CN105181608B - Rapid pesticide residue detection device and its detection method - Google Patents

Rapid pesticide residue detection device and its detection method Download PDF

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Publication number
CN105181608B
CN105181608B CN201510571933.0A CN201510571933A CN105181608B CN 105181608 B CN105181608 B CN 105181608B CN 201510571933 A CN201510571933 A CN 201510571933A CN 105181608 B CN105181608 B CN 105181608B
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China
Prior art keywords
screen holder
housing
light
optical filtering
reflective mirror
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Expired - Fee Related
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CN201510571933.0A
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Chinese (zh)
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CN105181608A (en
Inventor
张会妮
吴春芳
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Individual
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Abstract

The invention discloses a kind of Rapid pesticide residue detection device, including housing, screen holder slot is located at housing upper face, and the housing is provided with protecgulum and bonnet, it is characterised in that:Covered after described and circuit board is installed, ultraviolet high-pressure mercury-vapor lamp is arranged in front of control panel, and screen holder is inserted through screen holder slot and is laid in front of ultraviolet high-pressure mercury-vapor lamp, and optical filtering one and optical filtering two are provided with the screen holder;The present invention is simple to operate, quickly the residues of pesticides of food surface can be detected, detection speed is fast, compact, is easy to carry;Different optical filterings can be changed by the different screen holder of quick-replaceable simultaneously, can so detect different types of residues of pesticides, it is versatile, it is adapted to promote the use of.

