CN105131864A - Resin adhesive and preparation method thereof - Google Patents
Resin adhesive and preparation method thereof Download PDFInfo
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- CN105131864A CN105131864A CN201510438885.8A CN201510438885A CN105131864A CN 105131864 A CN105131864 A CN 105131864A CN 201510438885 A CN201510438885 A CN 201510438885A CN 105131864 A CN105131864 A CN 105131864A
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Abstract
The invention discloses a resin adhesive and a preparation method thereof. The resin adhesive includes the following raw materials, by weight, 15-20 parts of lac, 17-21 parts of Chinese lacquer, 8-10 parts of rosin, 16-20 parts of Arabic gum, 8-10 parts of unsaturated polyester resin, 5-8 parts of gelatin, 12-14 parts of room temperature vulcanized silicone rubber, 10-12 parts of ethanol, 8-13 parts of vinyl acetate, 7-10 parts of sodium pyrosulfite, 3-8 parts of tannic acid, 18-22 parts of oxidized starch, 40-44 parts of pure water, 4-6 parts of concentrated sulfuric acid, 13-15 parts of glycerin, 6-10 parts of salicylic acid and 6-8 parts of aluminum potassium sulfate dodecahydrate. The resin adhesive is excellent in adhesive performance and is free of toxic gas volatilization.
Description
Technical field
The present invention relates to a kind of resin adhesive and preparation method thereof.
Background technology
Glued joint (bonding, bonding, cementing, gluing) and refer to the technology that homogeneity or heterogeneous body surface stick with glue agent and link together to there is stress distribution continuous, lightweight, or sealing, the features such as most technological temperature is low.Glued joint the connection being specially adapted to unlike material, different thickness, ultra-thin specification and complex component.Glued joint RECENT DEVELOPMENTS the fastest, application industry is extremely wide, and has great effect to high-and-new science and technology progress and people's daily life improvement.Therefore, study, all kinds of tackiness agent of development and production is very important.
The environmental issue of tackiness agent is mainly to the pollution of environment and the harm of HUMAN HEALTH, this is due to the objectionable impurities in tackiness agent, as volatile organic compounds, poisonous solidifying agent, softening agent, thinner and other auxiliary agents, harmful filler etc. cause.
Summary of the invention
The technical problem to be solved in the present invention is to provide one and has adhesive property well, without resin adhesive that poison gas volatilizees and preparation method thereof.
For solving the problem, the present invention adopts following technical scheme:
A kind of resin adhesive and preparation method thereof, comprises the raw material of following parts by weight proportioning: lac 15-20 part, lacquer 17-21 part, rosin 8-10 part, gum arabic 16-20 part, unsaturated polyester resin 8-10 part, gelatin 5-8 part, room temperature vulcanized silicone rubber 12-14 part, ethanol 10-12 part, vinyl acetate between to for plastic 8-13 part, Sodium Pyrosulfite 7-10 part, Weibull 3-8 part, Sumstar 190 18-22 part, pure water 40-44 part, vitriol oil 4-6 part, glycerine 13-15 part, Whitfield's ointment 6-10 part, 12 hydrazine aluminum sulfate potassium 6-8 parts.
Further, the raw material of following parts by weight proportioning is comprised: lac 15 parts, lacquer 17 parts, rosin 8 parts, gum arabic 16 parts, unsaturated polyester resin 8 parts, 5 parts, gelatin, room temperature vulcanized silicone rubber 12 parts, ethanol 10 parts, vinyl acetate between to for plastic 8 parts, Sodium Pyrosulfite 7 parts, 3 parts, Weibull, Sumstar 190 18 parts, pure water 40 parts, the vitriol oil 4 parts, glycerine 13 parts, Whitfield's ointment 6 parts, 6 parts, 12 hydrazine aluminum sulfate potassium.
Further, the raw material of following parts by weight proportioning is comprised: lac 20 parts, lacquer 21 parts, rosin 10 parts, gum arabic 20 parts, unsaturated polyester resin 10 parts, 8 parts, gelatin, room temperature vulcanized silicone rubber 14 parts, ethanol 12 parts, vinyl acetate between to for plastic 13 parts, Sodium Pyrosulfite 10 parts, 8 parts, Weibull, Sumstar 190 22 parts, pure water 44 parts, the vitriol oil 6 parts, glycerine 15 parts, Whitfield's ointment 10 parts, 8 parts, 12 hydrazine aluminum sulfate potassium.
