CN105107232A - Precooling type cooling separation structure - Google Patents

Precooling type cooling separation structure Download PDF

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Publication number
CN105107232A
CN105107232A CN201510592146.4A CN201510592146A CN105107232A CN 105107232 A CN105107232 A CN 105107232A CN 201510592146 A CN201510592146 A CN 201510592146A CN 105107232 A CN105107232 A CN 105107232A
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CN
China
Prior art keywords
pipe
separation structure
cooling
separator
precooling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201510592146.4A
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Chinese (zh)
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CN105107232B (en
Inventor
高敏华
杨立新
林伯祥
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Huzhou Xiaote Pharmaceutical & Chemical Co Ltd
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Huzhou Xiaote Pharmaceutical & Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Huzhou Xiaote Pharmaceutical & Chemical Co Ltd filed Critical Huzhou Xiaote Pharmaceutical & Chemical Co Ltd
Priority to CN201510592146.4A priority Critical patent/CN105107232B/en
Publication of CN105107232A publication Critical patent/CN105107232A/en
Application granted granted Critical
Publication of CN105107232B publication Critical patent/CN105107232B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The invention discloses a precooling type cooling separation structure, and belongs to the field of chemical engineering processing equipment. The precooling type cooling separation structure comprises a cooling separator and is characterized in that a first feeding pipe for conveying raw materials below 150 DEG C is arranged at one side end of the cooling separator, and a discharging pipe is arranged on the upper portion of the other side end of the cooling separator; a cooling water outlet pipe is arranged below the discharging pipe, a cooling water inlet pipe is arranged on the upper end face of the cooling separator, a water phase output pipe for conveying lower-layer separators is arranged on the lower end face of the cooling separator, a precooling tank for precooling raw materials above 260 DEG C to below 150 DEG C is arranged at the inlet end of the first feeding pipe, and a second feeding pipe for conveying raw materials of 260 DEG C is arranged at the top of the precooling tank. The precooling type cooling separation structure has the advantages that energy is effectively saved, and meanwhile heat energy is efficiently utilized.

