CN105064874A - Method for preparing aerogel heat insulation glass - Google Patents
Method for preparing aerogel heat insulation glass Download PDFInfo
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- CN105064874A CN105064874A CN201510559824.7A CN201510559824A CN105064874A CN 105064874 A CN105064874 A CN 105064874A CN 201510559824 A CN201510559824 A CN 201510559824A CN 105064874 A CN105064874 A CN 105064874A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A30/00—Adapting or protecting infrastructure or their operation
- Y02A30/24—Structural elements or technologies for improving thermal insulation
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A30/00—Adapting or protecting infrastructure or their operation
- Y02A30/24—Structural elements or technologies for improving thermal insulation
- Y02A30/242—Slab shaped vacuum insulation
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A30/00—Adapting or protecting infrastructure or their operation
- Y02A30/24—Structural elements or technologies for improving thermal insulation
- Y02A30/249—Glazing, e.g. vacuum glazing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02B—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
- Y02B80/00—Architectural or constructional elements improving the thermal performance of buildings
- Y02B80/10—Insulation, e.g. vacuum or aerogel insulation
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02B—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
- Y02B80/00—Architectural or constructional elements improving the thermal performance of buildings
- Y02B80/22—Glazing, e.g. vaccum glazing
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- Securing Of Glass Panes Or The Like (AREA)
- Joining Of Glass To Other Materials (AREA)
Abstract
The invention provides a method for preparing aerogel heat insulation glass. The method includes the following steps that (1) glass cavity preparation is made, and at least two pieces of glass and spacing bars are bonded by glue into airtight cavities comprising at least one inlet and at least one outlet; (2) filling is conducted, and aerogel particles are added into the airtight cavities from the at least one inlet; (3) air is exhausted, and air exhausting treatment is conducted on the at least one outlet in the filling process; (4) inlet and outlet sealing is conducted, and the at least one inlet and the at least one outlet are sealed through sealing elements; (5) sealing is performed, and the periphery of the aerogel heat insulation glass is sealed by sealant. The aerogel heat insulation glass has good adiabaticity and transparency, and is suitable for the fields of doors and windows, curtain wall glass, lighting roofs and the like of green buildings, ultralow energy consumption buildings and almost zero energy consumption buildings.
Description
Technical field
The present invention relates to glass making techniques field, particularly a kind of preparation method of aerogel thermal insulation glass.
Background technology
Glass is that a kind of transparency, intensity and hardness are all very high, air-locked material, and glass in chemical inertness, also can not work with biology, so purposes widely in surroundings.For the glass of building in prior art, be mainly used for closing, daylighting, insulation.But in the winter of cold district, the heat insulation effect of glass is unsatisfactory, and in the summer of hot-summer and cold-winter area or hot summer and warm winter region, the effect of heat insulation of glass is also undesirable.Simultaneously along with China's rapid development of economy, the requirement of people to quality of life is more and more higher, and building doors and windows, curtain wall are increasing, result through door and window, curtain wall the proportion of exchange heat in building and outside heat exchange increasing.In order to be reduced by the exchange heat of glass door and window curtain wall, recent domestic develops many heat insulation glass, and it mainly contains three kinds by structure, the hollow glass that (1) is made up of two-layer or multilayer simple glass; (2) by the hollow glass being coated with low-radiation film coated glass and forming; (3) by the middle vacuum glass be pumped into negative pressure and formed of double-layer glass.The hollow glass that wherein heat reflection plated film or low-emission coated (low-E) glass are formed is the main product of current energy-saving glass.Heat-reflection coated glass and low radiation coated glass can stop sunshine to enter indoor in summer to greatest extent, and stop the far infrared radiation from outdoor to greatest extent.But needing the winter of heating, it is obviously outdated that the outer heat energy of air lock enters indoor, and affect the transmitance of visible ray.Vacuum glass is because of the reason such as safety and application life, and large-scale application is still needed the time.Therefore a kind of heat insulation glass with good thermal insulation and light transmission of exploitation is badly in need of.
