CN105063526A - Nickel strap heat treatment device and technology - Google Patents

Nickel strap heat treatment device and technology Download PDF

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Publication number
CN105063526A
CN105063526A CN201510456480.7A CN201510456480A CN105063526A CN 105063526 A CN105063526 A CN 105063526A CN 201510456480 A CN201510456480 A CN 201510456480A CN 105063526 A CN105063526 A CN 105063526A
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CN
China
Prior art keywords
nickel strap
protective gas
heat treatment
inner bag
furnace body
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510456480.7A
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Chinese (zh)
Inventor
沈凤良
朱建刚
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WUXI DONGYANG ELECTRONICS CO Ltd
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WUXI DONGYANG ELECTRONICS CO Ltd
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Filing date
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Priority to CN201510456480.7A priority Critical patent/CN105063526A/en
Publication of CN105063526A publication Critical patent/CN105063526A/en
Pending legal-status Critical Current

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Abstract

The invention provides a nickel strap heat treatment device which comprises an unwinding machine, a front carrier roller, a protective gas inner container, a heat treatment furnace body, a temperature control element, a cooling device, a rear carrier roller and a winding machine. The invention further provides a nickel strap heat treatment technology adopting the nickel strap heat treatment device. The new technology for continuous rapid annealing is adopted and the nickel strap heat treatment device and technology have the beneficial effects that the heating speed is high, the annealing temperature is high, the heat preservation time is short at high temperature, and rapid cooling is achieved after heat preservation is performed. According to continuous bright annealing, the furnace temperature should be much higher than the temperature needed by metal during annealing, the metal can rapidly reach the needed annealing temperature, and the recrystallization process is rapidly completed at high temperature; and the recrystallization process lasts only a few seconds at the temperature high enough, so that the annealing time is greatly shortened. The remaining time of a nickel strap is short at high temperature, the oxidation process of the metal surface will not be performed sufficiently, and therefore it is ensured that the surface of a product is smooth and clean.

