CN105312018A - Fully-intelligent variable-temperature chelating reactor - Google Patents
Fully-intelligent variable-temperature chelating reactor Download PDFInfo
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- CN105312018A CN105312018A CN201410370427.0A CN201410370427A CN105312018A CN 105312018 A CN105312018 A CN 105312018A CN 201410370427 A CN201410370427 A CN 201410370427A CN 105312018 A CN105312018 A CN 105312018A
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Abstract
The invention discloses a fully-intelligent variable-temperature chelating reactor. The fully-intelligent variable-temperature chelating reactor comprises a reactor body, a reactor cover, a liquid material input tube, three powdery material feeding hoppers, feeding metering pumps, a variable-frequency motor, a safe deflating valve, a heating coil pipe, a heat controller, a stirrer, an exterior-view liquid level tube, a temperature control meter, an end enclosure, a discharging pipeline, a shut-off valve, a discharging metering pump, an intelligent control system and a viewing window, wherein the liquid material input tube and the three powdery material feeding hoppers are arranged on the reactor cover, the feeding metering pumps are respectively mounted on the liquid material input tube and the powdery material feeding hoppers, the variable-frequency motor is mounted at the center of the reactor cover, the safe deflating valve is further mounted on the reactor cover, the heating coil pipe is arranged in the reactor, the stirrer is vertically arranged in the middle of the heating coil pipe, the exterior-view liquid level tube and the temperature control meter are mounted at the outer side of the reactor body, and the discharging pipeline is arranged at the bottom of the reactor body and communicates with the interior of the reactor. The fully-intelligent variable-temperature chelating reactor has the characteristics that feeding and discharging are accurate, laborsaving, power-saving; and liquid-state and solid-state synchronous or step-by-step feeding can be realized, so that the yield of products is increased, and the quality of the products is improved.
Description
Technical field
The present invention relates to a kind of chemical industry, chemical fertilizer reaction vessel, particularly a kind of complete intelligent alternating temperature chelatropic reaction still.
Background technology
Reactor is the reactor equipment that the industries such as oil, chemical industry, rubber, agricultural chemicals, dyestuff, medicine, food are commonly used, as equipment such as titanium reactor, laboratory reaction still, stainless steel cauldron, magnetic force reactors.China due to range of application little, in reactor apparatus field, scale is less, industrial concentration is not high, domestic keen competition affects the living space of enterprise on the one hand, be that production technology has gap compared with abroad on the other hand, lack competitiveness in the world, be mainly reflected in reactor technical matters outmoded, one be reactor feeding intake, run and discharging time mainly by Artificial Control, precision is low, labour intensity is large, crudy is unstable; Two is that the single passage that feeds intake can cause material chelatropic reaction insufficient, reduces product quality.
Summary of the invention
The object of the invention is the defect for overcoming background technology, a kind of complete intelligent alternating temperature chelatropic reaction still is provided, with meet emerging chemical industry, fertilizer industry implement product chelating technique time, need to measure multi-component masses feed intake, chelatropic reaction control, discharging control technical need.
For achieving the above object, technical scheme of the present invention is, complete intelligent alternating temperature chelatropic reaction still comprises kettle, kettle cover, liquid material input pipe, powder cast hopper, feed intake measuring pump, variable-frequency motor, safety air release valve, heating coil, heat controller, agitator, look liquid level pipe outward, temperature control meter, end socket, discharge pipe, stop valve, discharging measuring pump, intelligence control system, observation window, kettle is connected by flange seal with kettle cover, kettle cover is provided with a liquid material input pipe and three powder dog-houses, all the measuring pump that feeds intake is installed on liquid material input pipe and on powder cast hopper, center on kettle cover is provided with variable-frequency motor, kettle cover is also equipped with safety air release valve, heating coil is provided with in still, the heating of heating coil is derived end and is connected with steaming plant, heating imports after end connects heat controller and is connected with steaming plant, be provided with the agitator be made up of power transmission shaft and blade in heating coil intermediate vertical, agitator other end is connected with variable-frequency motor decelerator, looks liquid level pipe outside being provided with outside kettle, temperature control meter, communicates with in still depending on liquid level pipe lower end outward, and the temperature measuring head of temperature control meter is placed in still, and autoclave body bottom is provided with end socket, and have discharge pipe to communicate with in still in the middle of end socket, discharge pipe is separately installed with stop valve and discharging measuring pump, and feed intake measuring pump, discharging measuring pump, temperature control meter, heat controller, variable-frequency motor is controlled by intelligence control system, and kettle middle and lower part is provided with observation window 21.
