CN105135852B - For the continuous drying system of three wastes synthetical recovery treatment - Google Patents
For the continuous drying system of three wastes synthetical recovery treatment Download PDFInfo
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- CN105135852B CN105135852B CN201510587172.8A CN201510587172A CN105135852B CN 105135852 B CN105135852 B CN 105135852B CN 201510587172 A CN201510587172 A CN 201510587172A CN 105135852 B CN105135852 B CN 105135852B
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- 238000001035 drying Methods 0.000 title claims abstract description 58
- 238000011084 recovery Methods 0.000 title abstract description 12
- 239000002699 waste material Substances 0.000 title abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 50
- 239000002002 slurry Substances 0.000 claims abstract description 48
- 239000000843 powder Substances 0.000 claims abstract description 40
- 238000007599 discharging Methods 0.000 claims abstract description 28
- 238000007789 sealing Methods 0.000 claims abstract description 5
- 238000002485 combustion reaction Methods 0.000 claims description 33
- 238000010438 heat treatment Methods 0.000 claims description 23
- 239000002912 waste gas Substances 0.000 claims description 7
- 230000000630 rising effect Effects 0.000 claims description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 36
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 36
- 239000011574 phosphorus Substances 0.000 abstract description 36
- 239000002893 slag Substances 0.000 abstract description 14
- 239000007788 liquid Substances 0.000 abstract description 12
- ONIKNECPXCLUHT-UHFFFAOYSA-N 2-chlorobenzoyl chloride Chemical compound ClC(=O)C1=CC=CC=C1Cl ONIKNECPXCLUHT-UHFFFAOYSA-N 0.000 abstract description 7
- 238000001704 evaporation Methods 0.000 abstract description 6
- 230000008020 evaporation Effects 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 4
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 abstract description 3
- 239000001110 calcium chloride Substances 0.000 abstract description 3
- 229910001628 calcium chloride Inorganic materials 0.000 abstract description 3
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 abstract description 3
- 239000000292 calcium oxide Substances 0.000 abstract description 3
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 abstract description 3
- 238000004134 energy conservation Methods 0.000 abstract description 2
- 239000011499 joint compound Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 18
- 230000005540 biological transmission Effects 0.000 description 9
- 239000011344 liquid material Substances 0.000 description 8
- 230000000694 effects Effects 0.000 description 7
- 239000007789 gas Substances 0.000 description 7
- OBSZRRSYVTXPNB-UHFFFAOYSA-N tetraphosphorus Chemical compound P12P3P1P32 OBSZRRSYVTXPNB-UHFFFAOYSA-N 0.000 description 7
- 230000009286 beneficial effect Effects 0.000 description 6
- 238000009826 distribution Methods 0.000 description 6
- 239000007921 spray Substances 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000003818 cinder Substances 0.000 description 4
- 208000002925 dental caries Diseases 0.000 description 4
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 3
- 238000004220 aggregation Methods 0.000 description 3
- 230000002776 aggregation Effects 0.000 description 3
- 230000000903 blocking effect Effects 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 239000002360 explosive Substances 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 230000004936 stimulating effect Effects 0.000 description 3
- 230000001360 synchronised effect Effects 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 238000007664 blowing Methods 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 239000003245 coal Substances 0.000 description 2
- 238000005485 electric heating Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000010791 quenching Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000004093 laser heating Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000011236 particulate material Substances 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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- Drying Of Solid Materials (AREA)
Abstract
The present invention relates to a kind of continuous drying system for the treatment of three wastes synthetical recovery, the evaporation collection to the phosphorus in phosphorus mud, slag, calcium oxide or calcium chloride are can be applied to, the raffinate treatment of chlorobenzoyl chloride, chemical industry finished product is dried, three wastes synthetical recovery treatment etc..It includes main drying；The main drying includes：Main shaft, multilayer annular housing setting up and down；Each annular housing is matched with the main shaft by center through hole movable sealing, and the scraper plate being distributed in each annular housing is fixed with the main shaft；There is gap between two adjacent annular housings and sealed by blanking channel and be connected；Each annular housing is in heat conduction liquid container；The annular housing of top layer is provided with material inlet and exhaust outlet, and the bottom of the annular housing of bottom is provided with discharging opening.The system is suitable to continuous drying to slurry, powder, and production efficiency is higher and environmentally friendly, safety, energy-conservation；Slurry, powder are through successively evaporating, and volatilization area is larger, so the evaporation efficiency of volatile matter is higher, while the rate of recovery of volatile matter is higher.
Description
Technical field
The present invention relates to a kind of slurry or the continuous drying system of powder, the evaporation to the phosphorus in phosphorus mud, slag is can be applied to
Collection, calcium oxide or calcium chloride, the raffinate treatment of chlorobenzoyl chloride, chemical industry finished product are dried, three wastes synthetical recovery treatment etc..
Background technology
In the prior art, with producing yellow Phosphorus by electric oven, phosphorus mud, phosphorus slag the like waste can be produced, and discarded phosphorus mud, phosphorus slag
In also have substantial portion of yellow phosphorus do not produce completely, so cause the waste of resource.
