CN105158247A - Sulfur detector capable of removing chloride ions automatically - Google Patents
Sulfur detector capable of removing chloride ions automatically Download PDFInfo
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- CN105158247A CN105158247A CN201510531117.7A CN201510531117A CN105158247A CN 105158247 A CN105158247 A CN 105158247A CN 201510531117 A CN201510531117 A CN 201510531117A CN 105158247 A CN105158247 A CN 105158247A
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- beaker
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Abstract
The invention discloses an aldrin sulfur detector capable of removing chloride ions automatically, and belongs to the field of automatic measuring equipment for sulfur contents in coal. The sulfur detector comprises an aldrin sample manufacturing device, a combustion furnace, a solution stirring device, a first filtering device, a second filtering device, a chloride ion removing device, a filter paper ashing device and a room temperature weighing device which are fixed on a bottom plate; the chloride ion removing device is arranged between the second filtering device and the filter paper ashing device and comprises a high-definition camera, droppers, a first beaker, a second support, a second beaker, a funnel, filter paper and a glass rod; the high-definition camera is assembled on a camera frame; the droppers are assembled on a dropper frame; the first beaker is assembled on a beaker seat; and the funnel is assembled on a funnel stand. The aldrin sulfur detector is simple in structure and can remove chloride ions automatically.
Description
Technical field
The present invention relates generally to the automatic measuring equipment field of sulfur content in coal amount, refers in particular to a kind of Emhorn sulphur meter with automatic dechlorination ion function.
Background technology
Element sulphur, as one of important indicator evaluating ature of coal, needs accurately to measure.In prior art, in order to measure the sulfur content in combustible accurately and rapidly, general constant sulphur appliance or the sulphur meter of adopting is as conventional measuring equipment.In various measuring equipment, coulomb is all adopted to survey sulphur method.Coulomb surveys sulphur method to be needed with pump as power source, and the mode of employing continuous air extraction, continuous coverage measures.Due in gas containing sulphur concentration time to time change, therefore sulfur content is difficult to Accurate Determining, and the pump life-span also shortens because of laod unbalance simultaneously.
The standard method of the mensuration full content of Sulphur in coal content that classical Ai Shi Ce Liufashi various countries are general, has that accuracy is high, the advantage such as mensuration in batch.Chinese mugwort scholar surveys in sulphur step, and wherein one of most important step is: solution is heated to boiling, and under constantly stirring, drip barium chloride solution 10mL, under situation of closely boiling, keep about 2h, last liquor capacity is about 200mL; Filter with fine and close ashless quantitative filter paper after solution cooling or hold over night, and (check with silver nitrate) to without chlorion by hot water wash.Because this step adopts manual experiment method to carry out, therefore labour intensity is large, human error is large.
Summary of the invention
The technical matters that the present invention need solve is: the technical matters existed for prior art, the invention provides the Emhorn sulphur meter that a kind of structure is simple, automatically can remove chlorion.
In order to solve the problem, the solution that the present invention proposes is: a kind of Emhorn sulphur meter with automatic dechlorination ion function, it comprises the Emhorn sample making device be fixed on base plate, combustion furnace, solution stirring apparatus, first filtration unit, second filtration unit, removing chloride device, filter paper cineration device and room temperature meausring apparatus, described removing chloride device is located between described second filtration unit and described filter paper cineration device, it is characterized in that: described removing chloride device comprises the high-definition camera be installed on the shooting headstock, be installed in the dropper on Dropper stand, be installed in the first beaker on beaker seat, second support, second beaker, be installed in the funnel on filtration stand, filter paper and glass bar.
Described second support is installed on described base plate, and described filtration stand is installed in the top of described second support, and described filter paper is positioned in described funnel, and described glass bar is close to described filter paper and is placed; The tubular portion of described funnel is close to the inwall of described second beaker; Described first support is installed on described base plate, it is equiped with the shooting headstock, chuck, Dropper stand from top to bottom.
The spherical part of described dropper is installed on described chuck; Described first beaker, built with a certain amount of experimental solutions, is equiped with liquor argenti nitratis ophthalmicus in described dropper; Described PC is positioned on described first support, and is connected with the high-definition camera be installed on the described shooting headstock by signal wire; Described beaker seat is connected with described base plate by revolute pair.
