CN105084839A - Organosilicon high-performance environment-friendly waterproof powder with capillary crystalline active master batch and method of preparing waterproof layer - Google Patents
Organosilicon high-performance environment-friendly waterproof powder with capillary crystalline active master batch and method of preparing waterproof layer Download PDFInfo
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- CN105084839A CN105084839A CN201510545378.4A CN201510545378A CN105084839A CN 105084839 A CN105084839 A CN 105084839A CN 201510545378 A CN201510545378 A CN 201510545378A CN 105084839 A CN105084839 A CN 105084839A
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Abstract
The invention provides an organosilicon high-performance environment-friendly waterproof powder with capillary crystalline active master batch, which comprises capillary crystalline active master batch, the capillary crystalline active master batch contains calcium carbonate and calcium chloride, wherein the proportion of the calcium carbonate to the calcium chloride is 3.3:1, the granularity of quartz sand is 500 meshes, and the granularity of talcum powder is 2000 meshes. The waterproof powder disclosed by the invention has good capillary crystallinity, moreover, the waterproof powder has micro-expansibility, the density function and the high-effective waterproof effect also can be enhanced, and the waterproof powder also has the advantage of wide application range.
Description
Present patent application is application number: 201310738577.8, and the applying date: 2013.12.30, name is called: a kind of active organosilicon high-performance environment protection type water-proofing powder and utilize this water-proofing powder to prepare the divisional application of the method for waterproof layer.
Technical field
The present invention relates to construction waterproofing engineering technical field, particularly relate to a kind of water-proofing powder, specifically refer to a kind of organosilicon high-performance environment protection type water-proofing powder with the active masterbatch of penetrant crystalline and prepare the method for waterproof layer.
Background technology
At present, along with the development of science and technology, China's building had the development of advancing by leaps and bounds over the past two years, no matter be the construction of dwelling construction or business, development is all comparatively rapid, but meanwhile, the status of consequent buildings waterproof in building at present also more and more comes into one's own, the selection of water-proof material is also varied, and water-proofing powder is the product both arisen at the historic moment after waterproof roll, but also there are some problems.
Existing water-proof material is mainly main raw material with petroleum pitch, there is high temperature trickling, low-temperature embrittleness, deadly defect that easily aging, the life-span is short, can not meet the demand of modern high-grade covil construction and complex industrial building, although occurred that various new type waterproof coiled material is as EPDM rubber waterproof rolling material, PVC roll material and waste butyl rubber waterproof roll etc., but often its production technology and equipments is complicated, use and inconvenient maintenance, and part material is on the high side, cause cost to increase, lack the market competitiveness; On the other hand, various waterproof material quality is uneven, and product exists some problems in low temperature resistant, snappiness and tensile strength etc., and have impact on the quality of waterproofing work, generally speaking, the performance need of water-proof material improves further.
Summary of the invention
The technical problem to be solved in the present invention is for the weak point existing for prior art, a kind of organosilicon high-performance environment protection type water-proofing powder with the active masterbatch of penetrant crystalline is provided and prepares the method for waterproof layer, this water-proofing powder is a kind of novel rigid architectural waterproof material, there is good penetrant crystalline, and there is micro-expansibility, can also increase degree of compactness function and efficient waterproof action, this water-proofing powder also has use range comparatively widely.
Technical solution of the present invention is, a kind of organosilicon high-performance environment protection type water-proofing powder with the active masterbatch of penetrant crystalline is as follows provided, calculate by weight, comprise active silicic acid salt cement 35 ~ 45 parts, quartz sand 25 ~ 30 parts, talcum powder 5 ~ 12 parts, cement waterproof agent 3 ~ 7 parts, the active masterbatch 3 ~ 7 parts of penetrant crystalline, defoamer 0.2 ~ 0.8 part, frostproofer 1 ~ 3 part, air entrapment agent 0.05 ~ 0.2 part, water reducer 0.2 ~ 0.6 part and polysiloxane emulsion 0.2 ~ 0.7 part.
As preferably, the granularity of described quartz sand is 500 orders.
As preferably, described talcous granularity is 2000 orders.
As preferably, containing calcium carbonate and calcium chloride in the active masterbatch of described crystal permeability, wherein the ratio of calcium carbonate and calcium chloride is 3.3:1.
As preferably, described water reducer is powder polycarboxylate.