The existing method for reclaiming yellow phosphorus has steam filtration method, dry blowing method, chemical reagent reaction method etc.；Steam filtration method
It is to be put into phosphorus mud, slag to use steam laser heating in container, it is yellow to turn into finished product after the phosphorus for dissolve phosphorus body refuse, filtering out is refined
Phosphorus, the P elements for still having l 5-20% in phosphorus mud, the slag after processing in this way can not withdraw, and steam consumption quantity is big, raw
The product cycle is (20 days or so) long, pollutes still serious；Dry blowing method is to load phosphorus mud, slag heat iron pan in distillation iron pan, pass through
Phosphorus steam is imported in water bath and is refined into yellow phosphorus by guide pipeline, and this method can not be produced continuously, less efficient, use this side
The P elements for still having l 5-20% in phosphorus mud, slag after method treatment can not withdraw；Chemical reagent reaction method is made using carbon disulfide
Extractant, quenching takes yellow phosphorus, and two methods are advanced earlier above for this method, but its process cycle is long, and yield is small, once quench after taking
The phosphorus that recrement also has 2-5% is remained, and operating procedure is complicated, temperature is difficult to control, and whard to control to the quality of yellow phosphorus.
Chinese patent literature CN1152545 reclaims the Processes and apparatus of yellow phosphorus in disclosing a kind of body refuse from phosphorus.
It is in place of above-mentioned the deficiencies in the prior art：Need to shut down loading, unloading material, it is impossible to realize continuous work, cause production
It is less efficient.
The content of the invention
The technical problem to be solved in the present invention is to provide and a kind of is suitable to the continuous of the slurry continuous drying to slurry or powder
Drying system.
In order to solve the above-mentioned technical problem, it is the invention provides a kind of slurry or the continuous drying system of powder including dry
Dry main frame；The main drying includes：Annular housing that multilayer is coaxially disposed up and down, on the central axis of each annular housing
Main shaft；Multiple scraper plates being distributed in respectively in each annular housing are fixed with the main shaft；Have between two adjacent annular housings
There is gap between chamber, and seal connected by blanking channel；The bottom of the base plate of each annular housing is provided with heating wire, or each annular chamber
Body is in heating container；The annular housing of top layer is provided with material inlet and for discharging from the slurry or powder
The exhaust outlet of volatile matter, the bottom of the annular housing of bottom is provided with discharging opening.
As a kind of scheme：The heating container is a cover body, and a combustion furnace is located at the cover body bottom；The top of the cover body
It is provided with：The feeding mouth communicated with the material inlet of the annular housing of the top layer, and for discharging the waste gas of the combustion furnace
Exhaust outlet；Adjacent annular housing is connected by its central portion upper-lower seal, and forms center in the center of each annular housing
Passage；Wind deflector is provided between the chamber in gap, the outward flange of each wind deflector is connected with the inner wall sealing of the cover body, each wind-guiding
The upper and lower end face of plate respectively and the adjacent wall body of adjacent annular cavity between have gap, the inward flange of each wind deflector with it is described in
There is gap between the outer wall of centre passage.
Alternatively：The heating container is an electric heating liquid container for filling conductive fluid, and the electric heating liquid container leads to
Heat exchanging pipe is crossed to be connected with external heat system.Using heat exchange liquid heat, it can be ensured that each annular housing can obtain fully heat exchange,
Heat exchange is uniform, also ensure that larger heat exchange area.
To the preferred of above-mentioned each scheme, the annular housing between the top layer and the annular housing of bottom is intermediate cavity
Body, at least one middle chamber is provided with exhaust passage.Due to being equipped with slurry or powder, the ring of non-top layer in each annular housing
The gas volatilized in shape cavity not easily passs through the blanking channel and successively discharges upwards, therefore is set on the middle chamber
Exhaust passage, quickly discharges beneficial to gas.
To the preferred of above-mentioned each scheme, screw rod is axially arranged with the exhaust passage, the screw rod is suitable to rotation, in preventing
Between slurry in cavity or powder discharged through the exhaust passage.Output shaft of the outer end of screw rod directly with a motor is connected, or spiral shell
The outer end of bar is coordinated with motor by sprocket wheel or belt wheel transmission.
To the preferred of above-mentioned each scheme, the scraper plate is suitable to be close to the plate top surface of annular housing, to prevent shape on base plate
Into dirty layer, the heat conductivility of base plate is influenceed.
To the preferred of above-mentioned each scheme, the blast pipe being connected on the exhaust outlet is provided with rupture pressure disc and check valve, with
Inflammable and explosive volatile matter is avoided to be exploded in the annular housing.
To the preferred of above-mentioned each scheme, the main shaft is provided with screw thread, and during main shaft rotation, the screw thread is suitable to this
The slurry or powder of the middle and lower part of main shaft deliver to the middle and upper part of the main shaft；The exhaust outlet and exhaust passage are after chilling spray tower
It is connected with for reclaiming the recovery pond of volatile matter, to collect phosphorus or chlorobenzoyl chloride etc..The exhaust outlet of covering on top and a waste gas heat
Can reclaim and processing system is connected, to realize energy-saving and emission-reduction.
To the preferred of above-mentioned each scheme, in a ring, the outward flange of base plate is higher than inward flange to the base plate of the annular housing, with
The centroclinal angle of ring surface for making base plate is 1-5 °；To balance what the material in the annular housing was produced by rotation
Centrifugal force, it is to avoid outward flange aggregation of the material in the neighbouring annular housing, and then ensure drying efficiency and effect.Base plate
The centroclinal angular dimension of ring surface is relevant with material type with the corresponding relation of the rotating speed of main shaft, specific corresponding to relation
Can be obtained by testing.
To the preferred of above-mentioned each scheme, the lower section of the discharging opening is connected with the feeding mouth of a spiral feeder, passes through
The working condition of spiral feeder is controlled, can real-time control discharging speed.
To the preferred of above-mentioned each scheme, the side wall of the annular housing of the bottom is provided with transparent viewing port, with observation
After obtaining the dry materials in the annular housing of the bottom, the spiral feeder discharging is then turned on.
