CN105271430B - A kind of preparation method of the ultra-dispersed ferroso-ferric oxide of modification - Google Patents
A kind of preparation method of the ultra-dispersed ferroso-ferric oxide of modification Download PDFInfo
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- CN105271430B CN105271430B CN201510626184.7A CN201510626184A CN105271430B CN 105271430 B CN105271430 B CN 105271430B CN 201510626184 A CN201510626184 A CN 201510626184A CN 105271430 B CN105271430 B CN 105271430B
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- Prior art keywords
- ferriferrous oxide
- ferroso
- modified
- silane
- dispersed
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- SZVJSHCCFOBDDC-UHFFFAOYSA-N ferrosoferric oxide Chemical compound O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 title claims abstract description 63
- 229940056319 ferrosoferric oxide Drugs 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 230000004048 modification Effects 0.000 title claims abstract description 9
- 238000012986 modification Methods 0.000 title claims abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 65
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 34
- 239000002245 particle Substances 0.000 claims abstract description 32
- 238000003756 stirring Methods 0.000 claims abstract description 31
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims abstract description 21
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 229910052742 iron Inorganic materials 0.000 claims abstract description 16
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000006185 dispersion Substances 0.000 claims abstract description 15
- XDLMVUHYZWKMMD-UHFFFAOYSA-N 3-trimethoxysilylpropyl 2-methylprop-2-enoate Chemical compound CO[Si](OC)(OC)CCCOC(=O)C(C)=C XDLMVUHYZWKMMD-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000008187 granular material Substances 0.000 claims abstract description 13
- -1 iron ion Chemical class 0.000 claims abstract description 13
- 238000006243 chemical reaction Methods 0.000 claims abstract description 10
- 239000008367 deionised water Substances 0.000 claims abstract description 7
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 7
- 230000010355 oscillation Effects 0.000 claims abstract description 7
- 239000000243 solution Substances 0.000 claims description 25
- 235000019441 ethanol Nutrition 0.000 claims description 19
- 238000010792 warming Methods 0.000 claims description 18
- 239000012153 distilled water Substances 0.000 claims description 12
- 239000011259 mixed solution Substances 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 238000001914 filtration Methods 0.000 claims description 8
- 150000002500 ions Chemical class 0.000 claims description 8
- 239000001384 succinic acid Substances 0.000 claims description 7
- 229910021577 Iron(II) chloride Inorganic materials 0.000 claims description 6
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims description 6
- 230000032683 aging Effects 0.000 claims description 6
- 238000005119 centrifugation Methods 0.000 claims description 6
- 239000013049 sediment Substances 0.000 claims description 6
- 239000013078 crystal Substances 0.000 abstract description 9
- 238000000034 method Methods 0.000 abstract description 6
- 238000005406 washing Methods 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000000203 mixture Substances 0.000 abstract description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- 230000009286 beneficial effect Effects 0.000 abstract 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical group O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
- 230000000630 rising effect Effects 0.000 abstract 1
- 239000000047 product Substances 0.000 description 17
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 10
- 239000002105 nanoparticle Substances 0.000 description 10
- 230000005415 magnetization Effects 0.000 description 9
- 238000000975 co-precipitation Methods 0.000 description 5
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 description 5
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 5
- 230000005389 magnetism Effects 0.000 description 3
- 238000003466 welding Methods 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 230000001376 precipitating effect Effects 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- DQMUQFUTDWISTM-UHFFFAOYSA-N O.[O-2].[Fe+2].[Fe+2].[O-2] Chemical compound O.[O-2].[Fe+2].[Fe+2].[O-2] DQMUQFUTDWISTM-UHFFFAOYSA-N 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- 239000003082 abrasive agent Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000037452 priming Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000009938 salting Methods 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
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- Compounds Of Iron (AREA)
- Soft Magnetic Materials (AREA)
- Hard Magnetic Materials (AREA)
Abstract
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Priority Applications (1)
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CN201510626184.7A CN105271430B8 (en) | 2015-09-28 | 2015-09-28 | A kind of preparation method of the ultra-dispersed ferroso-ferric oxide of modification |
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CN201510626184.7A CN105271430B8 (en) | 2015-09-28 | 2015-09-28 | A kind of preparation method of the ultra-dispersed ferroso-ferric oxide of modification |
Publications (3)
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CN105271430A CN105271430A (en) | 2016-01-27 |
CN105271430B true CN105271430B (en) | 2016-08-24 |
CN105271430B8 CN105271430B8 (en) | 2016-10-12 |
