CN105133316A - Fabric conditioner and preparation method thereof - Google Patents
Fabric conditioner and preparation method thereof Download PDFInfo
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- CN105133316A CN105133316A CN201510631838.5A CN201510631838A CN105133316A CN 105133316 A CN105133316 A CN 105133316A CN 201510631838 A CN201510631838 A CN 201510631838A CN 105133316 A CN105133316 A CN 105133316A
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Abstract
The invention discloses a fabric conditioner and a preparation method thereof, and relates to the field of washing agents. The fabric conditioner comprises, by mass, 1-10 parts of palmityl quaternary ammonium ester, 0.1-5 parts of a cation thickening agent, 0.1-3 parts of essence, 0.01-1 part of caisson and the balance pure water. The preparation method comprises the steps that the pure water is added into a reaction kettle and heated to the temperature of 50-60 DEG C, the 1-10 parts of palmityl quaternary ammonium ester is added and stirring is performed for 20-30 min in a heat-preservation mode; then, the 0.1-5 parts of the cation thickening agent is added, stirring is performed for 5-10 min, and then the temperature is decreased to be lower than 40 DEG C; the 0.1-3 parts of essence and the 0.01-1 part of caisson are added, even stirring is performed, and then the mixture is filtered through a filter net with the mesh size larger than or equal to 240 to obtain a finished product. The fabric conditioner is low in cost, and the preparation difficulty is small.
Description
Technical field
The present invention relates to detergent applications, be specifically related to a kind of fabric softener and preparation method thereof.
Background technology
Clothing is usually woven by very thin linen-cotton or chemical fiber and forms, in the process of washing, after tiny fibrous absorbent, the frictional force on surface becomes large, during clothing phase mutual friction cleaning, fiber is easily wound around, intertwine, and frictional force is crossed conference and caused rupturing; Meanwhile, the alkaline matter contained in washing agent can corrode fiber, causes the ductility of fiber and elasticity to reduce, and then causes clothing to be out of shape, to fade and hardening.
Hardening for alleviating clothing, usually add containing benzyl acetate when washing, phenmethylol, citrene, linalool, the softener of chloroform etc., softener evenly can form diaphragm at the fiber surface of clothing, coefficient of friction between fiber is reduced, mobility strengthens, intrinsic level and smooth of fiber, extend, compression performance have also been obtained recovery, so fabric becomes more soft, fluffy, flexible, but, benzyl acetate, phenmethylol, citrene, linalool, after chloroform Long-Time Service, easily human body is damaged, therefore, select ester based quaternary ammonium salt at present, Gemini cationic softener prepares softener, but existing softener can add silicone oil usually, thickener, a large amount of composition such as Chinese medical extract, not only improve softener cost, and increase preparation difficulty.
Summary of the invention
For the defect existed in prior art, the object of the present invention is to provide a kind of fabric softener and preparation method thereof, not only cost is lower, and preparation difficulty is less.
For reaching above object, the technical scheme that the present invention takes is: a kind of fabric softener, by parts by mass, in every 100 parts of fabric softeners, is following composition:
On the basis of technique scheme, described cationic thickener is REWOQUATDM730.
On the basis of technique scheme, described essence is lavender oil, lily essence or cream jasmin france.
A preparation method for fabric softener according to any one of claims 1 to 3, comprises the following steps:
Pure water is added reactor and is heated to 50 ~ 60 DEG C, add 1 ~ 10 part of palmityl ester quat and after insulated and stirred 20 ~ 30min, add 0.1 ~ 5 part of cationic thickener, be cooled to lower than 40 DEG C after stirring 5 ~ 10min, add 0.1 ~ 3 part of essence and 0.01 ~ 1 part of KF88, after stirring, after being more than or equal to 240 object strainer filterings by order number, obtain finished product.
Compared with prior art, the invention has the advantages that:
(1) fabric softener in the present invention, in every 100 parts of fabric softeners, for following composition: 1 ~ 10 part of palmityl ester quat, 0.1 ~ 5 part of cationic thickener, in use, cationic surfactant can be adsorbed on fiber surface and form monomolecular film, between hydrophobic chain fiber directly being rubbed occur in cationic surfactant, and then the fibrous fracture avoiding direct friction between fiber to cause and accumulation of static electricity, and then prevent clothing from hardening and distortion.Cationic thickener can not only make palmityl ester quat dispersed, and can act synergistically with palmityl ester quat, strengthens the submissive effect of palmityl ester quat.
