CN105267752A - Natural plant bacteriostatic agent and preparation method thereof - Google Patents
Natural plant bacteriostatic agent and preparation method thereof Download PDFInfo
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Abstract
A natural plant bacteriostatic agent and a preparation method thereof are provided. The natural plant bacteriostatic agent comprises following materials by weight: Flos Lonicerae 300-350 parts, Fructus Forsythiae 300-350 parts, Herba Pogostemonis 200-220 parts, Folium Mori 100-110 parts, mint 100-120 parts, Folium Artemisiae Argyi 100-120 parts, Radix Arnebiae seu Lithospermi 200-210 parts, Radix Glycyrrhizae 100-110 parts, Rhizoma Phragmitis 100-110 parts, sodium benzoate 3-4 parts, and flavoring orange essence 20-24 parts. The natural plant bacteriostatic agent is prepared by: primary decocting, secondary decocting, tertiary decocting, concentrating, alcohol precipitation and separation, concentrating, and preparing. The invention has the advantages that the natural plant bacteriostatic agent is made from herbs, has improved bacteriostatic effect, has little side effect on human body and is nonirritating to the skin; the natural plant bacteriostatic agent is applicable to skin and mouth to play a good role in inhibiting Staphylococcus aureus, Escherichia coli and the like, is nonirritating to the skin and mouth, and is free of drug resistance; compared with market bacteriostatic agents, the natural plant bacteriostatic agent has a wide range of action and is safer and nonirritating.
Description
Technical field
The invention belongs to disinfecting articles for use antibacterial application, particularly a kind of natural plants antibacterial and preparation method thereof.
Background technology
The origin of anti-biotic material is just brought into use from ancient times people, it is found that the water with silver and copper container are retained should not go bad, imperial palace to reach when your rich has a meal again silver chopstick accustomed to using afterwards, among the peoplely made ornaments with silver again and wore, and among the people the beginning very early of China recognizes that silver has antibacterial action.Antibacterial is generally divided into inorganic antiseptic, organic antibacterial agent and natural antibacterial agent.Inorganic antiseptic, such as silver ion antibacterial; Organic antibacterial agent, such as quaternary ammonium salt antibacterial, chitosan class etc., natural antibacterial agent plant extract class such as Aloe, Radix Artemisia ordosicae etc.
Antibacterial at present on the market for external preparation for skin is wide in variety, and large multiaction is single, and such as silver ion class antibacterial, chitosan class, quaternary ammonium salt, be applicable to skin antibacterial.The antibacterial of extracted form natural plant class is applicable to skin mostly, the nursing in oral cavity, but antibacterial action is limited.Some product, in order to improve bacteriostasis, adds antibiotic and improves fungistatic effect.Natural plants antibacterial is compound recipe formula, and several kinds of Chinese medicinal materials combines, and increases bacteriostasis.The main component of product, Flos Lonicerae, modern medicine study shows that Flos Lonicerae is rich in chlorogenic acid, isochlorogenic acid, Flavonoid substances, lonicerin, inositol and trace volatile oil etc., and thus it has positive role to human body.Flos Lonicerae can resisting pathogenic microbes, experiment proves that Flos Lonicerae is to various pathogenic bacterium, virus, as staphylococcus aureus, Hemolytic streptococcus, Diplococcus pneumoniae, bordetella pertussis, Bacillus typhi, Salmonella paratyphi, dysentery bacterium, vibrio cholera, bacillus pyocyaneus, escherichia coli, meningococcus, dermatophytes, influenza virus, leptospira etc. all have inhibitory action in various degree.Herba Pogostemonis, has bacteriostasis to multiple human pathogen and fungus.Fructus Forsythiae, Fructus Forsythiae concentrated decotion has antibacterial action in vitro, can suppress Bacillus typhi, Salmonella paratyphi, escherichia coli, dysentery bacterium, diphtheria corynebacterium and vibrio cholera, staphylococcus, streptococcus etc.Vitro antibacterial activity is similar to Flos Lonicerae, and Flos Lonicerae is to Salmonella, and particularly the inhibitory action of Bacillus typhi and Hemolytic streptococcus seemingly exceedes Fructus Forsythiae, then seemingly better with Fructus Forsythiae to the suppression of dysentery bacterium, staphylococcus aureus.
