CN105211328A - A kind of autumn health-care edible oil and preparation method thereof - Google Patents

A kind of autumn health-care edible oil and preparation method thereof Download PDF

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CN105211328A
CN105211328A CN201510655871.1A CN201510655871A CN105211328A CN 105211328 A CN105211328 A CN 105211328A CN 201510655871 A CN201510655871 A CN 201510655871A CN 105211328 A CN105211328 A CN 105211328A
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oil
extract
pears
hundred
autumn
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吴苏喜
韩小苗
申甜甜
陆少兰
刘瑞兴
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Changsha University of Science and Technology
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Changsha University of Science and Technology
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Abstract

The invention discloses a kind of autumn health-care edible oil, comprise following composition and percentage by weight thereof: the extract 1-3% of grape-kernel oil 5-25%, peanut oil 30-50%, rice bran oil 20-40%, linseed oil 5-25%, hundred pears maizes, the extract of hundred pears maizes refer to lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf mixture extract.The preparation method of autumn health-care edible oil comprises the following steps: open vacuum oil refining cauldron, and start vavuum pump, is sucked in vacuum oil refining cauldron by the extract of grape-kernel oil, peanut oil, rice bran oil, linseed oil and hundred pears maizes in proportion.In setting pot, residual voltage is 60 ~ 80mmHg, temperature is 70 ~ 80 DEG C, turn on agitator, warming while stirring, high-visible when seeing in pot from mirror mouth, and when hanging mirror without water smoke wall built-up, continue stirring 20 ~ 40min, stop heating up, cold filtration, obtains autumn health-care edible oil.Autumn health-care edible oil provided by the invention can have promote the production of body fluid to quench thirst, dispel scorching, nourishing Yin and moistening lung, anti-ageing, promote that the effect of body nutritional status is digested and assimilated, improved to body, suitable autumn eats.

Description

A kind of autumn health-care edible oil and preparation method thereof
Technical field
The present invention relates to edible oil manufacture field, refer to a kind of autumn health-care edible oil and preparation method thereof especially.
Background technology
The dialectical opinion food theory of traditional Chinese medicine is thought, selects will suit measures to differing conditions in terms of time during food, is exactly select edible suitable food according to Various Seasonal.Because climate change throughout the year, also there is respective change in the physiological function of body, human body must be obedient to the rule of four seasons spring, summer, autumn and winter wane and wax of yin and yang, adapts to the warm cold and cool climate change of a year, longevity of just keeping fit thereupon.When selection, application food, treating dryness syndrome by moistening, cloudy person's sun.
Edible oil is as the necessity of daily life, and its nutrition and effect are paid close attention to day by day widely.Disclosed edible health-care oil has a variety of at present, and great majority contain traditional Chinese medicine ingredients, for the control of some chronic diseases or the improvement of physical function.But be not suitable for containing the edible health-care oil of traditional Chinese medicine ingredients that everybody is edible and eat everyday, be especially not suitable for edible health in autumn because dry in autumn, turn cool, windy mutability gradually, be commonly called as eventful period, easily bring out constipation and breathing problem.At present also not for the functional health-care edible oil of Autumn Climate feature.
Summary of the invention
In view of this, the object of the invention is to propose a kind of autumn health-care edible oil, the resistance of aged animal model to drying in autumn, windy weather can be strengthened, there is remarkable anti-aging effects, can promote that body is digested and assimilated simultaneously, improve body nutritional status, improve organism physiology biochemical indicator, suitable autumn eats.
A kind of autumn health-care edible oil is the invention provides based on above-mentioned purpose, comprise following composition and percentage by weight thereof: grape-kernel oil 5 ~ 25%, peanut oil 30 ~ 50%, rice bran oil 20 ~ 40%, linseed oil 5 ~ 25%, the extract 1 ~ 3% of hundred pears maizes, the extract of described hundred pears maizes refer to lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf mixture extract.
Preferably, described autumn health-care edible oil comprises following composition and percentage by weight thereof: grape-kernel oil 15%, peanut oil 38%, rice bran oil 30%, linseed oil 15%, hundred pears maize extracts 2%.
In some embodiments of the invention, described peanut oil adopts the squeezing of water content high fresh peanut to form, remain the physiologically active ingredient in peanut to greatest extent, such as: VE, Bai Quinoa reed alcohol, cupreol, wheat germ phenol, phosphatide, choline etc., these compositions have enhancing immunity, delay senility, prevent and treat the effect such as bacillary dysentery and intestinal obstruction.
