CN105220091A - A kind of manufacturing process of artificial aging state Al-Li alloy thin plate - Google Patents
A kind of manufacturing process of artificial aging state Al-Li alloy thin plate Download PDFInfo
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- CN105220091A CN105220091A CN201510661243.4A CN201510661243A CN105220091A CN 105220091 A CN105220091 A CN 105220091A CN 201510661243 A CN201510661243 A CN 201510661243A CN 105220091 A CN105220091 A CN 105220091A
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- artificial aging
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Abstract
The invention provides a kind of manufacturing process of artificial aging state Al-Li alloy thin plate, by using sanitising agent, clear mould glue to mold clean, improving the roughness of die surface, decreasing the scuffing to piece surface in forming process; By adopting the mode of induction rapid heating to sheet material preheating, the effective material property improved, in addition, because heat-up time is short, can not there is precipitated phase back dissolving, recrystallize in material, and therefore, in heat-processed, material property can not change; By carrying out cooling process to mold, can take away rapidly part heat in forming process, therefore, in forming process, material property can not change.Formed artificial aging state Al-Li alloy thin plate by the present invention, technique is simple, cost is lower, is easy to realize large-scale industrial production.
Description
Technical field
The present invention relates to a kind of manufacturing process of golden thin plate, specifically relate to a kind of manufacturing process of artificial aging state Al-Li alloy thin plate.
Background technology
Al-Li alloy, with over-all propertieies such as its higher fracture toughness property, good anti-fatigue performance and good solidity to corrosions, is widely used as the agent structure of metal plate parts and aircraft.Due to artificial aging state Al-Li alloy thin plate, room temperature forming property is 1/3rd of annealed state sheet material, unit elongation also only has about 10%, be significantly less than the unit elongation of 20% of annealing sheet material, therefore resilience is serious after causing part forming, portion parts manufacturing processed produces cracking, so, at present the annealed sheet that adopts is shaped more, carry out after shaping quenching, school shape, artificial aging.Although also can realize the manufacture of part through such art breading, there is grain coarsening, strength degradation, slip line, the surface tear such as repeating thermal treatment and cause, the drawback such as energy consumption is high, production efficiency is low.Therefore, need to seek a kind of cheap for manufacturing cost, workability better and can keep the manufacturing process of material property.
Disclosing one in CN103695817 can the synchronous quenching formed technique of heat-treatable aluminum alloy, quench comprising with water medium, but need again to quench and subsequent artefacts's timeliness makes material arrive using state, this forming efficiency is lower, energy consumption is larger, and it has certain limitation, below 1.0mm sheet material is not suitable for the material of repetition thermal treatment number of times.
CN102974675A discloses thermo shaping method after a kind of aluminum alloy sheet metal component solid solution shrend, this method needs mold heated, then by thermal conduction, Part temperature is improved, forming property is improved, but the material processed in the prior art is at 150 DEG C ~ 400 DEG C temperature range stay longer, and the time is uncertain, this means to produce considerable influence to material property.Disclosed in prior art, (" ML377 Al-Li alloy THERMAL STABILITY ") shows, Al-Li alloy stops more than 200 DEG C, and material property will decline to a great extent, and it is comparatively large to mold heated energy consumption, and efficiency is lower.
Summary of the invention
The object of the present invention is to provide a kind of manufacturing process of artificial aging state Al-Li alloy thin plate, the deficiency such as overcome that efficiency in existing preparation process of aluminium alloy is lower, energy consumption is comparatively large and material property is low, this technique have cheap for manufacturing cost, workability better and can keep the advantages such as material property.
For achieving the above object, the present invention is by the following technical solutions:
A manufacturing process for artificial aging state Al-Li alloy thin plate, described method comprises following processing step:
(1) cleaning solution is prepared;
(2) cleaning die is to Ra0.6 ~ 0.8 surfaceness;
(3) clean 2A97-T8 Al-Li alloy slab;
(4) bed die placed successively flexible heat insulating mattress and 2A97-T8 Al-Li alloy slab and be fixed;
(5) by Dry ice cleaning mold extremely-20 DEG C ~-10 DEG C surface temperatures;
(6) with induction heating, with 100 DEG C/s ~ 200 DEG C/s heat-up rate by 2A97-T8 Al-Li alloy heating of plate blank to 500 DEG C ~ 520 DEG C, insulation 2-5min, removes described heat insulating mattress, stamping and pressurize;
(7) part of trimming correction step (6) obtains final part shape.
First preferred version of a kind of described artificial aging state Al-Li alloy sheet moulding method, in described step (1), by mass, described cleaning solution comprises: hydrochloric acid 40-50g, EDTA0.2-0.3 gram, inhibiter 65-70g, water 1000-1100 gram.