Description

A kind of pre-cold mould refrigerated separation structure
Technical field
The invention belongs to chemical industry process equipment field, particularly relate to a kind of pre-cold mould refrigerated separation structure.
Background technology
High temperature raw material normally directly passes in cooling separator by existing refrigerated separation technique, then by cooling and staticly make organic phase be separated with aqueous phase, but part material consumes energy to the carrying out of technique to directly entering the cooling carrying out impact by cooling water in cooling separator in the condition of high temperature very much, in cooling procedure, need a large amount of energy to carry out cooling water circulation at a high speed, and the heat energy of high temperature raw material cannot obtain well utilizing causing waste.
Summary of the invention
A kind of pre-cold mould refrigerated separation structure is the invention provides for the deficiencies in the prior art part, during use precooling tank, high temperature raw material carries out mild precooling, and then the raw material of preference temperature is inputed in cooling separator, effectively slow down the circulation rate of cooling water, accomplish energy-conservation, heat pump effectively can be utilized simultaneously heat energy to be exported to other power consumptions place and use.
Technical scheme of the present invention is to provide a kind of pre-cold mould refrigerated separation structure, comprise cooling separator, it is characterized in that: described cooling separator one side is provided with the first feed pipe of the raw material for carrying less than 150 DEG C, and the top of another side is provided with discharge nozzle; The below of described discharge nozzle is provided with cooling water outlet pipe, described cooling separator upper surface is provided with cooling water inlet pipe, lower surface is provided with the aqueous phase efferent duct be provided with for carrying lower floor's separator, the entrance point of the first described feed pipe is provided with the precooling tank for the raw material of more than 260 DEG C being pre-chilled to less than 150 DEG C, and the top of described precooling tank is provided with the second feed pipe of the raw material for carrying 260 DEG C.
As preferably of the present invention, be provided with the first heat pipe in described precooling tank, the first described heat pipe is connected with the heat pump be arranged on outside described precooling tank, described heat pump is provided with the second heat pipe for exporting heat energy.
As preferably of the present invention, the bottom of described described cooling separator is downward-sloping to bottom centre by both side ends, forms the aqueous phase being used for water conservancy diversion and exports guide portion.
As preferably of the present invention, described precooling tank and described cooling separator are provided with thermometer.
As preferably of the present invention, the first described feed pipe, described cooling water inlet pipe, described cooling water outlet pipe, described discharge nozzle and described aqueous phase efferent duct are provided with ball valve.
As preferably of the present invention, the caliber of the second described feed pipe is greater than the caliber of described first feed pipe.
The present invention has following beneficial effect:
The present invention has effectively energy-conservation, simultaneously the advantage of efficiency utilization heat energy.
Accompanying drawing explanation
Fig. 1 is the structural representation of the embodiment of the present invention;
In figure, 1-cooling separator; 2-first feed pipe; 3-discharge nozzle; 4-cooling water outlet pipe; 5-cooling water inlet pipe; 6-aqueous phase efferent duct; 7-precooling tank; 8-second feed pipe; 9-first heat pipe; 10-heat pump; 11-second heat pipe; 12-aqueous phase exports guide portion; 13-thermometer; 14-ball valve.
Detailed description of the invention
Below in conjunction with accompanying drawing, the present invention is described in further detail.
As shown in Figure 1, the embodiment of the present invention comprises cooling separator 1, and the bottom of cooling separator 1 is downward-sloping to bottom centre by both side ends, forms the aqueous phase being used for water conservancy diversion and exports guide portion 12.Cooling separator 1 one side is provided with the first feed pipe 2 of the raw material for carrying less than 150 DEG C, and the top of another side is provided with discharge nozzle 3; The below of discharge nozzle 3 is provided with cooling water outlet pipe 4, cooling separator 1 upper surface is provided with cooling water inlet pipe 5, lower surface is provided with the aqueous phase efferent duct 6 be provided with for carrying lower floor's separator, the entrance point of the first feed pipe 2 is provided with the precooling tank 7 for the raw material of more than 260 DEG C being pre-chilled to less than 150 DEG C, and the top of precooling tank 7 is provided with the second feed pipe 8 of the raw material for carrying 260 DEG C.The caliber of the second feed pipe 8 is greater than the caliber of the first feed pipe 2.
As shown in Figure 1, being provided with the first heat pipe 9, first heat pipe 9 in embodiment of the present invention precooling tank 7 and being connected with the heat pump 10 be arranged on outside precooling tank 7, heat pump 10 being provided with the second heat pipe 11 for exporting heat energy.
As shown in Figure 1, embodiment of the present invention precooling tank 7 and cooling separator 1 are provided with thermometer 13.First feed pipe 2, cooling water inlet pipe 5, cooling water outlet pipe 4, discharge nozzle 3 and aqueous phase efferent duct 6 are provided with ball valve 14.
Embodiment recited above is only be described the preferred embodiment of the present invention, not limits the spirit and scope of the present invention.Under the prerequisite not departing from design concept of the present invention; the various modification that this area ordinary person makes technical scheme of the present invention and improvement; all should drop into protection scope of the present invention, the technology contents of request protection of the present invention, all records in detail in the claims.

