CN105176692A - Enzymolysis method for preparing Laifeng crossostephium essential oil through assistance of microwaves - Google Patents
Enzymolysis method for preparing Laifeng crossostephium essential oil through assistance of microwaves Download PDFInfo
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- CN105176692A CN105176692A CN201510702697.1A CN201510702697A CN105176692A CN 105176692 A CN105176692 A CN 105176692A CN 201510702697 A CN201510702697 A CN 201510702697A CN 105176692 A CN105176692 A CN 105176692A
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Abstract
The invention relates to an enzymolysis method for preparing Laifeng crossostephium essential oil through assistance of microwaves. The enzymolysis method comprises the first step of enzymolysis, the second step of microwave extraction, the third step of recycling, the fourth step of standing and the fifth step of separation. According to the enzymolysis method for preparing the Laifeng crossostephium essential oil through assistance of the microwaves, the technological condition requirement is low, and the technology is reasonable; the extraction technology is exclusive and suitable for industrial production conditions, the extraction efficiency is high, meanwhile, equipment is simple, the manufacturing cost is low, and application and popularization are easy. The prepared Laifeng crossostephium essential oil is oily, has the aroma and the taste of Laifeng crossostephium and is used for preparing various foods, various fragrances, various cigarettes, perfume, cosmetics, daily chemicals, health-care produces and medicine.
Description
Technical field
The present invention relates to the enzyme solution that a kind of microwave-assisted prepares Laifeng County's aromaticin oil.
Background technology
Dendranthema indicum is feverfew Dendranthema indicum Dendranthemaindicume (L1) DesMonl1var1aromaticumQ1H1L1iuet1S1E1Zhang, the dry capitulum of var1nov1, originate in Shennongjia in Hubei, be distributed in the open field of height above sea level more than 2000 meters on the sunny side, it is a new variant of composite family Chrysanthemum, complete stool has special strong fragrance, Dendranthema indicum sample picks up from Shennongjia, Hubei Province in October, 2004, feverfew Dendranthema indicum Dendranthemaindicum (L1) DesMonl1var1aromaticumQ1H1LiuetS1E1Zhang is accredited as by medicine academy, HuNan college of traditional Chinese medicine identification and assessment of Chinese medicines teaching and research room professor Chen Keli, the dry capitulum of var1nov1.
The diseases such as Dendranthema indicum is used for anti-curing cold by Mountain Area of Western Hubei Province, have a headache, bacillary dysentery, enteritis, constipation, coronary heart disease and hypertension.Its essential oil or medicinal extract are used for the aspects such as medicine, beverage, cigarette and makeup.Lu Jinqing, He Jun, kingdom are bright etc., and people once studied the chemical composition of Dendranthema indicum dried flower essential oil, therefrom identified multiple terpenoid; Gong Fujun etc. are the isolation identification compounds such as robinin, palmitinic acid, lauric acid, daucosterol, robinin 2 rhamnoglucoside, luteolin 272O2 β 2 glucoside, luteolin from Dendranthema indicum.
The fragrant chrysanthemum of Dragon Lord, as a kind of colored veriety with Mountain Area of Western Hubei Province characteristic, is not generally planted, the few places that its place of production mainly concentrates on Shennongjia and bestows favour at home.Bestowing favour, is the important planting area of the fragrant chrysanthemum of Dragon Lord in history, has plantation tradition for many years, has establishing in large scale especially in the east of Sichuan mountain area, and the fragrant chrysanthemum of Dragon Lord has become now local main characteristic and spent one of veriety.
Teng Sheng spices company of Laifeng County planted experimentally from 2012 plants the fragrant chrysanthemum of Dragon Lord, utilize the petal budding technology of its uniqueness, the long technology of fertilizer speed, the planting technologies such as interval mastery soil, successfully plant successfully fragrant chrysanthemum in height above sea level 600-1000 rice low altitude area, it is strong that its fragrant chrysanthemum is bright-colored, fragrance is fresh and sweet, and chrysanthemum head circle is evenly large, output is high, and pharmaceutical use is high.The fragrant chrysanthemum of Teng Sheng spices company plantation is from odour characteristics, mouthfeel, using value, and fragrant chrysanthemum has certain difference with Dragon Lord, becomes and has self-character---and " the fragrant chrysanthemum in Laifeng County ".