To the preferred of above-mentioned each scheme, in two adjacent annular housings, the base plate of the annular housing in upper strata
On 1 to 4 blanking port length direction it is radially distributed, that is, when working, the length direction of blanking port is suitable to the length with scraper plate
Degree direction is consistent, and when scraper plate promotes material to rotate to the blanking port, radially distributed material is suitable to synchronous whereabouts, relatively
In the blanking port of other angles, feed blocking blanking port can be avoided, it is ensured that volatile matter rises by the blanking port.Each blanking port leads to
The blanking channel is crossed to be connected with the opening on the top board of the annular housing in lower floor；Opening on the top board is in down with this
Blanking port on the base plate of the annular housing of layer is in staggered distribution, to ensure that material is suitable to successively dry.
To the preferred of above-mentioned each scheme, the side of the combustion furnace is provided with for will be during burning material sends into the combustion furnace
Screw rod hoister, in order to coal or combustiblerefuse etc. are sent directly into the combustion furnace；It is provided with combustion furnace for supporting burning
The burning rack of material, the burning rack is provided with criss-cross agitator arm, and the bottom center of the agitator arm is provided with rotating shaft, and the rotating shaft is lived
It is dynamic to coordinate in a pair of axis holes, and the rotating shaft is connected with the output shaft of a reductor by chain gear transmission；The reductor and an electricity
Machine transmission coordinates.When agitator arm slowly rotates, it is suitable to stir fiery heap, prevents cinder etc. from luming；And the fritter cinder by after-flame etc.
Above pushed away from burning rack and fallen.
The method of work of the continuous drying system of above-mentioned slurry or powder, including：
A, (can use and heat heating wire connection power supply, or to connecting in the heat conduction liquid container to the heating of each annular housing
Continuous circulation input thermal conductivity hydrothermal solution heating)；
B, the annular housing that slurry or powder are input into top layer, while making the main axis；
C, slurry or powder successively exchange heat, dry and fall, finally from the ring of bottom under the turning effort of each layer scraper plate
The discharging opening discharge of shape cavity；Volatile matter successively evaporates, up, and exported from the exhaust outlet and exhaust passage, is through collecting
System realizes the collection of volatile matter.
To the preferred of above-mentioned each scheme, the slurry or powder are phosphorus mud, phosphorus slag；The volatile matter is phosphorus.
To the preferred of above-mentioned each scheme, during annular housing each using the burning stove heat, the hot blast of combustion furnace generation from
The cover body bottom enters cover body；Then hot blast is in the presence of the wind deflector, the snakelike rising in gap between the chamber, most
Discharged from the exhaust outlet of the covering on top eventually.
In order to realize to the continuous drying of liquid material or slurry, present invention also offers a kind of continuous drying system, its
Including main drying；The main drying includes：Multilayer cavity setting up and down；Between having between chamber between two adjacent cavitys
Gap, and seal connected by blanking channel；The bottom of the base plate of each cavity is provided with heating wire, or each cavity is located at heat conduction liquid container
In, or the bottom of the main drying is provided with combustion furnace；The cavity of top layer is provided with material inlet and exhaust outlet, the cavity of bottom
Bottom be provided with discharging opening.Annular housing between the top layer and the annular housing of bottom is middle chamber, at least one
Individual middle chamber is provided with exhaust passage；It is axially arranged with screw rod in the exhaust passage, the screw rod is suitable to rotation, to prevent centre
Slurry or powder in cavity are discharged through the exhaust passage；The blast pipe and exhaust passage are after chilling spray tower and are used for back
The recovery pond for receiving volatile matter is connected；In two adjacent cavitys, 1 to 4 blanking on the base plate of the cavity in upper strata
Mouth is connected by the blanking channel with the opening on the top board of the cavity in lower floor；Opening on the top board is in down with this
Blanking port on the base plate of the cavity of layer is in staggered distribution.
Above-mentioned technical proposal of the invention has advantages below compared to existing technology：（1）Main drying entirety of the invention
Small volume, drying efficiency are higher；During work, slurry is input into from top in real time, and successively dries, falls, while by volatile matter
（Such as phosphorus, chlorobenzoyl chloride etc.）Successively evaporate, volatile matter is exported from top vent, and the receipts of volatile matter are realized using collection system
Collection；The slurry or powder of drying are in dry powder body, are discharged in real time from bottom；Therefore, the system is suitable to continuously do slurry, powder
It is dry, that is, it is suitable to charging in real time, discharging, without shutting down loading, unloading material, so production efficiency is higher；（2）Slurry, powder are through successively steaming
Hair, volatilization area is larger, so the evaporation efficiency of volatile matter is higher, while the rate of recovery of volatile matter is higher.To phosphorus mud, slag
In, the unrecovered phosphorus element content in dried phosphorus mud, slag is less than 1%.（3）Main drying of the invention, Ke Yizuo
For chemical reactor, distiller, reaction pot, main shaft and scraper plate can be used with or without according to material type selecting.（4）Due to each
Slurry or powder are equipped with annular housing, the gas volatilized in the annular housing of non-top layer not easily passs through the blanking channel
Successively discharge upwards, therefore exhaust passage is set on the middle chamber, quickly discharged beneficial to gas, beneficial to organic solvent
Reclaim, and prevent the air pressure in each annular housing too high and bring potential safety hazard.（5）The hot blast of combustion furnace generation is in the wind-guiding
In the presence of plate, the snakelike rising in gap between the chamber, make the heat exchange stroke of hot blast and the upper lower wall of each annular housing and
Time is more long, beneficial to fully heat exchange, beneficial to energy-saving and emission-reduction；In addition, making each annular housing to be exchanged heat, it is ensured that larger
Heat exchange area.