Summary of the invention
The technical problem to be solved in the present invention is: the preparation method providing a kind of aerogel thermal insulation glass, the heat insulation glass that this preparation method produces has good thermal insulation and light transmission, can be widely used in the fields such as the door and window of green building and super low energy consumption building and nearly zero energy consumption building, cladding glass and lighting roof.
Solution of the present invention is achieved in that a kind of preparation method of aerogel thermal insulation glass, comprises the following steps:
(1) at least two blocks of glass and spacer bar to be glued together to make with glue and comprise at least one import and at least one closed cavity exported by the making of glass cavity;
(2) filler, joins closed cavity by aerogel particle from import;
(3) bleed, in the process of filler, outlet is bled process;
(4) seal, with seal by import and exit seal;
(5) seal, the surrounding fluid sealant of aerogel thermal insulation glass is carried out encapsulation process.
So, pass through above-mentioned steps, one can be obtained by least two blocks of glass as housing, there is sealed cavity of at least one import and at least one outlet and in cavity, be provided with the aerogel thermal insulation glass of aerogel particle, this aerogel thermal insulation glass is because wherein set aeroge is graininess, thus there is good light scattering property, there is very excellent barrier property in radiation thermal conduction, simultaneously, because this aerogel thermal insulation glass chamber portion has carried out encapsulation process, the cavity of described aerogel thermal insulation inside glass is after process of bleeding, the drying property of its inside obtains sufficient guarantee, simultaneously, because there is negative pressure, spacer bar clamps closely knit by two blocks of glass, making it, in use air and steam can not enter cavity inside, be not easy to form dew condensation phenomenon, and, because Specific surface area that aeroge is very thin effectively limit the propagation of local thermal excitation, nanometer micropore hole inhibits gas molecule to heat conducting effect, the refractive index of silica-based aerogel is close to l, and more than 100 are reached to the ratio burying in oblivion coefficient that is infrared and visible ray, can effectively through sunshine, and stop the infrared emanation of environment temperature, therefore, the aerogel thermal insulation glass adopting said method to obtain not only has good radiation thermal conduction barrier property, also possesses good advection heat conduction barrier property simultaneously.
Another technical scheme of the present invention is on above-mentioned basis, in described filler step, the also closely knit treatment step of involving vibrations, when vibratory compaction treatment step is specially and is added in cavity by aerogel particle, adopts vibratory compaction device to carry out vibratory compaction process to aerogel particle.So, by the vibration of vibratory compaction device, make space between aerogel particle even, can prevent particle from making somebody a mere figurehead and cause the situation that space is uneven, cavity filler is discontented to occur, and, vibrate while filler, the acceleration being conducive to aerogel particle is filled, and the situation preventing charging aperture from blocking occurs.
Another technical scheme of the present invention is on such scheme basis, after described filler step, the also closely knit treatment step of involving vibrations, vibratory compaction treatment step is specially and is added after in cavity by aerogel particle, adopts vibratory compaction device to carry out vibratory compaction process to aerogel particle.So, by the vibration of vibratory compaction device, make space between aerogel particle even, can prevent particle from making somebody a mere figurehead and cause the situation that space is uneven, cavity filler is discontented to occur.
Another technical scheme of the present invention is on such scheme basis, described vibratory compaction device be mechanical vibrators, Pneumatic vibrator, hydraulic type vibratory device, ultrasonic wave vibration or electromagnetic vibrator in one or more.So, the diversity of vibratory compaction device facilitates and manufactures is selecting of equipment, selects suitable vibrator according to different Oscillation Amplitudes and frequency, is conducive to applying and reducing costs.
Another technical scheme of the present invention is on such scheme basis, and the vibration mode of described vibratory compaction device is rectilinear or horizontal or combined type.So, when adopt vertical filling time, rectilinear or combined vibrating can be adopted, the acceleration being conducive to aerogel particle flows into, and when adopting the mode of glass plate horizontal positioned to manufacture, then should adopt horizontal or combined vibrating, be conducive to aerogel particle levelling, closely knit.
