CN105078833A - Lepidium meyenii walp facial or breast mask and preparation method thereof - Google Patents

Lepidium meyenii walp facial or breast mask and preparation method thereof Download PDF

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CN105078833A
CN105078833A CN201510559580.2A CN201510559580A CN105078833A CN 105078833 A CN105078833 A CN 105078833A CN 201510559580 A CN201510559580 A CN 201510559580A CN 105078833 A CN105078833 A CN 105078833A
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skin
facial film
meyenii walp
facial
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CN105078833B (en
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马乐新
杨明丽
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Guangdong Changhao Pharmacy Co Ltd
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Guangdong Changhao Pharmacy Co Ltd
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Abstract

The invention discloses a lepidium meyenii walp facial or breast mask and a preparation method thereof. According to the method, non-woven fabric is soaked in essence and then the lepidium meyenii walp facial or breast mask can be prepared, wherein the essence comprises raw materials in parts by weight as follows: 80 parts of water, 1-3 parts of 1,2-propylene glycol, 2-6 parts of 1,3-butanediol, 0.5-3.5 parts of a lepidium meyenii root extract, 0.3-0.5 parts of sodium hyaluronate, 2-6 parts of a glycyrrhiza glabra root extract, 2-6 parts of a licorice extract, 0.5-1 part of nicotinamide, 1-3 parts of hydrolyzed vegetable protein, 0.1-0.3 parts of dipotassium glycyrrhizinate, 0.1-0.3 parts of dexpanthenol, 0.25-0.5 parts of xanthan gum, 0.1-0.3 parts of allantoin and 0.1-0.3 parts of sodium benzoate. The lepidium meyenii walp facial or breast mask can restrain excess grease effectively, balances oil and water of the skin, has a moisturizing effect while oil control is realized, keeps moisturizing and nourishing for a long time and softens the skin. The lepidium meyenii walp facial or breast mask is rich in the lepidium meyenii root extract, can enhance a dermal epidermal junction layer structure, has good anti-aging effect, skin tightening effect and the like, improves the skin elasticity, regenerates deep skin and guarantees skin vitality.

Description

Lepidinm meyenii Walp facial film, pleura and preparation method thereof
Technical field
The present invention relates to facial film, pleura and preparation method thereof, be specifically related to a kind of Lepidinm meyenii Walp facial film, pleura and preparation method thereof.
Background technology
Lepidinm meyenii Walp, formal name used at school: LepidiummeyeniiWalp, Spanish: Maca.Mainly producing in South America Andes normal pulse Chinese yunnan Lijing, is a kind of crucifer.Leaf is oval, and rhizome likeness in form turnip radish, edible is a kind of natural food, and nutrition is enriched, and has the reputation of " South America Radix Ginseng ".The hypocotyl of Lepidinm meyenii Walp may be golden or faint yellow, red, purple, blueness, black or green.Flaxen the most common, and shape, taste are also best.Lepidinm meyenii Walp is rich in high unit nutrient, human body is had to the function of nourishing and fit keeping function.
Lepidinm meyenii Walp originates in High aititude mountain area, is suitable for growing in High aititude, low latitudes, high day and night temperature, subacidity sandy loam, sun-drenched soil; Plantation area is mainly distributed in Andes, state, South America, and the Yulong Xueshan area of Chinese yunnan Lijing, and there is suitable kind of soil of larger area this two large main producing region.And also there is a small amount of plantation in other areas of Chinese yunnan and the area such as Xinjiang, Tibet.
Italian scientist DiniA has systematically drawn the chemical composition composition in the dry root of Maca first in 1994: protein content is more than 10% (protein content of the Maca kind of Hu Ning lakeside is more than 14%), the carbohydrate of 59%; The fiber of 8.5%, include the mineral such as abundant zinc, calcium, ferrum, titanium, rubidium, potassium, sodium, copper, manganese, magnesium, strontium, phosphorus, iodine, and containing vitamin C, B1, B2, B6, A, E, B12, B5, fat content is not high but mostly wherein be unsaturated fatty acid, the content of linoleic acid plus linolenic acid reaches more than 53%, and natural activity composition comprises alkaloid, glucosinolate and catabolite benzyl isothiocyanate, sterol, polyphenols etc.1999, American scientist has found vegetable active composition new containing two classes in Maca, macamides (macamides) and Maca rare (macaenes), and determine that these two kinds of materials have remarkable effect to balanced human's hormone secretion, the natural hormone electromotor so Maca is otherwise known as.In the specific aim research of Maca product, find again several special Maca alkaloid, along with going deep into of research, also had the activated novel substance of more tool in Maca and be isolated and identified.Ministry of Public Health is national new resource food at approval Lepidinm meyenii Walp in 2011.
Facial film is the important content in skin nursing, and for the regular application facial film of all kinds of skin characteristic, can make oily skin defat, thick pore is restrained, and the skin of withered gauffer recovers gloss, and the inflammation of skin sore skin is inhibited.Facial film makes skin seem salubrious after using, smooth and pure white delicacy, this is because when facial film is coated on skin, facial film and skin produce affinity, along with the drying gradually of facial film, skin temperature rise, blood circulation is accelerated, skin-tightening and tension force are strengthened, the sebum of skin secretion and moisture reverse osmosis are in horny layer, epidermis softness is unfolded, pore instinct is opened, effective ingredient in facial film infiltrates skin and is absorbed, facial film is tightly connected with skin simultaneously, when removing facial film, aging cutin on skin, in pore deep layer dirt also by while leukorrhagia, make skin totally pure and fresh.
The principle of facial film, utilize the blink covering face exactly, the air that temporary transient isolation is extraneous and pollution, improve skin temperature, the pore expansion of skin, promote sweat gland secretion and metabolism, make the oxygen content of skin increase, be conducive to the oil substances that skin gets rid of the metabolic product of epidermis cell and accumulation, the moisture in facial film infiltrates the horny layer of skin epidermis, skin becomes soft, and skin naturally light is flexible.
Along with the raising of people's quality of the life and people are to the pursuit of U.S., cosmetics kind is more and more various.At present, face mask of traditional Chinese medicine is one of beauty treatment educational circles effective whitening regime, and especially some Chinese medicine extraction liquid have the effect of good toxin expelling, speckle dispelling, reparation, skin care, also by being applied in facial film gradually.
Pleura is the important content in skin nursing, for all kinds of skin characteristic at female breast position regular application pleura, can make the defat of chest oily skin, thick pore is restrained, and the skin of withered gauffer recovers gloss, and the inflammation of skin sore skin is inhibited.
At present, a kind of Lepidinm meyenii Walp facial film, pleura is not had.
Summary of the invention
For above shortcomings in prior art, one of technical problem to be solved by this invention is to provide the preparation method of a kind of Lepidinm meyenii Walp facial film, pleura.
Two of technical problem to be solved by this invention is to provide a kind of Lepidinm meyenii Walp facial film, pleura.
The present invention seeks to be achieved through the following technical solutions:
The preparation method of a kind of Lepidinm meyenii Walp facial film, pleura, be made up of following step: non-woven fabrics is soaked in essence, described essence comprises the raw material of following weight parts: 80 parts, water, steps because of Semen Lepidii (LEPIDIUMMEYENII) root extract 0.5-3.5 part.
Preferably, described essence comprises the raw material of following weight parts: 80 parts, water, 1, 2-propylene glycol 1-3 part, 1, 3-butanediol 2-6 part, step because of Semen Lepidii (LEPIDIUMMEYENII) root extract 0.5-3.5 part, hyaluronate sodium 0.3-0.5 part, Glycyrrhiza glabra L. (GLYCYRRHIZAGLABRA) root extract 2-6 part, Radix Glycyrrhizae (GLYCYRRHIZAURALENSIS) extract 2-6 part, nicotiamide 0.5-1 part, hydrolyzed vegetable protein 1-3 part, glycyrrhizic acid dipotassium 0.1-0.3 part, Dexpanthenol 0.1-0.3 part, xanthan gum 0.25-0.5 part, allantoin 0.1-0.3 part, sodium benzoate 0.1-0.3 part.
Preferably, described essence is made up of the raw material of following weight parts: 80 parts, water, 1,2-propylene glycol 1-3 part, 1,3 butylene glycol 2-6 part, step because of Semen Lepidii root extract 0.5-3.5 part, hyaluronate sodium 0.3-0.5 part, Glycyrrhiza glabra L. root extract 2-6 part, Radix Glycyrrhizae extract 2-6 part, nicotiamide 0.5-1 part, hydrolyzed vegetable protein 1-3 part, glycyrrhizic acid dipotassium 0.1-0.3 part, Dexpanthenol 0.1-0.3 part, xanthan gum 0.25-0.5 part, allantoin 0.1-0.3 part, sodium benzoate 0.1-0.3 part, biological preservative 0.2-0.6 part.
Preferably, described biological preservative is made up of 40-60wt% α-curcumene and 40-60wt% demethoxycurcumin.
Preferably, the mass volume ratio of described non-woven fabrics and essence is 1g:10mL-1g:50mL.
Present invention also offers a kind of Lepidinm meyenii Walp facial film, pleura (that is: Lepidinm meyenii Walp facial film or pleura), be prepared from by said method.
Concrete, in the present invention:
1,2-PD, No. CAS: 57-55-6;
1,3 butylene glycol, No. CAS: 107-88-0;
Hyaluronate sodium, No. CAS: 9067-32-7;
Nicotiamide, No. CAS: 98-92-0;
Hydrolyzed vegetable protein, No. CAS: 100209-45-8;
Glycyrrhizic acid dipotassium, No. CAS: 68797-35-3;
Dexpanthenol, No. CAS: 81-13-0;
Xanthan gum, No. CAS: 11138-66-2;
Allantoin, No. CAS: 97-59-6;
Sodium benzoate, No. CAS: 532-32-1;
Glycyrrhiza glabra L. root extract, No. CAS: 84775-66-6;
Radix Glycyrrhizae extract, No. CAS: 97676-23-8;
α-curcumene, No. CAS: 644-30-4.Demethoxycurcumin, No. CAS: 24939-17-1.Curcumin, No. CAS: 458-37-7.
Step because of Semen Lepidii (LEPIDIUMMEYENII) root extract, have another name called Maca root extract, product English name: Macarootextract (macadermTM), product I NCI name: Lepidiummeyeniirootextract.Can by commercially available or prepare, as: natural organic pueraria root powder that Guangdong Chang Hao Pharmaceutical limited company produces.
Described non-woven fabrics, can prepare according to patent ZL200610054035.9 embodiment 1, also can adopt commercially available silk non-woven fabric, if the place of production is the high-quality silk non-woven fabric of Taiwan.
The using method of Lepidinm meyenii Walp facial film of the present invention is: before using facial film, first deeply clean facial, then facial film is overlying on face, and make facial film enter to paste skin, after 15-25 minute, facial film active substance is absorbed by the skin, and takes facial film, without the need to washing;
During first use, be used in conjunction 3 days, every day 1, effect is better, and follow-up suggestion uses weekly 2-4 time for good;
Hot weather uses, and is put into by facial film bag after refrigerator and cooled is hidden and uses, can feel more comfortable, more beautiful;
Cold snap uses, and soaks and uses for 5 minutes, make facial film temperature slightly higher than body temperature, use more comfortable in the warm water of 45 DEG C, and warm facial film is more conducive to skin absorption;
After shower, or use with after hot towel flush coat 10min, facial pores fully opens, advantageously in absorbing the nutritional labeling in facial film.
Facial film of the present invention effectively can suppress excess oil, balance skin profit, also has moisturizing effect, lasting moisturizing, softening skin while control oil.Especially, the present invention is rich in and is stepped because of Semen Lepidii root extract, can strengthen dermoepidermal articulamentum structure, and have good defying age and effects such as skin of compacting, strengthen elasticity of skin, deep layer repairs skin, makes skin dynamic.
In preferred scheme, Lepidinm meyenii Walp facial film of the present invention is after interpolation biological preservative, and the shelf-life is significantly extended.
The using method of Lepidinm meyenii Walp pleura of the present invention is: get Lepidinm meyenii Walp pleura, spreads on breast by Lepidinm meyenii Walp pleura, Lepidinm meyenii Walp pleura and skin is adjacent to, after 20-30 minute, throws off; Can massage gently after taking off Lepidinm meyenii Walp pleura, essential ingredient is more easily permeated.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.Stepping because Semen Lepidii root extract is natural organic pueraria root powder that Guangdong Chang Hao Pharmaceutical limited company produces in embodiment.
Embodiment 1
(1) take raw material according to the corresponding weight portion of table 1, be uniformly mixed, preparation essence;
(2) non-woven fabrics is prepared according to the corresponding embodiment 1 of patent ZL200610054035.9;
(3), after non-woven fabrics being cut into conventional facial film size, be immersed in above-mentioned essence; The mass volume ratio of non-woven fabrics and essence is 1g:25mL, and soak time is 30min, the Lepidinm meyenii Walp facial film of obtained embodiment 1.
In addition,
In step (3), as non-woven fabrics is cut to udder size, Lepidinm meyenii Walp pleura can be obtained.
Table 1: essence formula table unit: weight portion
Raw material Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5 Embodiment 6
Water 80 80 80 80 80 80
1,2-PD 2 2 2 2 2 2
1,3 butylene glycol 4 4 4 4 4 4
Step because of Semen Lepidii root extract 2 2 2 2 2 2
Hydrolyzed vegetable protein 2 2 2 2 2 2
Glycyrrhiza glabra L. root extract 4 4 4 4 4 4
Radix Glycyrrhizae extract 4 4 4 4 4 4
Hyaluronate sodium 0.4 0.4 0.4 0.4 0.4 0.4
Nicotiamide 0.8 0.8 0.8 0.8 0.8 0.8
Glycyrrhizic acid dipotassium 0.2 0.2 0.2 0.2 0.2 0.2
Dexpanthenol 0.2 0.2 0.2 0.2 0.2 0.2
Xanthan gum 0.4 0.4 0.4 0.4 0.4 0.4
Allantoin 0.2 0.2 0.2 0.2 0.2 0.2
Sodium benzoate 0.2 0.2 0.2 0.2 0.2 0.2
α-curcumene 0.2 0.4 - - - 0.2
Demethoxycurcumin 0.2 - 0.4 - - -
Curcumin - - - - 0.4 0.2
Test case 1
After respectively the Lepidinm meyenii Walp facial film that embodiment 1-6 is obtained being enclosed sealing bags respectively, place 10 days under being placed in ambient temperature 40 DEG C of relative humidity 85% environment, open packaging, adopt " GB/T4789.2-2010 microbiological test of food hygiene total plate count mensuration " to carry out total plate count test.Concrete test result, in table 2.
Table 2: total plate count test chart
Total plate count, cfu/g
Embodiment 1 5.0×10 4
Embodiment 2 7.2×10 4
Embodiment 3 7.6×10 4
Embodiment 4 4.9×10 5
Embodiment 5 8.7×10 4
Embodiment 6 8.1×10 4
After interpolation biological preservative, total plate count obviously declines, and shelf life of products is significantly extended.
Test case 2
After respectively the Lepidinm meyenii Walp facial film that embodiment 1-6 is obtained being enclosed sealing bags respectively, under being placed in ambient temperature 40 DEG C, relative humidity 85% environment, continuous observation is also tested, and concrete outcome sees the following form 3.
Table 3: preservative challenge testing result table
Observe phenomena
Embodiment 1 No abnormality seen after 100 days, pure in smell
Embodiment 2 Rose after 79 days bag, and occur mildew after unlatching, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient
Embodiment 3 Rose after 73 days bag, and occur mildew after unlatching, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient
Embodiment 4 Rose after 24 days bag, and occur mildew after unlatching, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient
Embodiment 5 Rose after 52 days bag, and occur mildew after unlatching, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient
Embodiment 6 Rose after 65 days bag, and occur mildew after unlatching, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient
Test case 3
The Lepidinm meyenii Walp facial film obtained to embodiment 1 carries out defying age test, and test index is skin elasticity and keratodermatitis moisture.
Skin elasticity year skin aging and reducing, therefore skin elasticity is one of important symbol judging skin aging, is the requisite project of efficacy detection of anti-aging cosmetics.
Experimental technique: select healthy, skin normal, without the tested crowd of cosmetic allergic contact dermatitis history, age 20-35 year, wherein male 50, women 50.Within one week, be a course for the treatment of, totally four courses for the treatment of, by facial cleansing at every turn before applying ointment or plaster, and at every turn clean time identical, corresponding product of applying ointment or plaster after skin dries, each group to be applied ointment or plaster corresponding product 1 time every day, and each one pastes.
Facial film group of the present invention, the facial film made in embodiment of applying ointment or plaster 1, matched group is applied ointment or plaster not containing the substrate facial film of essence, and its substrate is identical with the embodiment of the present invention 1 facial film.
Measure: select Face and cheek as test zone, test after product 10min to be used.Use skin elasticity tester to measure skin elasticity curve, according to amount of tension and the resilience data of skin, can assess the moisturizing of cosmetics and anti-senescence function.
Experimental result: skin elasticity test is based on suction and stretching principle, a negative pressure is produced on the surface of tested skin, by in skin inspiration special test probe, skin is inhaled into the degree of depth and is recorded by a non-contact optical detection system, measurement result represents with an index usually, unit is 1, and numerical value is larger, illustrates that skin elasticity is stronger.The impact of facial film of the present invention on skin elasticity is as shown in table 4.
Table 4: skin elasticity test value table
Group 0 week 1 week 2 weeks 3 weeks 4 weeks
Embodiment 1 facial film 0.495 0.523 0.610 0.651 0.675
Matched group 0.508 0.519 0.531 0.554 0.572
Note: compare p < 0.05 with matched group
As can be seen from Table 4, the embodiment of the present invention of applying ointment or plaster 1 facial film group buccal place's elasticity number and matched group compare, facial film of the present invention obviously can strengthen skin elasticity, illustrate that facial film of the present invention has good defying age and effects such as skin of compacting, strengthen elasticity of skin, deep layer repairs skin, makes skin dynamic.
Moisture is one of important moulding material of epiderm skin horny layer, and during skin aging, horny layer of epidermis is thinning, and in horny layer, natural moisture preserving component content reduces, and skin hydration ability declines, and moisture of skin is lost to be increased; Meanwhile, there is histological structure and morphological change and made skin engender fine wrinkles in cell shrinkage Telatrophy.
By the degree of skin aging and effect of Moisturizer can be reflected to a certain extent to the mensuration of moisture of skin.
Experimental technique: select healthy skin, without the tested crowd of cosmetic allergic contact dermatitis history, age 20-35 year, wherein male 50, women 50.Room temperature 25 DEG C ± 1 DEG C; Humidity 50% ± 5%.Clean face during test, and everyone clean time is identical, selects Face and cheek 4cm × 4cm skin as test zone, facial film of applying ointment or plaster after skin dries.
Facial film group of the present invention, the facial film that embodiment of applying ointment or plaster 1 is made; Matched group is applied ointment or plaster not containing the substrate facial film of essence, and its substrate is identical with the embodiment of the present invention 1 facial film.
Measure: at Face and cheek (4cm × 4cm) test zone, after product to be used, 10min tests.
(1) water content of Face and cheek skin is measured with digital skin moisture detector.Use after corresponding product after 1h, 2h, 4h, 6h, survey Face and cheek moisture content of skin, measure and average for three times.
(2) water loss amount of Face and cheek skin is measured with percutaneous moisture loss measuring instrument.Use after corresponding product after 1h, 2h, 4h, 6h, survey Face and cheek moisture of skin windage, measure and average for three times.
Experimental result: use the change of keratodermatitis capacitance before and after product weigh the change of water content of stratum corneum thus evaluate the moisture-keeping efficacy of cosmetics by test.The method carries out quantification to skin keratin moisture, can react the change of skin moisture content delicately, and favorable reproducibility, be one of method that current moisture-keeping cosmetics efficacy assessments is conventional.The impact of this product on skin moisture content is as shown in table 5.
Table 5: moisture test value table
Group 0h 1h 2h 4h 6h
Embodiment 1 facial film 30.12 59.98 58.67 56.24 55.77
Matched group 32.56 33.86 33.27 32.74 31.79
Note: compare p < 0.05 with matched group
As can be seen from Table 5, the embodiment of the present invention of applying ointment or plaster 1 facial film group horny layer moisture and matched group compare, facial film of the present invention can moisturizing effective, moisture preserving time is long, illustrate that facial film of the present invention effectively can suppress excess oil, balance skin profit, also there is moisturizing effect, lasting moisturizing, softening skin while control oil.
Moisture of skin windage reflects pilot region moisture loss Changing Pattern in time in test period, it represent the lock water function of cosmetics.Its value is less, and moisture loss is fewer, and lock water effect is stronger.The impact that facial film of the present invention scatters and disappears on moisture of skin is as shown in table 6.
Table 6: moisture loss test value table
Group 0h 1h 2h 4h 6h
Embodiment 1 facial film 11.46 8.11 7.03 7.68 8.22
Matched group 11.01 10.91 10.87 10.94 11.67
Note: compare p < 0.05 with matched group
As shown in Table 6, the embodiment of the present invention of applying ointment or plaster 1 facial film group horny layer moisture and matched group compare, and after facial film of the present invention, moisture of skin windage declines obviously, and can maintain the long period, illustrate that facial film of the present invention has the lasting lock water effect keeping moisture.

Claims (6)

1. a preparation method for Lepidinm meyenii Walp facial film, pleura, is made up of following step: soaked in essence by non-woven fabrics, it is characterized in that, described essence comprises the raw material of following weight parts: 80 parts, water, steps because of Semen Lepidii root extract 0.5-3.5 part.
2. the preparation method of Lepidinm meyenii Walp facial film according to claim 1, pleura, it is characterized in that, described essence comprises the raw material of following weight parts: 80 parts, water, 1,2-PD 1-3 part, 1,3-butanediol 2-6 part, step because of Semen Lepidii root extract 0.5-3.5 part, hyaluronate sodium 0.3-0.5 part, Glycyrrhiza glabra L. root extract 2-6 part, Radix Glycyrrhizae extract 2-6 part, nicotiamide 0.5-1 part, hydrolyzed vegetable protein 1-3 part, glycyrrhizic acid dipotassium 0.1-0.3 part, Dexpanthenol 0.1-0.3 part, xanthan gum 0.25-0.5 part, allantoin 0.1-0.3 part, sodium benzoate 0.1-0.3 part.
3. Lepidinm meyenii Walp facial film according to claim 2, the preparation method of pleura, it is characterized in that, described essence is made up of the raw material of following weight parts: 80 parts, water, 1, 2-propylene glycol 1-3 part, 1, 3-butanediol 2-6 part, step because of Semen Lepidii root extract 0.5-3.5 part, hyaluronate sodium 0.3-0.5 part, Glycyrrhiza glabra L. root extract 2-6 part, Radix Glycyrrhizae extract 2-6 part, nicotiamide 0.5-1 part, hydrolyzed vegetable protein 1-3 part, glycyrrhizic acid dipotassium 0.1-0.3 part, Dexpanthenol 0.1-0.3 part, xanthan gum 0.25-0.5 part, allantoin 0.1-0.3 part, sodium benzoate 0.1-0.3 part, biological preservative 0.2-0.6 part.
4. the preparation method of Lepidinm meyenii Walp facial film according to claim 3, pleura, is characterized in that, described biological preservative is made up of 40-60wt% α-curcumene and 40-60wt% demethoxycurcumin.
5. the Lepidinm meyenii Walp facial film according to any one of claim 1-4, the preparation method of pleura, is characterized in that, the mass volume ratio of described non-woven fabrics and essence is 1g:10mL-1g:50mL.
6. Lepidinm meyenii Walp facial film, a pleura, according to any one of claim 1-5, method is prepared from.
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CN105380898A (en) * 2015-12-09 2016-03-09 张雅红 Formula of chest/neck mask and manufacturing method thereof
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CN108888562A (en) * 2018-08-30 2018-11-27 广东长昊药业股份有限公司 A kind of eye mask and preparation method thereof
CN109125165A (en) * 2018-08-30 2019-01-04 广东长昊药业股份有限公司 A kind of compact face of repairing is releived facial mask and preparation method thereof

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