Description

Nickel strap thermal treatment unit and thermal treatment process
Technical field
The present invention relates to a kind of one of them equipment and the related process that make lithium ion battery negative carrier, especially a kind of nickel strap thermal treatment unit and thermal treatment process.
Background technology
In heavy non-ferrous metal plate, band production process, annealing thermal treatment is requisite important component part in whole production process, utilize thermal treatment not only can control the final performance of product, simultaneously for enabling the course of processing carry out smoothly, also must process material be heat-treated, to eliminate work hardening, recover deformable metal plasticity, thus ensure that machined material has certain process industrial art performance.
Determine that the significant parameter of annealing process is: rate of heating; Maximum heating temperature; Soaking time when top temperature; Speed of cooling.Thermal treatment temp and soaking time should strictly control, especially roll into before product with finished product thermal treatment, prevent the overheated coarse grains of sheet metal strip, produce surface " tangerine peel " phenomenon, affect surface quality or the final performance of product.
Summary of the invention
The object of the present invention is to provide a kind of nickel strap thermal treatment unit, and adopt the nickel strap thermal treatment process of this nickel strap thermal treatment unit, substantially reduce nickel strap annealing time, at high temperature soaking time is very short, and heating is also very even, substantially eliminates the uneven phenomenon of nickel strap performance, simultaneously, because the time at high temperature stopped is short, the oxidising process of metallic surface also can not fully be carried out, thus can ensure that product surface is bright and clean.Art breading speed of the present invention is fast, efficiency is high, fully can ensure the superior quality on nickel strap surface simultaneously.The technical solution used in the present invention is:
A kind of nickel strap thermal treatment unit, comprising: unreeling machine, front carrying roller, protective gas inner bag, heat treatment furnace body, temperature control element, refrigerating unit, rear carrying roller, winder;
Unreeling machine is for placing pending rolling nickel strap; Carrying roller, heat treatment furnace body, refrigerating unit, rear carrying roller, winder before establishing successively after unreeling machine;
Heat treatment furnace body inner transverse installs protective gas inner bag, and protective gas inner bag extends in refrigerating unit, and the two ends of protective gas inner bag expose the heat treatment furnace body of front end and the refrigerating unit of rear end respectively; At the outer side of protective gas inner bag, temperature control element is installed;
One or more heating zone is provided with in heat treatment furnace body.
Further, heat treatment furnace body inner bottom part is located in each heating zone, each heating zone and the temperature control element one_to_one corresponding above it.
Further, the inlet section of protective gas inner bag front end is provided with burner port.
Further, during work, in protective gas inner bag, pass into protective gas, and the flexible thing in two ends is closed.
Further, ribbon heater or nichrome wire is provided with in heating zone.
Further, unreeling machine and winder are equipped with tightening pulley, rolling nickel strap is sleeved on tightening pulley and by the harmomegathus of tightening pulley and is fixed.
Adopt a nickel strap thermal treatment process for as above any one nickel strap thermal treatment unit, comprise the steps:
S1. be positioned on unreeling machine by rolling nickel strap, leader tape has been welded in nickel strap termination, and leader tape is pressed through front carrying roller, through the protective gas inner bag in heat treatment furnace body and refrigerating unit, presses through rear carrying roller and around to winder;
S2. heat treatment furnace body starts heating, is heated to 550 ~ 600 DEG C;
S3. the flexible thing in the two ends of protective gas inner bag is closed, and first pass into nitrogen at back outlet place, with the air in emptying protective gas inner bag; Then continue to pass into protective gas, light protective gas at the burner port of protective gas inner bag front end;
S4. heat treatment furnace body heating, improves temperature to 850 ± 10 DEG C in body of heater;
S5. start winder, continued to drive process from protective gas inner bag by nickel strap, rolling is to winder; Nickel strap is cooled first be subject to radiation heating in protective gas inner bag after.
Further, in step S3, the protective gas passed into is hydrogen.
Further, unreeling machine and winder are equipped with tightening pulley, the minimum diameter of tightening pulley is 320mm, and maximum diameter is 345mm; When the length of heat treatment furnace body is 3800 ~ 4200mm, bottom heat treatment furnace body, be provided with three heating zone; Under these conditions, the rolling speed of nickel strap is:
Nickel strap thickness (mm), rolling speed ± 15% (rev/min)
0.4~0.3350~400
0.3~0.2400~500
0.2~0.15500~700
0.15~0.10700
0.10~0.07700~750
0.07~0.05750~850。
The invention has the advantages that: the novel process that present invention employs continous way short annealing, be characterized in that rate of heating is fast, annealing temperature is high, and at high temperature soaking time is short, insulation is rear cools fast.In continuous bright annealing, the temperature reached needed for metal when furnace temperature should be much higher than annealing, the annealing temperature that metal reaches rapidly required can be made, and at high temperature complete recrystallization process rapidly, in sufficiently high temperature, the perdurability of recrystallize only has a few second, thus substantially reduces annealing time.The time of at high temperature nickel strap stop is short, and the oxidising process of metallic surface also can not fully be carried out, thus can ensure that product surface is bright and clean.
