydrous compressed air, aluminum alloy slab surface is dried up.
3rd preferred version of described a kind of artificial aging state aluminium alloy sheet manufacturing process, described heat insulating mattress thickness is 1 ~ 3mm.
4th preferred version of described a kind of artificial aging state aluminium alloy sheet manufacturing process, in described step (5), comprise by the step of Dry ice cleaning mold: the bar-shaped dry ice of length 7-10mm and diameter 4 ~ 8mm adds in dry ice cleaner glacial cirque by (1); (2) the rifle mouth of dry ice cleaner is vertically placed in be cleaned of the mold of 20 ~ 25mm, goes out ice amount with 2 ~ 2.5kg/min, the expulsion pressure of 9 ~ 10bar and 0.2 ~ 0.25s/cm 2cleaning speed cleans.
5th preferred version of described a kind of artificial aging state aluminium alloy sheet manufacturing process, making top mold surface temperature reach-20 DEG C ~-10 DEG C times is 30s-60s.
6th preferred version of described a kind of artificial aging state aluminium alloy sheet manufacturing process, in described step (6), insulation 2min.
7th preferred version of described a kind of artificial aging state aluminium alloy sheet manufacturing process, in described step (6), stamping speed is 50mm/s ~ 95mm/s.
8th preferred version of described a kind of artificial aging state aluminium alloy sheet manufacturing process, in described step (6), dwell time 130 ~ 180s.
Compared with immediate prior art, the present invention has following beneficial effect:
1, technical scheme provided by the invention, by using cleaning agent, clear mould glue to mold clean, improving the roughness of die surface, decreasing the scuffing to piece surface in forming process.
2, by adopting the mode of induction Fast Heating to sheet material preheating, the effective material property improved.In addition, because the heat time is short, can not there is precipitated phase back dissolving, recrystallization in material, and therefore, in heating process, material property can not change.In addition, by carrying out cooling processing to mold, can take away rapidly part heat in forming process, therefore, in forming process, material property can not change.
3, formed artificial aging state aluminium alloy sheet by the present invention, technique is simple, cost is lower, is easy to realize large-scale industrial production.
Detailed description of the invention
Below in conjunction with embodiment, be clearly and completely described technical scheme of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1:
(1) prepare cleaning solution to clean the step of die surface according to cleaning, removal black film, cleaning fluid composition is that % includes by weight: hydrochloric acid 45g, EDTA0.2g, corrosion inhibiter 65g, water 1000g.Then adopt clear mould glue to clean die surface, make mold surface roughness be Ra0.6.
(2) use the clean cotton being moistened with ethanol by clean for 7475-T761 aluminum alloy slab (thickness 1.5mm) surface wipes, nothing oil on visual cotton, manual polishing aluminum alloy slab (thickness 1.5mm) surface of emergy that deionized water and granularity are 20 μm is dipped in fine sand felt, use washed with de-ionized water piece surface to wait to brush position 5min, with without oily anhydrous compressed air, aluminum alloy slab (thickness 1.5mm) surface is dried up.
(3) be positioned over above bed die by flexible heat insulating mattress, heat insulating mattress thickness is 2mm, is positioned over by 7475-T761 aluminum alloy slab (thickness 1.5mm) above flexible heat insulating mattress also fixing.
(4) the pole shape dry ice that length is 7-10mm, diameter is 4 ~ 8mm is chosen, dry ice is joined in the glacial cirque of dry ice cleaner, by perpendicular to mold to be cleaned of the rifle mouth of dry ice cleaner, rifle mouth is apart to be cleaned 20mm, treat cleaning surface injection dry ice to clean, going out ice amount is 2.5kg/min, and expulsion pressure is 10bar, and cleaning speed is 0.25s/cm 2, after 1min, top mold surface temperature reaches-18 DEG C.
(5) after adopting the mode of (and step 4 interval 20s) eddy-current heating, with the firing rate of 100 DEG C/s, 7475-T761 aluminum alloy slab (thickness 1.5mm) is warming up to 500 DEG C immediately, insulation 3min, used time, 3s removed heat insulating mattress fast, then carrying out stamping speed is 60mm/s, pressurize 130s.
(6) to part trimming correction, final part shape is obtained, part springback capacity <0.5%.
Embodiment 2:
(1) prepare cleaning solution to clean the step of die surface according to cleaning, removal black film, cleaning fluid composition is that % includes by weight: hydrochloric acid 45g, EDTA0.2g, corrosion inhibiter 65g, water 1000g.Then adopt clear mould glue to clean die surface, make mold surface roughness be Ra0.6.
(2) use the clean cotton being moistened with ethanol by clean for 7475-T761 aluminum alloy slab (thickness 1.5mm) surface wipes, nothing oil on visual cotton, manual polishing 7475-T761 aluminum alloy slab (thickness 1.5mm) surface of emergy that deionized water and granularity are 20 μm is dipped in fine sand felt, use washed with de-ionized water piece surface to wait to brush position 10min, with without oily anhydrous compressed air, aluminum alloy slab (thickness 1.5mm) surface is dried up.
(3) be positioned over above counterdie by flexible heat insulating mattress, heat insulating mattress thickness is 1mm, is positioned over by 7475-T761 aluminum alloy slab (thickness 1.5mm) above flexible heat insulating mattress also fixing.
(4) the pole shape dry ice that length is 7-10mm, diameter is 4 ~ 8mm is chosen, dry ice is joined in the glacial cirque of dry ice cleaner, by perpendicular to mold to be cleaned of the rifle mouth of dry ice cleaner, rifle mouth is apart to be cleaned 22mm, treat cleaning surface injection dry ice to clean, going out ice amount is 2.3kg/min, and expulsion pressure is 9bar, and cleaning speed is 0.22 second/cm 2, after 2min, top mold surface temperature reaches-12 DEG C.
(5) after adopting the mode of (and step 4 interval 10s) eddy-current heating, with the firing rate of 200 DEG C/s, 7475-T761 aluminum alloy slab (thickness 1.5mm) is warming up to 520 DEG C immediately, insulation 2min, used time, 2s removed heat insulating mattress fast, then carrying out stamping speed is 70mm/s, pressurize 160s.
(6) to part trimming correction, final part shape is obtained, part springback capacity <0.5%.
Comparative example:
(1) select thickness to be 1.5mm7475-O thin plate, adopt the mould in embodiment 1 to carry out part manufacture, stamping speed is 60mm/s, pressurize 130s.
(2) part after shaping is carried out solution hardening process, solid solubility temperature is 510 DEG C, and insulation 35min, then quench in aqueous medium, water temperature is 4 DEG C.
(3) part after quenching is positioned in mould corrects shape.
(4) to part trimming correction, final part shape is obtained, part springback capacity <0.5%.
(5) after high-ranking officers' shape, part carries out secondary artificial aging, and one-level artificial aging system is 121 DEG C/3h, and secondary artificial aging system is 163 DEG C/8h.
Experimentally standard HB5143-1996, cutting sample on the slab in above-described embodiment and comparative example and part respectively, carry out tensile property test, test result is as shown in table 1.
Table 1 tensile property is tested
Above embodiment is only in order to illustrate that technical scheme of the present invention is not intended to limit; those of ordinary skill in the field are to be understood that; can modify to the specific embodiment of the present invention with reference to above-described embodiment or equivalent to replace, these do not depart from any amendment of spirit and scope of the invention or equivalently to replace within the claims that all awaits the reply in application.