In one embodiment of the invention, the monounsaturated fatty acids of described autumn health-care edible oil and the ratio of polyunsaturated fatty acid are 1:0.99, and in polyunsaturated fatty acid, the ratio of ω-6 aliphatic acid and omega-fatty acid is 0.82:0.18.
The present invention also provides a kind of preparation method of autumn health-care edible oil, comprises the following steps:
Open vacuum oil refining cauldron, and start vavuum pump, in proportion the extract of grape-kernel oil, peanut oil, rice bran oil, linseed oil and hundred pears maizes is sucked in vacuum oil refining cauldron.
In setting pot, residual voltage is 60 ~ 80mmHg, temperature is 70 ~ 80 DEG C, turn on agitator, warming while stirring, high-visible when seeing in pot from mirror mouth, and when hanging mirror without water smoke wall built-up, continue stirring 20 ~ 40min, stop heating up, cold filtration, obtains autumn health-care edible oil.
In some embodiments of the invention, the preparation method of described hundred pears maize extracts comprises the following steps:
(1) dry at drying lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf being placed in 50 ~ 60 DEG C and reach 5 ~ 6% to moisture, then pulverize, cross 40 ~ 60 mesh sieves.
(2) to take etc. the lily of quality, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf powder, mix, obtain hundred pears maize mixed powder samples.
(3) described hundred pears maize mixed powder samples are loaded supercritical CO 2in the extraction kettle of extraction equipment, arranging extracting pressure is 20 ~ 30MPa, CO 2flow is 28 ~ 35L/h, 75% ethanol flow velocity is 2.7 ~ 3.5ml/min, first at temperature 25 ~ 35 DEG C, extracts 1.0 ~ 1.5h, then at temperature 35 ~ 45 DEG C, continues extraction 1.5 ~ 2.0h.
(4) released single extraction liquid every 15 minutes from separating still during extraction, the organoleptic quality according to different phase extract is different and carry out Fractional Collections, obtains hundred pears maize extracts.
Adopt supercritical carbon dioxide to add entrainer abstraction technique, the nonpolar active ingredient in lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf four kinds of foods and low pole active ingredient can be extracted.The hundred pears maize extracts containing nonpolar active ingredient and low pole active ingredient can be dissolved in the ready-mixed oil of grape seed oil, peanut oil, rice bran oil and linseed oil composition well.
Preferably, in described step (4), in order to obtain hundred pears maize extracts of high-quality, abandon the extract in first two stage in 15 minutes and in last 15 minutes, merge the extract that all the other interludes are collected, obtain limpid light yellow hundred pears maize extracts.Wherein, first extract obtained in 15 minutes is in muddy dark brown, color and luster and clarity not good enough, extract in last 15 minutes is white foam, lack effective active component, the extract in all the other interstages is limpid light yellow, therefore abandons the extract of first these two time period in 15 minutes and in last 15 minutes, collects the extract of all the other interludes.
As can be seen from above, autumn health-care edible oil provided by the invention has following good effect:
(1) dry in autumn, windy, should consumption Pingliang, be slightly cold; The food of the sweet acid of taste.Because property Pingliang, the food be slightly cold have scorching, strengthening the spleen and stomach, help health effect of dispelling.Taste acid food have promote the production of body fluid to quench thirst, nourishing Yin and moistening lung, restrain astringent or styptic treatment for spontaneous sweating, improve a poor appetite, the effect of spleen benefiting and stimulating the appetite.Sugariness food has mitigation spasm, be in harmonious proportion nature and flavor, take nourishing food to build up one's health, promoting production of body fluid and nourishing the lung effect.Autumn health-care edible oil adds lily, snow pear, radix polygonati officinalis and the nonpolar and low pole extract of the tuber of dwarf lilyturf in the ready-mixed oil of grape-kernel oil, peanut oil, rice bran oil and linseed oil composition, these compositions not only have promote the production of body fluid moisturize, effect that lung is supported in enriching yin, and there is the effects such as invigorating the spleen, appetizing, help health, it is scorching to eliminate autumn, strengthen health to the resistance of dry climate in autumn, suitable dry windy autumn eats.
(2) ω-6 (linoleic acid) in the monounsaturated fatty acids of this autumn health-care edible oil and the ratio of polyunsaturated fatty acid and polyunsaturated fatty acid and the ratio of ω-3 (leukotrienes) meet modern nutriology health oil standard to monounsaturated fatty acids and the ratio of polyunsaturated fatty acid and the proportion requirement of ω-6 (linoleic acid) and ω-3 (leukotrienes), and any natural oil and other ready-mixed oils are all difficult to reach this requirement.