Further, the raw material of following parts by weight proportioning is comprised: lac 18 parts, lacquer 19 parts, rosin 9 parts, gum arabic 18 parts, unsaturated polyester resin 9 parts, 7 parts, gelatin, room temperature vulcanized silicone rubber 13 parts, ethanol 11 parts, vinyl acetate between to for plastic 11 parts, Sodium Pyrosulfite 9 parts, 6 parts, Weibull, Sumstar 190 20 parts, pure water 42 parts, the vitriol oil 5 parts, glycerine 14 parts, Whitfield's ointment 8 parts, 7 parts, 12 hydrazine aluminum sulfate potassium.
Another technical problem that the present invention will solve is to provide a kind of preparation method of resin adhesive, comprises the following steps:
1) by vitriol oil 4-6 part slowly instillation pure water 40-44 part, fully dilute, then Sumstar 190 18-22 part is poured into and abundant stirring and dissolving, until form pasty state, for subsequent use;
2) step 1) is placed on slow fire heating on spirit lamp, is constantly stirred to and gradually becomes transparent liquid, for subsequent use;
3) Whitfield's ointment 6-10 part is poured in ethanol 10-12 part and glycerine 13-15 part together with Weibull 3-8 part fully stirs, until crystal dissolves completely, for subsequent use;
4) step 3) is poured in beaker, then by step 2) and 12 hydrazine aluminum sulfate potassium 6-8 parts add successively, fully stir and cool, for subsequent use;
5) lac 15-20 part, lacquer 17-21 part, rosin 8-10 part and gum arabic 16-20 part are placed in vessel, and heating in water bath to 100 DEG C, make it fully dissolve, miscible, for subsequent use;
6) vinyl acetate between to for plastic 8-13 part is put in reaction vessels, then add Sodium Pyrosulfite 7-10 part as initiator, make its polymerization reaction take place, for subsequent use;
7) step 6) is added appropriate clear water and be then heated to 65 DEG C, then gelatin 5-8 part, room temperature vulcanized silicone rubber 12-14 part and unsaturated polyester resin 8-10 part are poured into successively, and with spirit lamp heating, until become thick, for subsequent use;
8) be poured in step 6) after step 7) temperature being down to 45 DEG C, be then placed in refrigerated centrifuge, carry out centrifugal treating, and make temperature be down to 26 DEG C, for subsequent use;
9) step 4) is divided into A, B two parts according to weight proportion 4:6, for subsequent use;
10) B of step 9) is divided to be poured in sterile vacuum packing bottle seal, preserve, for subsequent use;
11) by the A part in step 9) and step 8) by weight ratio 2:4 admix, and be saved in sterile vacuum packing bottle and seal, preserve, for subsequent use;
12) by step 10) and step 11) packing, and shady and cool dry place is stored in.
The invention has the beneficial effects as follows: by being added with the natural resins such as lac, lacquer, rosin, gum arabic, not only there is good bond effect but also environmentally friendly, composition is harmless, and add unsaturated polyester resin, gelatin, room temperature vulcanized silicone rubber has ambient cure, solidification is very fast, bonding strength is higher, adhesive linkage has good toughness and weather resistance and not easily aging effect, and non-volatile poison gas, can not to environment.
Embodiment
Embodiment 1:
A preparation method for resin adhesive, comprises the raw material of following parts by weight proportioning: lac 15 parts, lacquer 17 parts, rosin 8 parts, gum arabic 16 parts, unsaturated polyester resin 8 parts, 5 parts, gelatin, room temperature vulcanized silicone rubber 12 parts, ethanol 10 parts, vinyl acetate between to for plastic 8 parts, Sodium Pyrosulfite 7 parts, 3 parts, Weibull, Sumstar 190 18 parts, pure water 40 parts, the vitriol oil 4 parts, glycerine 13 parts, Whitfield's ointment 6 parts, 6 parts, 12 hydrazine aluminum sulfate potassium.