Another technical scheme of the present invention is on above-mentioned basis, the preparation method of described aerogel thermal insulation glass, before the making step of described glass cavity, also comprise spacer bar treatment step, described spacer bar treatment step is specially and adds desiccant in spacer bar.So, add desiccant in spacer bar after, desiccant can continuous adsorption use in enter steam in glass enclosed cavity, make it in use be not easy to form dew condensation phenomenon, fully ensure that the quality of aerogel thermal insulation glass.
Another technical scheme of the present invention is on such scheme basis, the preparation method of described aerogel thermal insulation glass, before the making step of described glass cavity, also comprise spacer bar treatment step, described spacer bar treatment step is specially fill insulant material in spacer bar.So, in spacer bar after fill insulant material, the heat bridge effect of spacer bar in heat transfer process is weakened, and the heat-insulating capability of spacer bar is greatly improved, and correspondingly improves the heat-proof quality of aerogel thermal insulation glass.
Another technical scheme of the present invention is on such scheme basis, the preparation method of described aerogel thermal insulation glass, before the making step of described glass cavity, also comprise spacer bar treatment step, described spacer bar treatment step is specially at spacer bar outer cladding heat insulating material or the surface recombination one deck gas barrier film at spacer bar.So, the heat bridge effect of spacer bar in heat transfer process can be made to be weakened at spacer bar outer cladding heat insulating material, the heat-insulating capability of spacer bar is greatly improved, and correspondingly improves the heat-proof quality of aerogel thermal insulation glass.After surface recombination one deck gas barrier film of spacer bar, can intercept water vapour in use procedure in air and gas enters in the inner and glass cavity of spacer bar by fluid sealant and spacer bar, while ensure that in spacer bar desiccant application life, also ensure that the structure of aeroge between glass cavity and performance unaffected.
Another technical scheme of the present invention is on such scheme basis, the preparation method of described aerogel thermal insulation glass, and described heat insulating material is aeroge.So, adopt aeroge as the heat insulating material of spacer bar, the heat bridge effect between the two sides of described aerogel thermal insulation glass is very weak, further increases the heat-proof quality of aerogel thermal insulation glass.
Another technical scheme of the present invention is on such scheme basis, the preparation method of described aerogel thermal insulation glass, and described fluid sealant is bi-component polysulfide fluid sealant or bi-component silicone fluid sealant.So, adopt two component polysulfide sealant or bi-component silicone fluid sealant, can make that sealing step rapid curing completes, the performance that is bonded and sealed is better, decrease entering of a small amount of air in aerogel thermal insulation glazing gasket process, further ensure that the sealing of glass simultaneously.
Another technical scheme of the present invention is on such scheme basis, and before the making step of described glass cavity, also comprise spacer bar treatment step, described spacer bar treatment step is specially and is provided with import and/or outlet on spacer bar.Easy to process like this, cost of manufacture is low.
Another technical scheme of the present invention is on such scheme basis, and Sealed casing pipe is installed in described import and/or outlet.Like this, Sealed casing pipe is installed in import and/or outlet, with seal, import and/or outlet is sealed after being convenient to filler.
Another technical scheme of the present invention is on such scheme basis, the preparation method of described aerogel thermal insulation glass, after described pump step, also comprise inert gas and add step, add inert gas specifically by described import and/or outlet to described cavity.Like this, by adding inert gas between glass, the thermal transmittance of aerogel thermal insulation glass can be reduced, improving the performance such as heat-insulation and heat-preservation, sound insulation, Anti-dew of glass further.So, be filled with inert gas in the cavity of aerogel thermal insulation inside glass after, reduce cavity external and internal pressure difference, the security incident probability because the cold and hot temperature difference causes glass plate to be revealed can be reduced; And inert gas is added between glass, the heat trnasfer in aerogel thermal insulation glass cavity can be reduced, improve the performance such as heat-insulation and heat-preservation, sound insulation, Anti-dew of glass further.