Accompanying drawing explanation
Fig. 1 is nickel strap thermal treatment unit schematic diagram of the present invention.
Embodiment
Below in conjunction with concrete drawings and Examples, the invention will be further described.
As shown in Figure 1, a kind of nickel strap thermal treatment unit that the present invention proposes, comprising: unreeling machine 1, front carrying roller 21, protective gas inner bag 3, heat treatment furnace body 4, temperature control element 5, frame 6, refrigerating unit 7, rear carrying roller 22, winder 9; Refrigerating unit 7 is arranged in frame 6.
Unreeling machine 1 is for placing pending rolling nickel strap 8; Carrying roller 21, heat treatment furnace body 4, refrigerating unit 7, rear carrying roller 22, winder 9 before establishing successively after unreeling machine 1.Heat treatment furnace body 4 inner transverse installs protective gas inner bag 3, and protective gas inner bag 3 extends in refrigerating unit 7, and the two ends of protective gas inner bag 3 expose the heat treatment furnace body 4 of front end and the refrigerating unit 7 of rear end respectively; At the outer side of protective gas inner bag 3, temperature control element 5 is installed.One or more heating zone 41 is provided with at heat treatment furnace body 4 inner bottom part.
This unreeling machine 1 and winder 9 all adopt Manual expansion mechanism, and unreeling machine 1 and winder 9 are equipped with tightening pulley, and rolling nickel strap 8 is sleeved on tightening pulley and by the harmomegathus of tightening pulley and is fixed.The minimum diameter of tightening pulley is 320mm, and maximum diameter is 345mm.Unreeling machine 1 is unpowered device, winder 9 is by power drive mechanism rolling.Front carrying roller 21 and rear carrying roller 22 are all that bearing is installed at two ends, and level is fixed, flexible rotation.
Heat treatment furnace body 4 refractory material laying, inner installation protective gas inner bag 3, in refractory material laying under protective gas inner bag 3, an electric heating element is housed, such as ribbon heater or nichrome wire, thus forms several heating zone 41 at heat treatment furnace body 4 inner bottom part; Each heating zone 41 of heat treatment furnace body 4 inner bottom part and temperature control element 5 one_to_one corresponding above it, make the temperature-controllable of heating zone 41, conveniently set furnace temperature.Temperature control element 5 can adopt thermopair.
Protective gas inner bag 3 traverses in heat treatment furnace body 4 and refrigerating unit 7, Fig. 1, and its left end is import, and right-hand member is outlet; The flexible things such as the inlet section of protective gas inner bag 3 front end is provided with burner port 31, and during work, protective gas inner bag 3 needs to pass into hydrogen, protective gas inner bag 3 two ends wool felt are closed, and hydrogen is lighted at burner port 31.
Refrigerating unit 7 primarily of blower fan and water condenser composition, object be nickel strap 8 by time can cool fast.
Below for the heat treatment furnace body 4 that a length is 4000mm, the heat treated process of nickel strap continuous annealing is described.Experiment proves, when heat treatment furnace body 4 length is 3800 ~ 4200mm, when being 4000mm with this routine length, and the identical thermal effectiveness obtaining equal in quality of processing parameter.
When nickel strap 8 carries out annealing thermal treatment, rolling speed is crucial, because rolling speed has directly had influence on the residence time of nickel strap 8 in heat treatment furnace body 4, and the soaking time namely under high temperature; And have influence on cooling time and speed of cooling; Another heat treated key process parameter is the height of furnace temperature, furnace temperature needs to coordinate with rolling speed, need to ensure under current furnace temperature, under the rolling speed of correspondence, nickel strap reaches rapidly required annealing temperature, and at high temperature complete recrystallization process rapidly, the annealing temperature adopted, must meet and metal can be made to obtain sufficient recrystallize, but too highly can not cause crystal grain too grow up for limit, thus the size of stable material, shape and performance.
The heat treated process of nickel strap continuous annealing is as follows:
S1. be positioned on unreeling machine 1 by rolling nickel strap 8, leader tape has been welded in nickel strap 8 termination, leader tape is pressed through front carrying roller 21, through the protective gas inner bag 3 in heat treatment furnace body 4 and refrigerating unit 7, presses through rear carrying roller 22 and around to winder 9;
S2. heat treatment furnace body 4 starts heating, is heated to 550 ~ 600 DEG C;
S3. the two ends wool felt of protective gas inner bag 3 is closed, and first pass into nitrogen at back outlet place, with the air in emptying protective gas inner bag 3; Then continue to pass into hydrogen as protective gas, light hydrogen at the burner port 31 of protective gas inner bag 3 front end;
S4. heat treatment furnace body 4 heats, and improves temperature to 850 ± 10 DEG C in body of heater;
S5. start winder 9, continued to drive process from protective gas inner bag 3 by nickel strap 8, rolling is to winder; Nickel strap 8 is cooled first be subject to radiation heating in protective gas inner bag 3 after.The mode that annealing furnace charge (nickel strap) is heated is only radiative transfer.
Length is in the heat treatment furnace body 4 of 4000mm, needs to establish three heating zone 41; The thickness of the nickel strap 8 annealed is 0.05mm ~ 0.4mm, and the rolling speed of nickel strap 8 is:
Nickel strap thickness (mm), rolling speed ± 15% (rev/min)
0.4~0.3350~400
0.3~0.2400~500
0.2~0.15500~700
0.15~0.10700
0.10~0.07700~750
0.07~0.05750~850。
One volume nickel strap 8 is annealed complete, another volume nickel strap of repetitive operation.

