CN105130175A - Continuously operable chemically-toughened glass ultrasonic hydrothermal kettle - Google Patents
Continuously operable chemically-toughened glass ultrasonic hydrothermal kettle Download PDFInfo
- Publication number
- CN105130175A CN105130175A CN201510566617.4A CN201510566617A CN105130175A CN 105130175 A CN105130175 A CN 105130175A CN 201510566617 A CN201510566617 A CN 201510566617A CN 105130175 A CN105130175 A CN 105130175A
- Authority
- CN
- China
- Prior art keywords
- hydro
- kettle
- cover plate
- pressure
- thermal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention relates to a continuously operable chemically-toughened glass ultrasonic hydrothermal kettle. The continuously operable chemically-toughened glass ultrasonic hydrothermal kettle comprises a first hydrothermal kettle body and a second hydrothermal kettle body, wherein bottom cover plates are arranged at the lower ends of the first hydrothermal kettle body and the second hydrothermal kettle body; inner groove cover plates are installed below the bottom cover plates; ultrasonic wave generators are installed on the groove cover plates; liquid collection baffles are arranged on the inner sides of the bottom cover plates, and liquid in the kettle bodies is prevented from overflowing through the groove cover plates and the liquid collection baffles; the upper portions of the first hydrothermal kettle body and the second hydrothermal kettle body are connected through a gas communicating pipeline; a high-pressure explosion-proof electromagnetic valve is arranged in the middle of the gas communicating pipeline, and a pressure gauge and a pressure reducing valve are respectively arranged on the gas communicating pipeline on two sides of the high-pressure explosion-proof electromagnetic valve; the bottom portions of the first hydrothermal kettle body and the second hydrothermal kettle body are respectively connected with liquid drain pipelines, and the two liquid drain pipelines are connected through a liquid communicating pipeline. The continuously operable chemically-toughened glass ultrasonic hydrothermal kettle can be used to realize quick transfer of gas and liquid phase at high temperature and high pressure and facilitate the continuous operation of a glass utensil in a high-pressure kettle.
Description
Technical field
The present invention relates to chilled glass technical field of processing equipment, be specifically related to a kind of chemically reinforced glass using supersonic, water-heating still of operate continuously.
Background technology
Fused salt ion exchange method is that glass surface forms compressive stress layers, improves glasswork intensity effective ways.Because glass reinforced used temperature of molten salt is at 350 ~ 550 DEG C, under high temperature, fused salt is easy to cause corrosion in various degree to wall.In order to reduce use temperature, selecting the inorganic salt of low melting point or using composite salt all to contribute to reducing energy consumption.Therefore, the method changing chilled glass just becomes the important channel of consumption reduction.
Hydrothermal reaction process refers under certain temperature and pressure, in the fluids such as water, the aqueous solution or steam carry out the general name of relevant chemical reaction.Under hydrothermal conditions, water can work as a kind of chemical composition and participate in reaction, is that solvent and mineralizer also can be used as pressure transfer medium simultaneously; By participating in dialysis reaction and controlling physical chemical factor etc., realize formation and the modification of mineral compound.But the water heating kettle that is mainly limited in that hydrothermal method uses can not operate continuously.In general, the main device of hydrothermal method is autoclave, can hold the steel kettle of High Temperature High Pressure, generally can bear the temperature of 1100 DEG C and the pressure of 1GPa, have reliable tightness system and explosion-proof equipment.Because autoclave can not the limitation of operate continuously with pressure, greatly limit the use as glass reinforced equipment.In addition, in ion exchange process, glass surface there will be the phenomenon that sodium ion raises, thus is unfavorable for removing of sodium ion.So the rapid diffusion of ion is also to consider near glass surface.
Summary of the invention
Technical problem to be solved by this invention is the chemically reinforced glass using supersonic, water-heating still improving a kind of operate continuously, liquid phase fast transfer under High Temperature High Pressure can be realized, facilitate glassware being back to back in autoclave, thus solve autoclave can not the problem of operate continuously.
