CN105287235B - A kind of nano grade biological fiber whitening mask and its application method - Google Patents
A kind of nano grade biological fiber whitening mask and its application method Download PDFInfo
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- CN105287235B CN105287235B CN201510831447.8A CN201510831447A CN105287235B CN 105287235 B CN105287235 B CN 105287235B CN 201510831447 A CN201510831447 A CN 201510831447A CN 105287235 B CN105287235 B CN 105287235B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/21—Emulsions characterized by droplet sizes below 1 micron
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/51—Chelating agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/88—Two- or multipart kits
- A61K2800/882—Mixing prior to application
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/88—Two- or multipart kits
- A61K2800/884—Sequential application
Abstract
The invention discloses a kind of nano grade biological fiber whitening mask and its application methods.The nano grade biological fiber whitening mask, is made of nano grade biological tunica fibrosa and whitening nanoemulsions.The present invention is the fiber fines diameter using about 10 50 nanometers on nano biological tunica fibrosa; because it is tiny compared with sulci of skin; it can go deep into sulci of skin; therefore it can increase the surface area of nanoemulsions contact skin; in combination with nanoemulsions to the protective effect of whitening composition and the osmosis strong to skin; the bioavailable efficiency for improving functional component, to preferably play whitening effect in a relatively short period of time.
Description
Technical field
The present invention relates to a kind of facial masks, belong to cosmetic technical field, and in particular to a kind of nano grade biological fiber whitening
Facial mask and its application method.
Background technology
For mask product using more and more extensive, just nourishing nursing product by original deep layer becomes operational maintenance product.Mounted facial mask
Due to can load various facial treatment essence and it is easy to use the features such as, just become facial mask new lover at present.It is well known that patch
The best whitening effect that mainly obtained using purpose of formula whitening mask uses skin sense with preferable, therefore can facial mask cloth be given
Whitening composition in docile skin sense that skin has been brought, facial mask can rapid osmotic enter skin surface and play white-skinned face function to have become
Judge the major criterion of whitening mask quality.
Although Chinese patent CN102525837 provides a kind of bacteria cellulose membrane product containing astaxanthin, but the production
Product are that astaxanthin and other functional ingredient is added into culture medium of bacterial cellulose, then utilize the culture medium fermentation added with functional component
Culture is made.The Biofibre facial mask that Chinese patent CN201180052055 is provided is also that bacteria cellulose training is added in ginseng liquid
Base is supported, is made by static culture.It is this that biological facial mask obtained in static culture liquid is added in functional component, although certain journey
The stability of functional component is protected on degree, but in facial mask in use, since functional component is firmly locked in facial mask internal junction
In structure, to being short of power for Cutaneous permeation, slow and permanent release functional component is needed, but the usage time of facial mask is very
It is short, it is 20-30 minutes general, most of functional component can be caused to remain on inside facial mask within the time short in this way, cause work(
The utilization ratio of effect ingredient can substantially reduce.
Although Chinese patent CN102178639 also provides a kind of preparation side of the bacterial cellulose wet-coating lightened the stain
Method, whitening composition used in this method are that plurality of Chinese decocts later solution, but not to the mixing effect in the technology
Ingredient carries out nanoscale emulsification package protection, causes for a long time under light, heat, oxygen environment, the bioactivity meeting of these functional components
It continuously decreases, simultaneously because the Chinese Medicines color and luster after infusion is deeper, is easy to influence the appearance of product.
In summary, in existing mounted whitening mask product there is facial mask cloth cannot well docile skin, effect at
Divide stability bad, and be unable to rapid osmotic and enter the multiple technologies problem such as skin surface, needs those skilled in the art further
Improve perfect necessity.
Invention content
Of the existing technology in order to solve the problems, such as, the purpose of the present invention is to provide a kind of nano grade biological fiber whitenings
Facial mask, it is possible to increase nanoemulsions contact the surface area of skin, in combination with nanoemulsions to the protective effect of whitening composition and right
The strong osmosis of skin, improves the bioavailable efficiency of functional component, beautiful so as to preferably play in a relatively short period of time
White effect.
It is a further object of the present invention to provide a kind of application methods of nano grade biological fiber facial mask.
The purpose of the present invention is achieved through the following technical solutions：
A kind of nano grade biological fiber whitening mask, is made of nano grade biological tunica fibrosa and whitening nanoscale emulsion.