(3) this autumn health-care edible oil significantly can reduce the activity of MDA (MDA) content and monoamine oxidase (MAO), remarkable increase antioxidase, the i.e. activity of superoxide dismutase (SOD) or content, the resistance of aged animal model to dry windy weather in autumn can be strengthened, there is remarkable anti-aging effects, and have promote body digest and assimilate, improve body nutritional status, improve the effects such as organism physiology biochemical indicator.
(4) this autumn health-care eats one of oil composition peanut oil is adopt the squeezing of water content high fresh peanut to form, remain the physiologically active ingredient in peanut to greatest extent, such as: VE, Bai Quinoa reed alcohol, cupreol, wheat germ phenol, phosphatide, choline etc., these compositions have enhancing immunity, delay senility, prevent and treat the effect such as bacillary dysentery and intestinal obstruction.
(5) this in season in autumn edible health-care oil saturated fatty acid content ratio lower, eater is allowed to take in a certain amount of animal food high containing saturated fatty acid, meet the preference of eater to animal food, overcome other ready-mixed oils and health-care oil restriction eater ingests containing the shortcoming of the high animal food of saturated fatty acid.
(6) the present invention obtains autumn health-care edible oil by low-temperature fabrication, remains the biologically active of the active ingredient of four kinds of oil and four kinds of foods to greatest extent.Adopt supercritical carbon dioxide to add entrainer abstraction technique, the nonpolar active ingredient in lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf four kinds of foods and low pole active ingredient can be extracted.The hundred pears maize extracts containing nonpolar active ingredient and low pole active ingredient can be dissolved in the ready-mixed oil of grape-kernel oil, peanut oil, rice bran oil and linseed oil composition well.
Detailed description of the invention
For making the object, technical solutions and advantages of the present invention clearly understand, below in conjunction with specific embodiment, the present invention is described in more detail.
In autumn, not most, dry, the windy mutability of summer heat, easily brings out constipation, breathing problem and skin disease etc., is commonly called as eventful period.Theoretical according to the dialectical opinion food of the traditional Chinese medicine four property five tastes that are theoretical and food, autumn should be selected consumption Pingliang, be slightly cold; The food of the sweet acid of taste.Because property Pingliang, the food be slightly cold have scorching, strengthening the spleen and stomach, help health effect of dispelling.Taste acid food have promote the production of body fluid to quench thirst, nourishing Yin and moistening lung, restrain astringent or styptic treatment for spontaneous sweating, improve a poor appetite, the effect of spleen benefiting and stimulating the appetite.Sugariness food has mitigation spasm, be in harmonious proportion nature and flavor, take nourishing food to build up one's health, promoting production of body fluid and nourishing the lung effect.Through comparing screening, from tens kinds of property Pingliangs, be slightly cold; Find in the food of the sweet acid of taste or vegetable seeds, the refined oil squeezed by grape pip, peanut, linseed and rice bran and the health-care oil of combination of active principles extracted by lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf, effect that not only having promotes the production of body fluid moisturizes, lung is supported in enriching yin, and there is many health-care effects such as invigorating the spleen, appetizing, help health, the resistance of health to dry windy weather in autumn can be improved, be particularly suitable for edible health in autumn.
The nature and flavor of the various raw materials of autumn health-care edible oil of the present invention and function are in table 1.
Table 1 four kinds of feedstock oils, lily, snow pear, radix polygonati officinalis and the nature and flavor of the tuber of dwarf lilyturf and function
The aliphatic acid constituent of the grape-kernel oil selected by the present invention, linseed oil, peanut oil and rice bran oil is in table 2.
The aliphatic acid composition of table 2 four kinds of feedstock oils
embodiment 1
The extract preparation method of hundred pears maizes, comprises the steps:
(1) dry at drying lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf being placed in 60 DEG C and reach 5% to water content, then pulverize, cross 60 mesh sieves.
(2) to take etc. the lily of quality, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf powder, mix, obtain hundred pears maize mixed powder samples.
(3) described hundred pears maize mixed powder samples are loaded supercritical CO 2in the extraction kettle of extraction equipment, arranging extracting pressure is 20MPa, CO 2flow is 28L/h, 75% ethanol flow velocity is 2.7ml/min, first at temperature 25 DEG C, extracts 1.5h, then at temperature 35 DEG C, continues extraction 1.5h.