Technical problem to be solved by this invention realizes by the following technical solutions:
A kind of chemically reinforced glass using supersonic, water-heating still of operate continuously, comprise the first hydro-thermal kettle and the second hydro-thermal kettle, upper cover is equipped with at the first hydro-thermal kettle and the second hydro-thermal kettle upper end, first hydro-thermal kettle and the second hydro-thermal kettle lower end are equipped with bottom cover plate, inner groovy cover plate is installed below described bottom cover plate, described groove cover plate is provided with ultrasonic generator, gasket is provided with between described inner groovy cover plate and bottom cover plate, be provided with liquid inside described bottom cover plate and collect baffle plate, collect baffle plate by groove cover plate and liquid and prevent liquid flooding in kettle, described first hydro-thermal kettle is connected by gas communication pipeline with the second hydro-thermal kettle top, in the middle of described gas communication pipeline, be provided with a high-pressure anti-explosion solenoid valve door, described high-pressure anti-explosion solenoid valve door both sides are positioned at gas communication pipeline and are respectively equipped with tensimeter and reducing valve, described first hydro-thermal kettle and the second hydro-thermal kettle bottom part are not connected with liquid discharge tube road, connected, described fluid connection pipeline and liquid discharge tube road are equipped with high-temp liquid magnetic valve between two liquid discharge tube roads by fluid connection pipeline.
Described groove cover plate is symmetrically installed with two groups of ultrasonic generators.
Another object of the present invention is to provide a kind of working method of above-mentioned using supersonic, water-heating still, and step is as follows:
(1) first hydro-thermal kettle cover plate stows glasswork, and loadings is about the long-pending 60-80% of interior kettle, is slowly promoted by cover plate, be connected and seal with kettle after filling through hydraulic efficiency plant;
(2) by bottom connecting pipeline, inorganic salt solution is pumped into the first hydro-thermal kettle, submergence glasswork;
(3) solution in still is heated to 200-240 DEG C, constant temperature 6-18h, and it is ultrasonic to carry out intermittence;
(4) after hydrothermal treatment consists terminates, high-temp liquid magnetic valve is opened, utilize the high pressure in the first hydro-thermal kettle the solution in still to be entered the second reactor being pre-loaded into glasswork through connecting pipeline;
(5) close high-temp liquid magnetic valve, open high-pressure anti-explosion solenoid valve door, balance the pressure in two stills, after pressure equilibrium, close high-pressure anti-explosion solenoid valve door;
Remaining liquid in (6) first hydro-thermal kettlies utilizes overbottom pressure in still to be discharged by raffinate, and is decompressed to normal pressure;
(7) fluid pressure drop lower cover, takes out the glasswork after hydro-thermal strengthening, reinstalls new glasswork, and be again connected with kettle by cover plate and seal;
After (8) second hydro-thermal kettle hydrothermal treatment consists terminate, repeat step (4)-(7), realize two still cyclical operations.
The invention has the beneficial effects as follows:
1, the gas-liquid between two stills exchanges does not need cooling, liquids and gases in A still are transferred to B still by connecting pipeline by self high pressure in direct dependence A still, valve on A still escape route is regulated to lay down the overbottom pressure in A still, the handling of glassware in A still can be completed, circulate successively, thus complete operate continuously with pressure, solve a single still intermittent operation difficult problem;
2, the ultrasonic generator on bottom inner groovy cover plate provides intermittent ultrasonic, solves the concentration polarization phenomenon of glass surface, increases mass transfer force;
3, kettle is fixed, and reduces operation easier, and the handling of glassware are moved up and down by bottom cover plate, and kettle liquid collects baffle plate and inner groovy cover plate prevents liquid flooding;
4, gaseous tension is too high can be regulated by reducing valve, is released after bottom solution sodium ion exceeds standard by escape route.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention.
Embodiment
The technique means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, below in conjunction with concrete diagram, setting forth the present invention further.