The fibre diameter of nano grade biological fiber of the present invention at 10-50 nanometers, for 10-30 receive by more preferable fibre diameter
Rice.
Nano grade biological tunica fibrosa of the present invention was to use the wooden glucose acetobacter as fermentation strain, by 8-16 days
Static culture after the bacteria cellulose mycoderm that is formed.
Nano grade biological tunica fibrosa of the present invention is squeezed by flat-plate compressed water or double roller by nanometer bacteria cellulose
Row dehydration, obtains half wet film of nanometer bacteria cellulose.
Nanoemulsions of the present invention are by oil, surfactant, soluble small molecular, white-skinned face function ingredient, essence, prevent
Rotten agent and soft water etc. form pre-composition, are then homogenized to be formed to pre-composition high-pressure.
The grain size of whitening nanoemulsions of the present invention is more than 90% at 10-300 nanometers, preferably the grain of whitening nanoemulsions
Diameter is more than 90% at 10-150 nanometers.
Whitening nanoemulsions of the present invention include each raw material component of following weight percent：
The oil of 1%-22%；The oil is selected from oil with hydrogenated soybean, Queensland nut seed oil, jojoba oil, corn oil, avocado
Oil, mineral oil.
The emulsifier and emulsion adjuvant of 1%-8%；The emulsifier is selected from hexadecanyl phosphate sylvite, stearoylketene Ji Gu
Propylhomoserin sodium, stearoylketene base-sodium cocoyl glutamate；
The soluble small molecular of 1%-60%%；The soluble small molecular is selected from glycerine, 1,3 butanediol, propylene glycol；
The white-skinned face function ingredient of 0.1%-20%；The white-skinned face function ingredient includes ursin, 2 glucose of L-AA
At least one of glycosides, glycyrrhiza glabra extract, Pomegranate Peel Extract and its mixture；
The additive of 1%-90%, the additive include neutralizer, chelating agent, essence, preservative, thickener, pigment
And soft water.
The white-skinned face function ingredient of whitening nanoemulsions of the present invention includes ursin, 2 glucoside of L-AA, light fruit
At least one of licorice, Pomegranate Peel Extract and its mixture.
Wherein ursin is alpha-arbutin, and specific rotatory power is at+150.0 ° -+200.0 °.
A kind of application method of nano grade biological fiber whitening mask of the present invention, is carried with nano grade biological tunica fibrosa
Body adsorbs whitening nanoemulsions, is made whitening mask product, and when use directly opens facial mask bag, overlays on one on purported skin
It is removed after fixing time.
The application method of another kind nano grade biological fiber whitening mask of the present invention, is by nano grade biological tunica fibrosa
It is individually packed with whitening nanoemulsions, latter two right packaging is bundled as mask product.First by whitening nanometer when use
Lotion is coated on purported skin, is then covered with membrane of biological fibers stop again and is removed after a certain period of time.Or it will be biological fine when using
Dimension film impregnates certain time in whitening nanoemulsions, and the membrane of biological fibers containing nanoemulsions is then overlayed on purported skin again
Upper stop is removed after a certain period of time.
Compared with prior art, advantage of the invention is that：
The present invention is the fiber fines diameter using about 10-50 nanometers on nano biological tunica fibrosa, because it is tiny compared with sulci of skin,
It can go deep into sulci of skin, increase the surface area of nanoemulsions contact skin, the protection of whitening composition is made in combination with nanoemulsions
With with the osmosis strong to skin, improve the bioavailable efficiency of functional component, so as in a relatively short period of time preferably
Play whitening effect.
Description of the drawings
Fig. 1 subject evaluates figure to the beauty functions of embodiment 4.
Fig. 2 subject evaluates figure to the beauty functions of embodiment 5.
Specific implementation mode
Below by specific preferred embodiment combination attached drawing, the present invention is done and is further described in detail, but the present invention
Realization method is not limited thereto.
A kind of nano grade biological fiber whitening mask of the present invention, is the nano grade biological fiber by 10-50 nanometer ranges
Film and comprising white-skinned face function ingredient whitening nanoscale emulsion composition, which includes ursin, L-AA 2
At least one of glucoside, glycyrrhiza glabra extract, Pomegranate Peel Extract and its mixture.
We have found that whitening face made of the membrane of biological fibers cooperation nanoscale whitening emulsion of a diameter of 10-50 nanometer ranges
Film can go deep into sulci of skin since fibre diameter is very tiny, have good docile effect to skin, while can help essence
The extraordinary infiltration sulci of skin of effect ingredient in liquid increases the contact area of nanoemulsions and skin.On the other hand, nanoemulsions
The stability of white-skinned face function ingredient can not only be increased, while skin surface can be penetrated into faster, it within a short period of time can be with
Greatly improve the utilization ratio of functional component.
Embodiment 1
1) preparation of nanoemulsions：
2.0g oil with hydrogenated soybean is weighed, 5.0g jojoba oils are weighed, weighs 3.0g mineral oil, weighs 0.7g cetyl phosphorus
Acid esters sylvite weighs 0.3g polyethylene glycol 400 isostearates, weighs 0.1g alpha-arbutins, is heated to 45 DEG C and is uniformly mixed,
Then homogeneous stirs, and A phases are made；10g glycerine, 1,3 butanediols of 5g are weighed, appropriate soft water is uniformly mixed, and B phases are made；By A phases
It is mixed together with B, obtains pre-composition, it is equal to be then subjected to 6 cycles by 1300 bars of high pressure homogenisers for pre-composition
Matter is then cooled to room temperature, and obtains nanoemulsions.90% or more nanoemulsions grain size obtained is at 10-90 nanometers.
2) preparation of nano biological whitening mask：
Fermentation strain will be used as by the wooden glucose acetobacter, the bacteria cellulose formed after 10 days static cultures
Mycoderm double roller extrusion dehydration, 10-50 nanometers of fibre diameter, then carries out ionising radiation disinfection to it, is put into sterile facial mask bag,
The nanoemulsions of 28g are finally added into facial mask bag, mask product is made in sealing facial mask bag.
3) use of nano biological whitening mask：
In use, facial mask bag is opened, the membrane of biological fibers containing nanoemulsions is overlayed on and stops 30 points on purported skin
It is removed after clock.
Embodiment 2
1) preparation of nanoemulsions：
7.0g oil with hydrogenated soybean is weighed, 9.0g Queensland nuts seed oil is weighed, weighs 6.0g mineral oil, weigh 4.5g stearoylketenes
Base sodium glutamate weighs 100 isostearate of 3.5g polyethylene glycol, weighs 0.5g glycyrrhiza glabra extracts, weighs 1.7g α-bear
Fruit glycosides is heated to 45 DEG C and is uniformly mixed, and then homogeneous stirs, and A phases are made；Weigh 10g glycerine, 1,3 butanediols of 5g, in right amount
Soft water is uniformly mixed, and B phases are made；A phases and B are mixed together, pre-composition is obtained, pre-composition is then passed through 1500 bars
High pressure homogenisers, carry out 6 cycle homogeneous, be then cooled to room temperature, obtain nanoemulsions.Nanoemulsions grain size obtained
90% or more at 10-300 nanometers.
2) preparation of nano biological whitening mask：
Fermentation strain will be used as by the wooden glucose acetobacter, the bacteria cellulose formed after 16 days static cultures
Mycoderm double roller extrusion dehydration, 10-50 nanometers of fibre diameter, then carries out ionising radiation disinfection to it, is put into sterile facial mask bag,
The nanoemulsions of 30g are finally added into facial mask bag, mask product is made in sealing facial mask bag.
3) use of nano biological whitening mask：
In use, facial mask bag is opened, the membrane of biological fibers containing nanoemulsions is overlayed on and stops 25 points on purported skin
It is removed after clock.
Embodiment 3
1) preparation of nanoemulsions：
1.0g oil with hydrogenated soybean is weighed, 4.5g hexadecanyl phosphate sylvite is weighed, it is different hard to weigh 1.2g polyethylene glycol 100
Resin acid ester weighs 2 glucoside of 1.8g L-AAs, weighs 18.2g Pomegranate Peel Extracts, is heated to 45 DEG C and mixes equal
Even, then homogeneous stirs, and A phases are made；13g glycerine, 1,3 butanediols of 47g are weighed, appropriate soft water is uniformly mixed, and B phases are made；
A phases and B are mixed together, pre-composition is obtained, then pre-composition is carried out 6 and followed by 1500 bars of high pressure homogenisers
Ring homogeneous, is then cooled to room temperature, and obtains nanoemulsions.90% or more nanoemulsions grain size obtained is at 10-180 nanometers.
