CN105209523B - 用于利用糖基乳化剂从水性含氟聚合物分散体减少氟化乳化剂的方法 - Google Patents

用于利用糖基乳化剂从水性含氟聚合物分散体减少氟化乳化剂的方法 Download PDF

Info

Publication number
CN105209523B
CN105209523B CN201480027276.7A CN201480027276A CN105209523B CN 105209523 B CN105209523 B CN 105209523B CN 201480027276 A CN201480027276 A CN 201480027276A CN 105209523 B CN105209523 B CN 105209523B
Authority
CN
China
Prior art keywords
fluoropolymer
dispersion
sugar
emulsifier
fluorinated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201480027276.7A
Other languages
English (en)
Chinese (zh)
Other versions
CN105209523A (zh
Inventor
蒂尔曼·C·兹普利斯
阿尔内·塔勒
埃贡·奥伯迈尔
克劳斯·辛策
迈克尔·C·达达拉斯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
Original Assignee
3M Innovative Properties Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 3M Innovative Properties Co filed Critical 3M Innovative Properties Co
Publication of CN105209523A publication Critical patent/CN105209523A/zh
Application granted granted Critical
Publication of CN105209523B publication Critical patent/CN105209523B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D127/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers
    • C09D127/02—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
    • C09D127/12—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
    • C09D127/18—Homopolymers or copolymers of tetrafluoroethene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/14—Treatment of polymer emulsions
    • C08F6/16—Purification
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/14—Treatment of polymer emulsions
    • C08F6/20—Concentration
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • C08J3/05—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media from solid polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/06—Ethers; Acetals; Ketals; Ortho-esters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
    • C08K5/41—Compounds containing sulfur bound to oxygen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
    • C08K5/41—Compounds containing sulfur bound to oxygen
    • C08K5/42—Sulfonic acids; Derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/49—Phosphorus-containing compounds
    • C08K5/51—Phosphorus bound to oxygen
    • C08K5/52—Phosphorus bound to oxygen only
    • C08K5/521—Esters of phosphoric acids, e.g. of H3PO4
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D105/00—Coating compositions based on polysaccharides or on their derivatives, not provided for in groups C09D101/00 or C09D103/00
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/05—Alcohols; Metal alcoholates
    • C08K5/053—Polyhydroxylic alcohols
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/15—Heterocyclic compounds having oxygen in the ring
    • C08K5/151—Heterocyclic compounds having oxygen in the ring having one oxygen atom in the ring
    • C08K5/1545—Six-membered rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L27/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers
    • C08L27/02—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L27/12—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L71/00—Compositions of polyethers obtained by reactions forming an ether link in the main chain; Compositions of derivatives of such polymers
    • C08L71/02—Polyalkylene oxides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Paints Or Removers (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
CN201480027276.7A 2013-05-17 2014-05-16 用于利用糖基乳化剂从水性含氟聚合物分散体减少氟化乳化剂的方法 Active CN105209523B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP13168169.4 2013-05-17
EP13168169.4A EP2803690B1 (en) 2013-05-17 2013-05-17 Method for reducing fluorinated emulsifiers from aqueous fluoropolymer dispersions using sugar-based emulsifiers
PCT/US2014/038307 WO2014186647A1 (en) 2013-05-17 2014-05-16 Method for reducing fluorinated emulsifiers from aqueous fluoropolymer dispersions using sugar-based emulsifiers

Publications (2)

Publication Number Publication Date
CN105209523A CN105209523A (zh) 2015-12-30
CN105209523B true CN105209523B (zh) 2017-06-20

Family

ID=48482919

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201480027276.7A Active CN105209523B (zh) 2013-05-17 2014-05-16 用于利用糖基乳化剂从水性含氟聚合物分散体减少氟化乳化剂的方法

Country Status (6)