" the fragrant chrysanthemum in Laifeng County " that this technology is conceived to the plantation of area, Laifeng County is raw material, volatile for " the fragrant chrysanthemum in Laifeng County " unique fresh and sweet note composition, the features such as easy change, microwave radiation, the modern non-heat-flash technique means such as cellulase treatment, produce from the gradient of " the fragrant chrysanthemum in Laifeng County " full flavor compound and carry out " the fragrant chrysanthemum in Laifeng County " high-valued and industrialization key technology research with finger print identification two aspect systems of full flavor compound in a deep going way, exploitation high added value " the fragrant chrysanthemum in Laifeng County " characteristic perfumed product, and realize industrialization production and apply, eat raw and the transformation of simple processed goods to high added value intensely processed products from simple to realize " the fragrant chrysanthemum in Laifeng County ", improve " the fragrant chrysanthemum in Laifeng County " commodity value, drive " the fragrant chrysanthemum in Laifeng County " industrial chain extension and increase plantation family income, reduce field stockpiling of unsold product, increase agricultural performance, promote the higher value application level of local characteristic agricultural byproducts resource.Meanwhile, by the intensive processing product of " the fragrant chrysanthemum in Laifeng County ", obvious for this provincial characteristics distinguishing products are pushed to the whole nation, pushed the whole world to.
Summary of the invention
The technical problem to be solved in the present invention is to provide the enzyme solution that a kind of microwave-assisted prepares Laifeng County's aromaticin oil.
Technical scheme of the present invention is: a kind of microwave-assisted prepares the enzyme solution of Laifeng County's aromaticin oil, it is characterized in that comprising the following steps:
A. enzymolysis
In extractor, add the fragrant chrysanthemum in Laifeng County, water, cellulase, zytase, B-dextranase and polygalacturonase; Water add-on is 1-10 times of the fragrant chrysanthemum weight in Laifeng County, and auxiliary material add-on is the per-cent of the fragrant chrysanthemum weight in Laifeng County: cellulase 0.1-1%, zytase 0.1-1%, B-dextranase 0.3-3%, polygalacturonase 0.3-3%; Controlled enzymatic hydrolysis temperature 35-55 degree, starts stirring, enzymolysis time: 1-5 hour;
B. microwave extraction
Control extractor temperature 50-95 degree, microwave power is under 100-500kw condition, extracts 1-3 hour;
C. reclaim
Extractor is extracted material and is warmed up to 100 degree, water vapour cooling is reclaimed;
D. leave standstill
The cooling fluid reclaimed, leaves standstill 3-12 hour;
E. be separated
Aqueous portion is discharged, gets oil phase part, obtain Laifeng County's aromaticin oil.
A kind of microwave-assisted of the present invention prepares the enzyme solution of Laifeng County's aromaticin oil, it is characterized in that comprising the following steps:
A. enzymolysis
In extractor, add the fragrant chrysanthemum in Laifeng County, water, cellulase, zytase, B-dextranase and polygalacturonase; Water add-on is 1-10 times of the fragrant chrysanthemum weight in Laifeng County, and auxiliary material add-on is the per-cent of the fragrant chrysanthemum weight in Laifeng County: cellulase 0.1-1%, zytase 0.1-1%, B-dextranase 0.3-3%, polygalacturonase 0.3-3%; Controlled enzymatic hydrolysis temperature 35-55 degree, starts stirring, enzymolysis time: 1-5 hour;
B. microwave extraction
Control extractor temperature 50-95 degree, microwave power is under 100-500kw condition, extracts 1-3 hour; Microwave extraction system used: adopt the maet-6 microwave extraction system that Shanghai Jing Qiao drying plant factory produces;
C. reclaim
Extractor is extracted material and is warmed up to 100 degree, water vapour cooling is reclaimed;
D. leave standstill
The cooling fluid reclaimed, leaves standstill 3-12 hour;
E. be separated
Aqueous portion is discharged, gets oil phase part, obtain Laifeng County's aromaticin oil.