Second preferred version of a kind of described artificial aging state Al-Li alloy sheet moulding method, in described step (3), clean comprising to described 2A97-T8 Al-Li alloy steel slab surface: by the clean cotton wiping Al-Li alloy steel slab surface being moistened with ethanol or acetone, to wiping cotton without after greasy dirt, the emergy manual polished aluminum lithium alloy steel slab surface that deionized water and granularity are 20 μm is dipped in fine sand felt, at least clean 5min with deionized water again, with without oily anhydrous pressurized air, Al-Li alloy steel slab surface is dried up.
3rd preferred version of a kind of described artificial aging state Al-Li alloy sheet moulding method, described heat insulating mattress thickness is 1 ~ 3mm.
4th preferred version of a kind of described artificial aging state Al-Li alloy sheet moulding method, in described step (5), comprise by the step of Dry ice cleaning mold: the bar-shaped dry ice of length 7-10mm and diameter 4 ~ 8mm adds in dry ice cleaner glacial cirque by (1); (2) the rifle mouth of dry ice cleaner is vertically placed in be cleaned of the mold of 20 ~ 25mm, goes out ice amount with 2 ~ 2.5kg/min, the spraying pressure of 9 ~ 10bar and 0.2 ~ 0.25s/cm
2cleaning speed cleans.
5th preferred version of a kind of described artificial aging state Al-Li alloy sheet moulding method, making top mold surface temperature reach-20 DEG C ~-10 DEG C times is 30s-60s.
6th preferred version of a kind of described artificial aging state Al-Li alloy sheet moulding method, in described step (6), insulation 3-4min.
7th preferred version of a kind of described artificial aging state Al-Li alloy sheet moulding method, in described step (6), stamping speed is 50mm/s ~ 95mm/s.
8th preferred version of a kind of described artificial aging state Al-Li alloy sheet moulding method, in described step (6), dwell time 130 ~ 180s.
Compared with immediate prior art, the present invention has following beneficial effect:
1, technical scheme provided by the invention, by using sanitising agent, clear mould glue to mold clean, improving the roughness of die surface, decreasing the scuffing to piece surface in forming process.
2, by adopting the mode of induction rapid heating to sheet material preheating, the effective material property improved.In addition, because heat-up time is short, can not there is precipitated phase back dissolving, recrystallize in material, and therefore, in heat-processed, material property can not change.In addition, by carrying out cooling process to mold, can take away rapidly part heat in forming process, therefore, in forming process, material property can not change.
3, formed artificial aging state Al-Li alloy thin plate by the present invention, technique is simple, cost is lower, is easy to realize large-scale industrial production.
Embodiment
Below in conjunction with embodiment, be clearly and completely described technical scheme of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1:
(1) prepare cleaning solution to clean the step of die surface according to cleaning, removal black film, cleaning fluid composition is that % includes by weight: hydrochloric acid 45g, EDTA0.2g, inhibiter 65g, water 1000g.Then adopt clear mould glue to clean die surface, make mold surface roughness be Ra0.6.
(2) use the clean cotton being moistened with ethanol by clean for 2A97-T8 Al-Li alloy slab (thickness 1.5mm) surface wipes, nothing oil on visual cotton, manual polished aluminum lithium alloy slab (thickness 1.5mm) surface of emergy that deionized water and granularity are 20 μm is dipped in fine sand felt, use washed with de-ionized water piece surface to wait to brush position 5min, with without oily anhydrous pressurized air, Al-Li alloy slab (thickness 1.5mm) surface is dried up.
(3) be positioned over above bed die by flexible heat insulating mattress, heat insulating mattress thickness is 2mm, is positioned over by 2A97-T8 Al-Li alloy slab (thickness 1.5mm) above flexible heat insulating mattress also fixing.
(4) the pole shape dry ice that length is 7-10mm, diameter is 4 ~ 8mm is chosen, dry ice is joined in the glacial cirque of dry ice cleaner, by perpendicular to mold to be cleaned of the rifle mouth of dry ice cleaner, rifle mouth is apart to be cleaned 20mm, treat cleaning surface injection dry ice to clean, going out ice amount is 2.5kg/min, and spraying pressure is 10bar, and cleaning speed is 0.25s/cm
2, after 1min, top mold surface temperature reaches-18 DEG C.
(5) after adopting the mode of (and step 4 interval 20s) induction heating, with the rate of heating of 150 DEG C/s, 2A97-T8 Al-Li alloy slab (thickness 1.5mm) is warming up to 500 DEG C immediately, insulation 4min, used time, 3s removed heat insulating mattress fast, then carrying out stamping speed is 60mm/s, pressurize 130s.
