CN105254145A - Capsule-type active calcium emulsion and preparation method thereof - Google Patents

Capsule-type active calcium emulsion and preparation method thereof Download PDF

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Publication number
CN105254145A
CN105254145A CN201510505019.6A CN201510505019A CN105254145A CN 105254145 A CN105254145 A CN 105254145A CN 201510505019 A CN201510505019 A CN 201510505019A CN 105254145 A CN105254145 A CN 105254145A
Authority
CN
China
Prior art keywords
intensifiens
water
capsule
capsule type
calcium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510505019.6A
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Chinese (zh)
Inventor
孙保兴
谢维宣
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangzhou Haoyang Water Treatment Materials Co Ltd
Hainan Chief Biology Technique Empolder Co Ltd
Original Assignee
Guangzhou Haoyang Water Treatment Materials Co Ltd
Hainan Chief Biology Technique Empolder Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangzhou Haoyang Water Treatment Materials Co Ltd, Hainan Chief Biology Technique Empolder Co Ltd filed Critical Guangzhou Haoyang Water Treatment Materials Co Ltd
Priority to CN201510505019.6A priority Critical patent/CN105254145A/en
Publication of CN105254145A publication Critical patent/CN105254145A/en
Pending legal-status Critical Current

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/80Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
    • Y02A40/81Aquaculture, e.g. of fish

Abstract

The invention discloses a capsule-type active calcium emulsion and a preparation method thereof. The capsule-type active calcium emulsion comprises, by weight, 6-12% of lipophilic surfactant, 4-8% of a hydrophilic surfactant, 1-3% of a stabilizing agent, 3-7% of an organic acid salt, 50-70% of water and 14-22% of active calcium. The capsule-type active calcium emulsion is prepared according to safety, stability and slow release principles, realizes ingredient synergistic effects, prolongs time of contact with the lower water by slow release of calcium, prolongs effective time and realizes night soil settlement, algae contraction and ageing and water cleaning. The capsule-type active calcium emulsion thoroughly degrades organic garbage at water bottom and has a degradation rate of 80% or more. The capsule-type active calcium emulsion is in a liquid state, has good deformation performances, can completely cover the water bottom, has good self-cleaning and self-degradation effects and is suitable for polluted aquatic product culture water activity recovery. The preparation method has simple processes and is safe in construction.