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CN201510626184.7A Active CN105271430B8 (en) | 2015-09-28 | 2015-09-28 | A kind of preparation method of the ultra-dispersed ferroso-ferric oxide of modification |
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Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105883933A (en) * | 2016-03-15 | 2016-08-24 | 宁波江东波莫纳电子科技有限公司 | Preparation method of ferroferric oxide granules |
CN105645477B (en) * | 2016-03-21 | 2017-04-26 | 黄山学院 | Preparation method of ferroferric oxide |
CN107311237A (en) * | 2017-06-29 | 2017-11-03 | 成都磁动势科技有限公司 | The preparation method of nano-magnetic powder |
CN107522238A (en) * | 2017-07-11 | 2017-12-29 | 中国科学院合肥物质科学研究院 | Nano ferriferrous oxide liquid combines phase and the ion measurement method based on DGT |
CN107903074A (en) * | 2017-10-24 | 2018-04-13 | 当涂县瑞龙果树种植专业合作社 | A kind of ceramic material sintering aid and preparation method thereof |
CN114197047B (en) * | 2021-12-14 | 2022-07-19 | 安徽科瑞思创晶体材料有限责任公司 | Iron-doped lithium tantalate monocrystal and preparation method and application thereof |
CN117486567A (en) * | 2022-03-31 | 2024-02-02 | 黄伟 | Preparation method of radiation-proof diatom plate |
CN115159586A (en) * | 2022-07-15 | 2022-10-11 | 中国恩菲工程技术有限公司 | Ferroferric oxide magnetic powder for water treatment and preparation method thereof |
CN115725142B (en) * | 2022-11-18 | 2024-05-03 | 浙江工业大学 | Black talcum-based pre-dispersed rubber master batch and preparation method thereof |
CN116959834B (en) * | 2023-09-19 | 2023-12-12 | 河南天可汗科技有限公司 | Magnetic fluid and preparation method thereof |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101728047A (en) * | 2010-01-25 | 2010-06-09 | 上海交通大学 | Preparation method of ferroferric oxide magnetic nano particle emulsion |
CN102108353A (en) * | 2009-12-25 | 2011-06-29 | 华中科技大学 | Magnetic nano-particle immobilized basic protease and preparation method and application thereof |
CN102212162A (en) * | 2011-03-25 | 2011-10-12 | 浙江大学宁波理工学院 | Method for preparing thiolated nano ferroferric oxide magnetic polymer composite material |
CN102225785A (en) * | 2011-04-26 | 2011-10-26 | 东华大学 | Preparation method of APTS (aminopropyltriethoxysilane)-modified iron oxide magnetic nanoparticles |
-
2015
- 2015-09-28 CN CN201510626184.7A patent/CN105271430B8/en active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102108353A (en) * | 2009-12-25 | 2011-06-29 | 华中科技大学 | Magnetic nano-particle immobilized basic protease and preparation method and application thereof |
CN101728047A (en) * | 2010-01-25 | 2010-06-09 | 上海交通大学 | Preparation method of ferroferric oxide magnetic nano particle emulsion |
CN102212162A (en) * | 2011-03-25 | 2011-10-12 | 浙江大学宁波理工学院 | Method for preparing thiolated nano ferroferric oxide magnetic polymer composite material |
CN102225785A (en) * | 2011-04-26 | 2011-10-26 | 东华大学 | Preparation method of APTS (aminopropyltriethoxysilane)-modified iron oxide magnetic nanoparticles |
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CN105271430B8 (en) | 2016-10-12 |
CN105271430A (en) | 2016-01-27 |
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Correction item: Patentee|Address Correct: NINGBO JIANGDONG LINQING ENVIRONMENTAL PROTECTION TECHNOLOGY CO., LTD.|Jiangdong District 315000 Zhejiang city of Ningbo Province Yue Sheng Road No. 311 building 003 14-5 False: Jiangsu Zhenyu EnvironmentaL Technology Co., Ltd.|Gaocheng town Gaocheng street Yixing city 213164 Jiangsu city of Changzhou Province Number: 34 Volume: 32 |
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Correction item: Patentee|Address Correct: NINGBO JIANGDONG LINQING ENVIRONMENTAL PROTECTION TECHNOLOGY CO., LTD.|Jiangdong District 315000 Zhejiang city of Ningbo Province Yue Sheng Road No. 311 building 003 14-5 False: Jiangsu Zhenyu EnvironmentaL Technology Co., Ltd.|Gaocheng town Gaocheng street Yixing city 213164 Jiangsu city of Changzhou Province Number: 34 Page: The title page Volume: 32 |
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Inventor after: Ren Kangli Inventor before: Li Zhenyu Inventor before: Sheng Yanhua Inventor before: Gao Liqun |
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Effective date of registration: 20170904 Address after: 300380 Tianjin city temple town Xiqing District Great Village days Building No. 27, No. 301 2 Patentee after: Ren Kangli Address before: Jiangdong District 315000 Zhejiang city of Ningbo Province Yue Sheng Road No. 311 building 003 14-5 Patentee before: NINGBO JIANGDONG LINQING ENVIRONMENTAL PROTECTION TECHNOLOGY Co.,Ltd. |
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Effective date of registration: 20181221 Address after: 102600 3 floor, 2 building, No. 4 Daxing District Garden Road, Beijing, 1 unit 317 Patentee after: BEIJING ZHITOUJIA INTELLECTUAL PROPERTY OPERATION CO.,LTD. Address before: 300380 Tianjin Xiqing District Dasi Town Darenzhuang Village Tianrenli 27 Building 2 Gate 301 Patentee before: Ren Kangli Effective date of registration: 20181221 Address after: Room 11 409, Xuzhou Software Park, No. 6 Software Park Road, Quanshan District, Xuzhou City, Jiangsu Province, 221000 Patentee after: Chen Deyan Address before: 102600 3 floor, 2 building, No. 4 Daxing District Garden Road, Beijing, 1 unit 317 Patentee before: BEIJING ZHITOUJIA INTELLECTUAL PROPERTY OPERATION CO.,LTD. |
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Effective date of registration: 20190401 Address after: 221100 Ma Shan Village, Liguo Town, Tongshan District, Xuzhou City, Jiangsu Province Patentee after: XUZHOU RUNFENG NEW MATERIALS Co.,Ltd. Address before: Room 11 409, Xuzhou Software Park, No. 6 Software Park Road, Quanshan District, Xuzhou City, Jiangsu Province, 221000 Patentee before: Chen Deyan |
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