Kettle is connected by flange seal with kettle cover, cleaning for convenience detach.
Kettle is double-decker, and its hollow space is filled with heat preserving and insulating material and forms heat insulation layer.
Kettle is vertical cylindrical container, and kettle, kettle cover, agitator, heating coil etc. make by stainless steel.
The present invention is directed to the defect of background technology, change constant speed and stir as frequency control is stirred, make mixing of materials even, fuel factor strengthens, and can improve reaction effect; Change Manual material feeding, discharging be that intelligent fixing quantity feeds intake, discharging, can greatly improve feed intake, discharging precision, save man-hour and manpower; The conveying changing artificial temperature adjustment, heat as intelligent synchronization control temperature and heating steam, can improve product yield; Add the passage that feeds intake, material chelatropic reaction can be made complete.
Its beneficial effect is: 1, feed intake, discharging is accurate, saving of labor, save time, laborsaving; 2, can fast reaction speed, improve product yield; 3, can realize liquid state, synchronously solid-state or substep feed intake, improve the quality of products.
Accompanying drawing and explanation
Fig. 1 is cut-away view of the present invention;
Fig. 2 is top view of the present invention.
In figure: kettle 1, kettle cover 2, liquid material input pipe 3, powder cast hopper 4-1 ~ 4-3, the measuring pump 5 that feeds intake, variable-frequency motor 6, safety air release valve 7, heating coil 8, heating derive end 9, heating imports end 10, heat controller 11, power transmission shaft 12, blade 13, looks liquid level pipe 14, temperature control meter 15, end socket 16, discharge pipe 17, stop valve 18, discharging measuring pump 19, heat insulation layer 20, observation window 21 outward
Detailed description of the invention
Below in conjunction with accompanying drawing, the present invention is described in detail.
As Fig. 1, shown in 2, the present invention includes kettle 1, kettle cover 2, liquid material input pipe 3, powder cast hopper 4-1 ~ 4-3, feed intake measuring pump 5, variable-frequency motor 6, safety air release valve 7, heating coil 8, heat controller 11, agitator, look liquid level pipe 14 outward, temperature control meter 15, end socket 16, discharge pipe 17, stop valve 18, discharging measuring pump 19, intelligence control system, observation window 21, kettle 1 is connected by flange seal with kettle cover 2, kettle cover 2 is provided with a liquid material input pipe 3 and three powder dog-house 4-1 ~ 4-3, on liquid material input pipe 3 and on powder cast hopper 4, the measuring pump 5 that feeds intake all is installed, center on kettle cover 2 is provided with variable-frequency motor 6, kettle cover 2 is also equipped with safety air release valve 7, heating coil 8 is provided with in still, the heating of heating coil 8 is derived end 9 and is connected with steaming plant, heating imports after end 10 connects heat controller 11 and is connected with steaming plant, the agitator be made up of power transmission shaft 12 and blade 13 is provided with in heating coil 8 intermediate vertical, agitator other end is connected with variable-frequency motor decelerator, looks liquid level pipe 14 outside being provided with outside kettle 1, temperature control meter 15, communicates with in still depending on liquid level pipe 14 lower end outward, and the temperature measuring head of temperature control meter 15 is placed in still, autoclave body bottom is provided with end socket 16, have discharge pipe 17 to communicate with in still in the middle of end socket 16, discharge pipe 17 is separately installed with stop valve 18 and discharging measuring pump 19, and feed intake measuring pump 5, discharging measuring pump 19, temperature control meter 15, heat controller 11, variable-frequency motor 6 is controlled by intelligence control system, and kettle 1 middle and lower part is provided with observation window 21.