Brief description of the drawings
In order that present disclosure is more likely to be clearly understood, below according to specific embodiment and with reference to accompanying drawing,
The present invention is further detailed explanation, wherein
Fig. 1 is the slurry or the structural representation of the continuous drying system of powder in embodiment 1 to 2；
Fig. 2 is the structural representation of the main drying in Fig. 1；
Fig. 3 is the structural representation of the main drying of use electric-heating-wire-heating of the invention；
Fig. 4 is the top view of annular housing of the invention；
Fig. 5 is the A-A sectional structure charts of Fig. 4；
Fig. 6 is the B-B sectional structure charts of Fig. 4；
Fig. 7 is the sectional structure chart of multilayer annular housing setting up and down；
Fig. 8 is the structural representation of the main drying in embodiment 3；
Fig. 9 is the axial section of the multi-layer cavity in Fig. 8；
Figure 10 is the structural representation of the drying system with exhaust passage in embodiment 4；
Figure 11 is the cross-sectional view of the main drying in embodiment 4.
Specific embodiment
Below in conjunction with the accompanying drawings and embodiment the present invention is described in detail.
Specific embodiment
Embodiment 1
See Fig. 1-7, slurry or the continuous drying system of powder that the present embodiment is provided, including：Main drying and the drying
The connected collection system for collecting volatile matter of the exhaust outlet of main frame.
Main drying includes：Main shaft 1, multilayer annular housing 2 setting up and down；Each annular housing 2 is lived by center through hole
Dynamic sealing is matched with the main shaft 1, and the scraper plate 3 being distributed in one by one in each annular housing 2 is fixed with the main shaft 1；Adjacent two
There is gap between chamber between individual annular housing 2, directly exchanged heat with heat-conducting medium or heating wire with the base plate for facilitating annular housing 2,
And then ensure that drying effect.
Sealed by blanking channel 4 between two adjacent annular housings 2 and be connected；The bottom of the base plate of each annular housing 2
Heating wire 5 is provided with, or each annular housing is in heat conduction liquid container 6, or the main drying is located at the top of a combustion furnace 14；Top
The annular housing of layer is provided with material inlet and the exhaust outlet for discharging volatile matter, and the bottom of the annular housing of bottom is provided with use
In the discharging opening for discharging dried slurry or powder.Heat-conducting medium in heat conduction liquid container 6 is conduction oil etc..
The scraper plate 3 is suitable to be close to the plate top surface of annular housing 2, to prevent from forming dirty layer on base plate, influence base plate
Heat conductivility.
The blast pipe 7 being connected on the exhaust outlet is provided with rupture pressure disc 8 and check valve 9, to avoid inflammable and explosive waving
Stimulating food explodes in the annular housing.Wherein, during check valve 9 is suitable to avoid air to pour in down a chimney main drying.
The blast pipe 7 is connected after chilling spray tower 10 with the recovery pond 11 for reclaiming volatile matter, with collect phosphorus or
Chlorobenzoyl chloride etc..
In a ring, the outward flange of base plate 2-3 is higher than inward flange to the base plate 2-3 of the annular housing 2, so that the annular of base plate
The centroclinal angle in face is 1-5 °, to balance the material in the annular chamber 2 because of the centrifugation for rotating and producing around main shaft 1
Power, it is to avoid outward flange aggregation of the material in the neighbouring annular housing 2, and then ensure drying efficiency and effect.Base plate 2-3's
The centroclinal angular dimension of ring surface is relevant with material type with the corresponding relation of the rotating speed of main shaft 1, and specific corresponding to is closed
System can be obtained by testing.
As a kind of selectable implementation method, the feeding mouth phase of the lower section of the discharging opening and a spiral feeder 12
Even, by controlling the working condition of spiral feeder 12, can real-time control discharging speed.
The side wall of the annular housing of the bottom is provided with transparent viewing port, with observe the bottom annular housing
In dry materials after, be then turned on the spiral feeder 12 and discharge, to be discharged again after ensuring dry materials, and ensure volatilization
The abundant collection of thing.
In two adjacent annular housings 2,3 or 4 blanking port 2- on the base plate of the annular housing in upper strata
2；The length direction of each blanking port 2-2 radially, Central Symmetry distribution, that is, when working, the length direction of blanking port 2-2 be suitable to
The length direction of scraper plate 3 is consistent, and when scraper plate 3 promotes material to rotate to blanking port 2-2, radially distributed material is suitable to
Synchronous whereabouts, relative to the blanking port using other angles, can avoid feed blocking blanking port 2-2, it is ensured that volatile matter is by being somebody's turn to do
Blanking port 2-2 rises.
Opening 2-1 phases on top boards of each blanking port 2-2 by the blanking channel 4 with the annular housing in lower floor
Even；The opening 2-1 and blanking port 2-2 that should be on the base plate of the annular housing of lower floor on the top board is in staggered distribution, to ensure
Material is suitable to successively dry.
The hot waste gas of the top discharge of the combustion furnace 14 is input into and passes through from the hot waste gas input port of an air heat-exchange tower 17
Discharged from top after the heat exchanger tube crossed in the air heat-exchange tower 17, the new air and heat exchanger tube for being input into the air heat-exchange tower 17 exchange heat
Afterwards, it is input into the combustion furnace 14 through air-introduced machine 16, to improve the combustion heat value of the fuel in combustion furnace 14, realizes energy-conservation.