A kind of preparation method of resin adhesive comprises the following steps:
1) by the vitriol oil 4 parts slowly instillation pure water 40 parts, fully dilute, then Sumstar 190 18 parts is poured into and abundant stirring and dissolving, until form pasty state, for subsequent use;
2) step 1) is placed on slow fire heating on spirit lamp, is constantly stirred to and gradually becomes transparent liquid, for subsequent use;
3) fully stir being poured into together with 3 parts, Whitfield's ointment 6 parts and Weibull in ethanol 10 parts and glycerine 13 parts, until crystal dissolves completely, for subsequent use;
4) step 3) is poured in beaker, then by step 2) and 6 parts, 12 hydrazine aluminum sulfate potassium add successively, fully stir and cool, for subsequent use;
5) lac 15 parts, lacquer 17 parts, rosin 8 parts and gum arabic 16 parts are placed in vessel, and heating in water bath to 100 DEG C, make it fully dissolve, miscible, for subsequent use;
6) vinyl acetate between to for plastic 8 parts is put in reaction vessels, then add Sodium Pyrosulfite 7 parts as initiator, make its polymerization reaction take place, for subsequent use;
7) step 6) is added appropriate clear water and be then heated to 65 DEG C, then 5 parts, gelatin, room temperature vulcanized silicone rubber 12 parts and unsaturated polyester resin 8 parts are poured into successively, and with spirit lamp heating, until become thick, for subsequent use;
8) be poured in step 6) after step 7) temperature being down to 45 DEG C, be then placed in refrigerated centrifuge, carry out centrifugal treating, and make temperature be down to 26 DEG C, for subsequent use;
9) step 4) is divided into A, B two parts according to weight proportion 4:6, for subsequent use;
10) B of step 9) is divided to be poured in sterile vacuum packing bottle seal, preserve, for subsequent use;
11) by the A part in step 9) and step 8) by weight ratio 2:4 admix, and be saved in sterile vacuum packing bottle and seal, preserve, for subsequent use;
12) by step 10) and step 11) packing, and shady and cool dry place is stored in.
Embodiment 2:
A kind of resin adhesive and preparation method thereof, comprises the raw material of following parts by weight proportioning: lac 20 parts, lacquer 21 parts, rosin 10 parts, gum arabic 20 parts, unsaturated polyester resin 10 parts, 8 parts, gelatin, room temperature vulcanized silicone rubber 14 parts, ethanol 12 parts, vinyl acetate between to for plastic 13 parts, Sodium Pyrosulfite 10 parts, 8 parts, Weibull, Sumstar 190 22 parts, pure water 44 parts, the vitriol oil 6 parts, glycerine 15 parts, Whitfield's ointment 10 parts, 8 parts, 12 hydrazine aluminum sulfate potassium.
A preparation method for resin adhesive, comprises the following steps:
1) by the vitriol oil 6 parts slowly instillation pure water 44 parts, fully dilute, then Sumstar 190 22 parts is poured into and abundant stirring and dissolving, until form pasty state, for subsequent use;
2) step 1) is placed on slow fire heating on spirit lamp, is constantly stirred to and gradually becomes transparent liquid, for subsequent use;
3) fully stir being poured into together with 8 parts, Whitfield's ointment 10 parts and Weibull in ethanol 12 parts and glycerine 15 parts, until crystal dissolves completely, for subsequent use;
4) step 3) is poured in beaker, then by step 2) and 8 parts, 12 hydrazine aluminum sulfate potassium add successively, fully stir and cool, for subsequent use;
5) lac 20 parts, lacquer 21 parts, rosin 10 parts and gum arabic 20 parts are placed in vessel, and heating in water bath to 100 DEG C, make it fully dissolve, miscible, for subsequent use;
6) vinyl acetate between to for plastic 13 parts is put in reaction vessels, then add Sodium Pyrosulfite 10 parts as initiator, make its polymerization reaction take place, for subsequent use;
7) step 6) is added appropriate clear water and be then heated to 65 DEG C, then 8 parts, gelatin, room temperature vulcanized silicone rubber 14 parts and unsaturated polyester resin 10 parts are poured into successively, and with spirit lamp heating, until become thick, for subsequent use;
8) be poured in step 6) after step 7) temperature being down to 45 DEG C, be then placed in refrigerated centrifuge, carry out centrifugal treating, and make temperature be down to 26 DEG C, for subsequent use;
9) step 4) is divided into A, B two parts according to weight proportion 4:6, for subsequent use;
10) B of step 9) is divided to be poured in sterile vacuum packing bottle seal, preserve, for subsequent use;
11) by the A part in step 9) and step 8) by weight ratio 2:4 admix, and be saved in sterile vacuum packing bottle and seal, preserve, for subsequent use;
12) by step 10) and step 11) packing, and shady and cool dry place is stored in.