Claims (9)

1. a manufacturing process for artificial aging state aluminium alloy sheet, is characterized in that described method comprises following processing step:
(1) cleaning solution is prepared;
(2) cleaning die is to Ra0.6 ~ 0.8 surface roughness;
(3) clean 7475-T761 aluminum alloy slab;
(4) bed die placed successively flexible heat insulating mattress and 7475-T761 aluminum alloy slab and be fixed;
(5) by Dry ice cleaning mold extremely-20 DEG C ~-10 DEG C surface temperatures;
(6) with eddy-current heating, with 100 DEG C/s ~ 200 DEG C/s programming rate, 7475-T761 aluminum alloy slab is heated to 500 DEG C ~ 520 DEG C, insulation 2-3min, removes described heat insulating mattress, stamping and pressurize;
(7) part of trimming correction step (6) obtains final part shape.
2. a kind of artificial aging state aluminium alloy sheet manufacturing process according to claims 1, is characterized in that, in described step (1), by mass, described cleaning solution comprises: hydrochloric acid 40-50g, EDTA0.2-0.3 gram, corrosion inhibiter 65-70g, water 1000-1100 gram.
3. a kind of artificial aging state aluminium alloy sheet manufacturing process according to claims 1, it is characterized in that, in described step (3), described the clean of aluminum alloy slab surface is comprised: with the clean cotton wiping aluminum alloy slab surface being moistened with ethanol or acetone, to wiping cotton without after greasy dirt, the manual polishing aluminum alloy slab surface of emergy that deionized water and granularity are 20 μm is dipped in fine sand felt, at least clean 5min by deionized water again, with without oily anhydrous compressed air, aluminum alloy slab surface is dried up.
4. a kind of artificial aging state aluminium alloy sheet manufacturing process according to claims 1, described heat insulating mattress thickness is 1 ~ 3mm.
5. a kind of artificial aging state aluminium alloy sheet manufacturing process according to claims 1, it is characterized in that, in described step (5), comprise by the step of Dry ice cleaning mold: the bar-shaped dry ice of length 7 ~ 10mm and diameter 4 ~ 8mm adds in dry ice cleaner glacial cirque by (1); (2) the rifle mouth of dry ice cleaner is vertically placed in be cleaned of the mold of 20 ~ 25mm, goes out ice amount with 2 ~ 2.5kg/min, the expulsion pressure of 9 ~ 10bar and 0.2 ~ 0.25s/cm 2cleaning speed cleans.
6. a kind of artificial aging state aluminium alloy sheet manufacturing process according to claims 1, it is characterized in that, making top mold surface temperature reach-20 DEG C ~-10 DEG C times is 30s-60s.
7. a kind of artificial aging state aluminium alloy sheet manufacturing process according to claims 1, is characterized in that, in described step (6), and insulation 2min.
8. a kind of artificial aging state aluminium alloy sheet manufacturing process according to claims 1, it is characterized in that, in described step (6), stamping speed is 50mm/s ~ 95mm/s.
9. a kind of artificial aging state aluminium alloy sheet manufacturing process according to claims 1, is characterized in that, in described step (6), and dwell time 130 ~ 180s.
CN201510660966.2A 2015-10-12 2015-10-12 Forming method for artificial aging-state aluminum alloy sheet Pending CN105344786A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109487184A (en) * 2018-12-28 2019-03-19 中南大学 A kind of artificial aging state high strength alumin ium alloy recurrence forming synchronous process