A kind of microwave-assisted of the present invention prepares the enzyme solution of Laifeng County's aromaticin oil, the fragrant chrysanthemum main chemical compositions in Laifeng County used, research shows, in " the fragrant chrysanthemum in Laifeng County ", main component has luteolin, chlorogenic acid, linarin, amino acid, polysaccharide, flavonoid, chlorogenic acid, the compositions such as volatile essential oil, measure the volatile component of " the fragrant chrysanthemum in Laifeng County ", and the general flavone content of more different chrysanthemum and volatile oil yield, result shows, in " Laifeng County fragrant chrysanthemum " general flavone content and volatile oil content all higher, cis-oxidation phantol (21.84%) is had in volatile oil, spathulenol (4.25%), her Elemenum (8.23%), her eudesmol (13.90%), 2 are had in Static Headspace analysis, 3. butyleneglycol (5.69%), only. phellandrene (31.05%), Paracymene (38.08%), three. phantol (7.63%), linalool oxide (29.38), the basal component of dry " the fragrant chrysanthemum in Laifeng County " is mainly: dry-matter 80% ~ 90%, protein 1% ~ 1.8%, carbohydrate 6.3% ~ 10.8%, robust fibre 0.6% ~ 1.7%, fat 0.1%, calcium 0.2 ~ 0.5%, the mineral element such as iron, potassium, manganese, zinc of phosphorus 0.05% and abundant vitamin A, B1, B2, C and trace." the fragrant chrysanthemum in Laifeng County " is about containing the ethereal oil of 0.015% (dry product content is about 0.15%), mainly aromatic compound, although content is little, but these compounds constitute its distinctive local flavor and physiological function composition, be at present to one of focus that " the fragrant chrysanthemum in Laifeng County " physiologically active ingredient is studied.Main function composition in " the fragrant chrysanthemum in Laifeng County " specifically can be divided into following a few class:
Anti-oxidant activity.Luteolin and chlorogenic acid are the main components in " the fragrant chrysanthemum in Laifeng County ", and resistance of oxidation is also stronger; Flavonoids, is mainly present in leaf, stem and crust, with flavonoid, flavonols and anthocyan for representative; Phenylpropanoid glycoside, is mainly present in leaf, stem, comprises monomer and the derivatives thereof such as coffic acid, forulic acid, sinapinic acid; Steroidal compounds and nitrogenous compound.
" the fragrant chrysanthemum in Laifeng County " has its special Physiological Properties, " Laifeng County fragrant chrysanthemum " and " the fragrant chrysanthemum in Laifeng County " deep processed product has effect of bactericidal antiphlogistic, flat liver improving eyesight, loose wind step-down, the diseases such as fragrant chrysanthemum is used for anti-ly curing cold by Mountain Area of Western Hubei Province, have a headache, bacillary dysentery, enteritis, constipation, coronary heart disease and hypertension.
A kind of microwave-assisted of the present invention prepares the enzyme solution of Laifeng County's aromaticin oil, and processing condition require low, rational technology; Extraction process is created, and be applicable to commercial production conditions, extraction efficiency is high, and equipment is simple simultaneously, and low cost of manufacture, applies easy.
Laifeng County's aromaticin oil prepared by the present invention, in oily, possesses fragrance and the mouthfeel of the fragrant chrysanthemum in Laifeng County, for the preparation of various food, and various essence, various cigarette, perfume, makeup, cosmetics of everyday use, healthcare products and medicine.