(4) released single extraction liquid every 15 minutes from separating still during extraction, the organoleptic quality according to different phase extract is different and carry out Fractional Collections.Abandon first in 15 minutes with last 15 minutes in the extract of hundred pears maizes in these two stages, the extract collected by all the other interludes during extraction merges, and obtains the extract of hundred pears maizes.
The preparation method of autumn health-care edible oil, comprises the steps:
Step 1, open vacuum oil refining cauldron, and start vavuum pump, by weight percentage successively by grape-kernel oil 15%, peanut oil 38%, rice bran oil 30%, linseed oil 15%, hundred pears maize extracts 2% suck in vacuum oil refining cauldron.It should be noted that, peanut oil is here squeezed by the high fresh peanut of water content to form, concrete through clean, peeling off, broken, making beating, squeezing, filtration and obtain.
Step 2, in setting pot, residual voltage is 60mmHg, temperature is 80 DEG C, turn on agitator, warming while stirring, high-visible when seeing in pot from mirror mouth, and when hanging mirror without water smoke wall built-up, continue to stir 30min, stop heating up, cold filtration, obtains autumn health-care edible oil.
The aliphatic acid composition of the autumn health-care edible oil that the embodiment of the present invention prepares is in table 3.
The aliphatic acid composition of table 3 embodiment 1 autumn health-care edible oil
The health of modern nutriology is thought by oily theory, the optimal proportion of saturated fatty acid, monounsaturated fatty acids and polyunsaturated fatty acid is 1:1:1, in polyunsaturated fatty acid, the ratio of ω-6 (linoleic acid) and ω-3 (leukotrienes) should be respectively 0.8 ~ 0.86 and 0.14 ~ 0.2, and any one pure natural oil all can not meet these requirements.The monounsaturated fatty acids of the autumn health-care edible oil that the embodiment of the present invention provides and the ratio of polyunsaturated fatty acid are 1:0.99, are almost optimal proportion.ω-6 linoleic acid content and the linolenic ratio of ω-3 are 0.82:0.18, within modern nutriology ω-6 linoleic acid thought by oily theory of health and the linolenic proportion of ω-3, meet standard.
Embodiment 2
The extract preparation method of hundred pears maizes, comprises the steps:
(1) dry at drying lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf being placed in 60 DEG C and reach 6% to moisture, then pulverize, cross 40 mesh sieves.
(2) to take etc. the lily of quality, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf powder, mix, obtain hundred pears maize mixed powder samples.
(3) described hundred pears maize mixed powder samples are loaded supercritical CO 2in the extraction kettle of extraction equipment, arranging extracting pressure is 30MPa, CO 2flow is 35L/h, 75% ethanol flow velocity is 3.5ml/min, first at temperature 35 DEG C, extracts 1.5h, then under temperature 45 C, continues extraction 1.5h.
(4) released single extraction liquid every 15 minutes from separating still during extraction, the organoleptic quality according to different phase extract is different and carry out Fractional Collections.Abandon first in 15 minutes with last 15 minutes in the extract of hundred pears maizes in these two stages, the extract collected by all the other interludes during extraction merges, and obtains the extract of hundred pears maizes.
The preparation method of autumn health-care edible oil, comprises the steps:
Step 1, open vacuum oil refining cauldron, and start vavuum pump, by weight percentage successively by grape-kernel oil 25%, peanut oil 30%, rice bran oil 29%, linseed oil 15%, hundred pears maize extracts 1% suck in vacuum oil refining cauldron.It should be noted that, peanut oil is here squeezed by the high fresh peanut of water content to form, concrete through clean, peeling off, broken, making beating, squeezing, filtration and obtain.
Step 2, in setting pot, residual voltage is 80mmHg, temperature is 70 DEG C, turn on agitator, warming while stirring, high-visible when seeing in pot from mirror mouth, and when hanging mirror without water smoke wall built-up, continue to stir 20min, stop heating up, cold filtration, obtains autumn health-care edible oil.
The aliphatic acid composition of the autumn health-care edible oil that the embodiment of the present invention prepares is in table 4.
The aliphatic acid composition of table 4 embodiment 2 autumn health-care edible oil
The monounsaturated fatty acids of the autumn health-care edible oil that the embodiment of the present invention provides and the ratio of polyunsaturated fatty acid are 1:1.22, close to optimal proportion.ω-6 linoleic acid content and the linolenic ratio of ω-3 are 0.83:0.17 close to healthy ω-6 linoleic acid with oily theory calls of modern nutriology and the linolenic ratio of ω-3.
Embodiment 3
The extract preparation method of hundred pears maizes, comprises the steps:
(1) dry at drying lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf being placed in 60 DEG C and reach 6% to moisture, then pulverize, cross 50 mesh sieves.