Embodiment 3:
A kind of resin adhesive and preparation method thereof, comprises the raw material of following parts by weight proportioning: lac 18 parts, lacquer 19 parts, rosin 9 parts, gum arabic 18 parts, unsaturated polyester resin 9 parts, 7 parts, gelatin, room temperature vulcanized silicone rubber 13 parts, ethanol 11 parts, vinyl acetate between to for plastic 11 parts, Sodium Pyrosulfite 9 parts, 6 parts, Weibull, Sumstar 190 20 parts, pure water 42 parts, the vitriol oil 5 parts, glycerine 14 parts, Whitfield's ointment 8 parts, 7 parts, 12 hydrazine aluminum sulfate potassium.
A preparation method for resin adhesive, comprises the following steps:
1) by the vitriol oil 5 parts slowly instillation pure water 42 parts, fully dilute, then Sumstar 190 20 parts is poured into and abundant stirring and dissolving, until form pasty state, for subsequent use;
2) step 1) is placed on slow fire heating on spirit lamp, is constantly stirred to and gradually becomes transparent liquid, for subsequent use;
3) fully stir being poured into together with 6 parts, Whitfield's ointment 8 parts and Weibull in ethanol 11 parts and glycerine 14 parts, until crystal dissolves completely, for subsequent use;
4) step 3) is poured in beaker, then by step 2) and 7 parts, 12 hydrazine aluminum sulfate potassium add successively, fully stir and cool, for subsequent use;
5) lac 18 parts, lacquer 19 parts, rosin 9 parts and gum arabic 18 parts are placed in vessel, and heating in water bath to 100 DEG C, make it fully dissolve, miscible, for subsequent use;
6) vinyl acetate between to for plastic 11 parts is put in reaction vessels, then add Sodium Pyrosulfite 9 parts as initiator, make its polymerization reaction take place, for subsequent use;
7) step 6) is added appropriate clear water and be then heated to 65 DEG C, then 7 parts, gelatin, room temperature vulcanized silicone rubber 13 parts and unsaturated polyester resin 9 parts are poured into successively, and with spirit lamp heating, until become thick, for subsequent use;
8) be poured in step 6) after step 7) temperature being down to 45 DEG C, be then placed in refrigerated centrifuge, carry out centrifugal treating, and make temperature be down to 26 DEG C, for subsequent use;
9) step 4) is divided into A, B two parts according to weight proportion 4:6, for subsequent use;
10) B of step 9) is divided to be poured in sterile vacuum packing bottle seal, preserve, for subsequent use;
11) by the A part in step 9) and step 8) by weight ratio 2:4 admix, and be saved in sterile vacuum packing bottle and seal, preserve, for subsequent use;
12) by step 10) and step 11) packing, and shady and cool dry place is stored in.
The invention has the beneficial effects as follows: by being added with the natural resins such as lac, lacquer, rosin, gum arabic, not only there is good bond effect but also environmentally friendly, composition is harmless, and add unsaturated polyester resin, gelatin, room temperature vulcanized silicone rubber has ambient cure, solidification is very fast, bonding strength is higher, adhesive linkage has good toughness and weather resistance and not easily aging effect, and non-volatile poison gas, can not to environment.
The above, be only the specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, and any change of expecting without creative work or replacement, all should be encompassed in protection scope of the present invention.