Country Link
US (1) US10093820B2 (enExample)
EP (1) EP2803690B1 (enExample)
JP (1) JP6392856B2 (enExample)
CN (1) CN105209523B (enExample)
RU (1) RU2629069C2 (enExample)
WO (1) WO2014186647A1 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2803691B1 (en) 2013-05-17 2016-04-20 3M Innovative Properties Company Fluoropolymer compositions containing a polyhydroxy surfactant
EP2868674B1 (en) * 2013-10-30 2019-11-20 3M Innovative Properties Company Peroxide curable fluoropolymers obtainable by polymerization using non-fluorinated polyhydroxy emulsifiers
EP2902424B1 (en) 2014-01-31 2020-04-08 3M Innovative Properties Company Tetrafluoroethene polymer dispersions stabilized with aliphatic non-ionic surfactants
EP3284762A1 (en) * 2016-08-17 2018-02-21 3M Innovative Properties Company Fluoropolymers comprising tetrafluoroethene and one or more perfluorinated alkyl allyl ether comonomers
CN109563206A (zh) 2016-08-17 2019-04-02 3M创新有限公司 四氟乙烯和全氟化烯丙基醚共聚物
EP3548557A4 (en) * 2016-12-01 2020-07-29 3M Innovative Properties Company ETHYLENE-TETRAFLUOROETHYLENE COPOLYMER DISPERSIONS AND ARTICLES COATED THEREOF
US11473004B2 (en) 2016-12-02 2022-10-18 University Of Wyoming Microemulsions and uses thereof to displace oil in heterogeneous porous media
EP3896052A1 (en) 2017-05-19 2021-10-20 3M Innovative Properties Co. Methods of making a polyfluorinated allyl ether and compounds relating to the methods
CN120025473A (zh) * 2019-04-26 2025-05-23 大金工业株式会社 氟聚合物水性分散液的制造方法和氟聚合物水性分散液
US12134669B2 (en) * 2021-07-12 2024-11-05 3M Innovative Properties Company Fluoroelastomers with perfluorinated thermoplastic fillers

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060074178A1 (en) * 2004-09-24 2006-04-06 Agc Chemicals Americas, Inc. Process for preparing aqueous fluoropolymer dispersions and the concentrated aqueous fluoropolymer dispersions produced by such process
CN101331105A (zh) * 2005-12-21 2008-12-24 3M创新有限公司 用于制备含氟聚合物的氟化表面活性剂
CN102549060A (zh) * 2009-07-31 2012-07-04 3M创新有限公司 含有多元醇化合物的含氟聚合物组合物及其制备方法