(2) to take etc. the lily of quality, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf powder, mix, obtain hundred pears maize mixed powder samples.
(3) described hundred pears maize mixed powder samples are loaded supercritical CO 2in the extraction kettle of extraction equipment, arranging extracting pressure is 25MPa, CO 2flow is 30L/h, 75% ethanol flow velocity is 3.0ml/min, first at temperature 30 DEG C, extracts 1.5h, then at temperature 40 DEG C, continues extraction 1.5h.
(4) released single extraction liquid every 15 minutes from separating still during extraction, the organoleptic quality according to different phase extract is different and carry out Fractional Collections.Abandon first in 15 minutes with last 15 minutes in the extract of hundred pears maizes in these two stages, the extract collected by all the other interludes during extraction merges, and obtains the extract of hundred pears maizes.
The preparation method of autumn health-care edible oil, comprises the steps:
Step 1, open vacuum oil refining cauldron, and start vavuum pump, by weight percentage successively by grape-kernel oil 8%, linseed oil 22%, peanut oil 47%, rice bran oil 20%, hundred pears maize extracts 3% suck in vacuum oil refining cauldron.It should be noted that, peanut oil is here squeezed by the high fresh peanut of water content to form, concrete through clean, peeling off, broken, making beating, squeezing, filtration and obtain.
Step 2, in setting pot, residual voltage is 70mmHg, temperature is 70 DEG C, turn on agitator, warming while stirring, high-visible when seeing in pot from mirror mouth, and when hanging mirror without water smoke wall built-up, continue to stir 40min, stop heating up, cold filtration, obtains autumn health-care edible oil.
The aliphatic acid composition of the autumn health-care edible oil that the embodiment of the present invention prepares is in table 5.
The aliphatic acid composition of table 5 embodiment 3 autumn health-care edible oil
The monounsaturated fatty acids of the autumn health-care edible oil that the embodiment of the present invention provides and the ratio of polyunsaturated fatty acid are 1:0.83, close to optimal proportion.ω-6 linoleic acid content and the linolenic ratio of ω-3 are 0.68:0.32, close to the modern nutriology health theoretical ratio required ω-6 linoleic acid and ω-3 leukotrienes of oil.
Embodiment 4
The extract preparation method of hundred pears maizes, comprises the steps:
(1) dry at drying lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf being placed in 60 DEG C and reach 6% to moisture, then pulverize, cross 60 mesh sieves.
(2) to take etc. the easter lily of quality, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf powder, mix, obtain hundred pears maize mixed powder samples.
(3) described hundred pears maize mixed powder samples are loaded supercritical CO 2in the extraction kettle of extraction equipment, arranging extracting pressure is 27MPa, CO 2flow is 32L/h, 75% ethanol flow velocity is 3.2ml/min, first at temperature 27 DEG C, extracts 1.7h, then at temperature 42 DEG C, continues extraction 1.7h.
(4) released single extraction liquid every 15 minutes from separating still during extraction, the organoleptic quality according to different phase extract is different and carry out Fractional Collections.Abandon first in 15 minutes with last 15 minutes in the extract of hundred pears maizes in these two stages, the extract collected by all the other interludes during extraction merges, and obtains the extract of hundred pears maizes.
The preparation method of autumn health-care edible oil, comprises the steps:
Step 1, open vacuum oil refining cauldron, and start vavuum pump, by weight percentage successively by grape-kernel oil 20%, linseed oil 14%, peanut oil 36%, rice bran oil 28%, hundred pears maize extracts 2% suck in vacuum oil refining cauldron.It should be noted that, peanut oil is here formed by the fresh squeezing that water content is high, concrete through clean, peeling off, broken, making beating, squeezing, filtration and obtain.
Step 2, in setting pot, residual voltage is 72mmHg, temperature is 75 DEG C, turn on agitator, warming while stirring, high-visible when seeing in pot from mirror mouth, and when hanging mirror without water smoke wall built-up, continue to stir 40min, stop heating up, cold filtration, obtains autumn health-care edible oil.
The aliphatic acid composition of the autumn health-care edible oil that the embodiment of the present invention prepares is in table 6.
