CN205483895U - Rock core imbibition experimental apparatus - Google Patents

Rock core imbibition experimental apparatus Download PDF

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Publication number
CN205483895U
CN205483895U CN201620204083.0U CN201620204083U CN205483895U CN 205483895 U CN205483895 U CN 205483895U CN 201620204083 U CN201620204083 U CN 201620204083U CN 205483895 U CN205483895 U CN 205483895U
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China
Prior art keywords
imbibition
rock core
thermostat
cup
experimental provision
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Expired - Fee Related
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CN201620204083.0U
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Chinese (zh)
Inventor
杨胜来
吴润桐
马铨铮
陈璨
许洋
韩伟
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China University of Petroleum Beijing
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China University of Petroleum Beijing
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Abstract

The utility model provides a rock core imbibition experimental apparatus, include: constant temperature equipment, constant voltage equipment, electronic balance, imbibition cup, imbibition liquid pipe and rock core gallows, placed in the constant temperature equipment and be equipped with imbibition liquid the imbibition cup to keep predetermined temperature in the messenger constant temperature equipment, constant voltage equipment is through passing constant temperature equipment imbibition liquid pipe with the imbibition cup is connected, so that in the imbibition cup the level of imbibition liquid remains stationary, electronic balance place in on constant temperature equipment's the top surface, electronic balance is through passing constant temperature equipment the rock core gallows is connected with the rock core, is used for weighing the mass parameter of rock core, wherein, rock core suspension and submergence in in the imbibition liquid for the mass parameter of the gained rock core of rock core imbibition experimental apparatus obtains under the condition of constant temperature and constant voltage, improves and tests the accuracy.

Description

Rock core imbibition experimental provision
Technical field
This utility model relates to technical field of petrochemical industry, particularly relates to a kind of rock core imbibition experiment dress Put.
Background technology
In compact oil reservoir and low-permeability oil deposit displacement or the research handled up etc., by utilize rock core hole with Imbibition between substrate and substrate and crack thus obtain the imbibition effect of rock core, become important research class Topic.
In the prior art, often utilize high-precision indoor experimental apparatus to the rock under different experimental conditions The imbibition yield of the heart carries out quantitative, qualitative.In existing imbibition experiment, mainly utilize mass method to imbibition Effect is tested: its experimental provision is based on balance, counterweight, beaker, by utilizing lever principle Weighing is immersed in the core quality in imbibition liquid thus calculates imbibition rate.Its experimental provision is owing to using sky Flat lever is experiment basis, and error is the biggest;The more important thing is, due to experimental provision it cannot be guaranteed that measurement ring The stationarity in border so that measuring environment and change, such as variations in temperature and imbibition liquid volatilization etc., cause There is change in experiment condition, has a strong impact on the accuracy of experiment.
Therefore, in existing rock core imbibition is tested, it is badly in need of one and can ensure that experiment condition and experimental situation Stablize, enable experiment not by ectocine thus obtain the experimental provision of experimental result accurately.
Utility model content
This utility model provides a kind of rock core imbibition experimental provision, uses above-mentioned existing rock core in order to solving During imbibition experimental provision, it is impossible to ensure the fixing of experiment condition and the inaccurate problem of experimental result that causes.
On the one hand, this utility model provides a kind of rock core imbibition experimental provision, including: thermostat, permanent Pressure device, electronic balance, imbibition cup, imbibition fluid catheter and rock core suspension bracket;
Wherein, in described thermostat, it is placed with the described imbibition cup equipped with imbibition liquid, so that thermostat The temperature that interior holding is preset;
Described constant voltage equipment is by the described imbibition fluid catheter through described thermostat with described imbibition cup even Connect, so that the level height of the described imbibition liquid in described imbibition cup keeps fixing;
Described electronic balance is positioned on the end face of described thermostat, and described electronic balance is by through institute The described rock core suspension bracket stating thermostat is connected with rock core, for weighing the mass parameter of described rock core;Its In, described rock core suspends and is immersed in described imbibition liquid.
Further, also include: data collecting system;
Described electronic balance is connected with described data collecting system, so that described data collecting system obtains institute State mass parameter.
