CN105295429A - Preparing method for plant dye - Google Patents

Preparing method for plant dye Download PDF

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Publication number
CN105295429A
CN105295429A CN201510693025.9A CN201510693025A CN105295429A CN 105295429 A CN105295429 A CN 105295429A CN 201510693025 A CN201510693025 A CN 201510693025A CN 105295429 A CN105295429 A CN 105295429A
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CN
China
Prior art keywords
parts
sargent gloryvine
hours
vegetable dye
boiled
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Pending
Application number
CN201510693025.9A
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Chinese (zh)
Inventor
毕成林
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Anqing Fengyu Agriculture And Forestry Development Co Ltd
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Anqing Fengyu Agriculture And Forestry Development Co Ltd
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Application filed by Anqing Fengyu Agriculture And Forestry Development Co Ltd filed Critical Anqing Fengyu Agriculture And Forestry Development Co Ltd
Priority to CN201510693025.9A priority Critical patent/CN105295429A/en
Publication of CN105295429A publication Critical patent/CN105295429A/en
Pending legal-status Critical Current

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  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Enzymes And Modification Thereof (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention relates to the field of plant dyes, in particular to a preparing method for a plant dye. The method comprises the steps that firstly, by weight, 5 parts of digitaria ciliaris is selected, and 1 part of cellulase, 1 part of pectinase and 1 part of protease are added into a water solution accounting for 100 parts, boiled, stirred and filtered to obtain filter liquor, wherein the pH of the water solution is 4; secondly, sargentg loryvine stems are mashed, and a minced sargentg loryvine stem material is obtained; thirdly, the filter liquor prepared in the first step is added into the minced sargentg loryvine stem material prepared in the second step and stirred, and a mixture is obtained; fourthly, the mixture prepared in the third step is boiled and maintained for 5-6 hours in boiling, and the plant dye is obtained. By means of the method, the problems that synthetic dyes contain carcinogenic substances, can damage the human bodies and are not environmentally friendly are solved.