Summary of the invention
The present invention, in order to make up the deficiencies in the prior art, provides a kind of natural plants antibacterial.
The present invention is achieved through the following technical solutions:
Natural plants antibacterial, it is characterized in that, be made up of following raw material, by weight: Flos Lonicerae 300-350 part, Fructus Forsythiae 300-350 part, Herba Pogostemonis 200-220 part, Folium Mori 100-110 part, Herba Menthae 100-120 part, Folium Artemisiae Argyi 100-120 part, Radix Arnebiae (Radix Lithospermi) 200-210 part, Radix Glycyrrhizae 100-110 part, Rhizoma Phragmitis 100-110 part, sodium benzoate 3-4 part, flavoring orange essence 20-24 part.
Preferably, natural plants antibacterial, it is characterized in that, be made up of following raw material, by weight: Flos Lonicerae 310-340 part, Fructus Forsythiae 310-340 part, Herba Pogostemonis 205-215 part, Folium Mori 102-108 part, Herba Menthae 105-115 part, Folium Artemisiae Argyi 105-115 part, Radix Arnebiae (Radix Lithospermi) 202-208 part, Radix Glycyrrhizae 102-108 part, Rhizoma Phragmitis 102-108 part, sodium benzoate 3.2-3.8 part, flavoring orange essence 21-23 part.
More preferably, natural plants antibacterial, it is characterized in that, be made up of following raw material, by weight: Flos Lonicerae 330 parts, Fructus Forsythiae 330 parts, Herba Pogostemonis 210 parts, 105 parts, Folium Mori, Herba Menthae 110 parts, Folium Artemisiae Argyi 110 parts, Radix Arnebiae (Radix Lithospermi) 205 parts, 105 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 105 parts, sodium benzoate 3.5 parts, flavoring orange essence 22 parts.
The preparation method of natural plants antibacterial is:
Following raw material is by weight: Flos Lonicerae 300-350 part, Fructus Forsythiae 300-350 part, Herba Pogostemonis 200-220 part, Folium Mori 100-110 part, Herba Menthae 100-120 part, Folium Artemisiae Argyi 100-120 part, Radix Arnebiae (Radix Lithospermi) 200-210 part, Radix Glycyrrhizae 100-110 part, Rhizoma Phragmitis 100-110 part, sodium benzoate 3-4 part, flavoring orange essence 20-24 part.
1. Herba Pogostemonis 200-220 part, Folium Mori 100-110 part, Herba Menthae 100-120 part
Pure water 4000ml soaks 30 minutes, heating, and collect volatile oil 400ml, cold preservation is for subsequent use; Evaporated mother liquor is for soaking medical material;
2. decoct also wine to sink: Flos Lonicerae 300-350 part, Fructus Forsythiae 300-350 part, Radix Arnebiae (Radix Lithospermi) 200-210 part, Radix Glycyrrhizae 100-110 part, Rhizoma Phragmitis 100-110 part, Folium Mori 100-110 part;
One decocts: merge evaporated mother liquor as the soak of decocting herbs, add 10-12 times of water gaging (about 12 liters), soak 30 minutes, decoct 90 minutes.Collect decoction liquor, concentrating under reduced pressure.
Two decoct: the 8-10 times of water gaging that add water (about 9.6 liters) decocts 60 minutes, collect decoction liquor, concentrating under reduced pressure.
Three decoct: the 5-6 times of water gaging that add water (about 6 liters) decocts 30 minutes, collect decoction liquor, concentrating under reduced pressure.
Concentrated: merge decoction liquor, being evaporated to volume is 500-600ml.
Wine sinks: be placed in by concentrated solution in container, progressively adds high concentration ethanol when stirring, and finally obtaining containing alcohol is 65%-70% solution, and solution 10 ° is placed more than 12 hours.
Be separated, concentrated: slowly draw wine and sink supernatant, concentrating under reduced pressure, collect high concentration ethanol, be concentrated into without alcohol, volume is 500-600ml.
