CN105133387A - Coloring agent for wig composite fiber and capable of increasing smoothness and preparation method of coloring agent - Google Patents
Coloring agent for wig composite fiber and capable of increasing smoothness and preparation method of coloring agent Download PDFInfo
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- CN105133387A CN105133387A CN201510568995.6A CN201510568995A CN105133387A CN 105133387 A CN105133387 A CN 105133387A CN 201510568995 A CN201510568995 A CN 201510568995A CN 105133387 A CN105133387 A CN 105133387A
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- Prior art keywords
- coloring agent
- polyvinyl alcohol
- wig
- composite fiber
- smoothness
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Abstract
The invention discloses a coloring agent for wig composite fiber, and the coloring agent is capable of increasing smoothness. According to the coloring agent, reactive dyes are used for preparing dye liquor; cationization treatment is performed on polyvinyl alcohol by utilizing cationic etherified starch; the reactive dye liquor prepared in a way that the cationic polyvinyl alcohol reacts with the reactive dyes has high adhesion and dye uniformity, and has certain retarding and protecting effects, and the dyeing effect of the composite fiber is improved; an added oxidized polyethylene wax emulsion is adhered to the surface of the composite fiber, so as to form a soft anti-pollution waterproof coating, and good smoothness is given to the wig fiber. The wig fiber treated by utilizing the coloring agent provided by the invention is uniform and firm in color, is easy to care and clean and has the advantages of toughness, durability and good hand feeling.
Description
Technical field
The present invention relates to wig coloring agent technical field, particularly relate to a kind of wig composite fibre coloring agent improving smoothness and preparation method thereof.
Background technology
Wig is very common in daily life, the material of wig is also varied, wherein apply wider mainly artificial compounded fiber, wherein a class obtains with protein and the blend spinning of the material such as polyacrylonitrile, polyvinyl chloride, it has and really sends out the texture and feel that compare favourably, intensity, toughness and the performance such as fire-retardant are also better, and the market response is better.Because the color of consumer to wig has different demands, the dyeing of wig is an important link in process of production, swelling, sex change, the unequal situation of dyeing is easily there is in conventional coloring agent when processing above-mentioned composite fibre, composite fibre is caused to lose due intensity and toughness, fall flat, and the security of coloring agent itself also has problems.
Summary of the invention
The object of the invention is exactly the defect in order to make up prior art, provides a kind of wig composite fibre coloring agent improving smoothness and preparation method thereof.
The present invention is achieved by the following technical solutions:
Improve a wig composite fibre coloring agent for smoothness, this coloring agent is made up of the raw material of following weight portion: REACTIVE DYES 10-12, calgon 1-2, solid content are that oxidized polyethylene wax emulsion 4-5, the fatty alcohol-polyoxyethylene ether 0.2-0.3 of 20-25%, polyvinyl alcohol 4-5, acetic acid/sodium acetate buffer are appropriate, CATION etherification starch 0.4-0.5, Sodium hydroxide q. s, deionized water 150-180.
Described a kind of wig composite fibre coloring agent improving smoothness and preparation method thereof, its spy is, described preparation method is:
(1) first polyvinyl alcohol is added in the deionized water of 20-30 weight portion, be heated to 80-90 DEG C, be stirred to after it dissolves completely and be cooled to 40-50 DEG C, add CATION etherification starch subsequently, and be 7-8 by sodium hydrate regulator solution pH value, high-speed stirred hybrid reaction 2-3h, obtains cationized polyvinyl alcohol-etherification starch solution for standby;
(2) REACTIVE DYES is added in remaining deionized water, the aqueous solution is heated to 50-60 DEG C, add other residual components except acetic acid/sodium acetate buffer subsequently again, be uniformly mixed 40-50min, adding cationized polyvinyl alcohol-etherification starch solution prepared by step (1) subsequently again, is 7-7.5 by sodium hydrate regulator solution pH value, continues mix and blend reaction 40-50min, reaction terminates rear acetic acid/sodium acetate buffer regulator solution to neutrality, after being cooled to room temperature and get final product.
Advantage of the present invention is: with REACTIVE DYES preparation dye liquor, and utilize CATION etherification starch to carry out cationization process to polyvinyl alcohol, the active dye liquor that the polyvinyl alcohol of cationization and REACTIVE DYES prepare after reacting has high cementability and equalization, there is certain slow dye, protection effect, improve the Color of composite fibre, the oxidized polyethylene wax emulsion added sticks to composite fiber surface and forms anti-soil, water-fast, soft coating, give the smoothness that wig fiber is good, wig fiber colour after the coloring agent process utilizing the present invention to prepare is evenly firm, be easy to arrange clean, tough durable, feel is good.
Detailed description of the invention
The coloring agent of this embodiment is made up of the raw material of following weight portion: REACTIVE DYES 10, calgon 1, solid content are oxidized polyethylene wax emulsion 4, fatty alcohol-polyoxyethylene ether 0.2, polyvinyl alcohol 4, acetic acid/sodium acetate buffer appropriate, CATION etherification starch 0.4, Sodium hydroxide q. s, the deionized water 150 of 20%.