Embodiment
Below in conjunction with embodiment, the present invention is further described.
Embodiment 1: a kind of microwave-assisted of the present invention prepares the enzyme solution of Laifeng County's aromaticin oil, comprises the following steps:
A. enzymolysis
In extractor, add the fragrant chrysanthemum in Laifeng County, water, cellulase, zytase, B-dextranase and polygalacturonase; Water add-on is 1 times of the fragrant chrysanthemum weight in Laifeng County, and auxiliary material add-on is the per-cent of the fragrant chrysanthemum weight in Laifeng County: cellulase 0.1%, zytase 0.1%, B-dextranase 0.3%, polygalacturonase 0.3%; Controlled enzymatic hydrolysis temperature 35 degree, starts stirring, enzymolysis time: 1 hour;
B. microwave extraction
Control extractor temperature 50 degree, microwave power is under 100kw condition, extracts 1 hour; Microwave extraction system used: adopt the maet-6 microwave extraction system that Shanghai Jing Qiao drying plant factory produces;
C. reclaim
Extractor is extracted material and is warmed up to 100 degree, water vapour cooling is reclaimed;
D. leave standstill
The cooling fluid reclaimed, leaves standstill 3 hours;
E. be separated
Aqueous portion is discharged, gets oil phase part, obtain Laifeng County's aromaticin oil.
Embodiment 2: a kind of microwave-assisted of the present invention prepares the enzyme solution of Laifeng County's aromaticin oil, comprises the following steps:
A. enzymolysis
In extractor, add the fragrant chrysanthemum in Laifeng County, water, cellulase, zytase, B-dextranase and polygalacturonase; Water add-on is 10 times of the fragrant chrysanthemum weight in Laifeng County, and auxiliary material add-on is the per-cent of the fragrant chrysanthemum weight in Laifeng County: cellulase 1%, zytase 1%, B-dextranase 3%, polygalacturonase 3%; Controlled enzymatic hydrolysis temperature 55 degree, starts stirring, enzymolysis time: 5 hours;
B. microwave extraction
Control extractor temperature 95 degree, microwave power is under 500kw condition, extracts 3 hours; Microwave extraction system used: adopt the maet-6 microwave extraction system that Shanghai Jing Qiao drying plant factory produces;
C. reclaim
Extractor is extracted material and is warmed up to 100 degree, water vapour cooling is reclaimed;
D. leave standstill
The cooling fluid reclaimed, leaves standstill 12 hours;
E. be separated
Aqueous portion is discharged, gets oil phase part, obtain Laifeng County's aromaticin oil.
Embodiment 3: a kind of microwave-assisted of the present invention prepares the enzyme solution of Laifeng County's aromaticin oil, comprises the following steps:
A. enzymolysis
In extractor, add the fragrant chrysanthemum in Laifeng County, water, cellulase, zytase, B-dextranase and polygalacturonase; Water add-on is 5 times of the fragrant chrysanthemum weight in Laifeng County, and auxiliary material add-on is the per-cent of the fragrant chrysanthemum weight in Laifeng County: cellulase 0.5%, zytase 0.5%, B-dextranase 1.5%, polygalacturonase 1.5%; Controlled enzymatic hydrolysis temperature 45 degree, starts stirring, enzymolysis time: 3 hours;
B. microwave extraction
Control extractor temperature 75 degree, microwave power is under 250kw condition, extracts 1.5 hours; Microwave extraction system used: adopt the maet-6 microwave extraction system that Shanghai Jing Qiao drying plant factory produces;
C. reclaim
Extractor is extracted material and is warmed up to 100 degree, water vapour cooling is reclaimed;
D. leave standstill
The cooling fluid reclaimed, leaves standstill 7.5 hours;
E. be separated
Aqueous portion is discharged, gets oil phase part, obtain Laifeng County's aromaticin oil.