Preparation: when stirring, the volatile oil of collection slowly being added in concentrated solution, adds to 900ml.Dissolve sodium benzoate 3-4 part by a small amount of purified water, add in concentrated solution.Add flavoring orange essence 20-24 part again.Supplement volatile oil to 1000ml.
PH should be 4.0-6.0, and relative density should be 1.05-1.30.
The invention has the beneficial effects as follows: this product contains multiple Chinese herbal medicine, compatibility uses, little to the side effect of human body while increasing fungistatic effect, to no skin irritation.Can apply and skin, oral cavity, have fine bacteriostasis to staphylococcus aureus, escherichia coli etc., skin, oral cavity be had no stimulation, does not produce drug resistance.Compared with antibacterial on the market, sphere of action is large, safer, non-stimulated.
Detailed description of the invention
Embodiment 1:
Natural plants antibacterial, is made up of following raw material, by weight:
Flos Lonicerae 310 parts, Fructus Forsythiae 310 parts, Herba Pogostemonis 205 parts, 105 parts, Folium Mori, Herba Menthae 105 parts, Folium Artemisiae Argyi 105 parts, Radix Arnebiae (Radix Lithospermi) 205 parts, 105 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 105 parts, sodium benzoate 3 parts, flavoring orange essence 20 parts.
Embodiment 2:
Natural plants antibacterial, is made up of following raw material, by weight:
Flos Lonicerae 330 parts, Fructus Forsythiae 330 parts, Herba Pogostemonis 210 parts, 105 parts, Folium Mori, Herba Menthae 110 parts, Folium Artemisiae Argyi 110 parts, Radix Arnebiae (Radix Lithospermi) 205 parts, 105 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 105 parts, sodium benzoate 3.5 parts, flavoring orange essence 22 parts.
Embodiment 3:
Natural plants antibacterial, is made up of following raw material, by weight:
Flos Lonicerae 350 parts, Fructus Forsythiae 350 parts, Herba Pogostemonis 220 parts, 110 parts, Folium Mori, Herba Menthae 120 parts, Folium Artemisiae Argyi 120 parts, Radix Arnebiae (Radix Lithospermi) 210 parts, 110 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 110 parts, sodium benzoate 4 parts, flavoring orange essence 24 parts.
The preparation method of natural plants antibacterial is:
Embodiment 4: the concrete steps of the raw material of preparation described in embodiment 1 are:
Raw materials used: natural plants antibacterial, be made up of following raw material, by weight: Flos Lonicerae 310 parts, Fructus Forsythiae 310 parts, Herba Pogostemonis 205 parts, 105 parts, Folium Mori, Herba Menthae 105 parts, Folium Artemisiae Argyi 105 parts, Radix Arnebiae (Radix Lithospermi) 205 parts, 105 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 105 parts, sodium benzoate 3.5 parts, flavoring orange essence 22 parts.
Concrete steps are:
(1) Herba Pogostemonis 205 parts, Folium Artemisiae Argyi 105 parts, Herba Menthae 105 parts, pure water 4000ml soaks 30 minutes, heating, and collect volatile oil 400ml, cold preservation is for subsequent use, and evaporated mother liquor is for soaking medical material;
(2) decoct also wine to sink: Flos Lonicerae 310 parts, Fructus Forsythiae 310 parts, Radix Arnebiae (Radix Lithospermi) 205 parts, 105 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 105 parts, 105 parts, Folium Mori;
One decocts: merge evaporated mother liquor as the soak of decocting herbs, by weight, add 10-12 times of water gaging, soak 30 minutes, decoct 90 minutes, collect decoction liquor, concentrating under reduced pressure;
Two decoct: by weight, and add water 8 times of water gagings, decoct 60 minutes, collect decoction liquor, concentrating under reduced pressure;
Three decoct: by weight, and add water 5 times of water gagings, decoct 30 minutes, collect decoction liquor, concentrating under reduced pressure;
Concentrated: merge decoction liquor, being evaporated to volume is 500ml;
Wine sinks: be placed in by concentrated solution in container, progressively adds high concentration ethanol when stirring, and finally obtaining containing alcohol is 65% solution, and solution 10 DEG C is placed 12 hours.