Another technical scheme of the present invention is on such scheme basis, the preparation method of described aerogel thermal insulation glass, and described spacer bar is the outer gimbal support being provided with tongue.So, the outer gimbal support being provided with tongue is adopted to be arranged between two blocks of glass, tongue can play good support and sealing function, and its exposed parts can be used as the outside framework of aerogel thermal insulation glass, can directly be mounted on doorframe and window frame or in curtain wall support, considerably reduce the cost of heat-preservation door and window, simplify the manufacture craft of heat-preservation door and window, be conducive to large-scale promotion application.
Accompanying drawing explanation
The accompanying drawing forming a part of the present invention is used to provide a further understanding of the present invention, and schematic description and description of the present invention, for explaining the present invention, does not form inappropriate limitation of the present invention.
Fig. 1 is the flow chart of the preparation method of the aerogel thermal insulation glass that a kind of embodiment of this programme relates to;
Fig. 2 is the sectional drawing of the aerogel thermal insulation glass that a kind of embodiment of this programme relates to.
Wherein:
1 is glass; 2 is aerogel particle; 3 is butyl rubber; 4 is spacer bar; 5 is fluid sealant.
Detailed description of the invention
Describe the present invention below in conjunction with accompanying drawing, the description of this part is only exemplary and explanatory, should not have any restriction to protection scope of the present invention.In addition, those skilled in the art, according to the description of presents, can carry out respective combination to the feature in embodiment in presents and in different embodiment.
The embodiment of the present invention is as follows, and as shown in Figure 1, a kind of preparation method of aerogel thermal insulation glass, comprises the following steps:
(1) making of glass cavity, glue together to make by least two blocks of glass 1 and spacer bar 4 with butyl rubber 3 and comprises at least one import and at least one closed cavity exported;
(2) filler, joins closed cavity by aerogel particle 2 from import;
(3) bleed, in the process of filler, outlet is bled process;
(4) seal, with seal by import and exit seal;
(5) seal, the surrounding fluid sealant of aerogel thermal insulation glass is carried out encapsulation process.
So, as shown in Figure 2, pass through above-mentioned steps, one can be obtained by least two blocks of glass 1 as housing, there is sealed cavity of at least one import and at least one outlet and in cavity, be provided with the aerogel thermal insulation glass of aerogel particle 2, this aerogel thermal insulation glass is because wherein set aeroge is graininess, thus there is good light scattering property, there is very excellent barrier property in radiation thermal conduction, simultaneously, because this aerogel thermal insulation glass chamber portion has carried out encapsulation process, the cavity of described aerogel thermal insulation inside glass is after process of bleeding, the drying property of its inside obtains sufficient guarantee, simultaneously, because there is negative pressure, spacer bar clamps closely knit by two blocks of glass, making it, in use air and steam can not enter cavity inside, be not easy to form dew condensation phenomenon, and, because Specific surface area that aeroge is very thin effectively limit the propagation of local thermal excitation, nanometer micropore hole inhibits gas molecule to heat conducting effect, the refractive index of silica-based aerogel is close to l, and more than 100 are reached to the ratio burying in oblivion coefficient that is infrared and visible ray, can effectively through sunshine, and stop the infrared emanation of environment temperature, therefore, the aerogel thermal insulation glass adopting said method to obtain not only has good radiation thermal conduction barrier property, also possesses good advection heat conduction barrier property simultaneously.
On the basis of above-described embodiment, in another embodiment of the present invention, in described filler step, all right closely knit treatment step of involving vibrations, when vibratory compaction treatment step is specially and is added in cavity by aerogel particle, vibratory compaction device is adopted to carry out vibratory compaction process to aerogel particle.So, by the vibration of vibratory compaction device, make space between aerogel particle even, can prevent particle from making somebody a mere figurehead and cause the situation that space is uneven, cavity filler is discontented to occur, and, vibrate while filler, the acceleration being conducive to aerogel particle is filled, and the situation preventing charging aperture from blocking occurs.
On the basis of above-described embodiment, in another embodiment of the present invention, after described filler step, all right closely knit treatment step of involving vibrations, vibratory compaction treatment step is specially and is added after in cavity by aerogel particle, adopts vibratory compaction device to carry out vibratory compaction process to aerogel particle.So, by the vibration of vibratory compaction device, make space between aerogel particle even, can prevent particle from making somebody a mere figurehead and cause the situation that space is uneven, cavity filler is discontented to occur.
On the basis of above-described embodiment, in another embodiment of the present invention, described vibratory compaction device can be mechanical vibrators, Pneumatic vibrator, hydraulic type vibratory device, ultrasonic wave vibration or electromagnetic vibrator in one or more.So, the diversity of vibratory compaction device facilitates and manufactures is selecting of equipment, selects suitable vibrator according to different Oscillation Amplitudes and intensity, is conducive to applying and reducing costs.
On the basis of above-described embodiment, in another embodiment of the present invention, the vibration mode of described vibratory compaction device can be rectilinear or horizontal or combined type.So, when adopt vertical filling time, rectilinear or combined vibrating can be adopted, the acceleration being conducive to aerogel particle flows into, and when adopting the mode of glass plate horizontal positioned to manufacture, then should adopt horizontal or combined vibrating, be conducive to aerogel particle levelling, closely knit.
On the basis of above-described embodiment, in another embodiment of the present invention, the preparation method of described aerogel thermal insulation glass, before the making step of described glass cavity, can also comprise spacer bar treatment step, described spacer bar treatment step is specially and adds desiccant in spacer bar.So, add desiccant in spacer bar after, desiccant can continuous adsorption use in enter steam in glass enclosed cavity, make it in use be not easy to form dew condensation phenomenon, fully ensure that the quality of aerogel thermal insulation glass.
On the basis of above-described embodiment, in another embodiment of the present invention, the preparation method of described aerogel thermal insulation glass, before the making step of described glass cavity, can also comprise spacer bar treatment step, described spacer bar treatment step is specially fill insulant material in spacer bar.So, in spacer bar after fill insulant material, the heat bridge effect of spacer bar in heat transfer process is weakened, and the heat-insulating capability of spacer bar is greatly improved, and correspondingly improves the heat-proof quality of aerogel thermal insulation glass.
On the basis of above-described embodiment, in another embodiment of the present invention, the preparation method of described aerogel thermal insulation glass, before the making step of described glass cavity, can also comprise spacer bar treatment step, described spacer bar treatment step is specially at spacer bar outer cladding heat insulating material or the surface recombination one deck gas barrier film at spacer bar.So, the heat bridge effect of spacer bar in heat transfer process can be made to be weakened at spacer bar outer cladding heat insulating material, the heat-insulating capability of spacer bar is greatly improved, and correspondingly improves the heat-proof quality of aerogel thermal insulation glass.After surface recombination one deck gas barrier film of spacer bar, can intercept water vapour in use procedure in air and gas enters in the inner and glass cavity of spacer bar by fluid sealant and spacer bar, while ensure that in spacer bar desiccant application life, also ensure that the structure of aeroge between glass cavity and performance unaffected.
On the basis of above-described embodiment, in another embodiment of the present invention, the preparation method of described aerogel thermal insulation glass, described heat insulating material can be aeroge.So, adopt aeroge as the heat insulating material of spacer bar, the heat bridge effect between the two sides of described aerogel thermal insulation glass is very weak, further increases the heat-proof quality of aerogel thermal insulation glass.
On the basis of above-described embodiment, in another embodiment of the present invention, the preparation method of described aerogel thermal insulation glass, described fluid sealant can be bi-component polysulfide fluid sealant or bi-component silicone fluid sealant.So, adopt two component polysulfide sealant or bi-component silicone fluid sealant, can make that sealing step rapid curing completes, the performance that is bonded and sealed is better, decrease entering of a small amount of air in aerogel thermal insulation glazing gasket process, further ensure that the sealing of glass simultaneously.
Another technical scheme of the present invention is on such scheme basis, and before the making step of described glass cavity, also comprise spacer bar treatment step, described spacer bar treatment step is specially and is provided with import and/or outlet on spacer bar.Like this, easy to process, cost of manufacture is low.
Another technical scheme of the present invention is on such scheme basis, and Sealed casing pipe is installed in described import and/or outlet.Like this, Sealed casing pipe is installed in import and/or outlet, with seal, import and/or outlet is sealed after being convenient to filler.