As preferably, described defoamer is polysiloxane defoamers, and wherein polysiloxane defoamers is formed primarily of dimethione and silicon-dioxide, and wherein the ratio of dimethione and silicon-dioxide is 7:3.
As preferably, described frostproofer main component is propandiol butyl ether.
As preferably, described air entrapment agent is a-sodium olefin sulfonate or alkyl sodium sulfonate.
As preferably, when described water-proofing powder uses and the weight ratio of clear water be 3 ~ 5:1.
Organosilicon high-performance environment protection type water-proofing powder with the active masterbatch of penetrant crystalline prepares a method for waterproof layer,
Step 1: first according to the usage quantity of water-proofing powder, prepare aqueous solvent, the weight ratio of water-proofing powder and water is 3 ~ 5:1, and water temperature is 18 ~ 23 DEG C;
Step 2: first the water of 2/3 is put into pond, then pours in pond by the active silicic acid salt cement of 70%, the quartz sand of 70% and the talcum powder of 70%, and stirs;
Step 3: then add cement waterproof agent, penetrant crystalline active masterbatch, defoamer, frostproofer, air entrapment agent and water reducer while stirring, to stirring;
Step 4: according to the viscosity of mixing mud after stirring in step 3, add remaining active silicic acid salt cement, quartz sand and talcum powder, simultaneously by residue water add regulate form mud mobility be not less than 150mm;
Step 5: finally add polysiloxane emulsion, is stirred to evenly, leaves standstill 8 ~ 10 minutes, obtain anti-grout;
Step 6: anti-grout is smeared to the building surface needing to do WATER REPELLENT, as the first layer, the thickness of the first layer is 1 ~ 2mm, and 20 DEG C leave standstill 18 ~ 20 hours, treat that the first layer solidifies;
Step 7: smear the second layer on the first layer, the thickness of the second layer is 2 ~ 3mm, and 20 DEG C leave standstill 18 ~ 22 hours, treat that two-layer surface solidifies;
Step 8: at second layer surface bedding one deck straw mattress, then leave standstill 7 days, leave standstill in process, sprinkle water every day 3 ~ 5 times, every watering in 6 hours once, form water-proof coating after 7 days.
Organosilicon high-performance environment protection type water-proofing powder with the active masterbatch of penetrant crystalline prepares the method for waterproof layer, the maximum folding strength 5.5N/mm of described waterproof layer
2, maximum compressive strength 30N/mm
2, maximum impermeability pressure 2.0Mpa.
The beneficial effect adopting above technical scheme to bring is: the cement selected is active silicic acid salt cement, used in combination with cement waterproof agent, due to this water-resisting agent mainly with plant higher fatty acid for main component, be added in cement, when cement setting hardens, volumetric expansion thereupon, plays compensate for shrinkage and tension reinforcing steel bar produces prestress and abundant filling concrete gap; Quartz sand dynamics is chosen less, although quartz sand plays skeletal support effect, the quartz sand that particle is less can reduce contact surface, avoids space to produce, and contributes to the intensity and the height that improve waterproof layer, also has the characteristic suppressing material contracts simultaneously; The active masterbatch normality of penetrant crystalline is blended in water-proofing powder, form is comparatively stable, after adding water, there is polycondensation crystalline polamer, proportion relation that is general and active silicic acid salt cement is 8 ~ 15%, can infiltrate cement basic layer inside with water completely, form acicular crystals, the pore occurred in plugging cement basic unit or crackle; Powder polycarboxylate chosen by water reducer, although the price of this water reducer is relatively high, and the use of this water reducer, improve 30% of ultimate compression strength, also have low-shrinkage simultaneously, alkali content is low to moderate less than 0.2%, can save cement 15 ~ 20% with under intensity; In addition, the constituent materials that this water-proofing powder uses is nontoxic, and use range is wide, can be applicable to roofing, inside and outside metope, ground, toilet, kitchen, vault and warehouse waterproof and dampproof, and the gas barrier of skeleton construction is impermeable; Underground civil defense engineering, various pond, high water suction inorganic aggregate, water-soluble building coating waterproof can also be used for; protection color; preventing pollution, emulsion paint, water glass, the additive of 107 glue, petroleum drilling; adjustable mud viscosity and density; prevent drilling well from subsiding, oil well later stage turn on pump; inject producing horizon, prevent that the producing horizon earth's crust skeleton from subsiding, other to be to reduce the special purpose of water-absorbent and impervious waterproof.