Kettle 1 is double-decker, and its hollow space is filled with heat preserving and insulating material and forms heat insulation layer 20, and one can prevent operating personnel from scalding, and two is play Winter protection effect.
Stop valve 18 is mainly used in trouble hunting, maintenance, is in normally open when reactor normally works.
Specific embodiment: will treat that the powder of chelatropic reaction raw material adds in powder cast hopper 4-1 ~ 4-3 respectively, insert under the liquid level in liquid material container after liquid material input pipe 3 is connected flexible pipe, start raw material quantitative and add program, liquid material is quantitatively drawn in still by the measuring pump 5 that feeds intake by flexible pipe, open steam cock valve, steam enters heating coil 8 from heating importing end 10 by heat controller 11 and returns from heating derivation end 9, circulation is to heat temperature raising in still, now variable-frequency motor 6 starts, drive agitator Stirring, then according to the order of addition of chelatropic reaction raw material, the measuring pump 5 that feeds intake controlling three powder cast hopper 4-1 ~ 4-3 starts thereupon, make three groups of powders according to respective ratio requirement, quantitatively respectively add in still from respective powder cast hopper 4, different materials carries out chelatropic reaction by the stirring of friction speed at the temperature of setting, staff can observe chelatropic reaction situation at any time from observation window 21, temperature control meter 15 is monitored heating-up temperature by the operating temperature of setting, when temperature control meter 15 detects the temperature that chelatropic reaction completes, control instruction can be sent to heat controller 11 by intelligence control system, steam is imported end 10 from heating and closes by heat controller 11, after the chelatropic reaction time of setting to be achieved, discharging measuring pump 19 starts, from discharge pipe 17 quantitative discharging.
Claims (2)
1. a complete intelligent alternating temperature chelatropic reaction still, it is characterized in that, comprise kettle (1), kettle cover (2), liquid material input pipe (3), powder cast hopper (4-1 ~ 4-3), feed intake measuring pump (5), variable-frequency motor (6), safety air release valve (7), heating coil (8), heat controller (11), agitator, look liquid level pipe (14) outward, temperature control meter (15), end socket (16), discharge pipe (17), stop valve (18), discharging measuring pump (19), intelligence control system, observation window (21), kettle (1) is connected by flange seal with kettle cover (2), kettle cover (2) is provided with a liquid material input pipe (3) and three powder dog-houses (4-1 ~ 4-3), liquid material input pipe (3) above and on powder cast hopper (4) is all provided with the measuring pump that feeds intake (5), center on kettle cover (2) is provided with variable-frequency motor (6), safety air release valve (7) kettle cover (2) is also equipped with, heating coil (8) is provided with in still, the heating of heating coil (8) is derived end (9) and is connected with steaming plant, heating imports after end (10) connects heat controller (11) and is connected with steaming plant, the agitator be made up of power transmission shaft (12) and blade (13) is provided with in heating coil (8) intermediate vertical, agitator other end is connected with variable-frequency motor decelerator, liquid level pipe (14) is looked outside kettle (1) outside is provided with, temperature control meter (15), communicate with in still depending on liquid level pipe (14) lower end outward, the temperature measuring head of temperature control meter (15) is placed in still, autoclave body bottom is provided with end socket (16), discharge pipe (17) is had to communicate with in still in the middle of end socket (16), discharge pipe (17) is separately installed with stop valve (18) and discharging measuring pump (19), feed intake measuring pump (5), discharging measuring pump (19), temperature control meter (15), heat controller (11), variable-frequency motor (6) is controlled by intelligence control system, kettle (1) middle and lower part is provided with observation window (21).