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102216484A (en) * 2008-09-19 2011-10-12 帝国创新有限公司 Process for forming aluminium alloy sheet components
CN102615201A (en) * 2012-04-25 2012-08-01 哈尔滨工业大学 Cold-hot compound die molding method for aluminum alloy sheet metal component
CN103128267A (en) * 2011-12-01 2013-06-05 福特全球技术公司 Method for forming an F-temper aluminum alloy
CN103447467A (en) * 2013-08-21 2013-12-18 无锡蠡湖叶轮制造有限公司 Method for cleaning metal mould
CN103469221A (en) * 2013-09-05 2013-12-25 天津东义镁制品股份有限公司 Cleaning liquor and treatment method for removing residual magnesium alloys in die
CN103695817A (en) * 2013-12-12 2014-04-02 南京航空航天大学 Heat-treatable aluminum alloy synchronous-quenching thermal-forming process
WO2014068493A1 (en) * 2012-10-31 2014-05-08 Aisin Takaoka Co., Ltd. Die-quenching method and apparatus of an aluminum alloy material
WO2014097631A1 (en) * 2012-12-21 2014-06-26 川崎重工業株式会社 Method for manufacturing aluminum alloy molded component for aircraft, and molded component for aircraft
CN104959437A (en) * 2015-07-10 2015-10-07 中南大学 Forming method for improving forming performance of 6XXX series aluminum alloy plate

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102216484A (en) * 2008-09-19 2011-10-12 帝国创新有限公司 Process for forming aluminium alloy sheet components
CN103128267A (en) * 2011-12-01 2013-06-05 福特全球技术公司 Method for forming an F-temper aluminum alloy
CN102615201A (en) * 2012-04-25 2012-08-01 哈尔滨工业大学 Cold-hot compound die molding method for aluminum alloy sheet metal component
WO2014068493A1 (en) * 2012-10-31 2014-05-08 Aisin Takaoka Co., Ltd. Die-quenching method and apparatus of an aluminum alloy material
WO2014097631A1 (en) * 2012-12-21 2014-06-26 川崎重工業株式会社 Method for manufacturing aluminum alloy molded component for aircraft, and molded component for aircraft
CN103447467A (en) * 2013-08-21 2013-12-18 无锡蠡湖叶轮制造有限公司 Method for cleaning metal mould
CN103469221A (en) * 2013-09-05 2013-12-25 天津东义镁制品股份有限公司 Cleaning liquor and treatment method for removing residual magnesium alloys in die
CN103695817A (en) * 2013-12-12 2014-04-02 南京航空航天大学 Heat-treatable aluminum alloy synchronous-quenching thermal-forming process
CN104959437A (en) * 2015-07-10 2015-10-07 中南大学 Forming method for improving forming performance of 6XXX series aluminum alloy plate

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109487184A (en) * 2018-12-28 2019-03-19 中南大学 A kind of artificial aging state high strength alumin ium alloy recurrence forming synchronous process

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Application publication date: 20160224