On the basis of above-described embodiment, in another embodiment of the present invention, the preparation method of described aerogel thermal insulation glass, after described pump step, inert gas can also be comprised and add step, add inert gas specifically by described import and/or outlet to described cavity.Like this, by adding inert gas between glass, the thermal transmittance of aeroge glass can be reduced, improving the performance such as heat-insulation and heat-preservation, sound insulation, Anti-dew of glass further.So, be filled with inert gas in the cavity of aerogel thermal insulation inside glass after, reduce cavity external and internal pressure difference, the security incident probability because the cold and hot temperature difference causes glass plate to be revealed can be reduced; And inert gas is added between glass, the heat trnasfer in aerogel thermal insulation glass cavity can be reduced, improve the performance such as heat-insulation and heat-preservation, sound insulation, Anti-dew of glass further.
On the basis of above-described embodiment, in another embodiment of the present invention, the preparation method of described aerogel thermal insulation glass, described spacer bar can for being provided with the outer gimbal support of tongue.So, the outer gimbal support being provided with tongue is adopted to be arranged between two blocks of glass, tongue can play good support and sealing function, and its exposed parts can be used as the outside framework of aerogel thermal insulation glass, can directly be mounted on doorframe and window frame or in curtain wall support, considerably reduce the cost of heat-preservation door and window, simplify the manufacture craft of heat-preservation door and window, be conducive to large-scale promotion application.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: in spacer bar 4, fill silica aerogel material, with butyl rubber 3 two blocks of glass 1 and spacer bar 4 glued together and make an open cavity, aerogel particle 2 is inserted in cavity; In atmospheric environment, with butyl rubber 3 and spacer bar 4 by cavities seals, cavity presets air exhaust nozzle, then cavity is bled, shutoff air exhaust nozzle, finally the surrounding fluid sealant 5 of aerogel thermal insulation glass is carried out encapsulation process.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: at spacer bar 4 outer cladding silica aerogel material, with butyl rubber 3 two blocks of glass 1 and spacer bar 4 glued together and make an open cavity, aerogel particle 2 is inserted in cavity; In atmospheric environment, with butyl rubber 3 and spacer bar 4 by cavities seals, cavity presets air exhaust nozzle, then cavity is bled, inert gas is filled with subsequently by air exhaust nozzle, shutoff air exhaust nozzle, finally carries out encapsulation process by the surrounding bi-component silicone fluid sealant of aerogel thermal insulation glass.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: in spacer bar 4, fill silica aerogel material, with butyl rubber 3 two blocks of glass 1 and spacer bar 4 glued together and make an open cavity, aerogel particle 2 is inserted in cavity; In vacuum environment, with butyl rubber 3 and spacer bar 4 by cavities seals, finally the surrounding bi-component silicone fluid sealant of aerogel thermal insulation glass is carried out encapsulation process.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: at spacer bar 4 outer cladding silica aerogel material, with butyl rubber 3 two blocks of glass 1 and spacer bar 4 glued together and make an open cavity, aerogel particle 2 is inserted in cavity; In vacuum environment, with butyl rubber 3 and spacer bar 4 by cavities seals, finally the surrounding bi-component silicone fluid sealant of aerogel thermal insulation glass is carried out encapsulation process.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: adopt the outer gimbal support being provided with tongue to be spacer bar, silica aerogel material is filled in spacer bar 4, with butyl rubber 3 two blocks of glass 1 and spacer bar 4 glued together and make an open cavity, aerogel particle 2 is inserted in cavity; In atmospheric environment, with butyl rubber 3 and spacer bar 4 by cavities seals, cavity presets air exhaust nozzle, then cavity is bled, shutoff air exhaust nozzle, finally the surrounding bi-component silicone fluid sealant of aerogel thermal insulation glass is carried out encapsulation process.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: adopt the outer gimbal support being provided with tongue to be spacer bar, at spacer bar 4 outer cladding silica aerogel material, with butyl rubber 3 two blocks of glass 1 and spacer bar 4 glued together and make an open cavity, aerogel particle 2 is inserted in cavity; In atmospheric environment, with butyl rubber 3 and spacer bar 4 by cavities seals, cavity presets air exhaust nozzle, then cavity is bled, inert gas is filled with subsequently by air exhaust nozzle, shutoff air exhaust nozzle, finally carries out encapsulation process by the surrounding bi-component silicone fluid sealant of aerogel thermal insulation glass.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: adopt the outer gimbal support being provided with tongue to be spacer bar, at spacer bar 4 outer cladding silica aerogel material, with butyl rubber 3 two blocks of glass 1 and spacer bar 4 glued together and make an open cavity, aerogel particle 2 is inserted in cavity; In vacuum environment, with butyl rubber 3 and spacer bar 4 by cavities seals, finally the surrounding bi-component silicone fluid sealant of aerogel thermal insulation glass is carried out encapsulation process.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: in spacer bar 4, fill silica aerogel material, with butyl rubber 3 three blocks of glass 1 and spacer bar 4 glued together and make two open cavities, two pieces of aerogel particles 2 are inserted in cavity respectively; In atmospheric environment, with butyl rubber 3 and spacer bar 4 by cavities seals, cavity presets air exhaust nozzle, then cavity is bled, shutoff air exhaust nozzle, finally the surrounding bi-component silicone fluid sealant of aerogel thermal insulation glass is carried out encapsulation process.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: at spacer bar 4 outer cladding silica aerogel material, with butyl rubber 3 three blocks of glass 1 and spacer bar 4 glued together and make two open cavities, two pieces of aerogel particles 2 are inserted in cavity respectively; In vacuum environment, with butyl rubber 3 and spacer bar 4 by cavities seals, finally the surrounding bi-component silicone fluid sealant of aerogel thermal insulation glass is carried out encapsulation process.
On the basis of above-described embodiment, in another embodiment of the present invention, described import and/or outlet are arranged on spacer bar.Easy to process like this, cost of manufacture is low.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: adopt the outer gimbal support being provided with tongue to be spacer bar, silica aerogel material is filled in spacer bar 4, with butyl rubber 3 three blocks of glass 1 and spacer bar 4 glued together and make two open cavities, two pieces of aerogel particles 2 are inserted in cavity respectively; In atmospheric environment, with butyl rubber 3 and spacer bar 4 by cavities seals, cavity presets air exhaust nozzle, then cavity is bled, shutoff air exhaust nozzle, finally the surrounding bi-component silicone fluid sealant of aerogel thermal insulation glass is carried out encapsulation process.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: adopt the outer gimbal support being provided with tongue to be spacer bar, at spacer bar 4 outer cladding silica aerogel material, with butyl rubber 3 two blocks of glass 1 and spacer bar 4 glued together and make an open cavity, aerogel particle 2 is inserted in cavity; In atmospheric environment, with butyl rubber 3 and spacer bar 4 by cavities seals, cavity presets air exhaust nozzle, then cavity is bled, inert gas is filled with subsequently by air exhaust nozzle, shutoff air exhaust nozzle, finally carries out encapsulation process by the surrounding bi-component silicone fluid sealant of aerogel thermal insulation glass.
On the basis of above-described embodiment, in another embodiment of the present invention, a kind of preparation method of aerogel thermal insulation glass, comprise the following steps: adopt the outer gimbal support being provided with tongue to be spacer bar, at spacer bar 4 outer cladding silica aerogel material, with butyl rubber 3 three blocks of glass 1 and spacer bar 4 glued together and make two open cavities, two pieces of aerogel particles 2 are inserted in cavity respectively; In vacuum environment, with butyl rubber 3 and spacer bar 4 by cavities seals, finally the surrounding bi-component silicone fluid sealant of aerogel thermal insulation glass is carried out encapsulation process.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (10)
1. a preparation method for aerogel thermal insulation glass, is characterized in that, comprises the following steps:
(1) at least two blocks of glass and spacer bar to be glued together to make with glue and comprise at least one import and at least one closed cavity exported by the making of glass cavity;
(2) filler, joins closed cavity by aerogel particle from import;
(3) bleed, in the process of filler, outlet is bled process;
(4) seal, with seal by import and exit seal;
(5) seal, the surrounding fluid sealant of aerogel thermal insulation glass is carried out encapsulation process.