Embodiment 4: a kind of microwave-assisted of the present invention prepares the enzyme solution of Laifeng County's aromaticin oil, comprises the following steps:
A. enzymolysis
In extractor, add the fragrant chrysanthemum in Laifeng County, water, cellulase, zytase, B-dextranase and polygalacturonase; Water add-on is 8 times of the fragrant chrysanthemum weight in Laifeng County, and auxiliary material add-on is the per-cent of the fragrant chrysanthemum weight in Laifeng County: cellulase 0.8%, zytase 0.8%, B-dextranase 2.5%, polygalacturonase 2.5%; Controlled enzymatic hydrolysis temperature 50 degree, starts stirring, enzymolysis time: 4 hours;
B. microwave extraction
Control extractor temperature 80 degree, microwave power is under 400kw condition, extracts 2 hours; Microwave extraction system used: adopt the maet-6 microwave extraction system that Shanghai Jing Qiao drying plant factory produces;
C. reclaim
Extractor is extracted material and is warmed up to 100 degree, water vapour cooling is reclaimed;
D. leave standstill
The cooling fluid reclaimed, leaves standstill 10 hours;
E. be separated
Aqueous portion is discharged, gets oil phase part, obtain Laifeng County's aromaticin oil.
Embodiment 5: a kind of microwave-assisted of the present invention prepares the enzyme solution of Laifeng County's aromaticin oil, comprises the following steps:
A. enzymolysis
In extractor, add the fragrant chrysanthemum in Laifeng County, water, cellulase, zytase, B-dextranase and polygalacturonase; Water add-on is 1-10 times of the fragrant chrysanthemum weight in Laifeng County, and auxiliary material add-on is the per-cent of the fragrant chrysanthemum weight in Laifeng County: cellulase 0.3%, zytase 0.3%, B-dextranase 1%, polygalacturonase 1%; Controlled enzymatic hydrolysis temperature 40 degree, starts stirring, enzymolysis time: 2 hours;
B. microwave extraction
Control extractor temperature 70 degree, microwave power is under 200kw condition, extracts 2 hours; Microwave extraction system used: adopt the maet-6 microwave extraction system that Shanghai Jing Qiao drying plant factory produces;
C. reclaim
Extractor is extracted material and is warmed up to 100 degree, water vapour cooling is reclaimed;
D. leave standstill
The cooling fluid reclaimed, leaves standstill 10 hours;
E. be separated
Aqueous portion is discharged, gets oil phase part, obtain Laifeng County's aromaticin oil.
Embodiment 6: a kind of microwave-assisted of the present invention prepares the enzyme solution of Laifeng County's aromaticin oil, comprises the following steps:
A. enzymolysis
In extractor, add the fragrant chrysanthemum in Laifeng County, water, cellulase, zytase, B-dextranase and polygalacturonase; Water add-on is 4 times of the fragrant chrysanthemum weight in Laifeng County, and auxiliary material add-on is the per-cent of the fragrant chrysanthemum weight in Laifeng County: cellulase 0.4%, zytase 0.4%, B-dextranase 1.2%, polygalacturonase 1.2%; Controlled enzymatic hydrolysis temperature 50 degree, starts stirring, enzymolysis time: 4 hours;
B. microwave extraction
Control extractor temperature 65 degree, microwave power is under 450kw condition, extracts 2.8 hours; Microwave extraction system used: adopt the maet-6 microwave extraction system that Shanghai Jing Qiao drying plant factory produces;
C. reclaim
Extractor is extracted material and is warmed up to 100 degree, water vapour cooling is reclaimed;
D. leave standstill
The cooling fluid reclaimed, leaves standstill 9 hours;
E. be separated
Aqueous portion is discharged, gets oil phase part, obtain Laifeng County's aromaticin oil.
