CN105238637B - It is a kind of to produce the liquid mechanization wine-making technology rich in terpene compound - Google Patents

It is a kind of to produce the liquid mechanization wine-making technology rich in terpene compound Download PDF

Info

Publication number
CN105238637B
CN105238637B CN201510709864.5A CN201510709864A CN105238637B CN 105238637 B CN105238637 B CN 105238637B CN 201510709864 A CN201510709864 A CN 201510709864A CN 105238637 B CN105238637 B CN 105238637B
Authority
CN
China
Prior art keywords
incubated
warming
adds
mash
wine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201510709864.5A
Other languages
Chinese (zh)
Other versions
CN105238637A (en
Inventor
薛栋升
庾昌文
汪江波
蔡凤娇
沈永祥
余汉超
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hubei University of Technology
Original Assignee
Hubei University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hubei University of Technology filed Critical Hubei University of Technology
Priority to CN201510709864.5A priority Critical patent/CN105238637B/en
Publication of CN105238637A publication Critical patent/CN105238637A/en
Application granted granted Critical
Publication of CN105238637B publication Critical patent/CN105238637B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Seasonings (AREA)

Abstract

The invention discloses the technique that a kind of mechanization liquid rich in terpene compound is brewageed, belong to brewing technical field.The present invention is raising terpenoid substance content, use kamuning, thyme, perfume change to increase the content of the terpenoid substance in wine body, the method that the mode freezed suddenly using multiple high temp mode, high temperature baked coke, cold ethanol mash during the fermentation simultaneously promotes the leaching of terpenoid substance, the significant leaching for promoting terpenoid substance and the generation for promoting Sauce flavor, the wine of production have the characteristics of sauce aromatic flavour, mouthfeel is sweet ice-cold.