Compared with prior art, the invention has the advantages that: the present invention utilizes chuck to control the outflow of the liquor argenti nitratis ophthalmicus in dropper, and by the silver nitride precipitation situation that PC analysis is taken from high-definition camera, thus remove the chlorion being arranged in the first beaker experimental solutions quickly and accurately; Afterwards, beaker seat rotates by revolute pair, and the solution in the first beaker and precipitation are poured in the second beaker by glass bar and filter paper, and silver nitride precipitation residues on filter paper.It can thus be appreciated that structure of the present invention is simple, dechlorination ion precision is high, without the need to artificial participation, the robotization for complete machine provides reliable guarantee.
Accompanying drawing explanation
Fig. 1 is plane figure's schematic diagram with the Emhorn sulphur meter of automatic dechlorination ion function of the present invention.
Fig. 2 is the principle schematic of the dechlorination ion of removing chloride device of the present invention.
Fig. 3 is the principle schematic of the filter process of removing chloride device of the present invention.
In figure, 1-Emhorn sample making device; 2-combustion furnace; 3-solution stirring apparatus; 4-the first filtration unit; 5-the second filtration unit; 6-removing chloride device; 7-filter paper cineration device; 8-room temperature meausring apparatus; 9-base plate; 61-high-definition camera; 62-shooting headstock; 63-the first support; 64-chuck; 65-Dropper stand; 66-signal wire; 67-PC; 68-dropper; 69-the first beaker; 610-experimental solutions; 611-revolute pair; 612-glass bar; 613-funnel; 614-filter paper; 615-filtration stand; 616-the second support; 617-the second beaker; 618-beaker seat.
Embodiment
Below with reference to the drawings and specific embodiments, the present invention is described in further detail.
Shown in Fig. 1 and Fig. 2, the Emhorn sulphur meter with automatic dechlorination ion function of the present invention, it comprises the Emhorn sample making device 1 be fixed on base plate 9, combustion furnace 2, solution stirring apparatus 3, first filtration unit 4, second filtration unit 5, removing chloride device 6, filter paper cineration device 7 and room temperature meausring apparatus 8; Removing chloride device 6 is located between the second filtration unit 5 and filter paper cineration device 7, and it comprises high-definition camera 61, the dropper 68 be installed on Dropper stand 65 be installed on the shooting headstock 62, is installed in the first beaker 69, second support 616, second beaker 617 on beaker seat 618, the funnel 613 be installed on filtration stand 615, filter paper 614 and glass bar 612.
Shown in Fig. 1 and Fig. 2, the second support 616 is installed on base plate 9, and filtration stand 615 is installed in the top of the second support 616, and filter paper 614 is positioned in funnel 613, and glass bar 612 is close to filter paper 614 and is placed; The tubular portion of funnel 613 is close to the inwall of the second beaker 617; First support 63 is installed on base plate 9, it is equiped with the shooting headstock 62, chuck 64, Dropper stand 65 from top to bottom; The spherical part of dropper 68 is placed on chuck 64; First beaker 69, built with a certain amount of experimental solutions 610, is equiped with liquor argenti nitratis ophthalmicus in dropper 68; PC 67 is positioned on the first support 63, and by signal wire 66 be installed in the high-definition camera 61 of making a video recording on the headstock 62 and be connected; Beaker seat 618 is connected with base plate 9 by revolute pair 611.
Principle of work: first chuck 64 clamps the spherical part of dropper 68, what allow the liquor argenti nitratis ophthalmicus of its inside flows out in the first beaker 69, generate silver nitride precipitation, the high-definition camera 61 be located on the shooting headstock 62 is taken pictures in real time, and photo is passed to PC 67 by signal wire 66; Then, the increase situation of silver nitride precipitation analyzed by PC 67, judges whether there is chlorion in the first beaker 69 quickly and accurately, until dechlorination ion terminates; Afterwards, beaker seat 618 drives the first beaker 69 to tilt by revolute pair 611, and the precipitation of experiment 610 solution in the first beaker 69 and generation is poured in the second beaker 617 by glass bar 612 and filter paper 614, and silver nitride precipitation residues on filter paper 614.