Description

Rapid pesticide residue detection device and its detection method
Technical field
The present invention relates to a kind of pesticide detection device, and in particular to a kind of Fast Determination of Pesticide Residue dress on food Put and its detection method, belong to technical field of food detection.
Background technology
With the improvement of people ' s living standards, in recent years, people also increasingly pay attention to food Pesticide Residue.For This, many countries have formulated MRL (MRLs) of the agricultural chemicals in food, and the inlet and outlet of crops require that agricultural chemicals is residual Stay the MRLs of various countries to be less than.With China joined WTO, the inlet and outlet of crops will constantly expand, the inspection of food residues of pesticides Mark standard integrates with international standard and just becomes more and more important, thus analyze detect food agricultural chemicals remain important meaning Justice.
The pollution by pesticides of food surface is controlled and first have to detect the distribution kind of agricultural chemicals and dense with administering The information such as degree.It is that a needs are for a long time and huge that pollution by pesticides, which is detected, classified using conventional chemical analysis method The work of manpower and materials.And detected with laser Induced Fluorescence Technology, its sensitivity is higher, it is simple and easy, reality can be carried out When detection on the spot.As Patent publication No CN201589749U discloses a kind of embedded instrument for detecting pesticide residue through, its feature exists In, including persticide residue is transformed into telecommunications by photodetector system, data collecting system and touch-screen, photodetector system Number, it is amplified to send data collecting system that analog-signal transitions are detected into data signal, data signal transmission touch-screen As a result display and testing process control, the photodetector system by laser diode, optical filtering, cuvette, silicon photocell, put Big circuit composition, the data collecting system are made up of single-chip microcomputer, data acquisition chip and communication chip, and the touch-screen is selected TPC7062KX, communicated with data collecting system by serial ports RS232, detected in the photodetector system through silicon photocell Signal be sent to data acquisition chip;The data of data acquisition chip collection are transmitted after single-chip microcomputer is handled by communication chip To touch-screen, single-chip microcomputer receives the data command of touch-screen transmission simultaneously.
And for example Patent publication No CN103454435A discloses a kind of pesticide residue detection device, especially a kind of portable Dithiocarbamate pesticide residue detector.The portable dithiocarbamate pesticide residue detector includes Airway tube, charger, reactor, absorber and heater, reactor its to fill detected sample and stannous chloride solution Container, charger by be connected with reactor catheter import distilled water solution in the reactor is diluted, airway tube passes through It is connected with reactor and imports nitrogen, simultaneous reactions device bottom is by heating devices heat, aminodithioformic acid in detected sample Ester and stannous chloride solution generated reactive gas, and the nitrogen being passed through is sent in the nitrite ion in absorber by gas is produced The online colour developing of row.After appeal technical scheme, the utility model has that rational in infrastructure, simple to operate, detection speed is fast, cost Relatively low, operation side reaction is few and the advantages that detection efficiency is high.
At present, for the residues of pesticides for food surface, it is necessary to carry out extraction inspection to food, such speed is slow, as a result etc. Treat that the time is grown, it is impossible to meet the needs of high-volume quick detection.
The content of the invention
The problem of existing instant invention overcomes prior art, it is proposed that a kind of Rapid pesticide residue detection device and its detection Method, the device can be detected quickly to the residues of pesticides of food surface, and detection speed is fast, compact, while can lead to The different screen holder of quick-replaceable is crossed to change different optical filterings, can so detect different types of residues of pesticides, is led to It is strong with property.
The concrete technical scheme of the present invention is as follows:Rapid pesticide residue detection device, including housing, screen holder slot are set In housing upper face, the housing is provided with protecgulum and bonnet, it is characterised in that:Covered after described and circuit board is installed, ultraviolet High-pressure mercury-vapor lamp is arranged in front of circuit board, and screen holder is inserted through before screen holder slot is laid in ultraviolet high-pressure mercury-vapor lamp It is square, optical filtering one and optical filtering two are installed on the screen holder;The front of optical filtering one is provided with photomask one, described Photomask one is connected with fibre bundle one, and the front of fibre bundle one is provided with concavees lens one, before reflective mirror one is arranged on concavees lens one Side;The optical filtering two is connected with fibre bundle two, and fibre bundle two is connected with photomask two, before reflective mirror two is arranged on photomask two It is square, convex lens are installed on the protecgulum;Shoulder belt is connected with by lock on the housing, it is described to be locked on housing.
Preferentially, the screen holder bottom is provided with sleeve, and spring two is arranged on below sleeve;The screen holder side Side is provided with slide card structure, and case inside is provided with the notch for the insertion of slide card structure, and thimble is arranged on slide card structure side, the top Spring one is cased with pin, button is installed on the spring one, the button is placed in hull outside wall.The screen holder uses Mold injection forms.
Preferentially, it is additionally provided with control interface on the housing.
Preferentially, handle is installed above the housing, lithium battery is installed in the handle, dismounting lid is located at handle bottom Hold, be also equipped with switching on the handle.
In addition, present invention also offers a kind of method of fast detecting pesticide residue, it is characterised in that including following step Suddenly:
1) determine that the species that detect agricultural chemicals chooses different optical filtering one and optical filtering two first, lived by screen holder It is dynamic to load in screen holder slot;
2) it is powered by switching opening device, the light source that ultraviolet high-pressure mercury-vapor lamp is sent was carried out by optical filtering one Filter, then light source is converted into optical signal feeding fibre bundle one by photomask one and is transferred on concavees lens one;