Claims (10)

1. a nickel strap thermal treatment unit, it is characterized in that, comprising: unreeling machine (1), front carrying roller (21), protective gas inner bag (3), heat treatment furnace body (4), temperature control element (5), refrigerating unit (7), rear carrying roller (22), winder (9);
Unreeling machine (1) is for placing pending rolling nickel strap (8); Front carrying roller (21), heat treatment furnace body (4), refrigerating unit (7), rear carrying roller (22), winder (9) is established successively after unreeling machine (1);
Heat treatment furnace body (4) inner transverse installs protective gas inner bag (3), protective gas inner bag (3) extends in refrigerating unit (7), and the two ends of protective gas inner bag (3) expose the heat treatment furnace body (4) of front end and the refrigerating unit (7) of rear end respectively; At the outer side of protective gas inner bag (3), temperature control element (5) is installed;
One or more heating zone (41) is provided with in heat treatment furnace body (4).
2. nickel strap thermal treatment unit as described in claim 1, is characterized in that:
Heat treatment furnace body (4) inner bottom part is located in each heating zone (41), each heating zone (41) and temperature control element (5) one_to_one corresponding above it.
3. nickel strap thermal treatment unit as described in claim 1, is characterized in that:
The inlet section of protective gas inner bag (3) front end is provided with burner port (31).
4. nickel strap thermal treatment unit as described in claim 1, is characterized in that:
Pass into protective gas in protective gas inner bag (3) during work, and the flexible thing in two ends is closed.
5. nickel strap thermal treatment unit as described in claim 1, is characterized in that:
Heating zone is provided with ribbon heater or nichrome wire in (41).
6. nickel strap thermal treatment unit as described in claim 1, is characterized in that:
Unreeling machine (1) and winder (9) are equipped with tightening pulley, and rolling nickel strap (8) is sleeved on tightening pulley and by the harmomegathus of tightening pulley and is fixed.
7. adopt a nickel strap thermal treatment process for nickel strap thermal treatment unit according to any one of claim 1 ~ 6, it is characterized in that, comprise the steps:
S1. rolling nickel strap (8) is positioned on unreeling machine (1), leader tape has been welded in nickel strap (8) termination, leader tape is pressed through front carrying roller (21), through the protective gas inner bag (3) in heat treatment furnace body (4) and refrigerating unit (7), press through rear carrying roller (22) and around to winder (9);
S2. heat treatment furnace body (4) starts heating, is heated to 550 ~ 600 DEG C;
S3. the flexible thing in the two ends of protective gas inner bag (3) is closed, and first pass into nitrogen at back outlet place, with the air in emptying protective gas inner bag (3); Then continue to pass into protective gas, light protective gas at the burner port (31) of protective gas inner bag (3) front end;
S4. heat treatment furnace body (4) heating, improves temperature to 850 ± 10 DEG C in body of heater;
S5. start winder (9), continued to drive process from protective gas inner bag (3) by nickel strap (8), rolling is to winder; Nickel strap (8) is first subject to radiation heating in protective gas inner bag (3), after cooled.
8. nickel strap thermal treatment process as claimed in claim 7, is characterized in that:
In step S3, the protective gas passed into is hydrogen.
9. nickel strap thermal treatment process as claimed in claim 7, is characterized in that:
Unreeling machine (1) and winder (9) are equipped with tightening pulley, and the minimum diameter of tightening pulley is 320mm, and maximum diameter is 345mm; When the length of heat treatment furnace body (4) is 3800 ~ 4200mm, heat treatment furnace body (4) bottom is provided with three heating zone (31); Under these conditions, the rolling speed of nickel strap (8) is:
Nickel strap thickness (mm), rolling speed ± 15% (rev/min)
0.4~0.3350~400
0.3~0.2400~500
0.2~0.15500~700
0.15~0.10700
0.10~0.07700~750
0.07~0.05750~850。
10. nickel strap thermal treatment process as claimed in claim 7, is characterized in that:
The closed at both ends of protective gas inner bag (3) adopts wool felt with flexible thing.
CN201510456480.7A 2015-07-29 2015-07-29 Nickel strap heat treatment device and technology Pending CN105063526A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510456480.7A CN105063526A (en) 2015-07-29 2015-07-29 Nickel strap heat treatment device and technology

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510456480.7A CN105063526A (en) 2015-07-29 2015-07-29 Nickel strap heat treatment device and technology

Publications (1)

Publication Number Publication Date
CN105063526A true CN105063526A (en) 2015-11-18

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Country Link
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107557561A (en) * 2017-08-08 2018-01-09 东莞市灿煜金属制品有限公司 The copper material stress-removal process of appropriateness drop hardness
JP2018003107A (en) * 2016-07-04 2018-01-11 大同特殊鋼株式会社 PRODUCTION METHOD OF PRECIPITATE TYPE HEAT-RESISTANT Ni-BASED ALLOY
CN107815533A (en) * 2017-12-05 2018-03-20 谢思雨 The method for annealing and equipment of a kind of sheet metal strip
CN109355489A (en) * 2018-12-05 2019-02-19 常德力元新材料有限责任公司 A kind of annealing device of punched nickel-plated steel band
CN110218856A (en) * 2019-06-03 2019-09-10 宁波中科毕普拉斯新材料科技有限公司 A kind of apparatus for continuous heat treatment and its application method of thin-band material
CN112620349A (en) * 2020-12-01 2021-04-09 无锡市东杨新材料股份有限公司 Method for eliminating oil stain of thin nickel strip
CN113322366A (en) * 2021-05-28 2021-08-31 郑州大学 Contact type rapid annealing equipment

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1844440A (en) * 2006-04-20 2006-10-11 倪智勇 Horizontal non-oxidizing bright continuous annealing device and method
CN102251201A (en) * 2011-07-07 2011-11-23 广东省钢铁研究所 Preparation method of high purity nickel wire
CN102586576A (en) * 2012-02-24 2012-07-18 北京工业大学 Vertical annealing furnace for coated superconducting substrate
CN102672447A (en) * 2011-03-17 2012-09-19 沈翠珊 Manufacturing method of high-purity nickel strap
CN103322800A (en) * 2012-03-22 2013-09-25 东北师范大学 Fully transparent tube type resistance furnace
CN204237836U (en) * 2014-03-19 2015-04-01 丹阳市欧峰电器有限公司 Wire annealing device
CN104561511A (en) * 2013-10-18 2015-04-29 沈阳东宝海星金属材料科技有限公司 Continuous annealing device for periodically changing temperature of plate strip

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1844440A (en) * 2006-04-20 2006-10-11 倪智勇 Horizontal non-oxidizing bright continuous annealing device and method
CN102672447A (en) * 2011-03-17 2012-09-19 沈翠珊 Manufacturing method of high-purity nickel strap
CN102251201A (en) * 2011-07-07 2011-11-23 广东省钢铁研究所 Preparation method of high purity nickel wire
CN102586576A (en) * 2012-02-24 2012-07-18 北京工业大学 Vertical annealing furnace for coated superconducting substrate
CN103322800A (en) * 2012-03-22 2013-09-25 东北师范大学 Fully transparent tube type resistance furnace
CN104561511A (en) * 2013-10-18 2015-04-29 沈阳东宝海星金属材料科技有限公司 Continuous annealing device for periodically changing temperature of plate strip
CN204237836U (en) * 2014-03-19 2015-04-01 丹阳市欧峰电器有限公司 Wire annealing device

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2018003107A (en) * 2016-07-04 2018-01-11 大同特殊鋼株式会社 PRODUCTION METHOD OF PRECIPITATE TYPE HEAT-RESISTANT Ni-BASED ALLOY
CN107557561A (en) * 2017-08-08 2018-01-09 东莞市灿煜金属制品有限公司 The copper material stress-removal process of appropriateness drop hardness
CN107815533A (en) * 2017-12-05 2018-03-20 谢思雨 The method for annealing and equipment of a kind of sheet metal strip
CN109355489A (en) * 2018-12-05 2019-02-19 常德力元新材料有限责任公司 A kind of annealing device of punched nickel-plated steel band
CN110218856A (en) * 2019-06-03 2019-09-10 宁波中科毕普拉斯新材料科技有限公司 A kind of apparatus for continuous heat treatment and its application method of thin-band material
CN112620349A (en) * 2020-12-01 2021-04-09 无锡市东杨新材料股份有限公司 Method for eliminating oil stain of thin nickel strip
CN113322366A (en) * 2021-05-28 2021-08-31 郑州大学 Contact type rapid annealing equipment
CN113322366B (en) * 2021-05-28 2022-05-27 郑州大学 Contact type rapid annealing equipment

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Address after: 214116 Xishan City, Wuxi province Goose Lake Town Road, No. 99

Applicant after: Wuxi City, Dong Yang new materials Limited by Share Ltd

Address before: Lake town of Xishan District 214116 Jiangsu city of Wuxi Province on the posterior

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Application publication date: 20151118

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