Embodiment 2
The method of work of the continuous drying system of slurry or powder described in above-described embodiment 1, including：
A, heating wire 5 first connected into power supply heating, or to continuous circulation input thermal conductivity hydrothermal solution in the heat conduction liquid container 6,
Or heated to each annular housing 2 using the combustion furnace 14 located at the main drying bottom；So that the temperature of the annular housing 2
It is suitable to reach 50-700 DEG C（Actual temp needs to be selected according to different materials）.
B, by pump by slurry or material inlet by helicoid conveyer 13 by powder from the annular housing of top layer
Input, while opening main motor 15 to drive the main shaft 1 to rotate；
C, slurry or powder successively exchange heat, dry and fall, finally from bottom under the turning effort of each layer scraper plate 3
The discharging opening discharge of annular housing；Volatile matter successively evaporates, up, and from exhaust outlet output, realizes waving through collection system
The collection of stimulating food.
The slurry or powder are phosphorus mud, phosphorus slag；The volatile matter is phosphorus.
The slurry or powder can also be slurry or powder containing chlorobenzoyl chloride, or calcium oxide or calcium chloride.
After the plate top surface in the annular housing 2 forms dirty layer, in order to remove the dirty layer, the method for work of use
Including：
Stop sending into material to the main drying, main drying and spiral feeder 12 are opened, by main drying
Material empty；Then, heating wire 5 is connected into power supply heating, or to continuous circulation input thermal conductivity heat in the heat conduction liquid container 6
Liquid, or heated using the combustion furnace 14；The temperature for treating each annular housing is higher than preset value（80-150℃）, stop to described dry
Dry main frame heating, while by cold water（Less than 20 DEG C, the more poorly efficient fruit of water temperature is better）Material inlet from the annular housing of top layer
Input, is then turned on the main motor 15.After dirty layer on the base plate of each annular housing 2 is through rapid expanding with heat and contract with cold, due to dirty layer
The rate that collapses with the base plate 2-3 of stainless steel differs greatly, and each dirty layer is suitable to fragmentation frustillatum, and in each layer scraper plate 3
Under turning effort, successively fall, finally exported from discharging opening.
It is and defeated in the material inlet by pump by slurry from the annular housing of top layer when the slurry is phosphorus mud, phosphorus slag
It is fashionable, to avoid input air, ensuring production safety, in soft bag that the slurry is arranged on a sealing, vacuumizing, the soft bag
It is connected with the pump by pipeline.When the slurry in a soft bag takes out most, pump need to be only closed, connection is another to fill the soft of slurry
Bag, you can continue feeding, realize the continuous work of main drying.
Embodiment 3
If Fig. 8 is to 9, present embodiments provide a kind of for liquid material（Or slurry）Continuous drying system, it is including dry
The collection system for collecting volatile matter that dry main frame is connected with the exhaust outlet of the main drying.
The main drying includes：Multilayer cavity 20 setting up and down；There is gap between two adjacent cavitys 20, and
Sealed by blanking channel and be connected；The bottom of the base plate of each cavity 20 is provided with heating wire 5, or each cavity 20 is located at heat conduction liquid container
In, or the bottom of the main drying is provided with combustion furnace；The cavity of top layer is provided with material inlet and exhaust outlet, the cavity of bottom
Bottom be provided with discharging opening.
In two adjacent cavitys 20,1 to 4 blanking port on the base plate of the cavity in upper strata falls described in
Material passage 4 is connected with the opening on the top board of the cavity in lower floor；Opening and the cavity that lower floor should be on the top board
Blanking port on base plate is in staggered distribution.During work, the material inlet by pump 17 by liquid material from the annular housing of top layer
Input, liquid material falls from the discharging opening of each layer cavity, and is suitable to the underplate heat exchange in the cavity with each layer, so have change
The features such as hot area is larger, heat exchange efficiency is higher；While the small volume of main drying.
The system is used for the continuous drying of liquid material, so without scraper plate, it is adaptable to it is suitable to wave containing chlorobenzoyl chloride, phosphorus etc.
The liquid material of hair.Heating, evaporation of the liquid material by each layer cavity, the volatile matter needed for making evaporates, and is by collecting
System is collected.
The main drying can be as chemical reactor, distiller, reaction pot etc..
Embodiment 4
Such as Fig. 4 to 7 and 10, the slurry of the present embodiment or the continuous drying system of powder, including main drying 24；The drying
Main frame 24 includes：The annular housing 2 that multilayer is coaxially disposed up and down, the main shaft 1 on the central axis of each annular housing 2；Should
3 to 10 scraper plates 3 being distributed in respectively in each annular housing 2 are fixed with main shaft 1；Have between two adjacent annular housings 2
There is gap 25 between chamber, and seal connected by 3 to 5 blanking channels 4；Each annular housing 2 is in heating container；The ring of bottom
The bottom of shape cavity 2 is provided with discharging opening.
The heating container is a cover body 27, and a combustion furnace 14 is located at the bottom of cover body 27；The top of the cover body 27 is provided with：
The feeding mouth 270 communicated with the material inlet of the annular housing 2 of the top layer, and for discharging the waste gas of the combustion furnace 14
Exhaust outlet 271；Adjacent annular housing 2 is connected by its central portion upper-lower seal, and is formed in the center of each annular housing 2
Centre gangway；It is provided with wind deflector 29 between described chamber in gap 25, the inwall of the outward flange of each wind deflector 29 and the cover body 27
It is tightly connected, the upper and lower end face of each wind deflector 29 has gap, each wind-guiding and the adjacent wall body of adjacent annular cavity 2 between respectively
There is gap between the outer wall of the inward flange of plate 29 and the centre gangway.