As shown in Figure 1, a kind of chemically reinforced glass using supersonic, water-heating still of operate continuously, comprise the first hydro-thermal kettle 1 and the second hydro-thermal kettle 2, upper cover 3 is equipped with at the first hydro-thermal kettle 1 and the second hydro-thermal kettle 2 upper end, first hydro-thermal kettle 1 and the second hydro-thermal kettle 2 lower end are equipped with bottom cover plate 4, inner groovy cover plate 5 is installed below bottom cover plate 4, described groove cover plate 5 is provided with ultrasonic generator 6, described groove cover plate 5 is symmetrically installed with two groups of ultrasonic generators 6.Be provided with gasket 7 between described inner groovy cover plate 5 and bottom cover plate 4, be provided with liquid inside described bottom cover plate 4 and collect baffle plate 8, collect baffle plate 8 by groove cover plate 5 and liquid and prevent liquid flooding in kettle; Described first hydro-thermal kettle 1 is connected by gas communication pipeline 9 with the second hydro-thermal kettle 2 top, in the middle of described gas communication pipeline 9, be provided with a high-pressure anti-explosion solenoid valve door 10, described high-pressure anti-explosion solenoid valve door 10 both sides are positioned at gas communication pipeline 9 and are respectively equipped with tensimeter 11 and reducing valve 12; Liquid discharge tube road 13 is connected to bottom described first hydro-thermal kettle 1 and the second hydro-thermal kettle 2, connected by fluid connection pipeline 14 between two liquid discharge tube roads 13, described fluid connection pipeline 14 and liquid discharge tube road 13 are equipped with high-temp liquid magnetic valve 15.
The working method of above-mentioned using supersonic, water-heating still, step is as follows:
(1) first hydro-thermal kettle cover plate stows glasswork, and loadings is about the long-pending 60-80% of interior kettle, is slowly promoted by cover plate, be connected and seal with kettle after filling through hydraulic efficiency plant;
(2) by bottom connecting pipeline, inorganic salt solution is pumped into the first hydro-thermal kettle, submergence glasswork;
(3) solution in still is heated to 200-240 DEG C, constant temperature 6-18h, and it is ultrasonic to carry out intermittence;
(4) after hydrothermal treatment consists terminates, high-temp liquid magnetic valve is opened, utilize the high pressure in the first hydro-thermal kettle the solution in still to be entered the second reactor being pre-loaded into glasswork through connecting pipeline;
(5) close high-temp liquid magnetic valve, open high-pressure anti-explosion solenoid valve door, balance the pressure in two stills, after pressure equilibrium, close high-pressure anti-explosion solenoid valve door;
Remaining liquid in (6) first hydro-thermal kettlies utilizes overbottom pressure in still to be discharged by raffinate, and is decompressed to normal pressure;
(7) fluid pressure drop lower cover, takes out the glasswork after hydro-thermal strengthening, reinstalls new glasswork, and be again connected with kettle by cover plate and seal;
After (8) second hydro-thermal kettle hydrothermal treatment consists terminate, repeat step (4)-(7), realize two still cyclical operations.
Gas-liquid between two stills exchanges does not need cooling, liquids and gases in first hydro-thermal kettle 1 are transferred to the second hydro-thermal kettle 2 by gas communication pipeline 9 by self high pressure in direct dependence first hydro-thermal kettle 1, the reducing valve 12 on the first hydro-thermal kettle 1 gas communication pipeline 9 is regulated to lay down overbottom pressure in the first hydro-thermal kettle 1, the handling of glassware in the first hydro-thermal kettle 1 can be completed, circulate successively, thus complete operate continuously with pressure, solve a single still intermittent operation difficult problem.
More than show and describe ultimate principle of the present invention and principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (3)
1. the chemically reinforced glass using supersonic, water-heating still of an operate continuously, it is characterized in that: comprise the first hydro-thermal kettle and the second hydro-thermal kettle, upper cover is equipped with at the first hydro-thermal kettle and the second hydro-thermal kettle upper end, first hydro-thermal kettle and the second hydro-thermal kettle lower end are equipped with bottom cover plate, inner groovy cover plate is installed below described bottom cover plate, described groove cover plate is provided with ultrasonic generator, gasket is provided with between described inner groovy cover plate and bottom cover plate, be provided with liquid inside described bottom cover plate and collect baffle plate, collect baffle plate by groove cover plate and liquid and prevent liquid flooding in kettle, described first hydro-thermal kettle is connected by gas communication pipeline with the second hydro-thermal kettle top, in the middle of described gas communication pipeline, be provided with a high-pressure anti-explosion solenoid valve door, described high-pressure anti-explosion solenoid valve door both sides are positioned at gas communication pipeline and are respectively equipped with tensimeter and reducing valve, described first hydro-thermal kettle and the second hydro-thermal kettle bottom part are not connected with liquid discharge tube road, connected, described fluid connection pipeline and liquid discharge tube road are equipped with high-temp liquid magnetic valve between two liquid discharge tube roads by fluid connection pipeline.