Be separated, concentrated: slowly draw wine and sink supernatant, concentrating under reduced pressure, collect high concentration ethanol, be concentrated into without alcohol, volume is 500ml;
Preparation: when stirring, the volatile oil of collection slowly being added in concentrated solution, adds to 900ml, dissolve sodium benzoate 3 parts by a small amount of purified water, add in concentrated solution, then add flavoring orange essence 20 parts, supplement volatile oil and should be 4.0 to 1000ml, pH, relative density should be 1.05.
Embodiment 5: the concrete steps of the raw material of preparation described in embodiment 2 are:
Raw materials used: natural plants antibacterial, be made up of following raw material, by weight:
Flos Lonicerae 330 parts, Fructus Forsythiae 330 parts, Herba Pogostemonis 210 parts, 105 parts, Folium Mori, Herba Menthae 110 parts, Folium Artemisiae Argyi 110 parts, Radix Arnebiae (Radix Lithospermi) 205 parts, 105 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 105 parts, sodium benzoate 3.5 parts, flavoring orange essence 22 parts.
Concrete steps are:
(1) Herba Pogostemonis 210 parts, 105 parts, Folium Mori, Herba Menthae 110 parts, pure water 4000ml soaks 30 minutes, heating, and collect volatile oil 400ml, cold preservation is for subsequent use, and evaporated mother liquor is for soaking medical material;
(2) decoct also wine to sink: Flos Lonicerae 330 parts, Fructus Forsythiae 330 parts, Radix Arnebiae (Radix Lithospermi) 205 parts, 105 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 105 parts, 105 parts, Folium Mori;
One decocts: merge evaporated mother liquor as the soak of decocting herbs, by weight, add 10-12 times of water gaging, soak 30 minutes, decoct 90 minutes, collect decoction liquor, concentrating under reduced pressure;
Two decoct: by weight, and add water 9 times of water gagings, decoct 60 minutes, collect decoction liquor, concentrating under reduced pressure;
Three decoct: by weight, and add water 5.5 times of water gagings, decoct 30 minutes, collect decoction liquor, concentrating under reduced pressure;
Concentrated: merge decoction liquor, being evaporated to volume is 550ml;
Wine sinks: be placed in by concentrated solution in container, progressively adds high concentration ethanol when stirring, and finally obtaining containing alcohol is 68% solution, and solution 10 DEG C is placed 13 hours.
Be separated, concentrated: slowly draw wine and sink supernatant, concentrating under reduced pressure, collect high concentration ethanol, be concentrated into without alcohol, volume is 550ml;
Preparation: when stirring, the volatile oil of collection slowly being added in concentrated solution, adds to 900ml, dissolve sodium benzoate 3.5 parts by a small amount of purified water, add in concentrated solution, then add flavoring orange essence 22 parts, supplement volatile oil and should be 5.0 to 1000ml, pH, relative density should be 1.20.
Embodiment 6: the concrete steps of the raw material of preparation described in embodiment 3 are:
Natural plants antibacterial, is made up of following raw material, by weight:
Flos Lonicerae 350 parts, Fructus Forsythiae 350 parts, Herba Pogostemonis 220 parts, 110 parts, Folium Mori, Herba Menthae 120 parts, Folium Artemisiae Argyi 120 parts, Radix Arnebiae (Radix Lithospermi) 210 parts, 110 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 110 parts, sodium benzoate 4 parts, flavoring orange essence 24 parts.