The preparation method of this coloring agent is:
(1) first polyvinyl alcohol is added in the deionized water of 20 weight portions, be heated to 80 DEG C, be stirred to after it dissolves completely and be cooled to 40 DEG C, add CATION etherification starch subsequently, and be 7 by sodium hydrate regulator solution pH value, high-speed stirred hybrid reaction 2h, obtains the etherified starch solution of cationized polyvinyl for subsequent use;
(2) REACTIVE DYES is added in remaining deionized water, the aqueous solution is heated to 50 DEG C, add other residual components except acetic acid/sodium acetate buffer subsequently again, be uniformly mixed 40min, adding the etherified starch solution of cationized polyvinyl prepared by step (1) subsequently again, is 7 by sodium hydrate regulator solution pH value, continues mix and blend reaction 40min, reaction terminates rear acetic acid/sodium acetate buffer regulator solution to neutrality, after being cooled to room temperature and get final product.
Protein-the polyacrylonitrile composite fiber of the present embodiment coloring agent to wig is carried out dyeing process, the dye-uptake of composite fibre reaches 97.4%, and water-fastness COLOR FASTNESS is Pyatyi, and color fastness to light is Pyatyi, composite fibre intensity is 3.7CN/dtex, and elongation at break is 40.1%; The composite fibre look obtained is spent seldom, and bright color is even, and smooth being easy to is arranged.
Claims (2)
1. one kind can be improved the wig composite fibre coloring agent of smoothness, it is characterized in that, this coloring agent is made up of the raw material of following weight portion: REACTIVE DYES 10-12, calgon 1-2, solid content are that oxidized polyethylene wax emulsion 4-5, the fatty alcohol-polyoxyethylene ether 0.2-0.3 of 20-25%, polyvinyl alcohol 4-5, acetic acid/sodium acetate buffer are appropriate, CATION etherification starch 0.4-0.5, Sodium hydroxide q. s, deionized water 150-180.
2. a kind of wig composite fibre coloring agent improving smoothness and preparation method thereof as claimed in claim 1, its spy is, described preparation method is:
(1) first polyvinyl alcohol is added in the deionized water of 20-30 weight portion, be heated to 80-90 DEG C, be stirred to after it dissolves completely and be cooled to 40-50 DEG C, add CATION etherification starch subsequently, and be 7-8 by sodium hydrate regulator solution pH value, high-speed stirred hybrid reaction 2-3h, obtains cationized polyvinyl alcohol-etherification starch solution for standby;
(2) REACTIVE DYES is added in remaining deionized water, the aqueous solution is heated to 50-60 DEG C, add other residual components except acetic acid/sodium acetate buffer subsequently again, be uniformly mixed 40-50min, adding cationized polyvinyl alcohol-etherification starch solution prepared by step (1) subsequently again, is 7-7.5 by sodium hydrate regulator solution pH value, continues mix and blend reaction 40-50min, reaction terminates rear acetic acid/sodium acetate buffer regulator solution to neutrality, after being cooled to room temperature and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510568995.6A CN105133387A (en) | 2015-09-09 | 2015-09-09 | Coloring agent for wig composite fiber and capable of increasing smoothness and preparation method of coloring agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510568995.6A CN105133387A (en) | 2015-09-09 | 2015-09-09 | Coloring agent for wig composite fiber and capable of increasing smoothness and preparation method of coloring agent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105133387A true CN105133387A (en) | 2015-12-09 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510568995.6A Pending CN105133387A (en) | 2015-09-09 | 2015-09-09 | Coloring agent for wig composite fiber and capable of increasing smoothness and preparation method of coloring agent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105133387A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1094945A (en) * | 1993-05-08 | 1994-11-16 | 雷传喜 | The compound method of non-washing quick hair dyeing liquor |
| CN102051826A (en) * | 2010-11-12 | 2011-05-11 | 许昌恒源发制品股份有限公司 | Rapid dyeing assistant for imitation hair and preparation method thereof |
| CN103582474A (en) * | 2011-05-27 | 2014-02-12 | 宝洁公司 | Soluble solid hair coloring article |
| CN103596624A (en) * | 2011-05-27 | 2014-02-19 | 宝洁公司 | Soluble solid hair coloring article |
-
2015
- 2015-09-09 CN CN201510568995.6A patent/CN105133387A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1094945A (en) * | 1993-05-08 | 1994-11-16 | 雷传喜 | The compound method of non-washing quick hair dyeing liquor |
| CN102051826A (en) * | 2010-11-12 | 2011-05-11 | 许昌恒源发制品股份有限公司 | Rapid dyeing assistant for imitation hair and preparation method thereof |
| CN103582474A (en) * | 2011-05-27 | 2014-02-12 | 宝洁公司 | Soluble solid hair coloring article |
| CN103596624A (en) * | 2011-05-27 | 2014-02-19 | 宝洁公司 | Soluble solid hair coloring article |
Non-Patent Citations (2)
| Title |
|---|
| 丁彤等: "《中国化工产品大全 下》", 31 October 1994, 化学工业出版社 * |
| 侯毓汾等: "《染料化学》", 30 June 1994, 化学工业出版社 * |
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| PB01 | Publication | ||
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| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20151209 |