Further, also include: leveling device;
The end face of described leveling device contacts with the bottom surface of described thermostat, is used for adjusting described perseverance Temperature plane residing for device, so that being positioned at the described electronic balance holding level of the top side of described thermostat.
Further, bowl cover is also included;
The top of described imbibition cup is additionally provided with dismountable described bowl cover, being provided centrally with of described bowl cover One through hole, for making described rock core suspension bracket be connected through described through hole with the described rock core in described imbibition cup.
Further, it is additionally provided with the first valve in the junction of described imbibition cup and described imbibition fluid catheter, For controlling conducting and the Guan Bi of described imbibition fluid catheter.
Further, described constant voltage equipment is additionally provided with the second valve with the junction of described imbibition fluid catheter, For avoiding described imbibition liquid to flow backward in described constant voltage equipment.
Further, also include: temperature sensor;
Described temperature sensor is arranged in described thermostat, is connected with described data collecting system, uses Temperature parameter in measuring described thermostat, so that described data collecting system obtains described temperature ginseng Number.
Further, described constant voltage equipment is connected with described data collecting system, so that described data acquisition System obtains the pressure parameter in current described constant voltage equipment.
The rock core imbibition experimental provision that this utility model provides, including: thermostat, constant voltage equipment, electricity Sub-balance, imbibition cup, imbibition fluid catheter and rock core suspension bracket;Wherein, it is placed with dress in described thermostat There is the described imbibition cup of imbibition liquid, so that keeping the temperature preset in thermostat;Described constant voltage equipment leads to Cross the described imbibition fluid catheter through described thermostat to be connected with described imbibition cup, so that described imbibition cup The level height of interior described imbibition liquid keeps fixing;Described electronic balance is positioned over described thermostat On end face, described electronic balance is connected with rock core by the described rock core suspension bracket through described thermostat, For weighing the mass parameter of described rock core;Wherein, described rock core suspends and is immersed in described imbibition liquid. By above-mentioned setting so that the mass parameter of the rock core that rock core imbibition experimental provision is obtained be at constant temperature and Obtain in the case of constant voltage, eliminate the reality that the experiment condition such as variations in temperature and imbibition liquid volatilization is caused Test the error of result, be conducive to obtaining the imbibition rate of rock core oil reservoir accurately, enable research worker more preferable The imbibition effect of ground research rock core oil reservoir.
Accompanying drawing explanation
The structural representation of a kind of rock core imbibition experimental provision that Fig. 1 provides for this utility model embodiment one Figure;
The structural representation of another rock core imbibition experimental provision that Fig. 2 provides for this utility model embodiment one Figure;
The structural representation of a kind of rock core imbibition experimental provision that Fig. 3 provides for this utility model embodiment two Figure;
The structural representation of a kind of rock core imbibition experimental provision that Fig. 4 provides for this utility model embodiment three Figure.
Reference:
1-thermostat;2-constant voltage equipment;3-electronic balance;
4-imbibition cup;5-imbibition fluid catheter;6-rock core suspension bracket;
7-rock core;8-data collecting system;9-bowl cover;
10-through hole;11-temperature sensor.
Detailed description of the invention
For making the purpose of each embodiment of this utility model, technical scheme and advantage clearer, below will knot Closing the accompanying drawing in each embodiment of this utility model, the technical scheme in embodiment each to this utility model is carried out Clearly and completely describe.For convenience of explanation, the size in zoomed in or out different layers and region, So size shown in figure and ratio might not represent actual size, the most do not reflect that the ratio of size is closed System.
The structural representation of a kind of rock core imbibition experimental provision that Fig. 1 provides for this utility model embodiment one Figure, as it is shown in figure 1, this rock core imbibition experimental provision includes: thermostat 1, constant voltage equipment 2, electronics Balance 3, imbibition cup 4, imbibition fluid catheter 5 and rock core suspension bracket 6;
The imbibition cup 4 equipped with imbibition liquid it is placed with, so that keeping pre-in thermostat 1 in thermostat 1 If temperature.