2. the chemically reinforced glass using supersonic, water-heating still of a kind of operate continuously according to claim 1, is characterized in that: described groove cover plate is symmetrically installed with two groups of ultrasonic generators.
3. a working method for using supersonic, water-heating still described in claim 1, it is characterized in that, step is as follows:
(1) first hydro-thermal kettle cover plate stows glasswork, and loadings is about the long-pending 60-80% of interior kettle, is slowly promoted by cover plate, be connected and seal with kettle after filling through hydraulic efficiency plant;
(2) by bottom connecting pipeline, inorganic salt solution is pumped into the first hydro-thermal kettle, submergence glasswork;
(3) solution in still is heated to 200-240 DEG C, constant temperature 6-18h, and it is ultrasonic to carry out intermittence;
(4) after hydrothermal treatment consists terminates, high-temp liquid magnetic valve is opened, utilize the high pressure in the first hydro-thermal kettle the solution in still to be entered the second reactor being pre-loaded into glasswork through connecting pipeline;
(5) close high-temp liquid magnetic valve, open high-pressure anti-explosion solenoid valve door, balance the pressure in two stills, after pressure equilibrium, close high-pressure anti-explosion solenoid valve door;
Remaining liquid in (6) first hydro-thermal kettlies utilizes overbottom pressure in still to be discharged by raffinate, and is decompressed to normal pressure;
(7) fluid pressure drop lower cover, takes out the glasswork after hydro-thermal strengthening, reinstalls new glasswork, and be again connected with kettle by cover plate and seal;
After (8) second hydro-thermal kettle hydrothermal treatment consists terminate, repeat step (4)-(7), realize two still cyclical operations.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510566617.4A CN105130175B (en) | 2015-09-08 | 2015-09-08 | A kind of chemically reinforced glass supersonic, water-heating kettle of continuous operation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510566617.4A CN105130175B (en) | 2015-09-08 | 2015-09-08 | A kind of chemically reinforced glass supersonic, water-heating kettle of continuous operation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105130175A true CN105130175A (en) | 2015-12-09 |
| CN105130175B CN105130175B (en) | 2017-09-26 |
Family
ID=54715826
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510566617.4A Active CN105130175B (en) | 2015-09-08 | 2015-09-08 | A kind of chemically reinforced glass supersonic, water-heating kettle of continuous operation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105130175B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106237956A (en) * | 2016-09-30 | 2016-12-21 | 华南理工大学 | A kind of hydrothermal reaction kettle adding ultrasonic field |
| CN110668687A (en) * | 2019-10-24 | 2020-01-10 | 深圳市诸脉科技有限公司 | Method and device for online purification of salt bath |
| CN116143421A (en) * | 2022-11-10 | 2023-05-23 | 西部金属材料股份有限公司 | Reaction device for antibacterial and antiviral glass and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1446621A (en) * | 2003-04-18 | 2003-10-08 | 清华大学 | Tube type device respondent to water heat in high temperature and pressure |
| CN101134159A (en) * | 2006-08-30 | 2008-03-05 | 藤村通商株式会社 | Water-hot processing device and method by using the water or heat of the vapor |
| CN102120162A (en) * | 2011-01-06 | 2011-07-13 | 上海交通大学 | Combined type reactor for high-temperature high-voltage hydro-thermal treatment and treating method thereof |
| CN201944298U (en) * | 2010-11-24 | 2011-08-24 | 潍坊英轩实业有限公司 | Upwards-spreading discharge valve at bottom of normal pressure reaction kettle |
| CN103418323A (en) * | 2012-05-15 | 2013-12-04 | 嵩县开拓者钼业有限公司 | Industrial microwave ultrasonic reaction kettle |
| CN103933923A (en) * | 2014-04-30 | 2014-07-23 | 潘兆金 | Continuous reaction production line consisting of multiple serially connected reaction kettles |
-
2015
- 2015-09-08 CN CN201510566617.4A patent/CN105130175B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1446621A (en) * | 2003-04-18 | 2003-10-08 | 清华大学 | Tube type device respondent to water heat in high temperature and pressure |