(6) to part trimming correction, final part shape is obtained, part springback capacity <0.5%.
(7) the minimum required time of whole preparation flow 4 points 20 seconds (not containing steps such as mold clean, school shape, trimming corrections), wherein induction heating 4 seconds, forming process 4 points 16 seconds.Compared with comparative example 1, efficiency significantly increases.
Embodiment 2:
(1) prepare cleaning solution to clean the step of die surface according to cleaning, removal black film, cleaning fluid composition is that % includes by weight: hydrochloric acid 45g, EDTA0.2g, inhibiter 65g, water 1000g.Then adopt clear mould glue to clean die surface, make mold surface roughness be Ra0.6.
(2) use the clean cotton being moistened with ethanol by clean for 2A97-T8 Al-Li alloy slab (thickness 1.5mm) surface wipes, nothing oil on visual cotton, manual polishing 2A97-T8 Al-Li alloy slab (thickness 1.5mm) surface of emergy that deionized water and granularity are 20 μm is dipped in fine sand felt, use washed with de-ionized water piece surface to wait to brush position 10min, with without oily anhydrous pressurized air, Al-Li alloy slab (thickness 1.5mm) surface is dried up.
(3) be positioned over above counterdie by flexible heat insulating mattress, heat insulating mattress thickness is 1mm, is positioned over by 2A97-T8 Al-Li alloy slab (thickness 1.5mm) above flexible heat insulating mattress also fixing.
(4) the pole shape dry ice that length is 7-10mm, diameter is 4 ~ 8mm is chosen, dry ice is joined in the glacial cirque of dry ice cleaner, by perpendicular to mold to be cleaned of the rifle mouth of dry ice cleaner, rifle mouth is apart to be cleaned 22mm, treat cleaning surface injection dry ice to clean, going out ice amount is 2.3kg/min, and spraying pressure is 9bar, and cleaning speed is 0.22 second/cm
2, after 2min, top mold surface temperature reaches-12 DEG C.
(5) after adopting the mode of (and step 4 interval 10s) induction heating, with the rate of heating of 180 DEG C/s, 2A97-T8 Al-Li alloy slab (thickness 1.5mm) is warming up to 520 DEG C immediately, insulation 3min, used time, 2s removed heat insulating mattress fast, then carrying out stamping speed is 70mm/s, pressurize 160s.
(6) to part trimming correction, final part shape is obtained, part springback capacity <0.5%.
(7) the minimum required time of whole preparation flow 3 points 47 seconds (not containing steps such as mold clean, school shape, trimming corrections), wherein induction heating 3 seconds, forming process 3 points 44 seconds.Compared with comparative example 1, efficiency significantly increases.
Comparative example:
(1) select thickness to be 1.5mm2A97-T8 Al-Li alloy annealed state thin plate, adopt the mould in embodiment 1 to carry out part manufacture, stamping speed is 60mm/s, pressurize 130s.
(2) part after shaping is carried out solution hardening process, solid solubility temperature is 510 DEG C, and insulation 35min, then quench in water medium, water temperature is 4 DEG C.
(3) part after quenching is positioned in mould corrects shape.
(4) to part trimming correction, final part shape is obtained, part springback capacity <0.5%.
(5) after high-ranking officers' shape, part carries out secondary artificial aging, and one-level artificial aging system is 121 DEG C/3h, and secondary artificial aging system is 163 DEG C/8h.
(6) the minimum required time of whole preparation flow 11 hours 37 minutes 10 seconds (not containing steps such as mold clean, school shape, trimming corrections), wherein stamping 130s, quench treatment 35min, artificial aging 11h.
Experimentally standard HB5143-1996, cutting sample on the slab in above-described embodiment and comparative example and part respectively, carry out tensile property test, test result is as shown in table 1.
Table 1 tensile property is tested
Above embodiment is only in order to illustrate that technical scheme of the present invention is not intended to limit; those of ordinary skill in the field are to be understood that; can modify to the specific embodiment of the present invention with reference to above-described embodiment or equivalent to replace, these do not depart from any amendment of spirit and scope of the invention or equivalently to replace within the claims that all awaits the reply in application.
Claims (9)
1. a manufacturing process for artificial aging state Al-Li alloy thin plate, is characterized in that described method comprises following processing step:
(1) cleaning solution is prepared;
(2) cleaning die is to Ra0.6 ~ 0.8 surfaceness;
(3) clean 2A97-T8 Al-Li alloy slab;
(4) bed die placed successively flexible heat insulating mattress and 2A97-T8 Al-Li alloy slab and be fixed;
(5) by Dry ice cleaning mold extremely-20 DEG C ~-10 DEG C surface temperatures;
(6) with induction heating, with 100 DEG C/s ~ 200 DEG C/s heat-up rate by 2A97-T8 Al-Li alloy heating of plate blank to 500 DEG C ~ 520 DEG C, insulation 2-5min, removes described heat insulating mattress, stamping and pressurize;
(7) slab of trimming correction step (6) obtains final part shape.
2. a kind of artificial aging state Al-Li alloy sheet moulding method according to claims 1, is characterized in that, in described step (1), by mass, described cleaning solution comprises: hydrochloric acid 40-50g, EDTA0.2-0.3 gram, inhibiter 65-70g, water 1000-1100 gram.
3. a kind of artificial aging state Al-Li alloy sheet moulding method according to claims 1, it is characterized in that, in described step (3), described the clean of Al-Li alloy steel slab surface is comprised: by the clean cotton wiping Al-Li alloy steel slab surface being moistened with ethanol or acetone, to wiping cotton without after greasy dirt, the emergy manual polished aluminum lithium alloy steel slab surface that deionized water and granularity are 20 μm is dipped in fine sand felt, at least clean 5min with deionized water again, with without oily anhydrous pressurized air, Al-Li alloy steel slab surface is dried up.
4. a kind of artificial aging state Al-Li alloy sheet moulding method according to claims 1, described heat insulating mattress thickness is 1 ~ 3mm.
5. a kind of artificial aging state Al-Li alloy sheet moulding method according to claims 1, it is characterized in that, in described step (5), comprise by the step of Dry ice cleaning mold: the bar-shaped dry ice of length 7-10mm and diameter 4 ~ 8mm adds in dry ice cleaner glacial cirque by (1); (2) the rifle mouth of dry ice cleaner is vertically placed in be cleaned of the mold of 20 ~ 25mm, goes out ice amount with 2 ~ 2.5kg/min, the spraying pressure of 9 ~ 10bar and 0.2 ~ 0.25s/cm
2cleaning speed cleans.
6. a kind of artificial aging state Al-Li alloy sheet moulding method according to claims 1, it is characterized in that, making top mold surface temperature reach-20 DEG C ~-10 DEG C times is 30s-60s.
7. a kind of artificial aging state Al-Li alloy sheet moulding method according to claims 1, is characterized in that, in described step (6), and insulation 3-4min.
8. a kind of artificial aging state Al-Li alloy sheet moulding method according to claims 1, it is characterized in that, in described step (6), stamping speed is 50mm/s ~ 95mm/s.
9. a kind of artificial aging state Al-Li alloy sheet moulding method according to claims 1, is characterized in that, in described step (6), and dwell time 130 ~ 180s.
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| CN201510661243.4A CN105220091B (en) | 2015-10-12 | 2015-10-12 | A kind of manufacturing process of artificial aging state aluminium lithium alloy thin plate |
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| CN201510661243.4A CN105220091B (en) | 2015-10-12 | 2015-10-12 | A kind of manufacturing process of artificial aging state aluminium lithium alloy thin plate |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109487184A (en) * | 2018-12-28 | 2019-03-19 | 中南大学 | A kind of artificial aging state high strength alumin ium alloy recurrence forming synchronous process |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103447467A (en) * | 2013-08-21 | 2013-12-18 | 无锡蠡湖叶轮制造有限公司 | Method for cleaning metal mould |
| CN103469221A (en) * | 2013-09-05 | 2013-12-25 | 天津东义镁制品股份有限公司 | Cleaning liquor and treatment method for removing residual magnesium alloys in die |
| CN103695817A (en) * | 2013-12-12 | 2014-04-02 | 南京航空航天大学 | Heat-treatable aluminum alloy synchronous-quenching thermal-forming process |
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- 2015-10-12 CN CN201510661243.4A patent/CN105220091B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103447467A (en) * | 2013-08-21 | 2013-12-18 | 无锡蠡湖叶轮制造有限公司 | Method for cleaning metal mould |
| CN103469221A (en) * | 2013-09-05 | 2013-12-25 | 天津东义镁制品股份有限公司 | Cleaning liquor and treatment method for removing residual magnesium alloys in die |
| CN103695817A (en) * | 2013-12-12 | 2014-04-02 | 南京航空航天大学 | Heat-treatable aluminum alloy synchronous-quenching thermal-forming process |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109487184A (en) * | 2018-12-28 | 2019-03-19 | 中南大学 | A kind of artificial aging state high strength alumin ium alloy recurrence forming synchronous process |
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Address after: 100095 Haidian District hot springs town, Beijing Village Patentee after: AECC BEIJING INSTITUTE OF AERONAUTICAL MATERIALS Address before: 100095 Haidian District hot springs town, Beijing Village Patentee before: AVIC BEIJING INSTITUTE OF AERONAUTICAL MATERIALS |
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