Annular housing 2 between annular housing 2 in the top layer and bottom is middle chamber, one or all centres
Exhaust passage 30 is connected with the side wall of cavity.Due to being equipped with slurry or powder, the annular chamber of non-top layer in each annular housing 2
The gas volatilized in body 2 not easily passs through the successively discharge upwards of the blanking channel 4, therefore the row of setting on the middle chamber
Gas passage 30, quickly discharges beneficial to gas.
Screw rod 31 is axially arranged with the exhaust passage 30, the small―gap suture of screw rod 31 coordinates in the exhaust passage 30 and suitable
In rotation, to prevent slurry or powder in middle chamber from being discharged through the exhaust passage 30.The outer end of screw rod 31 is directly electric with one
The output shaft of machine is connected, or the outer end of screw rod 31 is coordinated with motor by sprocket wheel or belt wheel transmission.
The scraper plate 3 is suitable to be close to the plate top surface of annular housing 2, to prevent from forming dirty layer on base plate, influence base plate
Heat conductivility.
The blast pipe 7 being connected on the exhaust outlet 271 is provided with rupture pressure disc and check valve, to avoid inflammable and explosive waving
Stimulating food explodes in the annular housing 2.
The main shaft 1 is provided with screw thread 26, and during the main shaft 1 rotation, the screw thread 26 is suitable to the middle and lower part of the main shaft 1
Slurry or powder deliver to the middle and upper part of the main shaft 1；The exhaust outlet 271 and exhaust passage 30 after chilling spray tower 10 with
It is connected in the recovery pond 11 for reclaiming volatile matter.The exhaust outlet at the top of cover body 27 is reclaimed and the phase of processing system 32 with a heat energy from waste gas
Even, to realize energy-saving and emission-reduction.
The side of the combustion furnace 14 is provided with for the material that burns to be sent into the screw rod hoister 33 in the combustion furnace 14；Combustion
The burning rack for supporting burning material is provided with burning stove 14, the burning rack is provided with criss-cross agitator arm, the agitator arm
Bottom center is provided with rotating shaft, and the rotating shaft activity coordinates in a pair of axis holes, and the rotating shaft passes through chain with the output shaft of a reductor
Wheel drive connection；The reductor and motor transmission coordinate.
In a ring, the outward flange of base plate is higher than inward flange to the base plate of the annular housing 2, so that the annular of base plate is in
The inclined angle of the heart is 1-5 °；To balance the material in the annular housing 2（Especially powder or little particulate material）Because of rotation
The centrifugal force of generation, it is to avoid outward flange aggregation of the material in the neighbouring annular housing 2, and then ensure drying efficiency and effect
Really.The centroclinal angular dimension of ring surface of base plate is relevant with material type with the corresponding relation of the rotating speed of main shaft 1, specifically
Corresponding relation can by test obtain.
The lower section of the discharging opening is connected with the feeding mouth of a spiral feeder 12, by controlling spiral feeder 12
Working condition, can real-time control discharging speed.
The side wall of the annular housing 2 of the bottom is provided with transparent viewing port, with observe the bottom annular chamber
After dry materials in body 2, the spiral feeder discharging is then turned on.
In two adjacent annular housings 2,1 to 4 blanking port 2- on the base plate of the annular housing 2 in upper strata
1 length direction is radially distributed, that is, when working, the length direction of blanking port 2-1 be suitable to it is consistent with the length direction of scraper plate 3,
When scraper plate 3 promotes material to rotate to blanking port 2-1, radially distributed material is suitable to synchronous whereabouts, relative to other
The blanking port 2-1 of angle, can avoid feed blocking blanking port, it is ensured that volatile matter rises by blanking port 2-1.Each blanking port 2-
1 is connected by the blanking channel 4 with the opening on the top board of the annular housing 2 in lower floor；Opening on the top board with should
Blanking port 2-1 on the base plate of the annular housing 2 in lower floor is in staggered distribution, to ensure that material is suitable to successively dry.
The side of the combustion furnace 14 is provided with for the material that burns to be sent into the screw rod hoister in the combustion furnace 14, so as to
In coal or combustiblerefuse etc. are sent directly into the combustion furnace 14；The burning for supporting burning material is provided with combustion furnace 14
Frame, the burning rack is provided with criss-cross agitator arm, and the bottom center of the agitator arm is provided with rotating shaft, and the rotating shaft activity coordinates one
In to axis hole, and the rotating shaft is connected with the output shaft of a reductor by chain gear transmission；The reductor and motor transmission coordinate.
When agitator arm slowly rotates, it is suitable to stir fiery heap, prevents cinder etc. from luming；And the fritter cinder by after-flame etc. is above pushed away from burning rack
Fall.
The method of work of the continuous drying system of above-mentioned slurry or powder, including：
A, heated to each annular housing 2；
B, the annular housing 2 that slurry or powder are input into top layer, while rotating the main shaft 1；
C, slurry or powder successively exchange heat, dry and fall, finally from bottom under the turning effort of each layer scraper plate 3
The discharging opening discharge of annular housing 2；Volatile matter successively evaporates, up, and exported from the exhaust outlet 271 and exhaust passage 30,
The collection of volatile matter is realized through collection system.
The slurry or powder are phosphorus mud, phosphorus slag；The volatile matter is phosphorus.