Concrete steps are:
(1) Herba Pogostemonis 220 parts, 110 parts, Folium Mori, Herba Menthae 120 parts, pure water 4000ml soaks 30 minutes, heating, and collect volatile oil 400ml, cold preservation is for subsequent use, and evaporated mother liquor is for soaking medical material;
(2) decoct also wine to sink: Flos Lonicerae 350 parts, Fructus Forsythiae 350 parts, Radix Arnebiae (Radix Lithospermi) 210 parts, 110 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 110 parts, 110 parts, Folium Mori;
One decocts: merge evaporated mother liquor as the soak of decocting herbs, by weight, add 10-12 times of water gaging, soak 30 minutes, decoct 90 minutes, collect decoction liquor, concentrating under reduced pressure;
Two decoct: by weight, and add water 10 times of water gagings, decoct 60 minutes, collect decoction liquor, concentrating under reduced pressure;
Three decoct: by weight, and add water 6 times of water gagings, decoct 30 minutes, collect decoction liquor, concentrating under reduced pressure;
Concentrated: merge decoction liquor, being evaporated to volume is 600ml;
Wine sinks: be placed in by concentrated solution in container, progressively adds high concentration ethanol when stirring, and finally obtaining containing alcohol is 70% solution, and solution 10 DEG C is placed 15 hours.
Be separated, concentrated: slowly draw wine and sink supernatant, concentrating under reduced pressure, collect high concentration ethanol, be concentrated into without alcohol, volume is 600ml;
Preparation: when stirring, the volatile oil of collection slowly being added in concentrated solution, adds to 900ml, dissolve sodium benzoate 3 parts by a small amount of purified water, add in concentrated solution, then add flavoring orange essence 24 parts, supplement volatile oil and should be 6.0 to 1000ml, pH, relative density should be 1.30.
This product and other antibacterial contrast as follows:
| name of product | action effect | site of action |
| natural plants antibacterial | good antimicrobial effect, the time is lasting, safety. | skin, oral cavity |
| silver ion class antibacterial | good antimicrobial effect, the time is lasting, unsuitable a large amount of, uses for a long time. | skin |
| quaternary ammonium salt antibacterial | good antimicrobial effect, the time is lasting, but incompatibility is more, easily by organic substance influence. | skin |
| single plant extract antibacterial | fungistatic effect is limited | skin, oral cavity |
The present invention is through the inspection of Hainan Center for Disease Control & Prevention, and the survey report of beneficial effect of the present invention of must issuing a certificate (survey report is numbered: No. 3210th, fine jade disease control searching [2013] and No. 3209th, fine jade disease control searching [2013]).
Claims (6)
1. natural plants antibacterial, it is characterized in that, be made up of following raw material, by weight: Flos Lonicerae 300-350 part, Fructus Forsythiae 300-350 part, Herba Pogostemonis 200-220 part, Folium Mori 100-110 part, Herba Menthae 100-120 part, Folium Artemisiae Argyi 100-120 part, Radix Arnebiae (Radix Lithospermi) 200-210 part, Radix Glycyrrhizae 100-110 part, Rhizoma Phragmitis 100-110 part, sodium benzoate 3-4 part, flavoring orange essence 20-24 part.
2. natural plants antibacterial according to claim 1, it is characterized in that, be made up of following raw material, by weight: Flos Lonicerae 310-340 part, Fructus Forsythiae 310-340 part, Herba Pogostemonis 205-215 part, Folium Mori 102-108 part, Herba Menthae 105-115 part, Folium Artemisiae Argyi 105-115 part, Radix Arnebiae (Radix Lithospermi) 202-208 part, Radix Glycyrrhizae 102-108 part, Rhizoma Phragmitis 102-108 part, sodium benzoate 3.2-3.8 part, flavoring orange essence 21-23 part.
3. natural plants antibacterial according to claim 2, it is characterized in that: be made up of following raw material, by weight: Flos Lonicerae 330 parts, Fructus Forsythiae 330 parts, Herba Pogostemonis 210 parts, 105 parts, Folium Mori, Herba Menthae 110 parts, Folium Artemisiae Argyi 110 parts, Radix Arnebiae (Radix Lithospermi) 205 parts, 105 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 105 parts, sodium benzoate 3.5 parts, flavoring orange essence 22 parts.