Description

A kind of preparation method of vegetable dye
Technical field
The present invention relates to field of plant dye, especially a kind of preparation method of vegetable dye.
Background technology
Dyestuff to make fiber and the painted material of other materials, it in use directly contacts the skin of people, synthetic dyestuff conventional at present, and its raw material and intermediate are often containing carinogenicity material, not only severe contamination environment, also makes direct wearer or the producer come to harm.Along with the raising of quality of life, people more and more pay close attention to health, pursue the product of ecosystem and natural material, and the natural dyestuff extracted from plant materials, because itself and Environmental compatibility are good, biodegradable, nontoxic, even to human body, there is the favor that special health-care effect is subject to people; Glutene Rice Grass and Sargent gloryvine are two kinds of herbal medicine, and Glutene Rice Grass is the whole herb with root of contrayerva Herba Gonostegiae Hirtae, and its meridian distribution of property and flavor is pungent, puckery, cool, has strengthening the spleen to promote digestion, clearing heat and detoxicating, effect of synthetism myogenic.Sargent gloryvine is called: Stem of Sargentgloryvine, and Classification system: Sargentodoxacuneata. is Lardizabalaceae, Saggentodoxa fallen leaves, bejuco; Stem sorrel; Compound leaf three goes out, alternate; Bitter, property is put down; There is the baidu powder stasis of blood promoting blood circulation and removing obstruction in channels, effect of wind dispelling insecticide.At present, Glutene Rice Grass and Sargent gloryvine is not also utilized to prepare the report of dyestuff.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of preparation method of vegetable dye, and this method can solve synthetic dyestuff and contain carinogenicity material, damages and problem not environmentally to human body.
In order to solve the problem, the technical solution adopted in the present invention is: the preparation method of this vegetable dye, adopts the raw material of following parts by weight:
Glutene Rice Grass 4 parts ~ 5 parts; Sargent gloryvine 6 parts ~ 7 parts;
Its making step is as follows:
A, choose Glutene Rice Grass 5 parts, be ground into powder with medicinal herb grinder, be placed in extractor, add cellulase 1 part, polygalacturonase 1 part, 1 part, proteolytic enzyme in the aqueous solution of 100 parts of pH=4, boil to seething with excitement and keeping 15 minutes ~ 25 minutes, stir in the process of boiling, refilter and obtain filtrate;
B, Sargent gloryvine to be smashed to pieces, obtain Sargent gloryvine gruel material;
C, filtrate steps A obtained add in the obtained Sargent gloryvine gruel material of step B, and stir 0.5-1 hour, obtain compound;
D, compound obtained for step C to be boiled to seething with excitement and keeping 5 hours ~ 6 hours, obtain this vegetable dye.
In technique scheme, technical scheme can also be more specifically: described vegetable dye is mauve dyestuff.
Owing to have employed technique scheme, the present invention compared with prior art has following beneficial effect:
The present invention is prepared from natural herbal medicine Glutene Rice Grass and Sargent gloryvine, and unharmful substance adds in whole preparation process, do not have harmful waste to produce, its obtained dyestuff natural environmental-protective, to human body, there is strengthening the spleen to promote digestion, clearing heat and detoxicating yet, effect of promoting blood circulation and removing obstruction in channels and wind dispelling insecticide, the fabric, the dress ornament that contaminate be red-purple, color even, the soft nature of color and luster, colour fastness is higher, not easily fades, variable color.
Embodiment
For below in conjunction with embodiment, the invention will be further described:
Embodiment one
The preparation method of this vegetable dye, adopts the raw material of following weight:
Glutene Rice Grass 4 kilograms; Sargent gloryvine 6 kilograms;
Its making step is as follows:
A, choose Glutene Rice Grass 4 kilograms, powder is ground into medicinal herb grinder, be placed in extractor, add cellulase 100 milligrams, polygalacturonase 100 milligrams, 100 milligrams, proteolytic enzyme in the aqueous solution of 100 kilograms of pH=4, boil to seething with excitement and keeping 15 minutes ~ 25 minutes, stir in the process of boiling, refilter and obtain filtrate;
B, Sargent gloryvine to be smashed to pieces, obtain Sargent gloryvine gruel material;
C, filtrate steps A obtained add in the obtained Sargent gloryvine gruel material of step B, and stir 0.5-1 hour, obtain compound;
D, compound obtained for step C to be boiled to seething with excitement and keeping 5 hours ~ 6 hours, obtain this vegetable dye.
Embodiment two
The preparation method of this vegetable dye, adopts the raw material of following weight:
Glutene Rice Grass 5 kilograms; Sargent gloryvine 6.8 kilograms;
Its making step is as follows:
A, choose Glutene Rice Grass 5 kilograms, powder is ground into medicinal herb grinder, be placed in extractor, add cellulase 150 milligrams, polygalacturonase 150 milligrams, 150 milligrams, proteolytic enzyme in the aqueous solution of 150 kilograms of pH=4, boil to seething with excitement and keeping 15 minutes ~ 25 minutes, stir in the process of boiling, refilter and obtain filtrate;
B, Sargent gloryvine to be smashed to pieces, obtain Sargent gloryvine gruel material;
C, filtrate steps A obtained add in the obtained Sargent gloryvine gruel material of step B, and stir 0.5-1 hour, obtain compound;
D, compound obtained for step C to be boiled to seething with excitement and keeping 5 hours ~ 6 hours, obtain this vegetable dye.
Embodiment three
The preparation method of this vegetable dye, adopts the raw material of following weight:
Glutene Rice Grass 4.5 kilograms; Sargent gloryvine 7 kilograms;
Its making step is as follows:
A, choose Glutene Rice Grass 4.5 kilograms, powder is ground into medicinal herb grinder, be placed in extractor, add cellulase 120 milligrams, polygalacturonase 120 milligrams, 120 milligrams, proteolytic enzyme in the aqueous solution of 120 kg pH=4, boil to seething with excitement and keeping 15 minutes ~ 25 minutes, stir in the process of boiling, refilter and obtain filtrate;
B, Sargent gloryvine to be smashed to pieces, obtain Sargent gloryvine gruel material;
C, filtrate steps A obtained add in the obtained Sargent gloryvine gruel material of step B, and stir 0.5-1 hour, obtain compound;
D, compound obtained for step C to be boiled to seething with excitement and keeping 5 hours ~ 6 hours, obtain this vegetable dye.
More than show and describe ultimate principle of the present invention, principal character and advantage.The technician of the industry should understand; the present invention is not restricted to the described embodiments; description in above-described embodiment and specification sheets principle of the present invention is just described; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.