2) preparation of nano biological whitening mask：
Fermentation strain will be used as by the wooden glucose acetobacter, the bacteria cellulose formed after 10 days static cultures
Then mycoderm extrusion dehydration carries out ionising radiation disinfection to it, be put into sterile facial mask bag, 28g finally is added into facial mask bag
Nanoemulsions, sealing facial mask bag mask product is made.
3) application method of nano biological whitening mask：
In use, facial mask bag is opened, the membrane of biological fibers containing nanoemulsions is overlayed on and stops 30 points on purported skin
It is removed after clock.
Embodiment 4
1) preparation of nanoemulsions：
7.0g oil with hydrogenated soybean is weighed, 5.0g jojoba oils are weighed, weighs 6.0g mineral oil, weighs 4.5g cetyl phosphorus
Acid esters sylvite weighs 1.2g polyethylene glycol 400 isostearates, weighs 0.5g glycyrrhiza glabra extracts, weighs 1.7g α-black bearberry
Glycosides is heated to 45 DEG C and is uniformly mixed, and then homogeneous stirs, and A phases are made；10g glycerine is weighed, 1,3 butanediols of 5g are appropriate soft
Water is uniformly mixed, and B phases are made；A phases and B are mixed together, pre-composition is obtained, pre-composition is then passed through 1300 bars
High pressure homogenisers carry out 6 cycle homogeneous, are then cooled to room temperature, obtain nanoemulsions.Nanoemulsions grain size 90% obtained
Above at 10-150 nanometers.
2) preparation of half wet film of nano biological：
Fermentation strain will be used as by the wooden glucose acetobacter, the bacteria cellulose formed after 10 days static cultures
Mycoderm, by tablet extrusion dehydration, then 10-30 nanometers of fibre diameter carries out ionising radiation disinfection to it, is put into sterile facial mask
In bag, it is sealed.
3) use of nano biological whitening mask：
First the whitening nanoemulsions of 20g are coated on purported skin when use, then nano biological facial mask cloth is taken out, is covered
On same purported skin, removed after stopping 30 minutes.
Embodiment 5
1) preparation of nanoemulsions：
7.0g avocado oils are weighed, 5.0g jojoba oils are weighed, weigh 6.0g mineral oil, weigh 4.5g hexadecanyl phosphates
Sylvite weighs 1.2g polyethylene glycol 400 isostearates, weighs 2 glucoside of 0.5g L-AAs, weighs 1.7g α-black bearberry
Glycosides is heated to 45 DEG C and is uniformly mixed, and then homogeneous stirs, and A phases are made；10g glycerine is weighed, 1,3 butanediols of 5g are appropriate soft
Water is uniformly mixed, and B phases are made；A phases and B are mixed together, pre-composition is obtained, pre-composition is then passed through 1300 bars
High pressure homogenisers carry out 6 cycle homogeneous, are then cooled to room temperature, obtain nanoemulsions.Nanoemulsions grain size 90% obtained
Above at 10-180 nanometers.
2) preparation of half wet film of nano biological：
Fermentation strain will be used as by the wooden glucose acetobacter, the bacteria cellulose formed after 10 days static cultures
Mycoderm tablet extrusion dehydration, then carries out ionising radiation disinfection to it, is put into sterile facial mask bag, is sealed.
3) use of nano biological whitening mask：
Half wet film of nano biological is taken out when use, impregnates 2 hours in the whitening nanoemulsions of 30g, then will contain again
There is the membrane of biological fibers of nanoemulsions to overlay on to stop on purported skin and remove after twenty minutes.
Embodiment 6
1) preparation of nanoemulsions：
7.0g oil with hydrogenated soybean is weighed, 5.0g jojoba oils are weighed, weighs 6.0g mineral oil, weighs 4.5g cetyl phosphorus
Acid esters sylvite weighs 1.2g polyethylene glycol 400 isostearates, weighs 0.5g glycyrrhiza glabra extracts, weighs 1.7g α-black bearberry
Glycosides is heated to 45 DEG C and is uniformly mixed, and then homogeneous stirs, and A phases are made；1g glycerine is weighed, appropriate soft water is uniformly mixed, system
Obtain B phases；A phases and B are mixed together, pre-composition is obtained, then carries out pre-composition by 1300 bars of high pressure homogenisers
6 cycle homogeneous, are then cooled to room temperature, obtain nanoemulsions.90% or more nanoemulsions grain size obtained is received in 10-300
Rice.