4. prepare the method for natural plants antibacterial according to claim 1, it is characterized in that: following raw material by weight: Flos Lonicerae 300-350 part, Fructus Forsythiae 300-350 part, Herba Pogostemonis 200-220 part, Folium Mori 100-110 part, Herba Menthae 100-120 part, Folium Artemisiae Argyi 100-120 part, Radix Arnebiae (Radix Lithospermi) 200-210 part, Radix Glycyrrhizae 100-110 part, Rhizoma Phragmitis 100-110 part, sodium benzoate 3-4 part, flavoring orange essence 20-24 part;
Herba Pogostemonis 200-220 part, Folium Mori 100-110 part, Herba Menthae 100-120 part, pure water 4000ml soaks 30 minutes, heating, and collect volatile oil 400ml, cold preservation is for subsequent use; Evaporated mother liquor is for soaking medical material;
(2) decoct also wine to sink: Flos Lonicerae 300-350 part, Fructus Forsythiae 300-350 part, Radix Arnebiae (Radix Lithospermi) 200-210 part, Radix Glycyrrhizae 100-110 part, Rhizoma Phragmitis 100-110 part, Folium Mori 100-110 part;
One decocts: merge evaporated mother liquor as the soak of decocting herbs, add 10-12 times of water gaging, soak 30 minutes, decoct 90 minutes, collect decoction liquor, concentrating under reduced pressure;
Two decoct: add water 8-10 times of water gaging, decoct 60 minutes, collect decoction liquor, concentrating under reduced pressure;
Three decoct: add water 5-6 times of water gaging, decoct 30 minutes, collect decoction liquor, concentrating under reduced pressure;
Concentrated: merge decoction liquor, being evaporated to volume is 500-600ml;
Wine sinks: be placed in by concentrated solution in container, progressively adds high concentration ethanol when stirring, and finally obtaining containing alcohol is 65%-70% solution, and solution 10 DEG C is placed more than 12 hours;
Be separated, concentrated: slowly draw wine and sink supernatant, concentrating under reduced pressure, collect high concentration ethanol, be concentrated into without alcohol, volume is 500-600ml;
Preparation: when stirring, slowly being added in concentrated solution by the volatile oil of collection, adding to 900ml, dissolves sodium benzoate 3-4 part by a small amount of purified water, adds in concentrated solution, then add flavoring orange essence 20-24 part, supplements volatile oil to 1000ml;
PH should be 4.0-6.0, and relative density should be 1.05-1.30.
5. the method for natural plants antibacterial according to claim 4, it is characterized in that: raw materials used: natural plants antibacterial, be made up of following raw material, by weight: Flos Lonicerae 310 parts, Fructus Forsythiae 310 parts, Herba Pogostemonis 205 parts, 105 parts, Folium Mori, Herba Menthae 105 parts, Folium Artemisiae Argyi 105 parts, Radix Arnebiae (Radix Lithospermi) 205 parts, 105 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 105 parts, sodium benzoate 3.5 parts, flavoring orange essence 22 parts;
Concrete steps are:
(1) Herba Pogostemonis 205 parts, Folium Artemisiae Argyi 105 parts, Herba Menthae 105 parts, pure water 4000ml soaks 30 minutes, heating, and collect volatile oil 400ml, cold preservation is for subsequent use, and evaporated mother liquor is for soaking medical material;
(2) decoct also wine to sink: Flos Lonicerae 310 parts, Fructus Forsythiae 310 parts, Radix Arnebiae (Radix Lithospermi) 205 parts, 105 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 105 parts, 105 parts, Folium Mori;
One decocts: merge evaporated mother liquor as the soak of decocting herbs, by weight, add 10-12 times of water gaging, soak 30 minutes, decoct 90 minutes, collect decoction liquor, concentrating under reduced pressure;
Two decoct: by weight, and add water 8 times of water gagings, decoct 60 minutes, collect decoction liquor, concentrating under reduced pressure;
Three decoct: by weight, and add water 5 times of water gagings, decoct 30 minutes, collect decoction liquor, concentrating under reduced pressure;
Concentrated: merge decoction liquor, being evaporated to volume is 500ml;
Wine sinks: be placed in by concentrated solution in container, progressively adds high concentration ethanol when stirring, and finally obtaining containing alcohol is 65% solution, and solution 10 DEG C is placed 12 hours;
Be separated, concentrated: slowly draw wine and sink supernatant, concentrating under reduced pressure, collect high concentration ethanol, be concentrated into without alcohol, volume is 500ml;
Preparation: when stirring, the volatile oil of collection slowly being added in concentrated solution, adds to 900ml, dissolve sodium benzoate 3 parts by a small amount of purified water, add in concentrated solution, then add flavoring orange essence 20 parts, supplement volatile oil and should be 4.0 to 1000ml, pH, relative density should be 1.05.