When heating each annular housing 2 using the combustion furnace 14, the hot blast that the combustion furnace 14 is produced is from the cover body 27
Bottom enters cover body 27；Then hot blast is in the presence of the wind deflector 29, the snakelike rising in gap 25 between described chamber, most
Eventually from the exhaust outlet discharge at the top of the cover body 27.
Embodiment 5
On the basis of embodiment 3, the present embodiment for liquid material or the continuous drying system of slurry, exist as follows
Modification：
Annular housing 2 between annular housing 2 in the top layer and bottom is middle chamber, one or all centres
Exhaust passage 30 is connected with the side wall of cavity.
It is axially arranged with screw rod in the exhaust passage 30, the screw rod small―gap suture coordinates in the exhaust passage 30 and is suitable to rotation
Turn, to prevent slurry or powder in middle chamber from being discharged through the exhaust passage 30.
Specifically, output shaft of the outer end of screw rod directly with a motor is connected, or the outer end of screw rod passes through sprocket wheel with motor
Or belt wheel transmission coordinates.
The blast pipe 7 and exhaust passage 30 are connected after chilling spray tower with for reclaiming the recovery pond of volatile matter.
The side of the combustion furnace 14 is provided with for the material that burns to be sent into the screw rod hoister in the combustion furnace 14；Burning
The burning rack for supporting burning material is provided with stove 14, the burning rack is provided with criss-cross agitator arm, the bottom of the agitator arm
Portion center is provided with rotating shaft, and the rotating shaft activity coordinates in a pair of axis holes, and the rotating shaft passes through sprocket wheel with the output shaft of a reductor
Drive connection；The reductor and motor transmission coordinate.
Obviously, above-described embodiment is only intended to clearly illustrate example of the present invention, and is not to of the invention
The restriction of implementation method.For those of ordinary skill in the field, it can also be made on the basis of the above description
The change or variation of its multi-form.There is no need and unable to be exhaustive to all of implementation method.And these belong to this hair
Obvious change that bright spirit is extended out or among changing still in protection scope of the present invention.
Claims (1)
1. a kind of continuous drying system of slurry or powder, including main drying；It is characterized in that the main drying includes：Multilayer
Annular housing, the main shaft on the central axis of each annular housing being coaxially disposed up and down；
Multiple scraper plates being distributed in respectively in each annular housing are fixed with the main shaft；
There is gap between chamber between two adjacent annular housings, and seal connected by blanking channel；
Each annular housing is in heating container；
The annular housing of top layer is provided with material inlet and for discharging the exhaust from the volatile matter in the slurry or powder
Mouthful, the bottom of the annular housing of bottom is provided with discharging opening；
The heating container is a cover body, and a combustion furnace is located at the cover body bottom；It is provided with the top of the cover body：With the top layer
The feeding mouth that the material inlet of annular housing is communicated, and for discharging the exhaust outlet of the waste gas of the combustion furnace；Adjacent ring
Shape cavity is connected by its central portion upper-lower seal, and forms centre gangway in the center of each annular housing；Gap between the chamber
In be provided with wind deflector, the outward flange of each wind deflector is connected with the inner wall sealing of the cover body, the upper and lower end face of each wind deflector difference
There is gap and the adjacent wall body of adjacent annular cavity between, between the inward flange of each wind deflector and the outer wall of the centre gangway
With gap；
The hot blast of combustion furnace generation enters cover body from the cover body bottom；Then hot blast is in the presence of the wind deflector, in institute
Snakelike rising in gap between chamber is stated, is finally discharged from the exhaust outlet of the covering on top.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510587172.8A CN105135852B (en) | 2013-01-04 | 2013-10-29 | For the continuous drying system of three wastes synthetical recovery treatment |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201320001300 | 2013-01-04 | ||
| CN2013200013002 | 2013-01-04 | ||
| CN201510587172.8A CN105135852B (en) | 2013-01-04 | 2013-10-29 | For the continuous drying system of three wastes synthetical recovery treatment |
| CN201310524780.5A CN103591781B (en) | 2013-01-04 | 2013-10-29 | The continuous drying system of slurry or powder |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310524780.5A Division CN103591781B (en) | 2013-01-04 | 2013-10-29 | The continuous drying system of slurry or powder |
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| CN105135852A CN105135852A (en) | 2015-12-09 |
| CN105135852B true CN105135852B (en) | 2017-06-27 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510586768.6A Active CN105241223B (en) | 2013-01-04 | 2013-10-29 | A kind of continuous drying system of slurry or powder |
| CN201310524780.5A Active CN103591781B (en) | 2013-01-04 | 2013-10-29 | The continuous drying system of slurry or powder |
| CN201510585524.6A Active CN105197903B (en) | 2013-01-04 | 2013-10-29 | Drying system for the processing of calcium oxide, calcium chloride or chlorobenzoyl chloride raffinate |