(2) fabric softener in the present invention, under the following conditions: softener is 1:8 ~ 12 with the ratio of the use amount of water, treatment temperature is 15 ~ 30 DEG C, the pH value of water is 5 ~ 7, be under the condition of 5min in soak time, the pliability measuring clothing is greater than 31/mN, confficient of static friction is less than 0.4, angle of wetting is 70 ~ 100 °, creasy recovery angle is greater than 100 °, it can thus be appreciated that, the fabric softener of the embodiment of the present invention is under the condition that use amount is less, the pliability of clothing can be increased, reduce the coefficient of friction between clothing, reduce the angle of wetting of clothing, clothing is made to have better wettability power, and there is good wrinkling resistance.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
The embodiment of the present invention provides a kind of fabric softener, by parts by mass, in every 100 parts of fabric softeners, is following composition:
Palmityl ester quat is cationic surfactant, in use, cationic surfactant can be adsorbed on fiber surface and form monomolecular film, between hydrophobic chain fiber directly being rubbed occur in cationic surfactant, and then the fibrous fracture avoiding direct friction between fiber to cause and accumulation of static electricity, and then prevent clothing from hardening and distortion.
Cationic thickener can be selected according to actual needs, and in the embodiment of the present invention, cationic active agent is REWOQUATDM730 (a kind of thickener for cationic softener, also referred to as DM730).REWOQUATDM730 can not only make palmityl ester quat dispersed, and can act synergistically with palmityl ester quat, strengthens the submissive effect of palmityl ester quat.
Essence is selected according to actual needs, in the embodiment of the present invention, selects lavender oil, can use other essence such as lily essence, cream jasmin france.
By the fabric softener in the embodiment of the present invention in actual use, under the following conditions: softener is 1:8 ~ 12 with the ratio of the use amount of water, treatment temperature is 15 ~ 30 DEG C, the pH value of water is 5 ~ 7, be under the condition of 5min in soak time, the pliability measuring clothing is greater than 31/mN, confficient of static friction is less than 0.4, angle of wetting is 70 ~ 100 °, creasy recovery angle is greater than 100 °, it can thus be appreciated that, the fabric softener of the embodiment of the present invention is under the condition that use amount is less, the pliability of clothing can be increased, reduce the coefficient of friction between clothing, reduce the angle of wetting of clothing, clothing is made to have better wettability power, and there is good wrinkling resistance.
Because conventional running water pH value is 5 ~ 7, normal temperature is 15 ~ 30 DEG C, and therefore, the result of use of the softener in the embodiment of the present invention under daily condition is better, obtains requiring lower, can be widely used service condition.
Wherein, softener and the ratio of the use amount of water are 1:10, treatment temperature is 20 DEG C, and the pH value of water is 6, are under the condition of 5min in soak time, measuring the pliability obtaining clothing is 34/mN, and confficient of static friction is 0.32, angle of wetting is 70 °, creasy recovery angle is 157 °.
In sum, although the comparison of ingredients of the softener in the embodiment of the present invention is simple, and the palmityl ester quat used, cationic thickener are usual component, and are lower-cost component, but with use in prior art Multiple components composite compared with, can reduce costs.
A preparation method for fabric softener, comprises the following steps:
Pure water is added reactor and is heated to 50 ~ 60 DEG C, add 1 ~ 10 part of palmityl ester quat and after insulated and stirred 20 ~ 30min, add 0.1 ~ 5 part of cationic thickener, be cooled to lower than 40 DEG C after stirring 5 ~ 10min, add 0.1 ~ 3 part of essence and 0.01 ~ 1 part of KF88, after stirring, after being more than or equal to 240 object strainer filterings by order number, obtain finished product.
In the embodiment of the present invention, the preparation method of the preparation method of fabric softener is fairly simple, and preparation time is shorter, and temperature is lower, and preparation cost is lower, difficulty is lower.
Below, by 3 embodiments, preparation method of the present invention is described in detail.
Embodiment 1
Pure water is added reactor and is heated to 50 DEG C, add 10 parts of palmityl ester quats and after insulated and stirred 20min, add 0.1 part of cationic thickener, 35 DEG C are cooled to after stirring 8min, add 0.1 part of essence and 1 part of KF88, after stirring, after being 240 object strainer filterings by order number, obtain finished product.