Description

Capsule type Calcium of intensifiens emulsion and preparation method thereof
Technical field
Capsule type Calcium of intensifiens emulsion that the present invention relates to a kind of Ecological Recovery of Water and preparation method thereof.
Background technology
Because environmental pollution is day by day serious, industrial pollutants, agricultural pollutant, domestic pollutant are by rain drop erosion and collect through river, transfer to various cultivating pool, cause the water quality severe exacerbation of cultivating pool, cause have a strong impact on hydrocoles; Current raiser commonly uses strong oxidizer system and processes contaminated water body, but the potassium hydrogen persulfate in oxygenant, dioxide peroxide, bromine chlorine Hai Yin and polymerize aluminum chloride etc. are to can water bottom ecology damage, the microorganism cadaverine of more than 40 times can be raised time serious, simultaneously because the rich aluminium environment using oxygenant to cause for a long time can cause the cell damage of organism in water, if the edible biology be grown in such environment of people also can damage human body.
Summary of the invention
The object of the invention is to overcome above-mentioned the deficiencies in the prior art, provides a kind of and can administer, the capsule type Calcium of intensifiens emulsion of repairing contaminated water ecological setting and preparation method thereof, and can not cause other environmental pollution.
Technical scheme of the present invention is: a kind of capsule type Calcium of intensifiens, and its weight percentages of components is: lipophilic surfactant 6% ~ 12%, hydrophilic surfactant 4% ~ 8%, stablizer 1% ~ 3%, organic acid salt 3% ~ 7%, water 50% ~ 70%, Calcium of intensifiens 14% ~ 22%.
Described lipophilic surfactant is fatty alcohol-polyoxyethylene ether carboxylic acid sodium.
Described hydrophilic surface promoting agent is cocoyl glycine potassium.
Described stablizer is poly(oxyethylene glycol) 400.
Described Calcium of intensifiens is calcium lactate.
Described organic acid salt is tartaric acid sodium.
Described water is tap water.
Prepare the method for capsule type Calcium of intensifiens, comprise following steps:
Step one, be mixed in proportion hydrophilic surfactant active, organic acid salt, tap water, and abundant stirring and dissolving 60 minutes, solvent temperature is 60 ~ 70 DEG C, forms clear viscous stabilizing solution A;
Step 2, be mixed in proportion lipophilic surfactant, Calcium of intensifiens and stablizer, and abundant stirring and dissolving 30 minutes, solvent temperature is 50 ~ 60 DEG C, forms clear homogeneous solution B;
Step 3, mix and blend A, B two kinds of solution 2 hours, technological temperature is 25 ~ 35 DEG C, the finished product that the even emulsifiable paste of final formation is aqueous.
The invention has the beneficial effects as follows: the composite hydrophilic surfactant of the present invention, lipophilic surfactant strengthen interfacial activity and the interfacial film strength of encapsulation system and Ecological Recovery of Water system by reducing dynamical interfacial tension, the stability of raising encapsulation system; Restoration of the ecosystem system after packing extends the duration of contact with bottom pollutent by slow releasing Calcium of intensifiens, extend action time, reach sedimentation ight soil, shrink aging algae, clean water body object, and by active ion calcium stable water, bed mud pedosphere, for bottom microorganism provides excellent dissolved oxygen ecology, finally for hydrocoles provides the aquifer cultivation environment of high dissolved oxygen, low suspended substance.
The present invention is that principle is made according to security, stability, slow-releasing, gives full play to the coordinative role of each material, can thorough organic waste at the bottom of degradation water, and processing rate reaches more than 80%; The present invention is simultaneously that mobility is liquid, and deformation performance is good, and full operculum is water-bed, and self-cleaning is explained by oneself respond well, is applicable to contaminated aquaculture system activation recovering, and production technique is simple, construction safety.
Embodiment
Below by embodiment, technical scheme of the present invention is described in further detail.
Embodiment one,
Capsule type Calcium of intensifiens, its weight percentages of components is:
Cocoyl glycine potassium 5%, tartaric acid sodium 5%, tap water 60%, fatty alcohol-polyoxyethylene ether carboxylic acid sodium 10%, poly(oxyethylene glycol) 400 2%, calcium lactate 18%.
By proportioning mixing cocoyl glycine potassium, tartaric acid sodium, tap water, and abundant stirring and dissolving 60 minutes, solvent temperature is 60 ~ 70 DEG C, forms clear viscous stabilizing solution A; By proportioning mixing-in fat polyoxyethylenated alcohol carboxylic acid sodium, calcium lactate and poly(oxyethylene glycol) 400, and abundant stirring and dissolving 30 minutes, solvent temperature is 50 ~ 60 DEG C, forms clear homogeneous solution B; Last mix and blend A, B two kinds of solution 2 hours, technological temperature is 25 ~ 35 DEG C, the finished product that the even emulsifiable paste of final formation is aqueous.
For water treatment scene Calcium of intensifiens, get above-mentioned capsule type Calcium of intensifiens of preparing and carry out the two contaminated pond water quality improved experimentals in place, investigate the improvement in aging pond of capsule type Calcium of intensifiens and water treatmenting performance:
Experiment place: the aging shrimp-cultivation pool pool of sea-gull island, Fanyu, Guangzhou water colour black.
Injected volume: every depth of water 1 meter throws in 200 grams/acre.
Tool performance data are as shown in table 1:
Table 1
Add capsule type Calcium of intensifiens in contaminated water body after, 6 hours full dispersion to bottom environment, complete comprehensive reparation in 48 hours, Ecology dissolved oxygen stable after reparation, water transparency stablize leeward angle without dirty film, water body is without bad smell, and shrimp vigor obviously raises, nothing floating head and not sinkage.
Experiment place: the aging piscina that sea-gull island, Fanyu, Guangzhou water colour is dark green.
Injected volume: every depth of water 1 meter throws in 200 grams/acre.
Tool performance data are as shown in table 2:
Table 2
After being added capsule type Calcium of intensifiens in the water body that stains, within 6 hours, complete the full dispersion to bottom environment, within 48 hours, complete comprehensive reparation, Ecology dissolved oxygen stable after reparation, water transparency are stable, leeward angle is without dirty film and blue-green algae, water body is without bad smell, fish body surface is bright and clean, fish vigor obviously raises, nothing floating head and not sinkage.