Description

It is a kind of to produce the liquid mechanization wine-making technology rich in terpene compound
Technical field
The present invention relates to a kind of liquid mechanization wine-making technology rich in terpene compound, belong to brewing technical field.
Background technology
The features such as Maotai-flavor liquor has perfume without gorgeous, low without light, and fragrance is coordinated, its unique Sauce flavor is by one Some consumers like, but its price price in all white wine is higher, and reason is the production technology of Maotai-flavor flavor white wine, raw Cycle length is produced, labor intensity is high, and the cost of production is high, causes ordinary consumer and is difficult to receive its high price.
It is to reduce labor intensity that mechanization, which is brewageed, reduces one of feasible path of cost, but solid state fermentation is unfavorable for realizing Entire mechanization, and brewing liquid is advantageously implemented mechanization, and also to retain its certain for the Maotai-flavor liquor after brewing liquid Sauce flavor.
Research in recent years contains in Maotai-flavor liquor it has been shown that terpenoid substance has good anticancer effect A certain amount of terpenoid substance, the Dong Jiu using herbaceous plant as primary raw material contains substantial amounts of terpenoid substance, and flavor is suitable People.
In Maotai-flavor liquor brewing process, particularly during brewing liquid, the time brewageed is grown, the temperature phase brewageed To higher, this all determines that the brewage process of Maotai-flavor liquor is very beneficial for extracting out the terpenoid substance in herbaceous plant, So as to increase the content of terpenoid substance in wine body.
The content of the invention
The present invention is directed to insufficient present on, there is provided a kind of liquid mechanization vintager rich in terpene compound Skill, the present invention, using kamuning, thyme, change perfume to increase the terpenes thing in wine body to improve terpenoid substance content The content of matter;Create new brewage the high temperature of Maotai-flavor liquor to be combined together with the extraction of note alkenes material, promote terpenes The leaching of class material and the generation for promoting Sauce flavor, obtained white wine have the characteristics of sauce aromatic flavour, mouthfeel is sweet ice-cold.
In order to realize the purpose of the present invention, the present inventor is studied by lot of experiments and persistent exploration, be finally obtained as Lower technical scheme:
A kind of liquid mechanization wine-making technology rich in terpene compound, it is characterised in that:Comprise the following steps:
(1) prepared by saccharified liquid:Sorghum crushes by pulverizer, crosses 50 mesh sieve, adds α-amylase, and additional proportion is per ton Sorghum flour adds 0.3L, adds the running water of 3 times of sorghum flour quality, boils 10min in liquefied pot, adds carbohydrase, adds ratio Example adds 0.4L for sorghum powder per ton, and in saccharifying tank, 60 DEG C are incubated 2 hours, cool to 20 DEG C, obtain saccharified liquid and be placed on storage In tank.
(2) Maotai-flavor distiller's yeast is 20 according to saccharification liquid quality ratio:100 ratio is added in saccharified liquid, 500L hair Fermentation tank, zymotic fluid 400L, 28 DEG C of insulation 72h, 35 DEG C are then warming up to, are incubated after 24h and kamuning is added per tank, thyme, Repeatedly fragrant each 6200g of Ultramicro-powder pulverized powder, 55 DEG C are warming up to, are incubated 24h, fermentation tank is warming up to 68 DEG C, is incubated 4d, fermentation tank 82 DEG C are warming up to, is incubated 2d, 30L mash is taken out and is pre-chilled to -10 DEG C.
(3) remaining mash cools to 28 DEG C after taking out 30L, adds 20% Maotai-flavor distiller's yeast of mash gross mass, 28 DEG C It is incubated 72h.
(4) kamuning, thyme, repeatedly fragrant each 300g of Ultramicro-powder pulverized powder baked cokes in frying pan, when whole colors After blackening, it is added rapidly in -10 DEG C of 30L mash is pre-chilled to, is then warming up to 35 DEG C, is incubated 24h, is warming up to 55 DEG C 1d is incubated, the mash mixing of same step (3) is warming up to 65 DEG C of insulation 2d.
(5) filtering and concentrating:Plate and frame filter press filtration filters out vinasse, and diatomite filters, and micro-filtration membrane microfiltration is reverse osmosis concentrated Contracting wine body, stops counter-infiltration when alcoholic strength reaches 32 degree.
(6) vinosity is evaluated:Measure the content of terpenoid substance in wine body.
The present invention compared with prior art, has the following advantages that and significantly improved:(1) liquid fermentation production is rich in terpenes Class has the white wine of Sauce flavor, for improve terpenoid substance content, kamuning, thyme, repeatedly perfume (or spice) etc. be used to increase wine The content of terpenoid substance in body;(2) the new extraction knot high temperature of Maotai-flavor liquor brewageed with note alkenes material is created It is combined, promotes the leaching of terpenoid substance and promote the generation of Sauce flavor;(3) high temperature baked coke, cold ethanol wine with dregs are used The mode that liquid freezes suddenly promotes the leaching of terpenoid substance.
Specific embodiment
It is the specific embodiment of the present invention below, technical scheme is done and is further described, but it is of the invention Protection domain be not limited to these embodiments.It is every to be included in this hair without departing substantially from the change of present inventive concept or equivalent substitute Within bright protection domain.
Embodiment 1
1st, material and equipment
Sorghum is commercially available northeast sorghum;Maotai-flavor distiller's yeast is purchased from Shandong Xufang Daqu Co., Ltd;Sorghum pulverizer, storage Tank, saccharifying tank, liquefied pot, fermentation tank, plate and frame filter press, kettle formula distiller, micronizer etc. are all by good flourish machinery purchase; α-amylase and carbohydrase are bought from Shandong Long Yuan bioengineering Co., Ltd;Kamuning, thyme are repeatedly fragrant to be purchased from Wuhan City ;Koji for uncooked material is purchased from Yongzhou Yada Science and Technology Industry Co., Ltd..
2nd, preparation process
(1) prepared by saccharified liquid:Sorghum crushes by pulverizer, crosses 50 mesh sieve, adds α-amylase, and additional proportion is per ton Sorghum flour adds 0.3L, adds the running water of 3 times of sorghum flour quality, boils 10min in liquefied pot, adds carbohydrase, adds ratio Example adds 0.4L for sorghum powder per ton, and in saccharifying tank, 60 DEG C are incubated 2 hours, cool to 20 DEG C, obtain saccharified liquid and be placed on storage In tank.
(2) Maotai-flavor distiller's yeast is 20 according to saccharification liquid quality ratio:100 ratio is added in saccharified liquid, 500L hair Fermentation tank, the amount of zymotic fluid are 400L, 28 DEG C of insulation 72h, are then warming up to 35 DEG C, are incubated after 24h and kamuning is added per tank, in hundred Perfume (or spice), repeatedly fragrant each 6200g of Ultramicro-powder pulverized powder, is warming up to 55 DEG C, is incubated 24h, and fermentation tank is warming up to 68 DEG C, is incubated 4d, hair Fermentation tank is warming up to 82 DEG C, is incubated 2d, takes out 30L mash and is pre-chilled to -10 DEG C.
(3) remaining mash cools to 28 DEG C after taking out 30L, adds 20% Maotai-flavor distiller's yeast of mash gross mass, and 28 DEG C insulation 72h.
(4) kamuning, thyme, repeatedly fragrant each 300g of Ultramicro-powder pulverized powder baked cokes in frying pan, when whole colors After blackening, it is added rapidly in -10 DEG C of 30L mash is pre-chilled to, is then warming up to 35 DEG C, is incubated 24h, is warming up to 55 DEG C 1d is incubated, 65 DEG C of insulation 2d are warming up to after same step (3) mash mixing.
(4) filtering and concentrating:Plate and frame filter press filtration filters out vinasse, and diatomite filters, and micro-filtration membrane microfiltration is reverse osmosis concentrated Contracting wine body, stops counter-infiltration when alcoholic strength reaches 32 degree.
(5) vinosity is evaluated:Measure the content of terpenoid substance in wine body, detection method Hu Guangyuan detection method.[recklessly Light source, model essay come, Xu Yan, Jia Qiaoyan, the detection of terpenoid substance in Ran Xiao letter Dong Jius, brewing science and technology, and 2011,7], terpenes Material total content is added to obtain with the gross area of the chromatographic peak of all terpenoid substances, and the evaluation of wine body is shown in Table 1.
The wine body of table 1 is evaluated
Comparative example 1
Whole brewing process is all not added with kamuning, thyme, repeatedly perfume, replaces three kinds of Plant Powders using sorghum during baked coke End, baked coke technique is identical, the other the same as in Example 1, and the evaluation of wine body is shown in Table 2.
The wine body of table 2 is evaluated
Comparative example 2
Thyme, repeatedly fragrant not baked coke, is added directly into mash, the other the same as in Example 1, and the evaluation of wine body is shown in Table 3.
The wine body of table 3 is evaluated