2) preparation of half wet film of nano biological：
Fermentation strain will be used as by the wooden glucose acetobacter, the bacteria cellulose formed after 10 days static cultures
Then mycoderm extrusion dehydration carries out ionising radiation disinfection to it, be put into sterile facial mask bag, 30g finally is added into facial mask bag
Nanoemulsions, sealing facial mask bag mask product is made.
3) use of nano biological whitening mask：
In use, facial mask bag is opened, the membrane of biological fibers containing nanoemulsions is overlayed on and stops 30 points on purported skin
It is removed after clock.
Embodiment 7
1) preparation of nanoemulsions
7.0g corn oils are weighed, 5.0g jojoba oils are weighed, weigh 6.0g mineral oil, weigh 4.5g stearoylketenes base-cocounut oil
Acyl glutamic acid sodium weighs 100 isostearate of 1.2g polyethylene glycol, weighs 1.3g glycyrrhiza glabra extracts, weighs 1.0g α-
Ursin is heated to 45 DEG C and is uniformly mixed, and then homogeneous stirs, and A phases are made；Weigh 15g propylene glycol, appropriate soft water, mixing
Uniformly, B phases are made；A phases and B are mixed together, pre-composition is obtained, it is then that pre-composition is high-pressure homogeneous by 1500 bars
Device carries out 6 cycle homogeneous, is then cooled to room temperature, obtains nanoemulsions.90% or more nanoemulsions grain size obtained exists
10-90 nanometers.
2) preparation method of nano biological whitening mask：
Fermentation strain will be used as by the wooden glucose acetobacter, the bacteria cellulose formed after 8 days static cultures
Mycoderm double roller extrusion dehydration, then carries out ionising radiation disinfection to it, is put into sterile facial mask bag, is finally added into facial mask bag
Mask product is made in the nanoemulsions of 28g, sealing facial mask bag.
3) application method of nano biological whitening mask：
In use, facial mask bag is opened, the membrane of biological fibers containing nanoemulsions is overlayed on and stops 30 points on purported skin
It is removed after clock.
Effete test embodiment 1
Select have the health volunteer 35 being accustomed to using facial mask, one full year of life at age 18-30, according to usually use habit, often
The mask product that week is prepared using embodiment 4 twice is used continuously 12 weeks.Subject is after use to the whitening of tested material and U.S.
Hold effect to be evaluated, the evaluation of tested material is evaluated as comparing and is agreed to be considered as with what is agreed to very much by the way of questionnaire survey
Effectively, it is invalid to be otherwise considered as, and specific evaluation effect is as shown in Figure 1.
Subject by it can be seen from Fig. 1 results 77% thinks to feel that skin of face becomes glossy after use；77%
Subject think to feel that facial colour spot is light after use；80% subject feels that blee becomes uniform after thinking use
；85% subject thinks that feeling that skin of face is obscure after use is improved；100% subject thinks the patch of product
Skin is good.
Effete test embodiment 2
Select have the health volunteer 35 being accustomed to using facial mask, one full year of life at age 18-30, according to usually use habit, often
The mask product that week is prepared using embodiment 5 twice is used continuously 12 weeks.Subject is after use to the whitening of tested material and U.S.
Hold effect to be evaluated, the evaluation of tested material is evaluated as comparing and is agreed to be considered as with what is agreed to very much by the way of questionnaire survey
Effectively, it is invalid to be otherwise considered as, and specific evaluation effect is shown in Fig. 2.
Subject by it can be seen from Fig. 2 results 85% thinks to feel that skin of face becomes glossy after use；80%
Subject think to feel that facial colour spot is light after use；74% subject feels that blee becomes uniform after thinking use
；85% subject thinks that feeling that skin of face is obscure after use is improved；100% subject thinks the patch of product
Skin is good.
The above described is only a preferred embodiment of the present invention, be not intended to limit the present invention in any form, therefore
It is every without departing from technical solution of the present invention content, simply repaiied to any made by above example according to the technical essence of the invention
Change, equivalent variations and modification, in the range of still falling within technical solution of the present invention.
