CN105219327B - A kind of cementing material for colored road surface and preparation method thereof - Google Patents
A kind of cementing material for colored road surface and preparation method thereof Download PDFInfo
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- CN105219327B CN105219327B CN201510638091.6A CN201510638091A CN105219327B CN 105219327 B CN105219327 B CN 105219327B CN 201510638091 A CN201510638091 A CN 201510638091A CN 105219327 B CN105219327 B CN 105219327B
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Abstract
The invention discloses a kind of cementing material for colored road surface and preparation method thereof, cementing material is made up of component A, component B, and the component A includes adhesive, thixotropic agent, talcum powder, silica flour, light stabilizer, pigment;Component B includes I type curing agent, II type curing agent, talcum powder, silica flour.Its preparation method is mixed evenly in same container for component A each composition is proportionally prepared, divides bucket to pack;Component B each composition is proportionally prepared, is mixed evenly in same container, divides bucket to pack;The component A modulated, component B are placed in same container at normal temperatures, load weighted pigment is added, stirs, that is, the colored road surface cementing material is made.Colored road surface cementing material provided by the invention, preparation method is easy, and pliability is good, has stronger cementitiousness, and ageing resistance is strong, has preferable durability.
Description
Technical field
The present invention relates to road cementing material, more particularly, to a kind of cementing material for colored road surface and its preparation side
Method.
Background technology
For a long time, covering of roadway only has white (cement)Road surface and black(Pitch)Road surface, colored road surface draw
Interest and the concern of people are played, colored road surface can not only decorate road, play a part of beautifying the environment, and can conduct
The measure directly perceived of traffic administration, a kind of brand-new cementing material is desirable for when colored road surface is mated formation.
High polymer material, which is applied to colored road surface and mated formation, in recent years has attempted, but the defects of this or that always be present, it is main
Including:First, the pavement performance of cementing material and the durability of color are difficult to meet actual application demand, it is mainly manifested in
Durability deficiency, ultra-violet radiation resisting ability, because cementitious matter partially it is hard often occur cause colored road surface because deforming deficiency
The problems such as cracking, premature aging;Second, preparation technology is complicated, subsequent treatment difficulty is big, and not low carbon ring is protected;Third, cementitious matter valency
Lattice are expensive, limit its extent of spreading amd application.So colored road surface is mated formation, the research and development of the cementing material used seem particularly significant.
The existing cementing material for colored road surface is a lot, as Chinese patent application 201010535836.3 discloses one
Kind of color pavement cementing material and application, its by bisphenol A epoxide resin, polyamide curing agent and polypropylene glycol diglycidyl ether or
Phenmethylol forms, and stirs at normal temperatures obtained.But the cementing material is completely solid by bisphenol A epoxide resin, polyamide
Agent and polypropylene glycol diglycidyl ether or phenmethylol composition, cost is very high, is unfavorable for popularization and application.
And for example Chinese patent application 201310740021.2 discloses a kind of cementing material and its system for colored road surface
Preparation Method, cementing material are made up of component A, component B, component C and filler, and component A includes epoxy resin 72-75 parts, work
Property diluent 18-20 parts, toughener 6-8 parts, 3 parts of silane coupler, antioxidant 0.5-0.7 parts, ultra-violet absorber 0.5-
1 part;B component includes A type curing agent 18-20 parts, B type curing agent 23-25 parts, tough curing agent 7-10 parts, accelerator 2-
5 parts and white carbon 15-30 parts;Component C includes rosin 15-20 parts, aluminium hydroxide 10-12 parts, ethylene glycol diglycidyl
Ether 8-10 parts, toluene formaldehyde resin 3-5 parts and benzene sulfonic acid 1-2 parts;Filler includes aramid fiber 0.3-0.5 parts and inorganic
Pigment 0.2-3 parts;Its preparation method is:Component A each composition is proportionally prepared, places same container at normal temperatures
Interior mixing 8-10min, to uniform, bucket is divided to pack;Component B each composition is proportionally configured, at normal temperatures
Place and 4-5min is mixed in same container, to uniform, divide bucket to pack;Component C each composition is proportionally configured
It is good, it is placed in same container and mixes to uniformly, after heating 5 minutes at a temperature of 60-65 DEG C, divides bucket to pack;Will filling
Each composition of agent is proportionally configured, and each composition is independently packed, inorganic pigment combination collocation as needed;It will be adjusted to
Component A, B, C according to 100:50:10 ratio is placed in same container at normal temperatures, adds the filler configured, mixing
3-5min is stirred, to uniform, i.e., the obtained cementing material.But this method needs to heat, and mixing time is longer, preparation technology
It is complicated.