Wherein, imbibition liquid concretely saline, oil or the liquid such as distilled water, in order to imbibition liquid enters with rock core Row liquid displacement, i.e. ensures that imbibition liquid composition is different from the fluid composition in rock core, and the application is to this Do not limit.Thermostat 1 concretely small-sized thermostat, or be temperature-adjustable and holding temperature Any one constant thermostat, more preferably, the sidewall of thermostat 1 is also provided with observe Window, in order to research worker observation experiment is in progress.
Constant voltage equipment 2 is connected with imbibition cup 4 by the imbibition fluid catheter 5 through thermostat 1, so that The level height of the imbibition liquid in imbibition cup 4 keeps fixing.
Concrete, constant voltage equipment 2 is by the imbibition fluid catheter 5 through thermostat 1 with imbibition cup 4 even Connect, so that when volatilization occurs in the imbibition liquid in imbibition cup 4, and imbibition fluid catheter 5 and imbibition cup 4 occur When the pressure of junction declines, constant voltage equipment 2 supplements imbibition by imbibition fluid catheter 5 in imbibition cup 4 Liquid, thus ensure that the level height of the imbibition liquid in imbibition cup 4 is fixed, make experiment condition tend towards stability and carry The accuracy of high experimental result.
Electronic balance 3 is positioned on the end face of thermostat 1, and electronic balance 3 is by through thermostat The rock core suspension bracket 6 of 1 is connected with rock core 7, for weighing the mass parameter of rock core 7;Wherein, rock core 7 Suspend and be immersed in imbibition liquid.
Concrete, the top of rock core suspension bracket 6 is connected with the object stage of electronic balance 3, rock core suspension bracket 6 Bottom is connected with rock core 7, and ensures that rock core 7 suspends and is immersed in the imbibition liquid in imbibition cup 4, with Ensure that all surfaces of rock core 7 can carry out liquid displacement with imbibition liquid.And electronic balance 3 passes through rock core The mass parameter of rock core 7 can be weighed by suspension bracket 6, and its minimum measurement unit can be accurate to 0.0001 gram.
Further, another rock core imbibition experimental provision that Fig. 2 provides for this utility model embodiment one Structural representation, on the basis of Fig. 1, as in figure 2 it is shown, this device also includes: data acquisition system System 8;Wherein, electronic balance 3 is connected with data collecting system 8, so that data collecting system 8 obtains The mass parameter of rock core, so that research worker directly can obtain this quality from data collecting system 8 Parameter, simplifies operation.
Further, the using and ensure experiment safety, upper of this rock core imbibition experimental provision for convenience On the basis of stating Fig. 1 or Fig. 2 embodiment, also set in the junction of imbibition cup 4 and imbibition fluid catheter 5 Being equipped with the first valve, this first valve is for controlling conducting and the Guan Bi of imbibition fluid catheter 5, thus controls Experiment process, meanwhile, it also avoid contingent, leads owing to constant voltage equipment 2 sets hypertonia The liquid level of the imbibition liquid caused is too high so that imbibition hydrorrhea goes out the situation of imbibition cup 4, it is ensured that experiment Safety.
Further, in order to improve the accuracy of experiment, on the basis of any of the above-described embodiment, permanent Pressure device 2 is additionally provided with the second valve with the junction of imbibition fluid catheter 5, and this second valve is used for avoiding Imbibition liquid flows backward in constant voltage equipment 2.Concrete, this second valve check valve again forms so that imbibition Imbibition liquid in fluid catheter 5 will not flow backward to constant voltage equipment 2, it is to avoid imbibition liquid after imbibition flow backwards and Cause the error measured.
The rock core imbibition experimental provision that this utility model embodiment one provides, including: thermostat 1, permanent Pressure device 2, electronic balance 3, imbibition cup 4, imbibition fluid catheter 5 and rock core suspension bracket 6;Thermostat 1 Inside it is placed with the imbibition cup 4 equipped with imbibition liquid, so that keeping the temperature preset in thermostat 1;Constant voltage Device 2 is connected with imbibition cup 4 by the imbibition fluid catheter 5 through thermostat 1, so that imbibition cup 4 The level height of interior imbibition liquid keeps fixing;Electronic balance 3 is positioned on the end face of thermostat 1, Electronic balance 3 is connected with rock core 7 by the rock core suspension bracket 6 through thermostat 1, is used for weighing rock core The mass parameter of 7;Wherein, rock core 7 suspends and is immersed in imbibition liquid.By above-mentioned setting so that The mass parameter of the rock core that rock core imbibition experimental provision is obtained is to obtain in the case of constant temperature and constant voltage , eliminate the error of the experimental result that the experiment condition such as variations in temperature and imbibition liquid volatilization is caused, have It is beneficial to obtain the imbibition rate of rock core oil reservoir accurately, enables research worker preferably to study rock core oil reservoir Imbibition effect.
Further, the embodiment of the present application two provides a kind of rock core imbibition experimental provision, in order to make electronics Mass parameter measured by balance 3 is more accurate, on the basis of any of the above-described embodiment, and this rock core Imbibition experimental provision may also include that leveling device.
The end face of leveling device contacts with the bottom surface of thermostat 1, is used for adjusting described thermostat Plane residing for 1, so that being positioned at the electronic balance 3 holding level of the top side of thermostat 1.
Concrete, this leveling device can be existing any one manual horizontal regulating structure or automatic water The whole structure of Heibei provincial opera forms, to realize making to be positioned at the electronic balance 3 holding level of the top side of thermostat 1 Function, its concrete structure is not defined by the application.By arranging leveling device so that Mass parameter measured by electronic balance 3 is more accurate, improves the accuracy of experiment.
Preferably, leveling device concretely horizontal adjustment castor, so that at regulation electronic balance 3 On the basis of holding level, moreover it is possible to whole attemperator 1 is moved, improve rock core imbibition experiment dress The motility put and operability.
Further, a kind of rock core imbibition experimental provision that Fig. 3 provides for this utility model embodiment two Structural representation, the error brought to make reduction imbibition liquid volatilize, make experimental result more accurate, On the basis of any of the above-described embodiment, this rock core imbibition experimental provision may also include that bowl cover 9.
The top of imbibition cup 4 is additionally provided with dismountable bowl cover 9, bowl cover 9 be provided centrally with a through hole 10, for making rock core suspension bracket 6 be connected through through hole 10 with the rock core 7 in imbibition cup 4.By bowl cover 9 Setting, reduce the volatilization of imbibition liquid, improve the accuracy of experiment.
The rock core imbibition experimental provision that this utility model embodiment two provides, is provided by end face and constant temperature The Heibei provincial opera engagement positions of the bottom surface contact of device 1, to adjust the plane residing for thermostat 1, makes to be positioned at perseverance The electronic balance 3 of the top side of temperature device 1 keeps level so that the mass parameter measured by electronic balance 3 More accurate, improve the accuracy of experiment;Top at imbibition cup 4 is provided with dismountable cup Lid 9, and be provided centrally with a through hole 10 at bowl cover 9, be used for making rock core suspension bracket 6 through through hole 10 with Rock core 7 in imbibition cup 4 connects, thus reduces the volatilization of imbibition liquid, improves the standard of experiment further Really property.
Further, in order to make the measurement parameter of experiment in further detail, experimental result is more accurate, this reality A kind of rock core imbibition experimental provision is provided by new embodiment three, in above-mentioned Fig. 2 illustrated embodiment, This rock core imbibition experimental provision also includes: temperature sensor 11.
Temperature sensor 11 is arranged in thermostat 1, is connected with data collecting system 8, is used for measuring Temperature parameter in thermostat 1, so that data collecting system 8 obtains this temperature parameter.
Concrete, by arranging the temperature sensor 11 being connected with data collecting system 8 so that data acquisition Collecting system 8 is while obtaining the mass parameter of rock core 7, moreover it is possible to obtain the corresponding temperature of this mass parameter The calculating of parameter, beneficially experimental result, improves the accuracy of experiment.
Further, in order to make the measurement parameter of experiment in further detail, experimental result is more accurate, Fig. 4 The structural representation of a kind of rock core imbibition experimental provision provided for this utility model embodiment three, above-mentioned On the basis of Fig. 2 and embodiment three illustrated embodiment, constant voltage equipment 2 is with data collecting system 8 even Connect, so that data collecting system 8 obtains the pressure parameter in current constant voltage equipment 2.So that total According to acquisition system 8 while the mass parameter obtaining rock core 7 and temperature parameter, moreover it is possible to obtain corresponding The calculating of pressure parameter, beneficially experimental result, improves the accuracy of experiment.
The rock core imbibition experimental provision that present embodiment embodiment three provides, by arranging temperature sensor 11 are arranged in thermostat 1, are connected with data collecting system 8, for measuring in thermostat 1 Temperature parameter, so that data collecting system 8 obtains this temperature parameter;Also by by constant voltage equipment 2 and number Connect according to acquisition system 8, so that data collecting system 8 obtains the pressure ginseng in current constant voltage equipment 2 Number so that data collecting system 8 obtain rock core 7 mass parameter while, moreover it is possible to obtain with The corresponding temperature parameter of this mass parameter and pressure parameter, it is achieved real automatic measurement, the most also The accuracy of this rock core imbibition experimental provision can be improved further and improve conventional efficient.
Last it is noted that various embodiments above is only in order to illustrate the technical solution of the utility model, and Non-to its restriction;Although this utility model being described in detail with reference to foregoing embodiments, ability The those of ordinary skill in territory is it is understood that it still can be to the technical scheme described in foregoing embodiments Modify, or the most some or all of technical characteristic is carried out equivalent;And these amendment or Person replaces, and does not make the essence of appropriate technical solution depart from the model of this utility model each embodiment technical scheme Enclose.

Claims (8)

1. a rock core imbibition experimental provision, it is characterised in that including: thermostat, constant voltage equipment, Electronic balance, imbibition cup, imbibition fluid catheter and rock core suspension bracket;
Wherein, in described thermostat, it is placed with the described imbibition cup equipped with imbibition liquid, so that thermostat The temperature that interior holding is preset;
Described constant voltage equipment is by the described imbibition fluid catheter through described thermostat with described imbibition cup even Connect, so that the level height of the described imbibition liquid in described imbibition cup keeps fixing;
Described electronic balance is positioned on the end face of described thermostat, and described electronic balance is by through institute The described rock core suspension bracket stating thermostat is connected with rock core, for weighing the mass parameter of described rock core;Its In, described rock core suspends and is immersed in described imbibition liquid.
Rock core imbibition experimental provision the most according to claim 1, it is characterised in that also include: number According to acquisition system;
Described electronic balance is connected with described data collecting system, so that described data collecting system obtains institute State mass parameter.
Rock core imbibition experimental provision the most according to claim 2, it is characterised in that also include: temperature Degree sensor;
Described temperature sensor is arranged in described thermostat, is connected with described data collecting system, uses Temperature parameter in measuring described thermostat, so that described data collecting system obtains described temperature ginseng Number.
Rock core imbibition experimental provision the most according to claim 2, it is characterised in that described constant voltage fills Put and be connected with described data collecting system, so that described data collecting system obtains current described constant voltage dress Put interior pressure parameter.
5. according to the rock core imbibition experimental provision described in any one of claim 1-4, it is characterised in that also Including: leveling device;
The end face of described leveling device contacts with the bottom surface of described thermostat, is used for adjusting described perseverance Temperature plane residing for device, so that being positioned at the described electronic balance holding level of the top side of described thermostat.
6. according to the rock core imbibition experimental provision described in any one of claim 1-4, it is characterised in that also Including bowl cover;
The top of described imbibition cup is additionally provided with dismountable described bowl cover, being provided centrally with of described bowl cover One through hole, for making described rock core suspension bracket be connected through described through hole with the described rock core in described imbibition cup.
7. according to the rock core imbibition experimental provision described in any one of claim 1-4, it is characterised in that The junction of described imbibition cup and described imbibition fluid catheter is additionally provided with the first valve, be used for controlling described in ooze The conducting of imbibition conduit and Guan Bi.
8. according to the rock core imbibition experimental provision described in any one of claim 1-4, it is characterised in that institute The junction stating constant voltage equipment and described imbibition fluid catheter is additionally provided with the second valve, be used for avoiding described in ooze Imbibition flows backward in described constant voltage equipment.