Claims (8)

1. a capsule type Calcium of intensifiens emulsion, is characterized in that, its weight percentages of components is: lipophilic surfactant 6% ~ 12%, hydrophilic surfactant 4% ~ 8%, stablizer 1% ~ 3%, organic acid salt 3% ~ 7%, water 50% ~ 70%, Calcium of intensifiens 14% ~ 22%.
2. capsule type Calcium of intensifiens emulsion according to claim 1, is characterized in that: described lipophilic surfactant is fatty alcohol-polyoxyethylene ether carboxylic acid sodium.
3. capsule type Calcium of intensifiens emulsion according to claim 1, is characterized in that: described hydrophilic surface promoting agent is cocoyl glycine potassium.
4. capsule type Calcium of intensifiens emulsion according to claim 1, is characterized in that: described stablizer is poly(oxyethylene glycol) 400.
5. capsule type Calcium of intensifiens emulsion according to claim 1, is characterized in that: described Calcium of intensifiens is calcium lactate.
6. capsule type Calcium of intensifiens emulsion according to claim 1, is characterized in that: described organic acid salt is tartaric acid sodium.
7. capsule type Calcium of intensifiens emulsion according to claim 1, is characterized in that: described water is tap water.
8. prepare the method for capsule type Calcium of intensifiens emulsion as claimed in claim 1, it is characterized in that, comprise following steps:
Step one, be mixed in proportion hydrophilic surfactant active, organic acid salt, tap water, and abundant stirring and dissolving 60 minutes, solvent temperature is 60 ~ 70 DEG C, forms clear viscous stabilizing solution A;
Step 2, be mixed in proportion lipophilic surfactant, Calcium of intensifiens and stablizer, and abundant stirring and dissolving 30 minutes, solvent temperature is 50 ~ 60 DEG C, forms clear homogeneous solution B;
Step 3, mix and blend A, B two kinds of solution 2 hours, technological temperature is 25 ~ 35 DEG C, the finished product that the even emulsifiable paste of final formation is aqueous.
CN201510505019.6A 2015-08-18 2015-08-18 Capsule-type active calcium emulsion and preparation method thereof Pending CN105254145A (en)

Priority Applications (1)

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CN201510505019.6A CN105254145A (en) 2015-08-18 2015-08-18 Capsule-type active calcium emulsion and preparation method thereof

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Publications (1)

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CN105254145A true CN105254145A (en) 2016-01-20

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105800722A (en) * 2016-05-04 2016-07-27 无锡市嘉邦电力管道厂 Wastewater treatment agent as well as preparation method and application thereof
CN105883964A (en) * 2016-05-04 2016-08-24 无锡市嘉邦电力管道厂 Water purification composition as well as preparation method and application thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2549766C2 (en) * 1974-11-13 1984-11-08 The Procter & Gamble Co., Cincinnati, Ohio Spray-dried detergent
CN104212426A (en) * 2013-06-05 2014-12-17 中国石油天然气股份有限公司 Wrapped profile control degradation agent
CN104944563A (en) * 2010-11-15 2015-09-30 阿彻丹尼尔斯米德兰德公司 Compositions and uses thereof in converting contaminants

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2549766C2 (en) * 1974-11-13 1984-11-08 The Procter & Gamble Co., Cincinnati, Ohio Spray-dried detergent
CN104944563A (en) * 2010-11-15 2015-09-30 阿彻丹尼尔斯米德兰德公司 Compositions and uses thereof in converting contaminants
CN104212426A (en) * 2013-06-05 2014-12-17 中国石油天然气股份有限公司 Wrapped profile control degradation agent

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105800722A (en) * 2016-05-04 2016-07-27 无锡市嘉邦电力管道厂 Wastewater treatment agent as well as preparation method and application thereof
CN105883964A (en) * 2016-05-04 2016-08-24 无锡市嘉邦电力管道厂 Water purification composition as well as preparation method and application thereof

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