The content of the invention
The present invention is for overcome the deficiencies in the prior art, there is provided a kind of cementing material and its preparation side for colored road surface
Method, the cementing material have stronger cementitiousness, and rich in pliability, the road surface laid with the cementing material has preferable
Pavement performance, Rut resistance, water resistant damage ability are good, have preferable durability.
To achieve these goals, the present invention uses following technical scheme:A kind of cementing material for colored road surface, by
Component A, component B and pigment are formed, the component A include 80 ~ 100 parts of adhesive, 3 ~ 5 parts of thixotropic agent, 30 ~ 35 parts of talcum powder,
800 5 ~ 8 parts of mesh silica flours, 0.3 ~ 0.5 part of light stabilizer, 4 ~ 6 parts of pigment;Component B includes 40 ~ 60 parts of I type curing agent, II type is consolidated
24 ~ 32 parts of agent, 46 ~ 50 parts of talcum powder, 6 ~ 9 parts of 800 mesh silica flour;Number number meter by weight;Component A's and component B
Weight ratio is 100 ~ 120:100~140.
The adhesive is polyurethane modified epoxy resin TX-8810 or TX-8820.Asphalt mixtures modified by epoxy resin after polyurethane-modified
Fat has the characteristics of rigidity is good, pliability is high, and than ordinary epoxy resin, not only pliability is preferable, and cementitiousness is strong.
The I type curing agent is the series of rigid polyamide class curing agent 300 or 651, and II type curing agent is flexible poly
The series of amide-type curing agent 400 or 650.Wherein I type curing agent is rigid curing agent, makes the intensity enhancing of cementing material, II
Type curing agent is Flexible Curing Agent, the pliability of cementing material is improved, and not only intensity is high for this cementing material, and pliability also obtains
It is obviously improved;Meanwhile the hardening time of this cementing material greatly shortens.
The light stabilizer is 2-hydroxy-4-n-octoxybenzophenone or 2- [(the 1,1- diformazans of 2- hydroxyls -3,5- two
Base propyl group phenyl)] -2H- BTAs.
The thixotropic agent is precipitated silica or LBCB-1 thixotropic lubricants.
The preparation method of the cementing material is:
1)Component A each composition is proportionally configured, places in same container and mixes at normal temperatures, with 150 ~
200r/min rotating speed is stirred until homogeneous, and divides bucket to pack;Component B each composition is proportionally configured, at normal temperatures
Place in same container and mix, be stirred until homogeneous with 150 ~ 200r/min rotating speed, divide bucket to pack, anti-oxidation;
2)By the component A modulated, component B according to 100 ~ 120:100 ~ 140 ratio is placed on same appearance at normal temperatures
In device, load weighted pigment in step 2 is added, is stirred until homogeneous with 150 ~ 200r/min rotating speed, that is, the color road is made
Face cementing material.
Compared with prior art, the present invention has advantages below:The colored road surface cementing material can produce at normal temperatures
And preparation method is simple;With stronger cementitiousness, meet the stability on road surface;Pliability is preferable, will not be because of cementing material
It is partially hard to occur, because deforming the problems such as deficiency causes colored road surface cracking, premature aging, improving the durability of colored road surface;Color
Weatherability it is stronger, ensure that long period use will not fade, while ensure that the road surface that cements is colour-fast for a long time;After solidification
Cementing material can keep prolonged stability, water resistant damage, antifatigue, anti-ultraviolet aging ability is strong, adds color road
The service life in face.