| CN201510586769.0A Expired - Fee Related CN105157396B (en) | 2013-01-04 | 2013-10-29 | Continuous drying system and its method of work for the processing of three wastes synthetical recovery |
| CN201510585320.2A Active CN105202880B (en) | 2013-01-04 | 2013-10-29 | The continuous drying system of slurry or powder |
| CN201510587172.8A Active CN105135852B (en) | 2013-01-04 | 2013-10-29 | For the continuous drying system of three wastes synthetical recovery treatment |
| CN201320676779.XU Withdrawn - After Issue CN203668005U (en) | 2013-01-04 | 2013-10-29 | Main drying machine of continuous drying system for slurry or powder |
| CN201310522646.1A Active CN103591780B (en) | 2013-01-04 | 2013-10-29 | The main drying of the continuous drying system of slurry or powder |
| CN201510587192.5A Active CN105197904B (en) | 2013-01-04 | 2013-10-29 | Continuous drying system is used in the processing of three wastes synthetical recovery |
| CN201510587175.1A Active CN105157397B (en) | 2013-01-04 | 2013-10-29 | A kind of method of work of the continuous drying system of slurry or powder |
| CN201510586724.3A Active CN105236367B (en) | 2013-01-04 | 2013-10-29 | The drying system collected for the evaporation to the phosphorus in phosphorus mud, slag |
Family Applications Before (5)
| Application Number | Title | Priority Date | Filing Date |
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| CN201510586768.6A Active CN105241223B (en) | 2013-01-04 | 2013-10-29 | A kind of continuous drying system of slurry or powder |
| CN201310524780.5A Active CN103591781B (en) | 2013-01-04 | 2013-10-29 | The continuous drying system of slurry or powder |
| CN201510585524.6A Active CN105197903B (en) | 2013-01-04 | 2013-10-29 | Drying system for the processing of calcium oxide, calcium chloride or chlorobenzoyl chloride raffinate |
| CN201510586769.0A Expired - Fee Related CN105157396B (en) | 2013-01-04 | 2013-10-29 | Continuous drying system and its method of work for the processing of three wastes synthetical recovery |
| CN201510585320.2A Active CN105202880B (en) | 2013-01-04 | 2013-10-29 | The continuous drying system of slurry or powder |
Family Applications After (5)
| Application Number | Title | Priority Date | Filing Date |
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| CN201320676779.XU Withdrawn - After Issue CN203668005U (en) | 2013-01-04 | 2013-10-29 | Main drying machine of continuous drying system for slurry or powder |
| CN201310522646.1A Active CN103591780B (en) | 2013-01-04 | 2013-10-29 | The main drying of the continuous drying system of slurry or powder |
| CN201510587192.5A Active CN105197904B (en) | 2013-01-04 | 2013-10-29 | Continuous drying system is used in the processing of three wastes synthetical recovery |
| CN201510587175.1A Active CN105157397B (en) | 2013-01-04 | 2013-10-29 | A kind of method of work of the continuous drying system of slurry or powder |
| CN201510586724.3A Active CN105236367B (en) | 2013-01-04 | 2013-10-29 | The drying system collected for the evaporation to the phosphorus in phosphorus mud, slag |
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| CN (11) | CN105241223B (en) |
Families Citing this family (9)
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| CN105241223B (en) * | 2013-01-04 | 2017-06-13 | 何泽波 | A kind of continuous drying system of slurry or powder |
| CN103925779A (en) * | 2014-03-21 | 2014-07-16 | 沈阳新思维数控机床有限公司 | Efficient vertical pyrolysis drying equipment |
| CN106839739B (en) * | 2014-04-09 | 2019-10-15 | 江苏迪赛司自动化工程有限公司 | The working method of continuous drying system for chemical residual liquor processing |
| CN109569456A (en) * | 2018-12-28 | 2019-04-05 | 宁夏红山河食品股份有限公司 | A kind of microcapsule embedded high shear mixing device |
| CN110645777A (en) * | 2019-10-15 | 2020-01-03 | 江苏双虎环保节能设备科技有限公司 | Drying system and working method thereof |
| CN111892028B (en) * | 2020-07-20 | 2022-11-29 | 云南煜锜环保科技有限公司 | Method for recovering elemental phosphorus by distillation of phosphorus sludge |
| CN112254496A (en) * | 2020-09-25 | 2021-01-22 | 榆林学院 | Coal slime collection device |
| CN112923692A (en) * | 2021-02-01 | 2021-06-08 | 抚州市鹤达实业有限公司 | Rotary dehydration device for modified starch |
| CN116678197B (en) * | 2023-08-02 | 2023-09-29 | 江苏金陵干燥科技有限公司 | Energy-saving environment-friendly spiral type disc vacuum drying equipment |
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- 2013-10-29 CN CN201320676779.XU patent/CN203668005U/en not_active Withdrawn - After Issue
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Also Published As
| Publication number | Publication date |
|---|---|
| CN105197903A (en) | 2015-12-30 |
| CN103591781B (en) | 2015-11-04 |
| CN105157396B (en) | 2017-09-29 |
| CN105202880B (en) | 2017-06-13 |
| CN105197904B (en) | 2017-09-29 |
| CN103591780A (en) | 2014-02-19 |
| CN105157397A (en) | 2015-12-16 |
| CN203668005U (en) | 2014-06-25 |
| CN103591780B (en) | 2015-11-18 |
| CN105241223A (en) | 2016-01-13 |
| CN105236367A (en) | 2016-01-13 |
| CN105202880A (en) | 2015-12-30 |
| CN105157396A (en) | 2015-12-16 |
| CN105236367B (en) | 2017-09-29 |
| CN105241223B (en) | 2017-06-13 |
| CN105135852A (en) | 2015-12-09 |
| CN103591781A (en) | 2014-02-19 |
| CN105197903B (en) | 2017-09-29 |
| CN105157397B (en) | 2017-09-29 |
| CN105197904A (en) | 2015-12-30 |
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Inventor after: Yuan Qixia Inventor after: Li You Inventor after: Li Guo Inventor after: Lin Huiling Inventor before: Request for anonymity |
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Denomination of invention: Continuous drying system for three-waste comprehensive recycling treatment Effective date of registration: 20171214 Granted publication date: 20170627 Pledgee: Maoming silver pawn Co.,Ltd. Pledgor: Lin Huiling Registration number: 2017440000181 |
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