Claims (5)
1. a kind of nano grade biological fiber whitening mask, it is characterised in that：It is the nano grade biological fiber by 10-50 nanometer ranges
Film and whitening nanoemulsions composition；The nano grade biological tunica fibrosa is using the wooden glucose acetobacter as fermentation strain, warp
Cross the bacteria cellulose mycoderm formed after 8-16 days static cultures；The nano grade biological tunica fibrosa is by nanometer bacteria fiber
Element is dehydrated by flat-plate compressed water or double roller extruding, obtains half wet film of nanometer bacteria cellulose；
The whitening nanoemulsions be by oil, surfactant, soluble small molecular, white-skinned face function ingredient, essence, preservative and
Soft water forms pre-composition, is then homogenized to be formed to pre-composition high-pressure；The whitening nanoemulsions include following weight hundred
Divide each raw material component of ratio：
The oil of 1%-22%, the oil are selected from oil with hydrogenated soybean, Queensland nut seed oil, jojoba oil, corn oil, avocado oil, mine
It is one or more in object oil；
The emulsifier and assistant for emulsifying agent of 1%-8%, the emulsifier are selected from hexadecanyl phosphate sylvite, stearoylketene base glutamic acid
Sodium, it is one or more in stearoylketene base-sodium cocoyl glutamate；
The soluble small molecular of 1%-60%, the soluble small molecular are selected from glycerine, 1,3-BDO, one kind in propylene glycol
Or it is a variety of；
The white-skinned face function ingredient of 0.1%-20%, the white-skinned face function ingredient are selected from ursin, AA 2G, light
At least one of fruit licorice, Pomegranate Peel Extract and its mixture；
The additive of 1%-90%, the additive include neutralizer, chelating agent, essence, preservative, thickener, pigment and soft
Water.
2. nano grade biological fiber whitening mask according to claim 1, it is characterised in that：The whitening nanoemulsions
Grain size is more than 90% at 10-300 nanometers.
3. nano grade biological fiber whitening mask according to claim 1, it is characterised in that：The whitening nanoemulsions
Grain size is more than 90% at 10-150 nanometers.
4. nano grade biological fiber whitening mask according to claim 1, it is characterised in that：The ursin is α-black bearberry
Glycosides, specific rotatory power is at+150.0 ° -+200.0 °.
5. a kind of application method of nano grade biological fiber whitening mask, it is characterised in that：It is carried with nano grade biological tunica fibrosa
Body adsorbs whitening nanoemulsions, is made the whitening mask product described in any one of claim 1-4, directly by face when use
Film bag is opened, and is overlayed on purported skin and is removed after a certain period of time.
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| EA038449B1 (en) * | 2016-04-21 | 2021-08-30 | ЮНИЛЕВЕР АйПи ХОЛДИНГС Б.В. | Nanoemulsions comprising n-acylglutamic acid salt and process for making same |
| JP6867405B2 (en) | 2016-04-21 | 2021-04-28 | ユニリーバー・ナームローゼ・ベンノートシヤープ | A novel nanoemulsion containing N-acyl derivatives of fatty acids and amino acid salts |
| US11026869B2 (en) | 2016-04-21 | 2021-06-08 | Conopco, Inc. | Process for producing small droplet emulsions at low pressure |
| TWI663987B (en) * | 2016-05-17 | 2019-07-01 | 大江生醫股份有限公司 | Method for producing functional bio-cellulose membrane and the produced mask thereof |
| CN106860231A (en) * | 2017-01-18 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment antiallergic mask |
| EP3579813B1 (en) | 2017-02-08 | 2020-03-25 | Unilever PLC | Novel nanoemulsions comprising glycerol in aqueous phase |
| CN106860111A (en) * | 2017-02-24 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment repair latex |
| CN107811881A (en) * | 2017-11-01 | 2018-03-20 | 武汉百思凯瑞纳米科技有限公司 | A kind of α ursin nano-compositions of whitening antioxidation and preparation method and application |
| CN110734563B (en) * | 2018-07-20 | 2022-05-17 | 南京理工大学 | Bacterial cellulose/emu oil composite membrane and preparation method thereof |
| CN109091399A (en) * | 2018-09-06 | 2018-12-28 | 华南理工大学 | A kind of antibacterial anti-inflammatory whitening mask and preparation method thereof |
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