Embodiment
In order that those skilled in the art are better understood from the present invention program, it is right below in conjunction with the embodiment of the present invention
Technical scheme in the embodiment of the present invention carries out clear, complete description, it is clear that described embodiment is only the present invention's
A part of example, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not doing
Go out under the premise of creative work the every other embodiment obtained, should all belong to the scope of protection of the invention.
Embodiment 1
A kind of cementing material for colored road surface, preparation process are as follows:
Component A:90 parts of TX-8810 polyurethane modified epoxy resins being prepared by cross-linked modification method, precipitation two
4 parts of silica, 35 parts of talcum powder, 7 parts of 800 mesh silica flour, 0.3 part of light stabilizer 2-hydroxy-4-n-octoxybenzophenone, face
Expect 4 parts of pigment;After mentioned component configures, place in same container and mix at normal temperatures, stirred with 150r/min rotating speed
3min, to uniform, bucket is divided to pack, number number meter by weight;
Component B:40 parts of I type kymene, 00 curing agent, 24 parts of II type polyamide, 400 curing agent, 46 parts of talcum powder, 800 mesh
9 parts of silica flour;After mentioned component configures, place in same container and mix at normal temperatures, stirred with 150r/min rotating speed
3min, to uniform, bucket is divided to pack, number number meter by weight;
Component A, B that will finally modulate, according to A:B=110:130 ratio is placed in same container at normal temperatures, is added
Enter load weighted pigment, 5min is stirred with 150r/min rotating speed, to uniform, number number meter by weight, that is, obtain colour
Cementing material needed for road surface, its feature and performance meet the regulation of table 1.
Table 1 is that cementing material performance detection data and feature is made in embodiment 1
After tested, the indices of cementing material meet the regulation of table 1, the colored road surface formed with cementing material laying
Road surface stability is high, and adhesion strength is stronger, it is long-term use of after road surface is cracking, water damage phenomenon, and use for a long time will not
Fade.
Embodiment 2
A kind of cementing material for colored road surface, preparation process are as follows:
Component A:100 parts of TX-8820 polyurethane modified epoxy resins, the LBCB-1 being prepared by cross-linked modification method
3 parts of thixotropic lubricant, 32 parts of talcum powder, 5 parts of 800 mesh silica flour, light stabilizer 2- [(the 1,1- dimethyl propylenes of 2- hydroxyls -3,5- two
Base phenyl)] 0.5 part of -2H- BTAs, 6 parts of pigment;After mentioned component configures, place in same container and mix at normal temperatures
Close, 3min is stirred with 200r/min rotating speed, to uniform, divide bucket to pack, number number meter by weight;
Component B:I 56 parts of type polyamide 6 51A curing agent, II 32 parts of type polyamide 6 50A curing agent, 48 parts of talcum powder, 800
9 parts of mesh silica flour;After mentioned component configures, place in same container and mix at normal temperatures, stirred with 200r/min rotating speed
3min, to uniform, bucket is divided to pack, number number meter by weight;
Component A, B that will finally modulate, according to A:B=100:120 ratio is placed in same container at normal temperatures, is added
Enter load weighted pigment, 4min is stirred with 200r/min rotating speed, to uniform, number number meter by weight, that is, obtain colour
Cementing material needed for road surface, its feature and performance meet the regulation of table 2.
Table 2 is that cementing material performance detection data and feature is made in embodiment 2
After tested, the indices of cementing material meet the regulation of table 2, and prepared by the cementing material convenient, saves the time;It is soft
Good toughness;Not cracking, obscission after long-time use;Not ponding;It is substantially colour-fast and road surface is in bright colors.