Claims (2)
1. prepare an enzyme solution for Laifeng County's aromaticin oil with microwave-assisted, it is characterized in that comprising the following steps:
A. enzymolysis
In extractor, add the fragrant chrysanthemum in Laifeng County, water, cellulase, zytase, B-dextranase and polygalacturonase; Water add-on is 1-10 times of the fragrant chrysanthemum weight in Laifeng County, and auxiliary material add-on is the per-cent of the fragrant chrysanthemum weight in Laifeng County: cellulase 0.1-1%, zytase 0.1-1%, B-dextranase 0.3-3%, polygalacturonase 0.3-3%; Controlled enzymatic hydrolysis temperature 35-55 degree, starts stirring, enzymolysis time: 1-5 hour;
B. microwave extraction
Control extractor temperature 50-95 degree, microwave power is under 100-500kw condition, extracts 1-3 hour;
C. reclaim
Extractor is extracted material and is warmed up to 100 degree, water vapour cooling is reclaimed;
D. leave standstill
The cooling fluid reclaimed, leaves standstill 3-12 hour;
E. be separated
Aqueous portion is discharged, gets oil phase part, obtain Laifeng County's aromaticin oil.
2. prepare the enzyme solution of Laifeng County's aromaticin oil according to a kind of microwave-assisted according to claim 1, it is characterized in that comprising the following steps:
A. enzymolysis
In extractor, add the fragrant chrysanthemum in Laifeng County, water, cellulase, zytase, B-dextranase and polygalacturonase; Water add-on is 1-10 times of the fragrant chrysanthemum weight in Laifeng County, and auxiliary material add-on is the per-cent of the fragrant chrysanthemum weight in Laifeng County: cellulase 0.1-1%, zytase 0.1-1%, B-dextranase 0.3-3%, polygalacturonase 0.3-3%; Controlled enzymatic hydrolysis temperature 35-55 degree, starts stirring, enzymolysis time: 1-5 hour;
B. microwave extraction
Control extractor temperature 50-95 degree, microwave power is under 100-500kw condition, extracts 1-3 hour; Microwave extraction system used: adopt the maet-6 microwave extraction system that Shanghai Jing Qiao drying plant factory produces;
C. reclaim
Extractor is extracted material and is warmed up to 100 degree, water vapour cooling is reclaimed;
D. leave standstill
The cooling fluid reclaimed, leaves standstill 3-12 hour;
E. be separated
Aqueous portion is discharged, gets oil phase part, obtain Laifeng County's aromaticin oil.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110558446A (en) * | 2019-09-09 | 2019-12-13 | 青岛科技大学 | Natural plant extract composition for poultry feed additive, preparation method and application thereof |
| CN114133987A (en) * | 2021-12-10 | 2022-03-04 | 江西师范大学 | Method for extracting essential oil from cinnamomum camphora leaves |
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| CN101731748A (en) * | 2008-11-05 | 2010-06-16 | 湖北中烟工业有限责任公司 | Method for extracting Dendranthema indium leaves and application of extractive thereof in cigarettes |
| CN101928642A (en) * | 2010-06-22 | 2010-12-29 | 武汉神农天香生物科技有限公司 | Method for extracting and separating spice and medicinal components from whole plants of Dendranthema indicum |
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2015
- 2015-10-26 CN CN201510702697.1A patent/CN105176692A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101731748A (en) * | 2008-11-05 | 2010-06-16 | 湖北中烟工业有限责任公司 | Method for extracting Dendranthema indium leaves and application of extractive thereof in cigarettes |
| CN101928642A (en) * | 2010-06-22 | 2010-12-29 | 武汉神农天香生物科技有限公司 | Method for extracting and separating spice and medicinal components from whole plants of Dendranthema indicum |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110558446A (en) * | 2019-09-09 | 2019-12-13 | 青岛科技大学 | Natural plant extract composition for poultry feed additive, preparation method and application thereof |
| CN114133987A (en) * | 2021-12-10 | 2022-03-04 | 江西师范大学 | Method for extracting essential oil from cinnamomum camphora leaves |
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Inventor after: Liu Huaying Inventor before: Wu Jinwei Inventor before: Liu Huaying |
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Application publication date: 20151223 |