Claims (2)

1. a preparation method for vegetable dye, is characterized in that: the raw material adopting following parts by weight: Glutene Rice Grass 4 parts ~ 5 parts; Sargent gloryvine 6 parts ~ 7 parts;
Its making step is as follows:
A, choose Glutene Rice Grass 5 parts, be ground into powder with medicinal herb grinder, be placed in extractor, add cellulase 1 part, polygalacturonase 1 part, 1 part, proteolytic enzyme in the aqueous solution of 100 parts of pH=4, boil to seething with excitement and keeping 15 minutes ~ 25 minutes, stir in the process of boiling, refilter and obtain filtrate;
B, Sargent gloryvine to be smashed to pieces, obtain Sargent gloryvine gruel material;
C, filtrate steps A obtained add in the obtained Sargent gloryvine gruel material of step B, and stirring obtains compound;
D, compound obtained for step C to be boiled to seething with excitement and keeping 5 hours ~ 6 hours, obtain this vegetable dye.
2. the preparation method of vegetable dye according to claim 1, is characterized in that: in described step C, and churning time is 0.5-1 hour.
CN201510693025.9A 2015-10-20 2015-10-20 Preparing method for plant dye Pending CN105295429A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510693025.9A CN105295429A (en) 2015-10-20 2015-10-20 Preparing method for plant dye

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510693025.9A CN105295429A (en) 2015-10-20 2015-10-20 Preparing method for plant dye

Publications (1)

Publication Number Publication Date
CN105295429A true CN105295429A (en) 2016-02-03

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106189356A (en) * 2016-08-19 2016-12-07 南丹绣玉工艺品有限公司 Vegetable colour
CN108948781A (en) * 2018-07-04 2018-12-07 武汉纺织大学 The preparation method of spun gold emperor's chrysanthemum natural dye and the natural dye and colouring method prepared by this method

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103013936A (en) * 2012-12-25 2013-04-03 浙江惠松制药有限公司 Method for extracting anthocyanidin by using compound enzyme, and compound enzyme preparation thereof
CN103696277A (en) * 2013-12-20 2014-04-02 大连创达技术交易市场有限公司 Technology for dyeing cotton cloth by using safflower vegetable dye
CN104499310A (en) * 2015-01-06 2015-04-08 南丹绣玉工艺品有限公司 Cloth dyeing method of national dress
CN104497624A (en) * 2015-01-06 2015-04-08 南丹绣玉工艺品有限公司 Preparation method of vegetable dye

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103013936A (en) * 2012-12-25 2013-04-03 浙江惠松制药有限公司 Method for extracting anthocyanidin by using compound enzyme, and compound enzyme preparation thereof
CN103696277A (en) * 2013-12-20 2014-04-02 大连创达技术交易市场有限公司 Technology for dyeing cotton cloth by using safflower vegetable dye
CN104499310A (en) * 2015-01-06 2015-04-08 南丹绣玉工艺品有限公司 Cloth dyeing method of national dress
CN104497624A (en) * 2015-01-06 2015-04-08 南丹绣玉工艺品有限公司 Preparation method of vegetable dye

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
杨再 等: "天然植物有效成分的提取新技术-生物酶解技术", 《饲料博览》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106189356A (en) * 2016-08-19 2016-12-07 南丹绣玉工艺品有限公司 Vegetable colour
CN108948781A (en) * 2018-07-04 2018-12-07 武汉纺织大学 The preparation method of spun gold emperor's chrysanthemum natural dye and the natural dye and colouring method prepared by this method

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