Embodiment
In concrete enforcement, water-proofing powder forms as shown in table 1 by the raw material of mass parts:
Table 1:
Note: in table 1, numerical value calculates according to parts by weight.
In table 1, in the component contained by embodiment 1 ~ 5, the granularity of quartz sand is 500 orders, talcous granularity is 2000 orders, and described water reducer is powder polycarboxylate, and defoamer is polysiloxane defoamers, frostproofer main component is propandiol butyl ether, and air entrapment agent is alkyl sodium sulfonate.
The calcium carbonate contained in the active masterbatch of crystal permeability in embodiment 1, embodiment 3 and embodiment 5 and the ratio of calcium chloride are 3.3:1, the ratio of the dimethione that polysiloxane defoamers mainly comprises and silicon-dioxide is 7:3, but the proportion relation difference between each component added.
Proportion relation between each component added described in embodiment 2, embodiment 3 and embodiment 4 is identical, but the calcium carbonate contained in the active masterbatch of crystal permeability in embodiment 2 and the ratio of calcium chloride are 1:1, and the ratio of the dimethione that polysiloxane defoamers mainly comprises and silicon-dioxide is 2:3; The calcium carbonate contained in the active masterbatch of crystal permeability in embodiment 4 and the ratio of calcium chloride are 1:5, and the ratio of the dimethione that polysiloxane defoamers mainly comprises and silicon-dioxide is 3:7.
Proportioning raw materials listed in synopsis 1, a kind of organosilicon high-performance environment protection type water-proofing powder with the active masterbatch of penetrant crystalline prepares the method for waterproof layer,
Step 1: first according to the usage quantity of water-proofing powder, prepare aqueous solvent, the weight ratio of water-proofing powder and water is 3 ~ 5:1, and water temperature is 18 ~ 23 DEG C;
Step 2: first the water of 2/3 is put into pond, then pours in pond by the active silicic acid salt cement of 70%, the quartz sand of 70% and the talcum powder of 70%, and stirs;
Step 3: then add cement waterproof agent, penetrant crystalline active masterbatch, defoamer, frostproofer, air entrapment agent and water reducer while stirring, to stirring;
Step 4: according to the viscosity of mixing mud after stirring in step 3, add remaining active silicic acid salt cement, quartz sand and talcum powder, simultaneously by residue water add regulate form mud mobility be not less than 150mm;
Step 5: finally add polysiloxane emulsion, is stirred to evenly, leaves standstill 8 ~ 10 minutes, obtain anti-grout;
Step 6: anti-grout is smeared to the building surface needing to do WATER REPELLENT, as the first layer, the thickness of the first layer is 1 ~ 2mm, and 20 DEG C leave standstill 18 ~ 20 hours, treat that the first layer solidifies;
Step 7: smear the second layer on the first layer, the thickness of the second layer is 2 ~ 3mm, and 20 DEG C leave standstill 18 ~ 22 hours, treat that two-layer surface solidifies;
Step 8: at second layer surface bedding one deck straw mattress, then leave standstill 7 days, leave standstill in process, sprinkle water every day 3 ~ 5 times, every watering in 6 hours once, form water-proof coating after 7 days.
Through detecting the water-proof coating in above-described embodiment 1 ~ 5 made by water-proofing powder, the technical performance index reached is as shown in table 2:
Table 2:
According to shown in table 2, each embodiment of embodiment 1 ~ 5 is through identical using method, and obtained waterproof layer, learn through detection, embodiment 1 ~ 5 all can meet the service requirements of industry standard, but comprehensively each performance index, the waterproof layer performance that embodiment 3 water-proofing powder obtains is the highest, be a kind of technical scheme of optimum.
In the above-described embodiments, preferred forms of the present invention is described, obviously, under inventive concept of the present invention, still can make a lot of change.At this, should illustrate, any change made under inventive concept of the present invention all will fall within the scope of protection of the present invention.
Claims (3)
1. with an organosilicon high-performance environment protection type water-proofing powder for the active masterbatch of penetrant crystalline, it is characterized in that: comprise the active masterbatch of penetrant crystalline, containing calcium carbonate and calcium chloride in the active masterbatch of described penetrant crystalline, wherein the ratio of calcium carbonate and calcium chloride is 3.3:1.
2. the organosilicon high-performance environment protection type water-proofing powder with the active masterbatch of penetrant crystalline according to claim 1, it is characterized in that: also comprise quartz sand, the granularity of described quartz sand is 500 orders.