Family Cites Families (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3489595A (en) 1966-12-22 1970-01-13 Du Pont Coating compositions containing perfluorohalocarbon polymer,phosphoric acid and aluminum oxide,boron oxide or aluminum phosphate
CH616880A5 (en) 1977-03-23 1980-04-30 Crystalon Sa Process and means for the coating of surfaces for protecting against abrasion and corrosion
DE2949907A1 (de) 1979-12-12 1981-06-19 Hoechst Ag, 6230 Frankfurt Fluorpolymere mit schalenmodifizierten teilchen und verfahren zu deren herstellung
SE460274B (sv) 1988-02-18 1989-09-25 Perstorp Ab Foerfarande foer framstaellning av ett noetningsbestaendigt, dekorativt haerdplastlaminat
WO1994014904A1 (en) 1992-12-23 1994-07-07 E.I. Du Pont De Nemours And Company Coating composition for non-stick substrates
DE4340943A1 (de) 1993-12-01 1995-06-08 Hoechst Ag Wäßrige Dispersion von Fluorpolymerisaten, ihre Herstellung und Verwendung für Beschichtungen
DE19726802C1 (de) 1997-06-24 1998-06-10 Dyneon Gmbh Wäßrige Dispersion von Fluorpolymeren unterschiedlicher Teilchengröße
DE19824614A1 (de) 1998-06-02 1999-12-09 Dyneon Gmbh Verfahren zur Rückgewinnung von fluorierten Alkansäuren aus Abwässern
ITMI981520A1 (it) 1998-07-02 2000-01-02 Ausimont Spa Dispersioni di fluoropolimeri
DE19857111A1 (de) 1998-12-11 2000-06-15 Dyneon Gmbh Wäßrige Dispersionen von Fluorpolymeren
CN1094840C (zh) 1999-01-26 2002-11-27 克劳诺斯潘技术有限公司 制备地板的复合覆层的方法
US6291054B1 (en) 1999-02-19 2001-09-18 E. I. Du Pont De Nemours And Company Abrasion resistant coatings
US6761964B2 (en) 2001-04-02 2004-07-13 E. I. Du Pont De Nemours And Company Fluoropolymer non-stick coatings
US6770577B2 (en) 2001-10-29 2004-08-03 Gore Enterprise Holdings, Inc. Architectural fabric
MXPA04006460A (es) 2002-01-04 2004-10-04 Du Pont Dispersiones de fluoropolimeros concentradas.
AU2003268760A1 (en) * 2002-11-29 2004-06-23 Daikin Industries, Ltd. Method for purification of aqueous fluoropolymer emulsions, purified emulsions, and fluorine-containing finished articles
EP1452571B1 (en) 2003-02-28 2005-08-17 3M Innovative Properties Company Fluoropolymer dispersion containing no or little low molecular weight fluorinated surfactant
ATE529451T1 (de) 2003-11-17 2011-11-15 3M Innovative Properties Co Wässrige ptfe-dispersionen mit einem niedrigen gehalt an fluorierten emulgatoren
DE202004020048U1 (de) 2004-12-22 2005-03-17 Fitz Johannes Textile Verbunde aus Fluorpolymeren
ITMI20042554A1 (it) * 2004-12-30 2005-03-30 Solvay Solexis Spa Procedimento per la preparazione di dispersioni di fluoropolimeri
US7671111B2 (en) 2005-02-10 2010-03-02 E.I. Du Pont De Nemours And Company Monitoring column breakthrough in a process for removing fluorosurfactant from aqueous fluoropolymer dispersions
US7501356B2 (en) 2005-08-02 2009-03-10 Gore Enterprise Holdings, Inc. Architectural fabric
US8329813B2 (en) * 2009-05-08 2012-12-11 E I Du Pont De Nemours And Company Thermal reduction of fluoroether carboxylic acids or salts from fluoropolymer dispersions
EP2284200A1 (en) * 2009-07-31 2011-02-16 3M Innovative Properties Company Aqueous fluoropolymer dispersions containing a polyol comprising at least one long chain residue and method for producing them
EP2409998B1 (en) * 2010-07-23 2015-11-25 3M Innovative Properties Company High melting PTFE polymers suitable for melt-processing into shaped articles
EP2548897B1 (en) * 2011-07-22 2014-05-14 Arkema Inc. Fluoropolymer composition
EP2803691B1 (en) 2013-05-17 2016-04-20 3M Innovative Properties Company Fluoropolymer compositions containing a polyhydroxy surfactant

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060074178A1 (en) * 2004-09-24 2006-04-06 Agc Chemicals Americas, Inc. Process for preparing aqueous fluoropolymer dispersions and the concentrated aqueous fluoropolymer dispersions produced by such process
CN101331105A (zh) * 2005-12-21 2008-12-24 3M创新有限公司 用于制备含氟聚合物的氟化表面活性剂
CN102549060A (zh) * 2009-07-31 2012-07-04 3M创新有限公司 含有多元醇化合物的含氟聚合物组合物及其制备方法

Also Published As

Publication number Publication date
RU2629069C2 (ru) 2017-08-24
EP2803690A1 (en) 2014-11-19
EP2803690B1 (en) 2016-12-14
US10093820B2 (en) 2018-10-09
JP6392856B2 (ja) 2018-09-19
RU2015148830A (ru) 2017-06-22
WO2014186647A1 (en) 2014-11-20
US20160122572A1 (en) 2016-05-05
JP2016518510A (ja) 2016-06-23
CN105209523A (zh) 2015-12-30

Similar Documents

Publication Publication Date Title
CN105209523B (zh) 用于利用糖基乳化剂从水性含氟聚合物分散体减少氟化乳化剂的方法
JP7727207B2 (ja) ポリテトラフルオロエチレン水性分散液
JP5937870B2 (ja) 非イオン性界面活性剤組成物、及び、フルオロポリマー水性分散液
EP2902424B1 (en) Tetrafluoroethene polymer dispersions stabilized with aliphatic non-ionic surfactants
CN100393786C (zh) 不含或含少量低分子量氟化表面活性剂的含氟聚合物分散体
EP3385326B1 (en) Aqueous polytetrafluoroethylene dispersion
EP2459641A2 (en) Fluoropolymer compositions containing a polyol compound and methods of making them
EP4212556A1 (en) Aqueous modified polytetrafluoroethylene dispersion
US9969848B2 (en) Fluoropolymer compositions containing a polyhydroxy surfactant
EP3103836A1 (en) Fluoropolymer with improved transparency

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant