CN105153826A - Acid-resistant and alkali-resistant paint used for electric power grid outdoor box body and preparation method of acid-resistant and alkali-resistant paint - Google Patents
Acid-resistant and alkali-resistant paint used for electric power grid outdoor box body and preparation method of acid-resistant and alkali-resistant paint Download PDFInfo
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Abstract
The invention discloses acid-resistant and alkali-resistant paint used for an electric power grid outdoor box body and a preparation method of the acid-resistant and alkali-resistant paint. The acid-resistant and alkali-resistant paint which is resistant to corrosion and wear and can absorb heat is prepared through a step-by-step mixing method with graphene, silicone crosslinked polyethylene, cordierite, hexafluorobutyl methacrylate-acrylate copolymer emulsion, organosilicone modified fluorocarbon resin, mesocarbon microbeads, crylic acid, 2,4,6-tris(dimethylaminomethyl)phenol, dibutyltin dilaurate, zirconium silicate, calcium metasilicate, gas phase aluminium oxide, chlorinated polyvinyl chloride resin, isopropyl phenyl diphenyl phosphate, butyl acetate, titanium dioxide, steel fiber, coagulator, diluent, iron powder and silica solutions as raw materials, and the acid-resistant and alkali-resistant paint is suitable for the electric power grid outdoor box body.
Description
Technical field
The invention belongs to acid and alkali-resistance paint field, particularly a kind of electric power network outdoor case acid and alkali-resistance coating and preparation method thereof.
Background technology
Power equipment (powersystem) mainly comprises with generating set and the large class of power-supply unit two, generating set is station boiler, steam turbine, internal combustion turbine, water turbine, generator, transformer etc. mainly, the transmitting line, mutual inductor, contactor etc. of power-supply unit mainly various voltage range.
Along with industrial expansion, in electric power network outdoor case, acid and alkali-resistance coating for main coating can play anticorrosion, wear-resisting, acid and alkali-resistance effect is more and more important, at present, common acid and alkali-resistance coating is easily corroded with aging, can not play automatically cleaning, acid and alkali-resistance effect.
Summary of the invention
The object of the invention is for the problems referred to above, develop a kind of wear-resisting, corrosion-resistant, electric power network outdoor case acid and alkali-resistance coating that can absorb heat and preparation method thereof.
A kind of electric power network outdoor case acid and alkali-resistance coating, described casing is environment real-time monitoring system casing, is outdoor mechanism case, is provided with humidity sensor, humidity regulator, temperature sensor, temperature regulator in casing, well heater and power supply; This acid and alkali-resistance coating is made up of following weight part material: Graphene 35-55 part; Organosilane crosslinked polyethylene 35-55 part; Trichroite 35-55 part; Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate 35-55 part; Organic-silicon-modified fluorocarbon resin 35-55 part; MCMB 35-55 part; Vinylformic acid 1-17 part; 2,4,6-tri(dimethylaminomethyl)phenol 1-17 part; Dibutyl tin laurate 1-17 part; Zirconium silicate 1-17 part; Calcium metasilicate 1-17 part; Gas phase aluminium sesquioxide 1-17 part; Chlorinated polyvinyl chloride resin 1-17 part; ISOPROPYL PHENYL DIPHENYL PHOSPHATE 1-17 part; N-BUTYL ACETATE 1-17 part; Titanium dioxide 1-17 part; Steel fiber 1-17 part; Peptizer 1-17 part; Thinner 1-17 part; Iron powder 1-17 part; Silicon sol 1-17 part.
As preferred version of the present invention, this acid and alkali-resistance coating is made up of following weight part material: Graphene 35 parts; Organosilane crosslinked polyethylene 35 parts; Trichroite 35 parts; Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate 35 parts; Organic-silicon-modified fluorocarbon resin 35 parts; MCMB 35 parts; 5 parts, vinylformic acid; 2,4,6-tri(dimethylaminomethyl)phenol 5 parts; Dibutyl tin laurate 5 parts; Zirconium silicate 5 parts; Calcium metasilicate 5 parts; Gas phase aluminium sesquioxide 5 parts; Chlorinated polyvinyl chloride resin 5 parts; ISOPROPYL PHENYL DIPHENYL PHOSPHATE 5 parts; N-BUTYL ACETATE 5 parts; Titanium dioxide 5 parts; Steel fiber 5 parts; 5 parts, peptizer; Thinner 5 parts; Iron powder 5 parts; Silicon sol 5 parts.
As preferred version of the present invention, the particle diameter of described Graphene is 35-60nm.
The present invention also provides a kind of preparation method of acid and alkali-resistance coating, comprises the steps:
(1), prepare burden according to acid and alkali-resistance system component;
(2), Graphene, organosilane crosslinked polyethylene, trichroite, Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate and organic-silicon-modified fluorocarbon resin is first added according to formula ratio, shredder ground and mixed 3min, add MCMB more subsequently, stir 35min with homogenizer;
(3), at 45 DEG C, vinylformic acid, 2 is added again, 4,6-tri(dimethylaminomethyl)phenol, dibutyl tin laurate, zirconium silicate, calcium metasilicate, gas phase aluminium sesquioxide, chlorinated polyvinyl chloride resin, ISOPROPYL PHENYL DIPHENYL PHOSPHATE, N-BUTYL ACETATE, titanium dioxide, steel fiber, peptizer, thinner, iron powder and silicon sol, and stir 40min, obtain acid and alkali-resistance coating.
By the application of technique scheme, of the present invention have following beneficial effect:
(1), adopt Graphene, organosilane crosslinked polyethylene, trichroite, Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate, organic-silicon-modified fluorocarbon resin and MCMB are as the main component of acid and alkali-resistance coating, Graphene is as the main component of coating, electroconductibility or salt spray resistance can not only be improved, coat-thickness can also be reduced further simultaneously, increase the sticking power to base material, promote wear resistance and the resistance to acids and bases of coating, and the compound use of organosilane crosslinked polyethylene and organic-silicon-modified fluorocarbon resin, to greatly strengthen the wear-resisting of this acid and alkali-resistance coating, the performance of corrosion-resistant and acid and alkali-resistance, and inorganic materials trichroite and Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate, because self has reinforced effects for coating, as main component, the acid and alkali-resistance of this soda acid coating is strengthened greatly.
(2), select vinylformic acid, 2, 4, 6-tri(dimethylaminomethyl)phenol, dibutyl tin laurate, zirconium silicate, calcium metasilicate, gas phase aluminium sesquioxide, chlorinated polyvinyl chloride resin, ISOPROPYL PHENYL DIPHENYL PHOSPHATE, N-BUTYL ACETATE, titanium dioxide, steel fiber, peptizer, thinner, iron powder and silicon sol are ancillary component, not only make the wear-resisting of this acid and alkali-resistance coating, corrosion-resistant, acid-proof alkaline is improved, this acid and alkali-resistance coating is also made to have good hydrophobic performance, and owing to the addition of solar selectively absorptive function iron powder and silicon sol combination, this acid and alkali-resistance coating is made to can be used in the relevant electric power network outdoor case of sun power.
(3), this acid and alkali-resistance Paint preparation technology is simple, and be easy to industrialization, raw material sources are extensive, are applicable to very much being applied to production.
Embodiment
Below in conjunction with specific embodiment, and comparable data describes in further detail the present invention.Should be understood that these embodiments just in order to demonstrate the invention, but not limit the scope of the invention by any way.
Embodiment 1
The acid and alkali-resistance coating of the present embodiment is made up of following weight part material: Graphene 35 parts; Organosilane crosslinked polyethylene 35 parts; Trichroite 35 parts; Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate 35 parts; Organic-silicon-modified fluorocarbon resin 35 parts; MCMB 35 parts; 5 parts, vinylformic acid; 2,4,6-tri(dimethylaminomethyl)phenol 5 parts; Dibutyl tin laurate 5 parts; Zirconium silicate 5 parts; Calcium metasilicate 5 parts; Gas phase aluminium sesquioxide 5 parts; Chlorinated polyvinyl chloride resin 5 parts; ISOPROPYL PHENYL DIPHENYL PHOSPHATE 5 parts; N-BUTYL ACETATE 5 parts; Titanium dioxide 5 parts; Steel fiber 5 parts; 5 parts, peptizer; Thinner 5 parts; Iron powder 5 parts; Silicon sol 5 parts.The particle diameter of wherein said Graphene is 30nm.
The preparation method of the acid and alkali-resistance coating of the present embodiment, comprises the steps: (1), prepares burden according to acid and alkali-resistance system component; (2), Graphene, organosilane crosslinked polyethylene, trichroite, Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate and organic-silicon-modified fluorocarbon resin is first added according to formula ratio, shredder ground and mixed 3min, add MCMB more subsequently, stir 35min with homogenizer; (3), at 45 DEG C, vinylformic acid, 2 is added again, 4,6-tri(dimethylaminomethyl)phenol, dibutyl tin laurate, zirconium silicate, calcium metasilicate, gas phase aluminium sesquioxide, chlorinated polyvinyl chloride resin, ISOPROPYL PHENYL DIPHENYL PHOSPHATE, N-BUTYL ACETATE, titanium dioxide, steel fiber, peptizer, thinner, iron powder and silicon sol, and stir 40min, obtain acid and alkali-resistance coating.
Embodiment 2
The acid and alkali-resistance coating of the present embodiment is made up of following weight part material: Graphene 47 parts; Organosilane crosslinked polyethylene 47 parts; Trichroite 47 parts; Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate 47 parts; Organic-silicon-modified fluorocarbon resin 47 parts; MCMB 47 parts; 7 parts, vinylformic acid; 2,4,6-tri(dimethylaminomethyl)phenol 7 parts; Dibutyl tin laurate 7 parts; Zirconium silicate 7 parts; Calcium metasilicate 7 parts; Gas phase aluminium sesquioxide 7 parts; Chlorinated polyvinyl chloride resin 7 parts; ISOPROPYL PHENYL DIPHENYL PHOSPHATE 7 parts; N-BUTYL ACETATE 7 parts; Titanium dioxide 7 parts; Steel fiber 7 parts; 7 parts, peptizer; Thinner 7 parts; Iron powder 7 parts; Silicon sol 7 parts.The particle diameter of wherein said Graphene is 30nm.
The preparation method of the acid and alkali-resistance coating of the present embodiment, comprises the steps: (1), prepares burden according to acid and alkali-resistance system component; (2), Graphene, organosilane crosslinked polyethylene, trichroite, Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate and organic-silicon-modified fluorocarbon resin is first added according to formula ratio, shredder ground and mixed 3min, add MCMB more subsequently, stir 35min with homogenizer; (3), at 45 DEG C, vinylformic acid, 2 is added again, 4,6-tri(dimethylaminomethyl)phenol, dibutyl tin laurate, zirconium silicate, calcium metasilicate, gas phase aluminium sesquioxide, chlorinated polyvinyl chloride resin, ISOPROPYL PHENYL DIPHENYL PHOSPHATE, N-BUTYL ACETATE, titanium dioxide, steel fiber, peptizer, thinner, iron powder and silicon sol, and stir 40min, obtain acid and alkali-resistance coating.
Embodiment 3
The acid and alkali-resistance coating of the present embodiment is made up of following weight part material: Graphene 30 parts; Organosilane crosslinked polyethylene 30 parts; Trichroite 30 parts; Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate 30 parts; Organic-silicon-modified fluorocarbon resin 30 parts; MCMB 30 parts; 1 part, vinylformic acid; 2,4,6-tri(dimethylaminomethyl)phenol 1 part; Dibutyl tin laurate 1 part; Zirconium silicate 1 part; Calcium metasilicate 1 part; Gas phase aluminium sesquioxide 1 part; Chlorinated polyvinyl chloride resin 1 part; ISOPROPYL PHENYL DIPHENYL PHOSPHATE 1 part; N-BUTYL ACETATE 1 part; Titanium dioxide 1 part; Steel fiber 1 part; 1 part, peptizer; Thinner 1 part; Iron powder 1 part; Silicon sol 1 part.The particle diameter of wherein said Graphene is 40nm.
The preparation method of the acid and alkali-resistance coating of the present embodiment, comprises the steps: (1), prepares burden according to acid and alkali-resistance system component; (2), Graphene, organosilane crosslinked polyethylene, trichroite, Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate and organic-silicon-modified fluorocarbon resin is first added according to formula ratio, shredder ground and mixed 3min, add MCMB more subsequently, stir 35min with homogenizer; (3), at 45 DEG C, vinylformic acid, 2 is added again, 4,6-tri(dimethylaminomethyl)phenol, dibutyl tin laurate, zirconium silicate, calcium metasilicate, gas phase aluminium sesquioxide, chlorinated polyvinyl chloride resin, ISOPROPYL PHENYL DIPHENYL PHOSPHATE, N-BUTYL ACETATE, titanium dioxide, steel fiber, peptizer, thinner, iron powder and silicon sol, and stir 40min, obtain acid and alkali-resistance coating.
Embodiment 4
The acid and alkali-resistance coating of the present embodiment is made up of following weight part material: Graphene 35 parts; Organosilane crosslinked polyethylene 35 parts; Trichroite 35 parts; Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate 35 parts; Organic-silicon-modified fluorocarbon resin 35 parts; MCMB 35 parts; 17 parts, vinylformic acid; 2,4,6-tri(dimethylaminomethyl)phenol 17 parts; Dibutyl tin laurate 17 parts; Zirconium silicate 17 parts; Calcium metasilicate 17 parts; Gas phase aluminium sesquioxide 17 parts; Chlorinated polyvinyl chloride resin 17 parts; ISOPROPYL PHENYL DIPHENYL PHOSPHATE 17 parts; N-BUTYL ACETATE 17 parts; Titanium dioxide 17 parts; Steel fiber 17 parts; 17 parts, peptizer; Thinner 17 parts; Iron powder 17 parts; Silicon sol 17 parts.The particle diameter of wherein said Graphene is 40nm.
The preparation method of the acid and alkali-resistance coating of the present embodiment, comprises the steps: (1), prepares burden according to acid and alkali-resistance system component; (2), Graphene, organosilane crosslinked polyethylene, trichroite, Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate and organic-silicon-modified fluorocarbon resin is first added according to formula ratio, shredder ground and mixed 3min, add MCMB more subsequently, stir 35min with homogenizer; (3), at 45 DEG C, vinylformic acid, 2 is added again, 4,6-tri(dimethylaminomethyl)phenol, dibutyl tin laurate, zirconium silicate, calcium metasilicate, gas phase aluminium sesquioxide, chlorinated polyvinyl chloride resin, ISOPROPYL PHENYL DIPHENYL PHOSPHATE, N-BUTYL ACETATE, titanium dioxide, steel fiber, peptizer, thinner, iron powder and silicon sol, and stir 40min, obtain acid and alkali-resistance coating.
Carry out acid and alkali-resistance experiment to the electric power network outdoor case of the acid and alkali-resistance paint prepared by embodiment 1-4, acid resistance is flooded at 5%w/V at 5%w/V sulfuric acid dipping and alkali resistance, and the unchanged time is as follows, and result is as follows:
| Acid resistance | Alkali resistance | |
| Embodiment 1 | 1336 | 1763 |
| Embodiment 2 | 1335 | 1763 |
| Embodiment 3 | 1336 | 1760 |
| Embodiment 4 | 1331 | 1769 |
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present invention or essential characteristic, the present invention can be realized in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present invention is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the present invention.