3. the organosilicon high-performance environment protection type water-proofing powder with the active masterbatch of penetrant crystalline according to claim 1, it is characterized in that: also comprise talcum powder, described talcous granularity is 2000 orders.
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| CN201510545378.4A CN105084839B (en) | 2013-12-30 | 2013-12-30 | A kind of organosilicon high-performance environment protection type waterproof powder and the method for preparing waterproof layer with penetrant crystalline activity masterbatch |
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| CN201310738577.8A CN103708798B (en) | 2013-12-30 | 2013-12-30 | A kind of active organosilicon high-performance environment protection type water-proofing powder and utilize this water-proofing powder to prepare the method for waterproof layer |
| CN201510545378.4A CN105084839B (en) | 2013-12-30 | 2013-12-30 | A kind of organosilicon high-performance environment protection type waterproof powder and the method for preparing waterproof layer with penetrant crystalline activity masterbatch |
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| CN201510545017.XA Active CN105236815B (en) | 2013-12-30 | 2013-12-30 | A kind of froth breaking type organosilicon high-performance environment protection type waterproof powder and the method for preparing waterproof layer |
| CN201310738577.8A Active CN103708798B (en) | 2013-12-30 | 2013-12-30 | A kind of active organosilicon high-performance environment protection type water-proofing powder and utilize this water-proofing powder to prepare the method for waterproof layer |
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| CN201310738577.8A Active CN103708798B (en) | 2013-12-30 | 2013-12-30 | A kind of active organosilicon high-performance environment protection type water-proofing powder and utilize this water-proofing powder to prepare the method for waterproof layer |
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| CN104478261A (en) * | 2014-12-12 | 2015-04-01 | 宜兴天力化工纳米科技有限公司 | Calcium carbonate and calcium chloride complexing agent and preparation method thereof |
| CN104844079A (en) * | 2015-04-03 | 2015-08-19 | 杭州泰正建材有限公司 | Cement-based capillary crystalline waterproof material and preparation method thereof |
| CN108083719A (en) * | 2017-11-21 | 2018-05-29 | 四川铁科新型建材有限公司 | A kind of permanent seal cooling cracking resistance infiltration water proof anti-corrosive paint and preparation method thereof |
| CN108911649B (en) * | 2018-07-11 | 2021-01-05 | 重庆赛高建材有限公司 | Flowable tile glue |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1099364A (en) * | 1994-07-30 | 1995-03-01 | 阮庆生 | Organosilicon cement waterproof powder and its producing method |
| CN102718455A (en) * | 2012-07-02 | 2012-10-10 | 安徽朗凯奇建材有限公司 | Cement based capillary crystalline high-performance waterproofing powder and application thereof |
| CN102747751A (en) * | 2012-07-02 | 2012-10-24 | 安徽朗凯奇建材有限公司 | Underground waterproof system and construction method thereof |
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| GB0416952D0 (en) * | 2004-07-30 | 2004-09-01 | Renishaw Plc | Scale making method |
| CN102786275B (en) * | 2012-08-25 | 2014-12-31 | 广东韶钢松山股份有限公司 | Cement-based infiltration crystalline waterproof material |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1099364A (en) * | 1994-07-30 | 1995-03-01 | 阮庆生 | Organosilicon cement waterproof powder and its producing method |
| CN102718455A (en) * | 2012-07-02 | 2012-10-10 | 安徽朗凯奇建材有限公司 | Cement based capillary crystalline high-performance waterproofing powder and application thereof |
| CN102747751A (en) * | 2012-07-02 | 2012-10-24 | 安徽朗凯奇建材有限公司 | Underground waterproof system and construction method thereof |
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| CN103708798B (en) | 2015-11-18 |
| CN105084839B (en) | 2017-06-23 |
| CN103708798A (en) | 2014-04-09 |
| CN105236815A (en) | 2016-01-13 |
| CN105236815B (en) | 2017-06-23 |
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Effective date of registration: 20180410 Address after: Taiwan Town Industrial Park 262700 Shandong city in Weifang Province, Shouguang City (town, village head) Patentee after: Weifang Zhengtai Waterproof Material Co., Ltd. Address before: Taiwan Town Industrial Park 262700 Shandong city in Weifang Province, Shouguang City (town, village head) Patentee before: Liu Taian |
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