Claims (5)
1. resin adhesive and preparation method thereof, it is characterized in that, comprise the raw material of following parts by weight proportioning: lac 15-20 part, lacquer 17-21 part, rosin 8-10 part, gum arabic 16-20 part, unsaturated polyester resin 8-10 part, gelatin 5-8 part, room temperature vulcanized silicone rubber 12-14 part, ethanol 10-12 part, vinyl acetate between to for plastic 8-13 part, Sodium Pyrosulfite 7-10 part, Weibull 3-8 part, Sumstar 190 18-22 part, pure water 40-44 part, vitriol oil 4-6 part, glycerine 13-15 part, Whitfield's ointment 6-10 part, 12 hydrazine aluminum sulfate potassium 6-8 parts.
2. a kind of resin adhesive as claimed in claim 1 and preparation method thereof, it is characterized in that, comprise the raw material of following parts by weight proportioning: lac 15 parts, lacquer 17 parts, rosin 8 parts, gum arabic 16 parts, unsaturated polyester resin 8 parts, 5 parts, gelatin, room temperature vulcanized silicone rubber 12 parts, ethanol 10 parts, vinyl acetate between to for plastic 8 parts, Sodium Pyrosulfite 7 parts, 3 parts, Weibull, Sumstar 190 18 parts, pure water 40 parts, the vitriol oil 4 parts, glycerine 13 parts, Whitfield's ointment 6 parts, 6 parts, 12 hydrazine aluminum sulfate potassium.
3. a kind of resin adhesive as claimed in claim 1 and preparation method thereof, it is characterized in that, comprise the raw material of following parts by weight proportioning: lac 20 parts, lacquer 21 parts, rosin 10 parts, gum arabic 20 parts, unsaturated polyester resin 10 parts, 8 parts, gelatin, room temperature vulcanized silicone rubber 14 parts, ethanol 12 parts, vinyl acetate between to for plastic 13 parts, Sodium Pyrosulfite 10 parts, 8 parts, Weibull, Sumstar 190 22 parts, pure water 44 parts, the vitriol oil 6 parts, glycerine 15 parts, Whitfield's ointment 10 parts, 8 parts, 12 hydrazine aluminum sulfate potassium.
4. a kind of resin adhesive as claimed in claim 1 and preparation method thereof, it is characterized in that, comprise the raw material of following parts by weight proportioning: lac 18 parts, lacquer 19 parts, rosin 9 parts, gum arabic 18 parts, unsaturated polyester resin 9 parts, 7 parts, gelatin, room temperature vulcanized silicone rubber 13 parts, ethanol 11 parts, vinyl acetate between to for plastic 11 parts, Sodium Pyrosulfite 9 parts, 6 parts, Weibull, Sumstar 190 20 parts, pure water 42 parts, the vitriol oil 5 parts, glycerine 14 parts, Whitfield's ointment 8 parts, 7 parts, 12 hydrazine aluminum sulfate potassium.
5. a preparation method for resin adhesive, is characterized in that, comprises the following steps:
1) by vitriol oil 4-6 part slowly instillation pure water 40-44 part, fully dilute, then Sumstar 190 18-22 part is poured into and abundant stirring and dissolving, until form pasty state, for subsequent use;
2) step 1) is placed on slow fire heating on spirit lamp, is constantly stirred to and gradually becomes transparent liquid, for subsequent use;
3) Whitfield's ointment 6-10 part is poured in ethanol 10-12 part and glycerine 13-15 part together with Weibull 3-8 part fully stirs, until crystal dissolves completely, for subsequent use;
4) step 3) is poured in beaker, then by step 2) and 12 hydrazine aluminum sulfate potassium 6-8 parts add successively, fully stir and cool, for subsequent use;
5) lac 15-20 part, lacquer 17-21 part, rosin 8-10 part and gum arabic 16-20 part are placed in vessel, and heating in water bath to 100 DEG C, make it fully dissolve, miscible, for subsequent use;
6) vinyl acetate between to for plastic 8-13 part is put in reaction vessels, then add Sodium Pyrosulfite 7-10 part as initiator, make its polymerization reaction take place, for subsequent use;
7) step 6) is added appropriate clear water and be then heated to 65 DEG C, then gelatin 5-8 part, room temperature vulcanized silicone rubber 12-14 part and unsaturated polyester resin 8-10 part are poured into successively, and with spirit lamp heating, until become thick, for subsequent use;