Claims (1)

  1. A kind of 1. liquid mechanization wine-making technology rich in terpene compound, it is characterised in that:Comprise the following steps:
    (1)It is prepared by saccharified liquid:Sorghum crushes by pulverizer, crosses 50 mesh sieve, adds α-amylase, additional proportion is sorghum per ton Powder adds 0.3 L, adds the running water of 3 times of sorghum flour quality, boils 10 min in liquefied pot, adds carbohydrase, additional proportion 0.4 L is added for sorghum flour per ton, 60 DEG C are incubated 2 hours in saccharifying tank, cool to 20 DEG C, obtain saccharified liquid and be placed on storage tank It is interior;
    (2)Maotai-flavor distiller's yeast is 20 according to saccharification liquid quality ratio:100 ratio is added in saccharified liquid, 500 L fermentation Tank, the total amount for adding zymotic fluid are 400L, 28 DEG C of 72 h of insulation, are then warming up to 35 DEG C, are incubated 24 h, now add per tank Enter kamuning, thyme, repeatedly each 6200 g of fragrant Ultramicro-powder pulverized powder, is warming up to 55 DEG C, is incubated 24 h, fermentation tank heating To 68 DEG C, be incubated 4 d, fermentation tank is warming up to 82 DEG C, is incubated 2 d, take out wherein 30 L mash be pre-chilled to -10 DEG C it is standby;
    (3)Step(2)Middle remaining mash cools to 28 DEG C, adds the Maotai-flavor distiller's yeast of mash gross mass 20%, 28 DEG C of insulations 72 h;
    (4)Kamuning, thyme, repeatedly each 300 g baked cokes in frying pan of fragrant Ultramicro-powder pulverized powder are fast after whole color blackening Speed is added to step(2)In be cooled in advance in -10 DEG C of mash, be then warming up to 35 DEG C, be incubated 24 h, be warming up to 55 DEG C of guarantors 1 d of temperature, same to step(3)Mash mixing be warming up to 65 DEG C insulation 2 d;
    (5)Filtering and concentrating:Plate and frame filter press filtration filters out vinasse, diatomite filtering, micro-filtration membrane microfiltration, reverse osmosis concentration wine Body, stop counter-infiltration when alcoholic strength reaches 32 degree.
CN201510709864.5A 2015-10-28 2015-10-28 It is a kind of to produce the liquid mechanization wine-making technology rich in terpene compound Expired - Fee Related CN105238637B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510709864.5A CN105238637B (en) 2015-10-28 2015-10-28 It is a kind of to produce the liquid mechanization wine-making technology rich in terpene compound