3) divergence of beam that concavees lens one will transmit, its light enter reflective mirror one, and a part of light is through reflective Mirror one gathers light the food surface to be detected into convex lens, and another part is reflexed on reflective mirror two;
4) returned by the principle of reversibility of light, light along former road above reflective mirror one, carry out reflexing to reflective mirror again On two;
5) light source is converted into optical signal feeding fibre bundle two and is transferred on optical filtering two by photomask two, and optical filtering two is right The light passed back wavelength is analyzed into spectroanalysis instrument after filtering screening;
6) result is shown in control interface after spectroanalysis instrument analysis, detection is completed.
Beneficial effects of the present invention:The present invention is simple to operate, and quickly the residues of pesticides of food surface can be detected, Detection speed is fast, compact, is easy to carry;Different optical filterings can be changed by the different screen holder of quick-replaceable simultaneously Mirror, different types of residues of pesticides can be so detected, it is versatile, it is adapted to promote the use of.
Brief description of the drawings
Fig. 1 is the structural representation of Rapid pesticide residue detection device of the present invention;
Fig. 2 is the cut-away view of Rapid pesticide residue detection device of the present invention;
Fig. 3 is the structural representation of screen holder.
Embodiment
As Figure 1-3, a kind of Rapid pesticide residue detection device of the present invention, including housing 51, screen holder slot 2 are set On housing 51, control interface 3 is additionally provided with housing 51, control interface 3 lies in the top of housing 51, and it is provided with regulation and control above Button.The top of housing 51 is provided with handle 15, and lithium battery 14 is provided with the handle 15, and dismounting lid 8 is located at the bottom of handle 15, Switch 6 is also equipped with the handle 15, switch 6 is reset switch;Shoulder belt 31 is connected with by lock 32 on the housing 51, The lock 32 is locked on housing 51, when usually carrying, can be carried on the back instrument piggyback by shoulder belt 31.Housing 51 is provided with Protecgulum 4 and bonnet 1, the protecgulum 4 is provided with detachable protective set 33, circuit board 9 is provided with the bonnet 1 above, ultraviolet Line high-pressure mercury-vapor lamp 10 is arranged on the front of circuit board 9, and ultraviolet high-pressure mercury-vapor lamp 10 selects intensive ultraviolet high-pressure mercury-vapor lamp.Filter Mirror holder 12 is inserted through screen holder slot 2 and is laid in the front of ultraviolet high-pressure mercury-vapor lamp 10, and filter is provided with the screen holder 12 Light microscopic 1 and optical filtering 2 24, optical filtering 1 and optical filtering 2 24 are detachable installation.The front of optical filtering 1 is provided with Photomask 1, the photomask 1 are connected with fibre bundle 1, and the front of fibre bundle 1 is provided with concavees lens 1, instead Light microscopic 1 is arranged on the front of concavees lens 1;The optical filtering 2 24 is connected with fibre bundle 2 22, and fibre bundle 2 22 is connected with Photomask 2 21, reflective mirror 2 20 are arranged on the front of photomask 2 21, convex lens 19 are provided with the protecgulum 4.Fibre bundle one 16 and fibre bundle 2 22 be fixed on stock, concavees lens 1 and photomask 2 21 are mounted side by side on mirror holder two, reflective mirror one 18 and reflective mirror 2 20 side by side and tilt installation, meet the reflection demand of light.
The bottom of screen holder 12 is provided with sleeve 1205, and spring 2 1206 is arranged on the lower section of sleeve 1205;The optical filtering The side of frame 12 is provided with slide card structure 1204, and the inner side of housing 51 is provided with the notch being embedded in for slide card structure 1204, and thimble 1201 is installed Spring 1 is cased with the side of slide card structure 1204, the thimble 1201, button 7 is installed on the spring 1, The button 7 is placed in the lateral wall of housing 51.The screen holder 12 is formed using mold injection.The present invention in order to adapt to detection not Same agricultural chemicals, screen holder 12 are movably arranged on the inside of housing 51, optical filtering intraoral by the card entry slot of slide card structure 1204 Frame 12 is fixed.When needing to take out, make thimble 1201 to medial motion that slide card structure 1204 is inside by pressing button 7 Extruding, while resilience when slide card structure 1204 loses constraint mechanism of the spring 2 1206 of the bottom of screen holder 12, will be filtered Light microscopic 1 and optical filtering 2 24 are changed in the ejection of light microscopic frame 12.
In addition, being based on said apparatus, present invention also offers a kind of method of fast detecting pesticide residue, its feature exists In comprising the following steps:
1) determine that the species that detect agricultural chemicals chooses different optical filtering 1 and optical filtering 2 24 first, pass through optical filtering The activity of frame 12 loads in screen holder slot 2, and the effect of optical filtering 1 and optical filtering 2 24 is to filter the veiling glare in light Fall;
2) it is powered by switching 6 opening devices, the light source that ultraviolet high-pressure mercury-vapor lamp 10 is sent is entered by optical filtering 1 Row filtering, then light source is converted into optical signal feeding fibre bundle 1 by photomask 1 and is transferred to concavees lens 1 On, the effect of concavees lens 1 is to close line to be dissipated;
3) divergence of beam that concavees lens 1 transmit fibre bundle 1, its light enter reflective mirror 1, one Light splitter gathers light the food surface to be detected through reflective mirror 1 into convex lens 19, and another part reflexes to instead On light microscopic 2 20;
4) principle of reversibility of the light on food surface by light is impinged upon, light is returned on reflective mirror 1 along former road Face, carry out reflexing on reflective mirror 2 20 again;
5) light source is converted into optical signal feeding fibre bundle 2 22 and is transferred on optical filtering 2 24 by photomask 2 21, filters The light that 2 24 pairs of mirror is passed back wavelength is analyzed into spectroanalysis instrument after filtering screening;
6) result is shown in control interface 3 after spectroanalysis instrument analysis, detection is completed.
In addition to the implementation, the present invention can also have other embodiment.It is all to use equivalent substitution or equivalent transformation shape Into technical scheme, all fall within the protection domains of application claims.