Embodiment 3
A kind of cementing material for colored road surface, preparation process are as follows:
Component A:80 parts of TX-8820 polyurethane modified epoxy resins, the LBCB-1 being prepared by cross-linked modification method
5 parts of thixotropic lubricant, 30 parts of talcum powder, 8 parts of 800 mesh silica flour, light stabilizer 2- [(the 1,1- dimethyl propylenes of 2- hydroxyls -3,5- two
Base phenyl)] 0.4 part of -2H- BTAs, 5 parts of pigment;After mentioned component configures, place in same container and mix at normal temperatures
Close, 3min is stirred with 180r/min rotating speed, to uniform, divide bucket to pack, number number meter by weight;
Component B:I 60 parts of type polyamide 6 51B curing agent, II 24 parts of type polyamide 6 50B curing agent, 50 parts of talcum powder, 800
6 parts of mesh silica flour;After mentioned component configures, place in same container and mix at normal temperatures, stirred with 180r/min rotating speed
3min, to uniform, bucket is divided to pack, number number meter by weight;
Component A, B that will finally modulate, according to A:B=120:140 ratio is placed in same container at normal temperatures, is added
Enter load weighted pigment, 4min is stirred with 200r/min rotating speed, to uniform, number number meter by weight, that is, obtain colour
Cementing material needed for road surface, its feature and performance meet the regulation of table 3.
Table 3 is that cementing material performance detection data and feature is made in embodiment 3
After tested, the indices of cementing material meet the regulation of table 2, and prepared by the cementing material convenient, saves the time;It is soft
Good toughness;Not cracking, obscission after long-time use;Not ponding;It is substantially colour-fast and road surface is in bright colors.
Claims (4)
1. a kind of cementing material for colored road surface, it is made by component A, component B, it is characterised in that:The component A includes glue
Glutinous 80 ~ 100 parts of agent, 3 ~ 5 parts of thixotropic agent, 30 ~ 35 parts of talcum powder, 5 ~ 8 parts of 800 mesh silica flour, 0.3 ~ 0.5 part of light stabilizer, face
4 ~ 6 parts of material;Component B includes 40 ~ 60 parts of I type curing agent, 24 ~ 32 parts of II type curing agent, 46 ~ 50 parts of talcum powder, 800 mesh silica flours
6 ~ 9 parts;Number number meter by weight;Component A and component B weight ratio are 100 ~ 120:100~140;The adhesive is poly-
Urethane modified epoxy TX-8810 or TX-8820;The I type curing agent is the polyamide-based series of curing agent 300 or 651,
II type curing agent is the polyamide-based series of curing agent 400 or 650.
2. according to a kind of cementing material for colored road surface described in claim 1, it is characterised in that:The light stabilizer is 2-
Hydroxyl -4- oxy-octyl benzophenones or 2- [2- hydroxyls -3,5- two (1,1- dimethyl propyls phenyl)] -2H- BTAs.
3. according to a kind of cementing material for colored road surface described in claim 1, it is characterised in that:The thixotropic agent is precipitation
Silica or LBCB-1 thixotropic lubricants.
A kind of 4. method for preparing the cementing material for being used for colored road surface any one of claim 1-3, it is characterised in that:
Comprise the following steps:
Step 1, component A each composition proportionally prepared, place in same container and mix at normal temperatures, with 150 ~
200r/min rotating speed stirs, and divides bucket to pack standby;Component B each composition is proportionally prepared, in normal temperature
Lower place in same container mixes, and is stirred with 150 ~ 200r/min rotating speed, divides bucket to pack standby;
Step 2, by the component A modulated, component B according to 100 ~ 120:100 ~ 140 ratio is placed on same appearance at normal temperatures
In device, stirred with 150 ~ 200r/min rotating speed, that is, the colored road surface cementing material is made.
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CN109370378B (en) * | 2018-10-19 | 2021-04-20 | 北京中科安途交通科技有限公司 | Water-based wear-resistant anti-ultraviolet curing material for pavement sealing layer and preparation method thereof |
CN110511708A (en) * | 2019-08-13 | 2019-11-29 | 上海闰龙电子材料有限公司 | A kind of high-bond epoxy resin structural adhesive and preparation method thereof |
CN112980371B (en) * | 2021-04-08 | 2023-03-31 | 湖北海星瑞新材料科技有限公司 | High-toughness glass fiber reinforced plastic adhesive and preparation method thereof |
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CN103627140B (en) * | 2013-11-01 | 2015-06-03 | 鲲鹏建设集团有限公司 | Cementing material for durable colored pavement and preparation method thereof |
CN103555145B (en) * | 2013-11-08 | 2016-01-13 | 西北永新涂料有限公司 | A kind of epoxy self-leveling floor coating and preparation method thereof |
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