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510709864.5A CN105238637B (en) 2015-10-28 2015-10-28 It is a kind of to produce the liquid mechanization wine-making technology rich in terpene compound

Publications (2)

Publication Number Publication Date
CN105238637A CN105238637A (en) 2016-01-13
CN105238637B true CN105238637B (en) 2017-12-05

Family

ID=55036462

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510709864.5A Expired - Fee Related CN105238637B (en) 2015-10-28 2015-10-28 It is a kind of to produce the liquid mechanization wine-making technology rich in terpene compound

Country Status (1)

Country Link
CN (1) CN105238637B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108018163B (en) * 2018-01-30 2021-06-22 林州红旗渠酒业有限责任公司 Brewing method for increasing content of terpene compounds in Daqu Luzhou-flavor liquor

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103320286A (en) * 2013-06-20 2013-09-25 苏州市养生花酒业有限公司 Composite-flavor health-preserving jade-like white wine and production technique thereof
CN104120066A (en) * 2014-08-11 2014-10-29 湖北工业大学 Method for producing Maotai-flavor liquor through liquid fermentation

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103320286A (en) * 2013-06-20 2013-09-25 苏州市养生花酒业有限公司 Composite-flavor health-preserving jade-like white wine and production technique thereof
CN104120066A (en) * 2014-08-11 2014-10-29 湖北工业大学 Method for producing Maotai-flavor liquor through liquid fermentation

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
新型酱香型白酒的生产;时卫平;《酿酒科技》;20051231(第8期);第54-55页 *

Also Published As

Publication number Publication date
CN105238637A (en) 2016-01-13

Similar Documents

Publication Publication Date Title
CN103642583B (en) A kind of natural fragrance of osmanthus tea-seed oil and preparation method thereof
CN101691533B (en) Technique for producing cool-type low-alcohol rice wine
CN103555554A (en) Black rice vinegar and preparation method thereof
CN104560610A (en) Production method of rosemary tea vinegar
CN103602576B (en) Preparation method of barley vinegar
CN104877858A (en) Fruit glutinous rice wine
CN103651988A (en) Production method for flavoring sesame oil
CN103564380A (en) Production technology of green Chinese prickly ash numb-taste components
CN106047590A (en) Process for making soy sauce aroma style baijiu
CN105238637B (en) It is a kind of to produce the liquid mechanization wine-making technology rich in terpene compound
CN103695235A (en) Production method of kiwi fruit syrup tea wine
CN104087493B (en) The preparation method of wine liquid is sipped in a kind of fully natural green health care
CN104286785A (en) Shii-take cooking wine preparation method
CN104250599A (en) Mulberry brandy preparation method
CN109430430A (en) A kind of preparation method seasoning capsicum chicken fat
CN105238638B (en) It is a kind of to produce the mechanization liquid brewage process rich in terpenes Sauce flavor white wine
CN106974254A (en) A kind of fresh sauce zymotechnique
CN105238658B (en) The brewing method of a plant Maotai-flavor liquor
CN104928115A (en) Dendrobe and bamboo shaving liquor and making method thereof
CN104479956A (en) Preparation method of rhodomyrtus tomentosa, silky ant and glutinous rice wine
CN103627582A (en) Brewing method for sweet potato yellow wine
CN104026545A (en) Brewing method for cooking wine
CN101899371B (en) Jujube beer
CN103897921A (en) Method for preparing healthcare tea wine for middle and old age people
CN108936492A (en) A kind of production method of muscat follicarpium sauce

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20171205

Termination date: 20181028