8) be poured in step 6) after step 7) temperature being down to 45 DEG C, be then placed in refrigerated centrifuge, carry out centrifugal treating, and make temperature be down to 26 DEG C, for subsequent use;
9) step 4) is divided into A, B two parts according to weight proportion 4:6, for subsequent use;
10) B of step 9) is divided to be poured in sterile vacuum packing bottle seal, preserve, for subsequent use;
11) by the A part in step 9) and step 8) by weight ratio 2:4 admix, and be saved in sterile vacuum packing bottle and seal, preserve, for subsequent use;
12) by step 10) and step 11) packing, and shady and cool dry place is stored in.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510438885.8A CN105131864A (en) | 2015-07-24 | 2015-07-24 | Resin adhesive and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510438885.8A CN105131864A (en) | 2015-07-24 | 2015-07-24 | Resin adhesive and preparation method thereof |
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| CN105131864A true CN105131864A (en) | 2015-12-09 |
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| CN201510438885.8A Pending CN105131864A (en) | 2015-07-24 | 2015-07-24 | Resin adhesive and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105780472A (en) * | 2016-05-13 | 2016-07-20 | 温州职业技术学院 | Tennis racket string |
| CN106218056A (en) * | 2016-08-31 | 2016-12-14 | 阜南县天亿工艺品有限公司 | A kind of ferrum skill artware packaging thermal insulation board preparation method |
| CN108285763A (en) * | 2018-01-26 | 2018-07-17 | 南阳理工学院 | A kind of preparation method of environment protection architecture adhesive |
| CN109266285A (en) * | 2018-09-06 | 2019-01-25 | 顶立新材料科技有限公司 | A kind of environment-friendly water-based adhesive of multi-layered board gluing processing of lac modified polyvinyl acetate |
| CN109852279A (en) * | 2018-12-27 | 2019-06-07 | 绍兴明基新材料有限公司 | Vegetable and fruit binding plant base adhesive tape and preparation method thereof |
| CN112662372A (en) * | 2020-12-24 | 2021-04-16 | 烟台大学 | Shellac capable of being heated and used repeatedly and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103666368A (en) * | 2013-12-21 | 2014-03-26 | 栾晓健 | Natural adhesive |
| CN104629648A (en) * | 2013-11-11 | 2015-05-20 | 哈尔滨隆迪建材有限公司 | Building finishing decoration adhesive and preparation method thereof |
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2015
- 2015-07-24 CN CN201510438885.8A patent/CN105131864A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104629648A (en) * | 2013-11-11 | 2015-05-20 | 哈尔滨隆迪建材有限公司 | Building finishing decoration adhesive and preparation method thereof |
| CN103666368A (en) * | 2013-12-21 | 2014-03-26 | 栾晓健 | Natural adhesive |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105780472A (en) * | 2016-05-13 | 2016-07-20 | 温州职业技术学院 | Tennis racket string |
| CN106218056A (en) * | 2016-08-31 | 2016-12-14 | 阜南县天亿工艺品有限公司 | A kind of ferrum skill artware packaging thermal insulation board preparation method |
| CN108285763A (en) * | 2018-01-26 | 2018-07-17 | 南阳理工学院 | A kind of preparation method of environment protection architecture adhesive |
| CN108285763B (en) * | 2018-01-26 | 2019-11-08 | 南阳理工学院 | A kind of preparation method of environment protection architecture adhesive |
| CN109266285A (en) * | 2018-09-06 | 2019-01-25 | 顶立新材料科技有限公司 | A kind of environment-friendly water-based adhesive of multi-layered board gluing processing of lac modified polyvinyl acetate |
| CN109852279A (en) * | 2018-12-27 | 2019-06-07 | 绍兴明基新材料有限公司 | Vegetable and fruit binding plant base adhesive tape and preparation method thereof |
| CN109852279B (en) * | 2018-12-27 | 2021-06-01 | 绍兴明基新材料有限公司 | Vegetable and fruit binding plant base adhesive tape and preparation method thereof |
| CN112662372A (en) * | 2020-12-24 | 2021-04-16 | 烟台大学 | Shellac capable of being heated and used repeatedly and preparation method thereof |
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Application publication date: 20151209 |
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