The aliphatic acid composition of table 6 embodiment 4 autumn health-care edible oil
The monounsaturated fatty acids of the autumn health-care edible oil that the embodiment of the present invention provides and the ratio of polyunsaturated fatty acid are 1:1.11, closely optimal proportion.ω-6 linoleic acid content and the linolenic ratio of ω-3 are 0.84:0.16, and closely modern nutriology health oil is theoretical to ω-6 linoleic acid with ω-3 is linolenic requires ratio.
experimental example 1: prove autumn health-care edible oil of the present invention have anti-ageing, promote to digest and assimilate, the experiment of enhancing development effect
1, animal used as test:
Healthy kunming mice, purchased from animal used as test portion of Central South University, the age is 5 weeks Age, and body weight is 20 ± 2g
2, experiment grouping:
30 kunming mices are divided into three groups at random, are respectively experimental group, aging model group and control group, often organize 10, comprise 5 male and 5 female, 5 male and 5 female KM mouse separately raisings, permission kunming mice free choice feeding and drinking-water.
3, experimental period:
From 1 day September in 2014, to end of day October 12 in 2014, amount to 42 days, namely 6 weeks.Whole feeding experiment is carried out under midautumn natural room temperature, does not take any insulation, lowers the temperature or heats measure.
4, experimental technique:
Experimental group: every day, consumption counted 125mg/kg by Mouse Weight at the neck hypodermic injection D galactolipin of mouse, give autumn health-care edible oil by gavage every day, consumption counts 5g/kg by Mouse Weight simultaneously.
Aging model group: every day, consumption counted 125mg/kg by Mouse Weight at the neck hypodermic injection D galactolipin of mouse, gives the distilled water of equal-volume (0.25mL) every day simultaneously by gavage.
Control group: every day, at neck hypodermic injection equal-volume (0.2mL) physiological saline of mouse, gives the distilled water of 0.25mL every day simultaneously by gavage.
After having processed as stated above, carry out clinical observation, record the general status of all animals.After experiment starts, every day records food consumption quantity, and per weekend measures body weight.Experiment carries out 6 weeks continuously, puts to death animal used as test at the 6th weekend, and inspection pathological change, gets brain and hepatic tissue for biochemical analysis.Brain and liver tissues is made 10% homogenate respectively, with the centrifugal 12min of 2000r/min, collects supernatant and be used for biochemical analysis.The activity of SOD, MAO, MDA of brain hepatic tissue or content adopt corresponding biochemical reagents box (Nanjing is built up Bioengineering Research Institute and produced) and UV754N ultraviolet specrophotometer (Shanghai Precision Scientific Apparatus Co., Ltd's production) to measure respectively.
The present invention adopts variance analysis (SNK) the analysis design mothod group in SPSS11.5 software, the significance of difference between aging model group and control group.
3, experimental result:
After experiment terminates, the behavior expression of experimental mice is active, fur gloss, fecaluria are normal, similar to control group mice, is obviously better than aging model group mouse.
Each group of Mouse Weight delta data is in table 7, and food consumption quantity is in table 8.Wherein, in table 7, the body weight of each group mouse is the mean value of this group Mouse Weight, and in table 8, each group mouse chow consumption is the food consumption quantity of this group mouse mouse average every day every.
Adopt biochemical reagents box to measure the MDA content of each group of mouse brain and liver tissues protein and the activity of MAO and SOD, the results are shown in Table 9.In table 9, the activity of MDA content and MAO and SOD is the mean value of each group of 10 mouse.
Table 7 experimental group, old and feeble group and control group mice weight ratio be (unit=g/ only) comparatively
Note: a represent the 6th weekend experimental group and control group between body weight there is no significant difference (P>0.05);
B represent the 6th weekend experimental group and aging model group between body weight there were significant differences (p<0.05);
C to represent between aging model group and control group body weight, and there were significant differences (p<0.05).
The comparison of table 8 experimental group, old and feeble group and control group mice food consumption (unit=g/ days/only)
Note: a represents that, at the 6th weekend, between experimental group and aging model group, Food consumption does not have significant difference (P>0.05);
B represents at the 6th weekend, and the food consumption quantity of experimental group and aging model group mouse is significantly lower than control group (p<0.05).
The comparison of table 9 experimental group, old and feeble group and control group mice brain and liver tissues MDA content, SOD and MAO activity
Note: a represents does not have significant difference (p>0.05) between experimental group and control group;
B represents has pole significant difference (p<0.01) between experimental group and old and feeble group;
C represents with old and feeble, experimental group organizes that there were significant differences (p<0.05);
D represents has pole significant difference (p<0.01) between old and feeble group and control group.