Claims (2)
1. one kind has the Emhorn sulphur meter of automatic dechlorination ion function, it comprises the Emhorn sample making device (1) be fixed on base plate (9), combustion furnace (2), solution stirring apparatus (3), first filtration unit (4), second filtration unit (5), removing chloride device (6), filter paper cineration device (7) and room temperature meausring apparatus (8), described removing chloride device (6) is located between described second filtration unit (5) and described filter paper cineration device (7), it is characterized in that: described removing chloride device (6) comprises the high-definition camera (61) be installed in the shooting headstock (62), be installed in the dropper (68) on Dropper stand (65), be installed in the first beaker (69) on beaker seat (618), second support (616), second beaker (617), be installed in the funnel (613) on filtration stand (615), filter paper (614) and glass bar (612).
2. the Emhorn sulphur meter with automatic dechlorination ion function according to claim 1, it is characterized in that: described second support (616) is installed on described base plate (9), described filtration stand (615) is installed in the top of described second support (616), described filter paper (614) is positioned in described funnel (613), and described glass bar (612) is close to described filter paper (614) and is placed; The tubular portion of described funnel (613) is close to the inwall of described second beaker (617); Described first support (63) is installed on described base plate (9), it is equiped with the shooting headstock (62), chuck (64), Dropper stand (65) from top to bottom; The spherical part of described dropper (68) is installed on described chuck (64); Described first beaker (69) is built with a certain amount of experimental solutions (610), and described dropper is equiped with liquor argenti nitratis ophthalmicus in (68); Described PC (67) is positioned on described first support (63), and is connected with the high-definition camera (61) be installed on the described shooting headstock (62) by signal wire (66); Described beaker seat (618) is connected with described base plate (9) by revolute pair (611).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510531117.7A CN105158247A (en) | 2015-08-26 | 2015-08-26 | Sulfur detector capable of removing chloride ions automatically |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510531117.7A CN105158247A (en) | 2015-08-26 | 2015-08-26 | Sulfur detector capable of removing chloride ions automatically |
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| CN105158247A true CN105158247A (en) | 2015-12-16 |
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| CN201510531117.7A Pending CN105158247A (en) | 2015-08-26 | 2015-08-26 | Sulfur detector capable of removing chloride ions automatically |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2793727Y (en) * | 2005-03-02 | 2006-07-05 | 鹤壁科力测控技术有限公司 | Sampler feeder of sulfur measuring device |
| JP2007064688A (en) * | 2005-08-29 | 2007-03-15 | Toyo Seiki Kk | Quantitative liquid feeder |
| CN201402267Y (en) * | 2009-04-15 | 2010-02-10 | 河南鑫科分析仪器有限公司 | Automatic multi-sample sulphur measuring instrument |
| CN102539622A (en) * | 2010-11-22 | 2012-07-04 | 株式会社堀场制作所 | Titration apparatus |
| CN202614774U (en) * | 2012-06-14 | 2012-12-19 | 李晓乐 | Sulfur measuring instrument |
| US20130217134A1 (en) * | 2012-02-17 | 2013-08-22 | Toyota Motor Engineering & Manufacturing North America, Inc. | Methods and Systems for Monitoring Content of Coating Solutions Using Automated Titration Devices |
-
2015
- 2015-08-26 CN CN201510531117.7A patent/CN105158247A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2793727Y (en) * | 2005-03-02 | 2006-07-05 | 鹤壁科力测控技术有限公司 | Sampler feeder of sulfur measuring device |
| JP2007064688A (en) * | 2005-08-29 | 2007-03-15 | Toyo Seiki Kk | Quantitative liquid feeder |
| CN201402267Y (en) * | 2009-04-15 | 2010-02-10 | 河南鑫科分析仪器有限公司 | Automatic multi-sample sulphur measuring instrument |
| CN102539622A (en) * | 2010-11-22 | 2012-07-04 | 株式会社堀场制作所 | Titration apparatus |
| US20130217134A1 (en) * | 2012-02-17 | 2013-08-22 | Toyota Motor Engineering & Manufacturing North America, Inc. | Methods and Systems for Monitoring Content of Coating Solutions Using Automated Titration Devices |
| CN202614774U (en) * | 2012-06-14 | 2012-12-19 | 李晓乐 | Sulfur measuring instrument |
Non-Patent Citations (2)
| Title |
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| 中华人民共和国国家质量监督检验检疫总局等发布: "煤中全硫的测定方法", 《中华人民共和国国家标准 GB/T 214-2007 煤中全硫的测定方法》 * |
| 高永生: "基于 Internet 多机器人遥操作系统安全机制的研究", 《中国博士学位论文全文数据信息科技辑》 * |
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Application publication date: 20151216 |