In addition, be to be understood that, although this specification sheets is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of specification sheets is only for clarity sake, those skilled in the art should by specification sheets integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (4)
1. an electric power network outdoor case acid and alkali-resistance coating, described casing is environment real-time monitoring system casing, is outdoor mechanism case, is provided with humidity sensor, humidity regulator, temperature sensor, temperature regulator in casing, well heater and power supply; It is characterized in that: this acid and alkali-resistance coating is made up of following weight part material: Graphene 35-55 part; Organosilane crosslinked polyethylene 35-55 part; Trichroite 35-55 part; Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate 35-55 part; Organic-silicon-modified fluorocarbon resin 35-55 part; MCMB 35-55 part; Vinylformic acid 1-17 part; 2,4,6-tri(dimethylaminomethyl)phenol 1-17 part; Dibutyl tin laurate 1-17 part; Zirconium silicate 1-17 part; Calcium metasilicate 1-17 part; Gas phase aluminium sesquioxide 1-17 part; Chlorinated polyvinyl chloride resin 1-17 part; ISOPROPYL PHENYL DIPHENYL PHOSPHATE 1-17 part; N-BUTYL ACETATE 1-17 part; Titanium dioxide 1-17 part; Steel fiber 1-17 part; Peptizer 1-17 part; Thinner 1-17 part; Iron powder 1-17 part; Silicon sol 1-17 part.
2. electric power network outdoor case acid and alkali-resistance coating according to claim 1, is characterized in that: this acid and alkali-resistance coating is made up of following weight part material: Graphene 35 parts; Organosilane crosslinked polyethylene 35 parts; Trichroite 35 parts; Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate 35 parts; Organic-silicon-modified fluorocarbon resin 35 parts; MCMB 35 parts; 5 parts, vinylformic acid; 2,4,6-tri(dimethylaminomethyl)phenol 5 parts; Dibutyl tin laurate 5 parts; Zirconium silicate 5 parts; Calcium metasilicate 5 parts; Gas phase aluminium sesquioxide 5 parts; Chlorinated polyvinyl chloride resin 5 parts; ISOPROPYL PHENYL DIPHENYL PHOSPHATE 5 parts; N-BUTYL ACETATE 5 parts; Titanium dioxide 5 parts; Steel fiber 5 parts; 5 parts, peptizer; Thinner 5 parts; Iron powder 5 parts; Silicon sol 5 parts.
3. the electric power network outdoor case acid and alkali-resistance coating according to claim 1 or 3, is characterized in that: the particle diameter of described Graphene is 35-60nm.
4. prepare a method for the acid and alkali-resistance coating described in the claims, it is characterized in that: comprise the steps:
(1), prepare burden according to graphene-based acid and alkali-resistance system component;
(2), Graphene, organosilane crosslinked polyethylene, trichroite, Copolymer Emulsion of Hexafluorobutyl Methacrylate-Acrylate and organic-silicon-modified fluorocarbon resin is first added according to formula ratio, shredder ground and mixed 3min, add MCMB more subsequently, stir 35min with homogenizer;
(3), at 45 DEG C, vinylformic acid, 2 is added again, 4,6-tri(dimethylaminomethyl)phenol, dibutyl tin laurate, zirconium silicate, calcium metasilicate, gas phase aluminium sesquioxide, chlorinated polyvinyl chloride resin, ISOPROPYL PHENYL DIPHENYL PHOSPHATE, N-BUTYL ACETATE, titanium dioxide, steel fiber, peptizer, thinner, iron powder and silicon sol, and stir 40min, obtain acid and alkali-resistance coating.
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| CN110862743A (en) * | 2019-11-21 | 2020-03-06 | 安徽新大陆特种涂料有限责任公司 | Iron oxide red epoxy anticorrosive paint for engineering machinery |
| CN116376412A (en) * | 2023-02-24 | 2023-07-04 | 上海蓝欧化工科技有限公司 | Front-end spray water-based paint for automobile sealing strip, and preparation method and application method thereof |
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| CN116376412A (en) * | 2023-02-24 | 2023-07-04 | 上海蓝欧化工科技有限公司 | Front-end spray water-based paint for automobile sealing strip, and preparation method and application method thereof |
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