Claims (5)

1. Rapid pesticide residue detection device, including housing (51), screen holder slot (2) is located at housing (51) above, described Housing (51) is provided with protecgulum (4) and bonnet (1), it is characterised in that:Circuit board (9), ultraviolet are installed on the bonnet (1) High-pressure mercury-vapor lamp (10) is arranged in front of circuit board (9), and screen holder (12) is inserted through screen holder slot (2) and is laid in ultraviolet In front of high-pressure mercury-vapor lamp (10), optical filtering one (23) and optical filtering two (24) are installed on the screen holder (12);The filter Photomask one (13) is installed in front of light microscopic one (23), the photomask one (13) is connected with fibre bundle one (16), the optical fiber Concavees lens one (17) are provided with front of beam one (16), reflective mirror one (18) is arranged in front of concavees lens one (17);The optical filtering two (24) fibre bundle two (22) is connected with, fibre bundle two (22) is connected with photomask two (21), and reflective mirror two (20) is arranged on light harvesting Cover in front of two (21), convex lens (19) are installed on the protecgulum (4);On the housing (51) shoulder is connected with by latching (32) Band (31), the lock (32) are locked on housing (51);Screen holder (12) bottom is provided with sleeve (1205), spring Two (1206) are arranged on below sleeve (1205);Screen holder (12) side is provided with slide card structure (1204), housing (51) Inner side is provided with is arranged on slide card structure (1204) side, the top for the embedded notch of slide card structure (1204), thimble (1201) Spring one (1202) is cased with pin (1201), button (7) is installed on the spring one (1202), the button (7) is placed in shell Body (51) lateral wall.
2. Rapid pesticide residue detection device according to claim 1, it is characterised in that:The screen holder (12) uses Mold injection forms.
3. according to the Rapid pesticide residue detection device described in any one in claim 1-2, it is characterised in that:The housing (51) control interface (3) is additionally provided with.
4. Rapid pesticide residue detection device according to claim 1, it is characterised in that:Installed above the housing (51) There is handle (15), lithium battery (14) is installed in the handle (15), dismounting lid (8) is located at handle (15) bottom, the handle (15) it is also equipped with switching (6) on.
5. the method for the device fast detecting pesticide residue described in a kind of usage right requirement 1, it is characterised in that including following step Suddenly:1) determine that the species that detect agricultural chemicals chooses different optical filtering one (23) and optical filtering two (24) first, pass through optical filtering Frame (12) activity loads in screen holder slot (2);
2) it is powered by switching (6) opening device, the light source that ultraviolet high-pressure mercury-vapor lamp (10) is sent passes through optical filtering one (23) Filtered, then light source is converted into optical signal feeding fibre bundle one (16) by photomask one (13) and is transferred to concavees lens On one (17);
3) divergence of beam that concavees lens one (17) will transmit, its light enter reflective mirror one (18), and a part of light passes through Reflective mirror one (18) gathers light the food surface to be detected into convex lens (19), and another part reflexes to reflective mirror two (20) on;
4) reflective mirror one (18) is returned above along former road by the principle of reversibility of light, light, carries out reflexing to reflective mirror again On two (20);
5) light source is converted into optical signal feeding fibre bundle two (22) and is transferred on optical filtering two (24) by photomask two (21), filters Light microscopic two (24) carries out analyzing wavelength into spectroanalysis instrument after filtering screening to the light passed back;
6) result is shown in control interface (3) after spectroanalysis instrument analysis, detection is completed.
CN201510571933.0A 2015-09-10 2015-09-10 Rapid pesticide residue detection device and its detection method Expired - Fee Related CN105181608B (en)

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106770084A (en) * 2016-11-23 2017-05-31 百奥森(江苏)食品安全科技有限公司 A kind of vegetable pesticide residue detection means
CN108489936B (en) * 2018-04-08 2024-03-19 吉林省富生医疗器械有限公司 Household cystatin C concentration rapid tester and testing method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2593187Y (en) * 2002-12-19 2003-12-17 上海精密科学仪器有限公司 Multi-channel spectral apparatus of pesticide residue rapid-measuring instrument
CN102818225A (en) * 2011-06-07 2012-12-12 海洋王照明科技股份有限公司 Quick changing device of optical filter of dodging lamp
CN103499528A (en) * 2013-09-30 2014-01-08 重庆大学 Quick spectrum detection system for pesticide residues

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7400405B2 (en) * 2005-02-18 2008-07-15 Bio-Chek Llc Pesticide detector and method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2593187Y (en) * 2002-12-19 2003-12-17 上海精密科学仪器有限公司 Multi-channel spectral apparatus of pesticide residue rapid-measuring instrument
CN102818225A (en) * 2011-06-07 2012-12-12 海洋王照明科技股份有限公司 Quick changing device of optical filter of dodging lamp
CN103499528A (en) * 2013-09-30 2014-01-08 重庆大学 Quick spectrum detection system for pesticide residues

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