2. the complete intelligent alternating temperature chelatropic reaction still of one according to claim 1, it is characterized in that, kettle (1) is double-decker, and its hollow space is filled with heat preserving and insulating material and forms heat insulation layer (20).
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CN201410370427.0A CN105312018B (en) | 2014-07-31 | 2014-07-31 | Full intelligence alternating temperature chelatropic reaction kettle |
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CN201410370427.0A CN105312018B (en) | 2014-07-31 | 2014-07-31 | Full intelligence alternating temperature chelatropic reaction kettle |
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CN105312018B CN105312018B (en) | 2018-05-25 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105797670A (en) * | 2016-05-26 | 2016-07-27 | 安庆盛峰化工股份有限公司 | Diisobutyl phthalate neutralizing, washing and dealcoholizing integrated reaction kettle |
CN105837443A (en) * | 2016-05-26 | 2016-08-10 | 安庆盛峰化工股份有限公司 | Diisobutyl phthalate production mechanism |
CN107335396A (en) * | 2017-08-28 | 2017-11-10 | 浙江新时代海创锂电科技有限公司 | One kind heating annexs formula synthesis reactor with water conservancy diversion |
CN108295790A (en) * | 2018-04-11 | 2018-07-20 | 吉林工程技术师范学院 | A kind of Hydrin polymerization reaction kettle and its control method |
Citations (4)
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JPS61283338A (en) * | 1985-06-11 | 1986-12-13 | Michio Watanabe | Stirring tank type reaction apparatus |
CN201357070Y (en) * | 2009-02-04 | 2009-12-09 | 宁波科博特钴镍有限公司 | Spherical cobaltosic oxide reaction kettle |
CN203196633U (en) * | 2013-03-04 | 2013-09-18 | 三惠(福建)工贸有限公司 | Measuring-conveying system for alkali liquor |
CN203253428U (en) * | 2013-03-31 | 2013-10-30 | 湖北海翔化工科技有限公司 | Full-automatic multi-kettle charging production system for producing scale-inhibiting dispersion polymer |
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2014
- 2014-07-31 CN CN201410370427.0A patent/CN105312018B/en active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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JPS61283338A (en) * | 1985-06-11 | 1986-12-13 | Michio Watanabe | Stirring tank type reaction apparatus |
CN201357070Y (en) * | 2009-02-04 | 2009-12-09 | 宁波科博特钴镍有限公司 | Spherical cobaltosic oxide reaction kettle |
CN203196633U (en) * | 2013-03-04 | 2013-09-18 | 三惠(福建)工贸有限公司 | Measuring-conveying system for alkali liquor |
CN203253428U (en) * | 2013-03-31 | 2013-10-30 | 湖北海翔化工科技有限公司 | Full-automatic multi-kettle charging production system for producing scale-inhibiting dispersion polymer |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105797670A (en) * | 2016-05-26 | 2016-07-27 | 安庆盛峰化工股份有限公司 | Diisobutyl phthalate neutralizing, washing and dealcoholizing integrated reaction kettle |
CN105837443A (en) * | 2016-05-26 | 2016-08-10 | 安庆盛峰化工股份有限公司 | Diisobutyl phthalate production mechanism |
CN107335396A (en) * | 2017-08-28 | 2017-11-10 | 浙江新时代海创锂电科技有限公司 | One kind heating annexs formula synthesis reactor with water conservancy diversion |
CN108295790A (en) * | 2018-04-11 | 2018-07-20 | 吉林工程技术师范学院 | A kind of Hydrin polymerization reaction kettle and its control method |
CN108295790B (en) * | 2018-04-11 | 2023-09-08 | 吉林工程技术师范学院 | Poly (epichlorohydrin) polymerization reaction kettle and control method thereof |
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