Claims (6)

1. a pre-cold mould refrigerated separation structure, comprise cooling separator (1), it is characterized in that: described cooling separator (1) side is provided with first feed pipe (2) of the raw material for carrying less than 150 DEG C, and the top of another side is provided with discharge nozzle (3); The below of described discharge nozzle (3) is provided with cooling water outlet pipe (4), described cooling separator (1) upper surface is provided with cooling water inlet pipe (5), lower surface is provided with the aqueous phase efferent duct (6) be provided with for carrying lower floor's separator, the entrance point of described the first feed pipe (2) is provided with the precooling tank (7) for the raw material of more than 260 DEG C being pre-chilled to less than 150 DEG C, and the top of described precooling tank (7) is provided with second feed pipe (8) of the raw material for carrying 260 DEG C.
2. one according to claim 1 pre-cold mould refrigerated separation structure, it is characterized in that: in described precooling tank (7), be provided with the first heat pipe (9), described the first heat pipe (9) is connected with the heat pump (10) being arranged on described precooling tank (7) outside, described heat pump (10) is provided with the second heat pipe (11) for exporting heat energy.
3. one according to claim 1 pre-cold mould refrigerated separation structure, is characterized in that: the bottom of described described cooling separator (1) is downward-sloping to bottom centre by both side ends, forms the aqueous phase being used for water conservancy diversion and exports guide portion (12).
4. one according to claim 1 pre-cold mould refrigerated separation structure, is characterized in that: described precooling tank (7) and described cooling separator (1) are provided with thermometer (13).
5. one according to claim 1 pre-cold mould refrigerated separation structure, is characterized in that: described the first feed pipe (2), described cooling water inlet pipe (5), described cooling water outlet pipe (4), described discharge nozzle (3) and described aqueous phase efferent duct (6) are provided with ball valve (14).
6. one according to claim 1 pre-cold mould refrigerated separation structure, is characterized in that: the caliber of described the second feed pipe (8) is greater than the caliber of described first feed pipe (2).
CN201510592146.4A 2015-09-17 2015-09-17 A kind of pre- cold mould refrigerated separation structure Expired - Fee Related CN105107232B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510592146.4A CN105107232B (en) 2015-09-17 2015-09-17 A kind of pre- cold mould refrigerated separation structure

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510592146.4A CN105107232B (en) 2015-09-17 2015-09-17 A kind of pre- cold mould refrigerated separation structure

Publications (2)

Publication Number Publication Date
CN105107232A true CN105107232A (en) 2015-12-02
CN105107232B CN105107232B (en) 2017-03-29

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Family Applications (1)

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CN201510592146.4A Expired - Fee Related CN105107232B (en) 2015-09-17 2015-09-17 A kind of pre- cold mould refrigerated separation structure

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5209907A (en) * 1990-12-24 1993-05-11 Phillips Petroleum Company Fluid flow control and isolation
CN1687342A (en) * 2005-05-16 2005-10-26 浙江大学 Method for preparing fatty acid through continuous hydrolyzing grease without catalysis in near critical aqueous medium
CN102389684A (en) * 2011-10-14 2012-03-28 中科同创(厦门)环境科技有限公司 Recycling device for exhaust gas of painted organic solvent and method for recycling organic solvent
CN203281068U (en) * 2013-06-19 2013-11-13 温州市森博轻工机械有限公司 Multifunctional extraction concentration recycling set
CN204932941U (en) * 2015-09-17 2016-01-06 湖州新奥特医药化工有限公司 A kind of pre-cold mould refrigerated separation structure

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5209907A (en) * 1990-12-24 1993-05-11 Phillips Petroleum Company Fluid flow control and isolation
CN1687342A (en) * 2005-05-16 2005-10-26 浙江大学 Method for preparing fatty acid through continuous hydrolyzing grease without catalysis in near critical aqueous medium
CN102389684A (en) * 2011-10-14 2012-03-28 中科同创(厦门)环境科技有限公司 Recycling device for exhaust gas of painted organic solvent and method for recycling organic solvent
CN203281068U (en) * 2013-06-19 2013-11-13 温州市森博轻工机械有限公司 Multifunctional extraction concentration recycling set
CN204932941U (en) * 2015-09-17 2016-01-06 湖州新奥特医药化工有限公司 A kind of pre-cold mould refrigerated separation structure

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Granted publication date: 20170329

Termination date: 20170917