CN201620204083.0U 2016-03-16 2016-03-16 Rock core imbibition experimental apparatus Expired - Fee Related CN205483895U (en)

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Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106198298A (en) * 2016-08-29 2016-12-07 长安大学 A kind of negative pressure water absorber of material
CN106226193A (en) * 2016-09-22 2016-12-14 中国矿业大学(北京) A kind of coal petrography capillary water absorption measuring method
CN107144515A (en) * 2017-07-05 2017-09-08 西安石油大学 Imbibition experimental provision and its method
CN108195732A (en) * 2017-11-30 2018-06-22 中国石油天然气股份有限公司 A kind of compact rock core imbibition experimental provision and imbibition weight testing method
CN108387478A (en) * 2017-05-18 2018-08-10 惠州市宙邦化工有限公司 A kind of imbibition test method and device
CN109856030A (en) * 2019-02-15 2019-06-07 中国石油大学(北京) The determination method of imbibition experimental provision and imbibition recovery percent of reserves
CN109915126A (en) * 2019-04-03 2019-06-21 中国石油大学(北京) The measuring method and imbibition experimental rig of the imbibition recovery percent of reserves of oil-bearing rock
CN111024544A (en) * 2019-12-02 2020-04-17 中国石油大学(北京) Imbibition experimental system and imbibition experimental method
CN113324468A (en) * 2021-06-28 2021-08-31 山东科技大学 Testing device and testing method for measuring seepage height of reverse seepage experiment
CN113670778A (en) * 2021-08-26 2021-11-19 中国石油大学(华东) Shale imbibition experimental apparatus of magnetic suspension measurement
CN114295531A (en) * 2022-03-07 2022-04-08 成都理工大学 Device and method for accurately simulating self-absorption amount of drilling completion fluid under in-situ condition

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106198298A (en) * 2016-08-29 2016-12-07 长安大学 A kind of negative pressure water absorber of material
CN106226193A (en) * 2016-09-22 2016-12-14 中国矿业大学(北京) A kind of coal petrography capillary water absorption measuring method
CN108387478A (en) * 2017-05-18 2018-08-10 惠州市宙邦化工有限公司 A kind of imbibition test method and device
CN107144515A (en) * 2017-07-05 2017-09-08 西安石油大学 Imbibition experimental provision and its method
CN108195732B (en) * 2017-11-30 2021-09-28 中国石油天然气股份有限公司 Compact rock core imbibition experimental device and imbibition amount testing method
CN108195732A (en) * 2017-11-30 2018-06-22 中国石油天然气股份有限公司 A kind of compact rock core imbibition experimental provision and imbibition weight testing method
CN109856030A (en) * 2019-02-15 2019-06-07 中国石油大学(北京) The determination method of imbibition experimental provision and imbibition recovery percent of reserves
CN109856030B (en) * 2019-02-15 2024-05-24 中国石油大学(北京) Imbibition experimental device and method for determining imbibition extraction degree
CN109915126A (en) * 2019-04-03 2019-06-21 中国石油大学(北京) The measuring method and imbibition experimental rig of the imbibition recovery percent of reserves of oil-bearing rock
CN109915126B (en) * 2019-04-03 2021-01-05 中国石油大学(北京) Method for measuring imbibition production degree of oil-bearing rock and imbibition test device
CN111024544A (en) * 2019-12-02 2020-04-17 中国石油大学(北京) Imbibition experimental system and imbibition experimental method
CN113324468A (en) * 2021-06-28 2021-08-31 山东科技大学 Testing device and testing method for measuring seepage height of reverse seepage experiment
CN113324468B (en) * 2021-06-28 2022-06-21 山东科技大学 Testing device and testing method for measuring seepage height of reverse seepage experiment
CN113670778A (en) * 2021-08-26 2021-11-19 中国石油大学(华东) Shale imbibition experimental apparatus of magnetic suspension measurement
CN114295531A (en) * 2022-03-07 2022-04-08 成都理工大学 Device and method for accurately simulating self-absorption amount of drilling completion fluid under in-situ condition

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