6. the method for natural plants antibacterial according to claim 4, is characterized in that: natural plants antibacterial, is made up of following raw material, by weight:
Flos Lonicerae 350 parts, Fructus Forsythiae 350 parts, Herba Pogostemonis 220 parts, 110 parts, Folium Mori, Herba Menthae 120 parts, Folium Artemisiae Argyi 120 parts, Radix Arnebiae (Radix Lithospermi) 210 parts, 110 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 110 parts, sodium benzoate 4 parts, flavoring orange essence 24 parts;
Concrete steps are:
(1) Herba Pogostemonis 220 parts, 110 parts, Folium Mori, Herba Menthae 120 parts, pure water 4000ml soaks 30 minutes, heating, and collect volatile oil 400ml, cold preservation is for subsequent use, and evaporated mother liquor is for soaking medical material;
(2) decoct also wine to sink: Flos Lonicerae 350 parts, Fructus Forsythiae 350 parts, Radix Arnebiae (Radix Lithospermi) 210 parts, 110 parts, Radix Glycyrrhizae, Rhizoma Phragmitis 110 parts, 110 parts, Folium Mori;
One decocts: merge evaporated mother liquor as the soak of decocting herbs, by weight, add 10-12 times of water gaging, soak 30 minutes, decoct 90 minutes, collect decoction liquor, concentrating under reduced pressure;
Two decoct: by weight, and add water 10 times of water gagings, decoct 60 minutes, collect decoction liquor, concentrating under reduced pressure;
Three decoct: by weight, and add water 6 times of water gagings, decoct 30 minutes, collect decoction liquor, concentrating under reduced pressure;
Concentrated: merge decoction liquor, being evaporated to volume is 600ml;
Wine sinks: be placed in by concentrated solution in container, progressively adds high concentration ethanol when stirring, and finally obtaining containing alcohol is 70% solution, and solution 10 DEG C is placed 15 hours;
Be separated, concentrated: slowly draw wine and sink supernatant, concentrating under reduced pressure, collect high concentration ethanol, be concentrated into without alcohol, volume is 600ml;
Preparation: when stirring, the volatile oil of collection slowly being added in concentrated solution, adds to 900ml, dissolve sodium benzoate 3 parts by a small amount of purified water, add in concentrated solution, then add flavoring orange essence 24 parts, supplement volatile oil and should be 6.0 to 1000ml, pH, relative density should be 1.30.
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| CN107668093A (en) * | 2017-08-08 | 2018-02-09 | 深圳沃海森科技有限公司 | Environment-friendly long-life type air conditioner filter element bacteriostatic agent and preparation method thereof |
| CN109805035A (en) * | 2017-11-20 | 2019-05-28 | 柳州市皇之品贸易有限公司 | A kind of Chinese herbal medicine natural bacteriostatic agent and preparation method thereof |
| CN107811956A (en) * | 2017-11-30 | 2018-03-20 | 安徽省丰康农业科技有限公司蚌埠农业科技研发中心 | A kind of honey bacteriostatic agent and preparation method thereof |
| CN108308203A (en) * | 2018-01-31 | 2018-07-24 | 南京紫源康医药科技有限公司 | A kind of preparation method of Chinese medicinal compound extract, extract and bacteria inhibiting composition |
| CN108902645A (en) * | 2018-06-29 | 2018-11-30 | 苏州汉德瑞生物工程有限公司 | A kind of plant bacteriostatic agent and preparation method thereof |
| CN109125180A (en) * | 2018-10-15 | 2019-01-04 | 山东麦德森医疗科技有限公司 | A kind of preparation and its detection test method of Traditional Chinese medicinal hand lotion |
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