2. the preparation method of aerogel thermal insulation glass according to claim 1, it is characterized in that, in described filler step, the also closely knit treatment step of involving vibrations, when vibratory compaction treatment step is specially and is added in cavity by aerogel particle, vibratory compaction device is adopted to carry out vibratory compaction process to aerogel particle.
3. the preparation method of aerogel thermal insulation glass according to claim 1, it is characterized in that, after described filler step, the also closely knit treatment step of involving vibrations, vibratory compaction treatment step is specially and is added after in cavity by aerogel particle, adopts vibratory compaction device to carry out vibratory compaction process to aerogel particle.
4. the preparation method of the aerogel thermal insulation glass according to Claims 2 or 3, it is characterized in that, described vibratory compaction device be mechanical vibrators, Pneumatic vibrator, hydraulic type vibratory device, ultrasonic wave vibration or electromagnetic vibrator in one or more.
5. the preparation method of aerogel thermal insulation glass according to claim 1, is characterized in that, the vibration mode of described vibratory compaction device is rectilinear or horizontal or combined type.
6. the preparation method of aerogel thermal insulation glass according to claim 1, is characterized in that, before the making step of described glass cavity, also comprise spacer bar treatment step, described spacer bar treatment step is specially and adds desiccant in spacer bar.
7. the preparation method of aerogel thermal insulation glass according to claim 1, is characterized in that, before the making step of described glass cavity, also comprise spacer bar treatment step, described spacer bar treatment step is specially fill insulant material in spacer bar.
8. the preparation method of aerogel thermal insulation glass according to claim 1, it is characterized in that, before the making step of described glass cavity, also comprise spacer bar treatment step, described spacer bar treatment step is specially at spacer bar outer cladding heat insulating material or the surface recombination one deck gas barrier film at spacer bar.
9. the preparation method of the aerogel thermal insulation glass according to claim 7 or 8, is characterized in that, described heat insulating material is aeroge.
10. the preparation method of aerogel thermal insulation glass according to claim 1, is characterized in that, described fluid sealant is bi-component polysulfide fluid sealant or bi-component silicone fluid sealant; Or before the making step of described glass cavity, also comprising spacer bar treatment step, described spacer bar treatment step is specially and is provided with import and/or outlet on spacer bar; Or described import and/or outlet on Sealed casing pipe is installed; Or after described pump step, also comprise inert gas and add step, add inert gas specifically by described outlet to described closed cavity; Or described spacer bar is the outer gimbal support being provided with tongue.
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| CN109989684A (en) * | 2017-12-30 | 2019-07-09 | 长沙星纳气凝胶有限公司 | A kind of temperature sensitive heat-insulation and heat-preservation daylighting glass of aerogel-congtg and preparation method thereof |
| CN111925135A (en) * | 2020-08-17 | 2020-11-13 | 巩义市泛锐熠辉复合材料有限公司 | Method for preparing aerogel glass by utilizing efficient powder filling device |
| CN113818605A (en) * | 2021-09-14 | 2021-12-21 | 广东恒锋装饰工程有限公司 | Energy-saving curtain wall |
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| CN109989684A (en) * | 2017-12-30 | 2019-07-09 | 长沙星纳气凝胶有限公司 | A kind of temperature sensitive heat-insulation and heat-preservation daylighting glass of aerogel-congtg and preparation method thereof |
| CN111925135A (en) * | 2020-08-17 | 2020-11-13 | 巩义市泛锐熠辉复合材料有限公司 | Method for preparing aerogel glass by utilizing efficient powder filling device |
| CN113818605A (en) * | 2021-09-14 | 2021-12-21 | 广东恒锋装饰工程有限公司 | Energy-saving curtain wall |
| CN113818605B (en) * | 2021-09-14 | 2023-02-14 | 广东恒锋装饰工程有限公司 | Energy-saving curtain wall |
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| CN105064874B (en) | 2017-12-29 |
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