From table 7, table 8 and table 9, to the 6th weekend, total food ration and the aging model group of experimental mice do not have significant difference, but significantly lower than control group, and the body weight of experimental mice and control group do not have significant difference, but be significantly higher than aging model group.This shows that experimental mice eats like a bird, looking fast, also illustrate autumn health-care edible oil have promote to digest and assimilate, the effect of enhancing development and saving feed.There were significant differences for the old and feeble associated biochemical composition of aging model group mouse and control group mice, and this proves that the aging model that this experiment is set up is successful.And the old and feeble Related Component MDA content of experimental mice, SOD and MAO active comparison with control group mice does not have significant difference (p>0.05), but there are pole significant difference (p<0.01) or significant difference (p<0.05) compared with aging model group mouse.Animal is between declining period, MDA (MDA) content and monoamine oxidase (MAO) activity can increase, and superoxide dismutase (SOD) activity can reduce, MDA content, MAO and SOD activity evaluates the important parameter of body aging and health degree.
Judge according to table 7, table 8 and table 9 result, autumn health-care edible oil of the present invention has the resistance of enhancing body to dry windy weather in autumn, promote to digest and assimilate, enhancing development, saving feed, improve body nutritional status and physiological and biochemical index, the activity of old and feeble Related Component MDA (MDA) content of remarkable reduction and monoamine oxidase (MAO), remarkable increase superoxide dismutase (SOD), namely increase antioxidase (anti-ageing enzyme) activity or content, there is significant anti-aging effects.
As can be seen from foregoing description, first, autumn health-care edible oil provided by the invention adds lily, snow pear, radix polygonati officinalis and the low pole of the tuber of dwarf lilyturf and apolar extraction liquid in the ready-mixed oil of grape-kernel oil, linseed oil, peanut oil, rice bran oil composition.These composition nature and flavor be property Pingliang or be slightly cold, the sweet acid of taste, can nutrition complement, suitable dry windy autumn eats.Because autumn should consumption Pingliang, be slightly cold, the food of the sweet acid of taste.Property Pingliang, the food that is slightly cold have scorching, strengthening the spleen and stomach, help health effect of dispelling.Taste acid food have promote the production of body fluid to quench thirst, nourishing Yin and moistening lung, restrain astringent or styptic treatment for spontaneous sweating, improve a poor appetite, the effect of spleen benefiting and stimulating the appetite.Sugariness food has mitigation spasm, be in harmonious proportion nature and flavor, take nourishing food to build up one's health, promoting production of body fluid and nourishing the lung effect.
Secondly, the monounsaturated fatty acids of this autumn health-care edible oil and the ratio of polyunsaturated fatty acid and essential fatty acid ω-6 linoleic acid and ω-3 leukotrienes ratio meet modern nutriology health oil standard to the ratio of monounsaturated fatty acids and polyunsaturated fatty acid and essential fatty acid ω-6 linoleic acid and the linolenic proportion requirement of ω-3.Any natural oil and other ready-mixed oils are all difficult to reach this requirement.
3rd, this autumn health-care edible oil significantly can reduce the activity of MDA (MDA) content and monoamine oxidase (MAO), remarkable increase antioxidase (anti-ageing enzyme), the i.e. activity of superoxide dismutase (SOD), the resistance of aged animal model to dry windy weather in autumn can be strengthened, have significantly anti-ageing, promote body digest and assimilate, promote that body growth is grown, improve body nutritional status, improve the effects such as organism physiology biochemical indicator.
4th, it is adopt the squeezing of water content high fresh peanut to form that this autumn health-care eats one of oil composition peanut oil, remain the physiologically active ingredient in peanut to greatest extent, such as: VE, Bai Quinoa reed alcohol, cupreol, wheat germ phenol, phosphatide, choline etc., these compositions have enhancing immunity, delay senility, prevent and treat the effect such as bacillary dysentery and intestinal obstruction.
5th, the saturated fatty acid content ratio of this autumn health-care oil is lower, eater is allowed to take in a certain amount of animal food high containing saturated fatty acid, the preference of eater to animal food can be met, overcome other ready-mixed oils and health-care oil restriction eater ingests containing the shortcoming of the high animal food of saturated fatty acid.
6th, the present invention obtains autumn health-care edible oil by low-temperature fabrication, remains the biologically active of the active ingredient of four kinds of oil and four kinds of foods to greatest extent.Adopt supercritical carbon dioxide to add entrainer abstraction technique, the nonpolar active ingredient in lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf four kinds of foods and low pole active ingredient can be extracted.The extract of the hundred pears maizes containing nonpolar active ingredient and low pole active ingredient can be good at being dissolved in the ready-mixed oil of grape-kernel oil, linseed oil, peanut oil, rice bran oil composition.