| CN101134159A (en) * | 2006-08-30 | 2008-03-05 | 藤村通商株式会社 | Water-hot processing device and method by using the water or heat of the vapor |
| JP2008055285A (en) * | 2006-08-30 | 2008-03-13 | Fujimura Tsusho Kk | Hydrothermal treatment device and method of carrying out hydrothermal treatment of object to be treated by water component of steam and heat of steam |
| CN201944298U (en) * | 2010-11-24 | 2011-08-24 | 潍坊英轩实业有限公司 | Upwards-spreading discharge valve at bottom of normal pressure reaction kettle |
| CN102120162A (en) * | 2011-01-06 | 2011-07-13 | 上海交通大学 | Combined type reactor for high-temperature high-voltage hydro-thermal treatment and treating method thereof |
| CN103418323A (en) * | 2012-05-15 | 2013-12-04 | 嵩县开拓者钼业有限公司 | Industrial microwave ultrasonic reaction kettle |
| CN103933923A (en) * | 2014-04-30 | 2014-07-23 | 潘兆金 | Continuous reaction production line consisting of multiple serially connected reaction kettles |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106237956A (en) * | 2016-09-30 | 2016-12-21 | 华南理工大学 | A kind of hydrothermal reaction kettle adding ultrasonic field |
| CN110668687A (en) * | 2019-10-24 | 2020-01-10 | 深圳市诸脉科技有限公司 | Method and device for online purification of salt bath |
| CN110668687B (en) * | 2019-10-24 | 2024-02-20 | 深圳市诸脉科技有限公司 | Method and device for purifying salt bath on line |
| CN116143421A (en) * | 2022-11-10 | 2023-05-23 | 西部金属材料股份有限公司 | Reaction device for antibacterial and antiviral glass and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105130175B (en) | 2017-09-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102865765B (en) | Single-tank heat-storage system and single-tank heat-storage method | |
| CN105130175A (en) | Continuously operable chemically-toughened glass ultrasonic hydrothermal kettle | |
| CN203520890U (en) | Double-channel natural circulating system device | |
| CN202594819U (en) | Liquid hollow fiber film degassing device | |
| CN109851187B (en) | Sludge supercritical water oxidation system with heat transfer oil as heat exchange medium and sludge treatment method | |
| CN205300303U (en) | Boiler deoxidization tail vapour waste heat recoverer | |
| CN202018832U (en) | Test device for loss of coolant accident (LOCA) of nuclear power station | |
| CN106813411A (en) | Useless geothermal well reutilization system and its construction method | |
| CN203837530U (en) | High-efficiency energy-saving tube type heat exchanger | |
| CN202392997U (en) | Electromagnetic heating water heater and water tank with spiral water passages | |
| CN204154144U (en) | A kind of fermentation tank vapour-recovery unit | |
| CN203550178U (en) | Electro-thermal film heating tube immersion type water heater | |
| CN203408704U (en) | Energy-saving, emission-reducing and consumption-reducing heating device for reaction kettle | |
| CN207227051U (en) | A kind of oxygen-eliminating device without a head | |
| CN206766790U (en) | A kind of high-temperature resistant anti-corrosive tank body | |
| CN206210540U (en) | The two-way oiling device of transformer | |
| CN201589062U (en) | Heater | |
| CN205482473U (en) | Residual heat recycling device | |
| CN215217278U (en) | Heat exchanger for industrial waste heat recovery | |
| CN217928725U (en) | Boiler hot water recycling device | |
| CN106885385A (en) | Individual well hot dry rock heat energy extraction system | |
| CN206683028U (en) | Individual well hot dry rock heating system | |
| CN105836819A (en) | Medicine production wastewater treatment mechanism | |
| CN204447417U (en) | A kind of supporting boiling water gas-liquid separation device for reaction pot | |
| CN204522359U (en) | A kind of destilling tower device of energy-saving safe |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A continuous operation of chemically strengthened glass ultrasonic hydrothermal kettle Effective date of registration: 20220812 Granted publication date: 20170926 Pledgee: Anhui Fengyang Rural Commercial Bank Co.,Ltd. Pledgor: ANHUI FENGYANG HUAIHE GLASS Co.,Ltd. Registration number: Y2022980012486 |