Embodiment 2
Pure water is added reactor and is heated to 60 DEG C, add 5 parts of palmityl ester quats and after insulated and stirred 30min, add 3 parts of cationic thickeners, 30 DEG C are cooled to after stirring 10min, add 0.1 part of essence and 0.01 part of KF88, after stirring, after being 300 object strainer filterings by order number, obtain finished product.
Embodiment 3
Pure water is added reactor and is heated to 55 DEG C, add 1 part of palmityl ester quat and after insulated and stirred 25min, add 3 parts of cationic thickeners, lowering the temperature 32 DEG C after stirring 5min, add 1 part of essence and 0.3 part of KF88, through obtaining finished product by after order number 500 object strainer filtering after stirring.
The present invention is not limited to above-mentioned embodiment, and for those skilled in the art, under the premise without departing from the principles of the invention, can also make some improvements and modifications, these improvements and modifications are also considered as within protection scope of the present invention.The content be not described in detail in this description belongs to the known prior art of professional and technical personnel in the field.
Claims (4)
1. a fabric softener, is characterized in that: by parts by mass, in every 100 parts of fabric softeners, is following composition:
2. fabric softener as claimed in claim 1, is characterized in that: described cationic thickener is REWOQUATDM730.
3. fabric softener as claimed in claim 1, is characterized in that: described essence is lavender oil, lily essence or cream jasmin france.
4. a preparation method for the fabric softener according to any one of claims 1 to 3, is characterized in that: comprise the following steps:
Pure water is added reactor and is heated to 50 ~ 60 DEG C, add 1 ~ 10 part of palmityl ester quat and after insulated and stirred 20 ~ 30min, add 0.1 ~ 5 part of cationic thickener, be cooled to lower than 40 DEG C after stirring 5 ~ 10min, add 0.1 ~ 3 part of essence and 0.01 ~ 1 part of KF88, after stirring, after being more than or equal to 240 object strainer filterings by order number, obtain finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510631838.5A CN105133316A (en) | 2015-09-29 | 2015-09-29 | Fabric conditioner and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510631838.5A CN105133316A (en) | 2015-09-29 | 2015-09-29 | Fabric conditioner and preparation method thereof |
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| CN105133316A true CN105133316A (en) | 2015-12-09 |
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| CN201510631838.5A Pending CN105133316A (en) | 2015-09-29 | 2015-09-29 | Fabric conditioner and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105484024A (en) * | 2015-12-21 | 2016-04-13 | 无锡科莱欣机电制造有限公司 | Printing and dyeing softener with mouldproof and anti-static functions |
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| JP2009144280A (en) * | 2007-12-14 | 2009-07-02 | Kao Corp | Method for producing liquid softener composition |
| CN102493185A (en) * | 2011-12-15 | 2012-06-13 | 青岛海芬海洋生物科技有限公司 | Marine organism antibacterial fabric softener |
| CN102499259A (en) * | 2011-11-18 | 2012-06-20 | 北京崇高纳米科技有限公司 | Clothing degerming liquid and preparation method thereof |
| CN102517164A (en) * | 2011-12-06 | 2012-06-27 | 江南大学 | Sterilizing laundry detergent containing hairyvein agrimony extract |
| CN103046320A (en) * | 2012-12-06 | 2013-04-17 | 青岛海芬海洋生物科技有限公司 | High-efficiency softening agent applied to laundry room |
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2015
- 2015-09-29 CN CN201510631838.5A patent/CN105133316A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009144280A (en) * | 2007-12-14 | 2009-07-02 | Kao Corp | Method for producing liquid softener composition |
| CN102499259A (en) * | 2011-11-18 | 2012-06-20 | 北京崇高纳米科技有限公司 | Clothing degerming liquid and preparation method thereof |
| CN102517164A (en) * | 2011-12-06 | 2012-06-27 | 江南大学 | Sterilizing laundry detergent containing hairyvein agrimony extract |
| CN102493185A (en) * | 2011-12-15 | 2012-06-13 | 青岛海芬海洋生物科技有限公司 | Marine organism antibacterial fabric softener |
| CN103046320A (en) * | 2012-12-06 | 2013-04-17 | 青岛海芬海洋生物科技有限公司 | High-efficiency softening agent applied to laundry room |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105484024A (en) * | 2015-12-21 | 2016-04-13 | 无锡科莱欣机电制造有限公司 | Printing and dyeing softener with mouldproof and anti-static functions |
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Application publication date: 20151209 |