Those of ordinary skill in the field are to be understood that: the discussion of above any embodiment is only exemplary, and not intended to be implies that the scope of the present disclosure (comprising claim) is limited to these examples; Under thinking of the present invention, also can combine between technical characteristic in above embodiment or different embodiment, step can realize with random order, and there are other changes many of different aspect of the present invention as above, for the sake of simplicity, they do not provide in details.Therefore, within the spirit and principles in the present invention all, any omission made, amendment, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.

Claims (7)

1. an autumn health-care edible oil, is characterized in that, comprises following composition and percentage by weight thereof:
The extract 1-3% of grape-kernel oil 5-25%, peanut oil 30-50%, rice bran oil 20-40%, linseed oil 5-25%, hundred pears maizes, the extract of described hundred pears maizes refer to lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf mixture extract.
2. autumn health-care edible oil according to claim 1, is characterized in that, described autumn health-care edible oil comprises following composition and percentage by weight thereof: grape-kernel oil 15%, peanut oil 38%, rice bran oil 30%, linseed oil 15%, hundred pears maize extract 2%.
3. autumn health-care edible oil according to claim 1, is characterized in that, described peanut oil adopts the squeezing of water content high fresh peanut to form.
4. autumn health-care edible oil according to claim 2, it is characterized in that, the monounsaturated fatty acids of described autumn health-care edible oil and the ratio of polyunsaturated fatty acid are 1:0.99, and in described polyunsaturated fatty acid, the ratio of ω-6 aliphatic acid and ω-3 type aliphatic acid is 0.82:0.18.
5. a preparation method for autumn health-care edible oil, is characterized in that, comprises the following steps:
Open vacuum oil refining cauldron, and start vavuum pump, in proportion the extract of grape-kernel oil, peanut oil, rice bran oil, linseed oil and hundred pears maizes is sucked in vacuum oil refining cauldron;
In setting pot, residual voltage is 60 ~ 80mmHg, temperature is 70 ~ 80 DEG C, turn on agitator, warming while stirring, high-visible when seeing in pot from mirror mouth, and when hanging mirror without water smoke wall built-up, continue stirring 20 ~ 40min, stop heating up, cold filtration, obtains autumn health-care edible oil.
6. the preparation method of autumn health-care edible oil according to claim 5, is characterized in that, described hundred pears maize extract preparation methods comprise the following steps:
(1) dry at drying lily, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf being placed in 50 ~ 60 DEG C and reach 5-6% to moisture, then pulverize, cross 40 ~ 60 mesh sieves;
(2) to take etc. the lily of quality, snow pear, radix polygonati officinalis and the tuber of dwarf lilyturf powder, mix, obtain hundred pears maize mixed powder samples;
(3) described hundred pears maize mixed powder samples are loaded supercritical CO 2in the extraction kettle of extraction equipment, arranging extracting pressure is 20-30MPa, CO 2flow is 28 ~ 35L/h, 75% ethanol flow velocity is 2.7 ~ 3.5ml/min, first at temperature 25-35 DEG C, extracts 1.0-1.5h, then at temperature 35-45 DEG C, continues extraction 1.5-2.0h;
(4) released single extraction liquid every 15 minutes from separating still during extraction, the organoleptic quality according to different phase extract is different and carry out Fractional Collections, obtains the extract of hundred pears maizes.
7. the preparation method of autumn health-care edible oil according to claim 6, it is characterized in that, in described step (4), abandon the extract in first two stage in 15 minutes and in last 15 minutes, the extract that all the other interludes are collected merges, and obtains the extract of hundred pears maizes.
CN201510655871.1A 2015-10-12 2015-10-12 A kind of autumn health-care edible oil and preparation method thereof Pending CN105211328A (en)

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CN107251957A (en) * 2017-07-20 2017-10-17 贵州黔香园油脂有限公司 A kind of tea oil with stomach-nourishing function
CN108308283A (en) * 2017-12-01 2018-07-24 广东金妮宝科技发展有限公司 A kind of peanut ready-mixed oil and preparation method thereof of linoleic acid and alpha-linolenic acid balanced proportion

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CN105901166A (en) * 2016-04-15 2016-08-31 安徽华安食品有限公司 Student healthcare edible oil having effects of invigorating the brain and improving eyesight and a preparing method thereof
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CN108308283A (en) * 2017-12-01 2018-07-24 广东金妮宝科技发展有限公司 A kind of peanut ready-mixed oil and preparation method thereof of linoleic acid and alpha-linolenic acid balanced proportion

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